#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:07 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180832 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/63/2016330.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016330_Fobs loop_ _publ_author_name 'De, Subhasis' 'Day, Cynthia S.' 'Welker, Mark E.' _publ_section_title ; An unusual oligomerization/oxidation reaction of a 3-boron-substituted 1-phenylbuta-1,3-diene produces 6,9,16,19-tetraphenyl-5,15-distyryl-3,13,25,26-tetraoxa-2,12-diborapentacyclo[16.2.2.2^8,11^.1^2,5^.1^12,15^]hexacosa-1(20),7,10,17-tetraene ; _journal_coeditor_code GG3111 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o729 _journal_page_last o730 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.764 _cell_angle_gamma 90.000 _cell_length_a 13.2115 _cell_length_b 6.0975 _cell_length_c 29.0280 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high 0.9000 _cod_data_source_file gg3111Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a79l2m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 206.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 43.87 59.88 16.35 o 6 0 0 2155.75 2156.84 43.38 o 8 0 0 219.78 239.94 20.76 o 10 0 0 84.51 96.40 32.75 o 12 0 0 5.17 12.10 29.95 o 14 0 0 44.00 66.64 37.99 o 2 1 0 4183.60 4469.78 50.53 o 3 1 0 15702.99 16890.29 166.29 o 4 1 0 3553.91 3734.60 42.45 o 5 1 0 169.00 182.76 14.99 o 6 1 0 2779.18 2708.91 51.84 o 7 1 0 433.87 449.09 21.78 o 8 1 0 37.29 58.80 13.71 o 9 1 0 14.26 17.98 12.61 o 10 1 0 4.21 17.91 18.23 o 11 1 0 22.57 -7.50 17.93 o 12 1 0 21.93 25.51 22.12 o 13 1 0 1.86 -8.72 21.34 o 14 1 0 32.65 30.12 24.44 o 0 2 0 3.08 5.14 9.44 o 1 2 0 849.36 787.63 32.80 o 2 2 0 51.65 65.99 9.08 o 3 2 0 6155.85 5975.33 115.00 o 4 2 0 78.90 78.46 12.28 o 5 2 0 177.73 183.64 16.37 o 6 2 0 96.92 103.86 15.00 o 7 2 0 981.98 935.82 40.60 o 8 2 0 21.32 20.39 12.72 o 9 2 0 20.29 27.44 14.20 o 10 2 0 0.61 2.91 12.69 o 11 2 0 84.94 71.52 19.10 o 12 2 0 11.00 21.40 20.07 o 13 2 0 39.56 61.60 30.52 o 1 3 0 2699.38 2538.69 103.76 o 2 3 0 12.57 25.19 9.36 o 3 3 0 51.64 46.14 10.78 o 4 3 0 18.11 18.57 8.29 o 5 3 0 198.61 202.39 16.56 o 6 3 0 299.69 328.18 23.09 o 7 3 0 9.73 -3.50 11.70 o 8 3 0 224.19 254.18 23.81 o 9 3 0 373.91 367.89 28.87 o 10 3 0 204.96 193.17 24.73 o 11 3 0 0.68 -7.23 18.10 o 12 3 0 1.91 12.64 19.99 o 0 4 0 117.82 154.72 22.24 o 1 4 0 1.41 -2.65 9.54 o 2 4 0 109.84 107.16 14.63 o 3 4 0 6.13 14.06 10.35 o 4 4 0 0.10 0.56 9.01 o 5 4 0 46.98 42.02 15.67 o 6 4 0 42.49 54.59 16.48 o 7 4 0 5.81 3.17 14.71 o 8 4 0 8.79 20.94 18.55 o 9 4 0 138.16 149.10 27.95 o 10 4 0 56.50 67.02 28.49 o 11 4 0 5.01 17.28 24.60 o 1 5 0 509.02 529.55 28.23 o 2 5 0 7.58 2.80 13.93 o 3 5 0 16.26 23.37 15.17 o 4 5 0 50.49 45.99 19.52 o 5 5 0 31.15 25.96 22.25 o 6 5 0 11.98 36.56 23.81 o 7 5 0 0.98 -6.50 20.84 o 8 5 0 1.21 21.68 24.42 o 9 5 0 12.91 14.01 24.42 o 0 6 0 4.38 -1.92 26.44 o 1 6 0 1.03 21.53 19.43 o 2 6 0 48.83 83.87 27.65 o 3 6 0 65.42 54.28 33.71 o 4 6 0 60.23 75.23 34.01 o 5 6 0 32.01 37.45 29.85 o 6 6 0 3.33 24.36 29.63 o -13 0 1 151.70 121.06 41.45 o -11 0 1 50.85 53.89 31.21 o -9 0 1 386.63 435.53 45.09 o -7 0 1 339.80 440.92 23.80 o -5 0 1 3476.87 3740.98 121.21 o -3 0 1 7754.33 8459.20 84.43 o 3 0 1 6884.10 8113.21 83.24 o 5 0 1 3924.24 4009.50 54.61 o 7 0 1 75.39 70.14 14.50 o 9 0 1 251.79 268.44 38.49 o 11 0 1 126.31 136.77 37.68 o 13 0 1 357.33 278.70 51.63 o -14 1 1 30.05 9.99 24.42 o -13 1 1 0.83 -13.20 21.01 o -12 1 1 104.16 157.47 29.32 o -11 1 1 297.81 287.93 32.19 o -10 1 1 110.83 125.91 24.49 o -9 1 1 53.26 45.54 13.80 o -8 1 1 121.30 130.97 16.36 o -7 1 1 26.25 16.72 10.34 o -6 1 1 314.71 349.05 19.23 o -5 1 1 1055.42 940.18 25.03 o -4 1 1 5.24 -2.35 7.31 o -3 1 1 244.61 245.46 13.57 o -2 1 1 406.48 318.99 17.97 o 1 1 1 1275.89 1078.90 41.32 o 2 1 1 3923.45 3781.77 40.27 o 3 1 1 13847.75 14757.20 225.73 o 4 1 1 1063.40 1107.54 24.74 o 5 1 1 143.76 176.34 14.69 o 6 1 1 1.62 1.07 8.74 o 7 1 1 111.15 132.77 15.64 o 8 1 1 1.12 4.14 10.13 o 9 1 1 23.06 22.89 12.18 o 10 1 1 83.01 99.95 22.16 o 11 1 1 75.03 78.61 23.89 o 12 1 1 74.03 87.40 26.33 o 13 1 1 4.72 13.58 21.98 o 14 1 1 1.22 1.96 21.88 o -13 2 1 8.70 21.74 21.68 o -12 2 1 21.14 23.18 20.54 o -11 2 1 160.77 191.79 24.41 o -10 2 1 29.89 20.91 15.15 o -9 2 1 23.88 25.63 14.31 o -8 2 1 4.62 14.08 11.23 o -7 2 1 363.03 380.92 23.77 o -6 2 1 3.38 2.83 9.86 o -5 2 1 240.49 257.62 18.15 o -4 2 1 1.97 3.54 9.09 o -3 2 1 2513.57 2589.90 48.11 o -2 2 1 3079.53 2773.74 108.01 o -1 2 1 6.29 0.45 6.56 o 0 2 1 1406.27 1396.01 42.85 o 1 2 1 0.74 2.80 6.54 o 2 2 1 0.01 6.19 8.02 o 3 2 1 2.64 12.56 6.88 o 4 2 1 13.03 1.15 7.26 o 5 2 1 56.30 46.54 11.60 o 6 2 1 115.83 149.75 16.28 o 7 2 1 22.27 22.71 11.84 o 8 2 1 432.15 425.88 25.81 o 9 2 1 32.34 31.51 14.84 o 10 2 1 23.71 19.07 14.81 o 11 2 1 95.20 114.48 21.35 o 12 2 1 98.99 55.88 28.96 o 13 2 1 1.71 0.40 24.80 o -12 3 1 5.10 22.90 20.21 o -11 3 1 76.68 59.54 19.56 o -10 3 1 262.69 257.00 26.89 o -9 3 1 65.02 63.80 17.93 o -8 3 1 23.26 17.36 14.09 o -7 3 1 29.62 29.88 13.97 o -6 3 1 70.45 74.42 15.27 o -5 3 1 828.30 767.10 23.72 o -4 3 1 11.65 9.84 10.31 o -3 3 1 122.70 144.91 13.78 o -2 3 1 269.25 300.80 17.21 o -1 3 1 652.27 674.25 21.26 o 0 3 1 1353.27 1332.98 59.64 o 1 3 1 126.03 170.09 14.16 o 2 3 1 189.76 240.25 15.96 o 3 3 1 1923.34 1926.49 52.94 o 4 3 1 109.09 106.87 11.58 o 5 3 1 84.86 93.43 12.54 o 6 3 1 139.93 168.10 18.86 o 7 3 1 58.68 70.95 16.19 o 8 3 1 4.75 0.29 13.08 o 9 3 1 9.23 -2.45 13.64 o 10 3 1 4.24 -14.99 15.74 o 11 3 1 28.98 33.06 21.12 o 12 3 1 10.70 -12.50 18.78 o -11 4 1 4.87 -20.96 20.96 o -10 4 1 4.33 5.09 23.01 o -9 4 1 128.51 113.75 30.52 o -8 4 1 6.67 15.58 14.98 o -7 4 1 37.77 38.33 16.38 o -6 4 1 4.37 6.62 13.75 o -5 4 1 31.74 28.96 14.51 o -4 4 1 226.06 225.95 18.58 o -3 4 1 4.49 3.73 10.00 o -2 4 1 2.95 -5.27 9.38 o -1 4 1 91.65 93.41 14.00 o 0 4 1 130.86 129.41 15.03 o 1 4 1 0.70 -5.28 9.64 o 2 4 1 253.13 267.26 18.97 o 3 4 1 5.24 1.77 9.22 o 4 4 1 1.19 0.01 9.17 o 5 4 1 0.30 2.60 13.34 o 6 4 1 120.99 134.77 20.04 o 7 4 1 2.60 11.62 18.17 o 8 4 1 6.93 27.60 18.88 o 9 4 1 2.53 -4.47 18.36 o 10 4 1 0.00 21.77 21.06 o 11 4 1 5.27 1.68 19.68 o -9 5 1 40.93 40.66 26.36 o -8 5 1 79.18 82.18 30.09 o -7 5 1 0.32 -10.06 20.38 o -6 5 1 22.23 13.25 23.64 o -5 5 1 6.58 12.63 18.03 o -4 5 1 71.01 71.49 21.53 o -3 5 1 10.90 12.39 14.77 o -2 5 1 2.65 -6.37 13.91 o -1 5 1 12.04 11.20 14.35 o 0 5 1 6.16 14.22 13.83 o 1 5 1 41.02 42.63 14.81 o 2 5 1 50.34 47.62 15.38 o 3 5 1 253.50 266.60 22.62 o 4 5 1 33.84 20.69 21.97 o 5 5 1 24.89 18.00 21.90 o 6 5 1 16.99 35.00 24.32 o 7 5 1 100.14 101.60 29.49 o 8 5 1 0.00 2.46 23.29 o 9 5 1 30.83 28.02 26.94 o -6 6 1 92.70 119.35 31.83 o -5 6 1 13.50 19.01 22.65 o -4 6 1 1.32 30.34 29.25 o -3 6 1 13.25 2.09 27.73 o -2 6 1 79.58 86.82 23.09 o -1 6 1 2.82 -0.14 18.15 o 0 6 1 33.29 33.90 20.62 o 1 6 1 123.23 155.23 26.13 o 2 6 1 23.59 36.66 19.98 o 3 6 1 0.03 -2.28 27.22 o 4 6 1 57.52 38.09 32.37 o 5 6 1 5.42 11.94 27.96 o 6 6 1 9.81 18.14 29.72 o -14 0 2 54.36 60.17 38.05 o -12 0 2 116.61 129.75 40.66 o -10 0 2 216.47 202.02 53.55 o -8 0 2 237.16 214.00 19.05 o -6 0 2 746.67 766.31 26.86 o -4 0 2 9343.98 9129.17 210.59 o 4 0 2 4135.52 4364.20 53.09 o 6 0 2 170.29 186.23 18.31 o 8 0 2 996.68 951.75 40.08 o 10 0 2 30.63 24.83 26.02 o 12 0 2 4.36 2.39 29.72 o 14 0 2 28.96 34.19 36.20 o -14 1 2 1.28 -5.49 23.20 o -13 1 2 4.51 4.67 20.93 o -12 1 2 103.56 119.92 27.37 o -11 1 2 42.71 68.44 23.18 o -10 1 2 0.03 9.42 17.31 o -9 1 2 5.77 -1.77 9.32 o -8 1 2 16.46 20.72 11.44 o -7 1 2 544.02 523.14 22.97 o -6 1 2 716.74 784.49 25.31 o -5 1 2 1057.23 1017.89 25.86 o -4 1 2 2260.86 2098.51 32.20 o -3 1 2 145.94 166.93 12.12 o -2 1 2 244.38 262.27 14.91 o -1 1 2 7420.18 6175.28 94.44 o 1 1 2 1553.37 1460.12 35.50 o 2 1 2 68.25 72.69 11.00 o 3 1 2 2132.16 2108.60 35.20 o 4 1 2 4243.02 4063.30 77.24 o 5 1 2 1060.61 1104.91 27.22 o 6 1 2 202.95 249.38 17.95 o 7 1 2 25.67 33.92 11.38 o 8 1 2 20.29 33.26 11.92 o 9 1 2 238.39 255.40 22.00 o 10 1 2 16.07 10.47 17.38 o 11 1 2 9.00 26.48 19.73 o 12 1 2 6.76 -1.39 19.54 o 13 1 2 116.25 104.90 27.30 o 14 1 2 1.66 -4.21 25.99 o -13 2 2 2.40 10.83 21.49 o -12 2 2 26.44 34.02 20.92 o -11 2 2 329.24 346.65 28.98 o -10 2 2 16.56 22.56 14.99 o -9 2 2 16.24 30.85 14.12 o -8 2 2 190.88 203.80 20.39 o -7 2 2 98.46 107.36 16.36 o -6 2 2 1700.03 1585.80 36.47 o -5 2 2 20.98 20.77 10.50 o -4 2 2 24.37 22.44 9.79 o -3 2 2 720.01 757.15 21.97 o -2 2 2 2099.59 2138.68 51.10 o -1 2 2 499.57 481.29 18.78 o 0 2 2 592.48 584.54 19.78 o 1 2 2 169.29 178.05 11.56 o 2 2 2 788.76 701.20 18.65 o 3 2 2 369.42 337.34 14.90 o 4 2 2 306.70 328.64 15.57 o 5 2 2 160.52 162.55 12.73 o 6 2 2 28.82 21.40 10.89 o 7 2 2 132.54 142.04 17.27 o 8 2 2 60.41 72.65 15.16 o 9 2 2 301.94 310.49 25.26 o 10 2 2 0.18 -6.65 13.00 o 11 2 2 168.72 178.57 23.66 o 12 2 2 0.38 -11.44 22.70 o 13 2 2 25.58 32.62 28.13 o -13 3 2 58.16 69.96 31.17 o -12 3 2 2.21 -3.26 17.93 o -11 3 2 67.43 72.14 20.68 o -10 3 2 1.43 -9.95 14.47 o -9 3 2 110.20 111.59 20.34 o -8 3 2 27.29 43.93 15.57 o -7 3 2 389.05 397.17 30.02 o -6 3 2 308.93 310.35 22.73 o -5 3 2 2.27 0.48 7.42 o -4 3 2 168.63 173.03 14.48 o -3 3 2 25.15 7.49 8.78 o -2 3 2 1983.33 1921.12 84.98 o -1 3 2 193.01 207.95 15.04 o 0 3 2 2147.05 2008.50 57.75 o 1 3 2 1298.63 1279.72 27.52 o 2 3 2 158.45 176.11 13.35 o 3 3 2 147.46 147.30 12.75 o 4 3 2 616.41 603.53 21.52 o 5 3 2 133.76 140.79 14.10 o 6 3 2 8.30 1.07 11.33 o 7 3 2 37.65 35.76 14.54 o 8 3 2 795.99 821.49 39.64 o 9 3 2 2.54 0.34 16.13 o 10 3 2 154.75 187.93 27.82 o 11 3 2 3.70 3.98 18.21 o 12 3 2 7.41 9.38 20.74 o -11 4 2 1.95 -5.17 22.05 o -10 4 2 1.76 -7.70 20.64 o -9 4 2 191.40 206.23 29.41 o -8 4 2 12.62 43.02 20.15 o -7 4 2 35.40 64.01 20.68 o -6 4 2 74.84 62.23 19.30 o -5 4 2 95.19 123.26 18.10 o -4 4 2 5.61 18.00 11.00 o -3 4 2 36.05 19.22 10.79 o -2 4 2 2.63 5.73 10.15 o -1 4 2 23.08 23.76 11.04 o 0 4 2 65.32 87.46 13.80 o 1 4 2 551.46 517.03 23.26 o 2 4 2 11.88 7.36 9.76 o 3 4 2 87.29 92.96 13.01 o 4 4 2 55.82 53.39 11.51 o 5 4 2 128.60 161.57 20.41 o 6 4 2 188.15 193.29 27.05 o 7 4 2 398.23 423.86 41.17 o 8 4 2 101.93 94.22 23.45 o 9 4 2 69.91 69.19 22.97 o 10 4 2 83.86 88.09 25.18 o 11 4 2 4.68 18.57 20.40 o -9 5 2 20.56 29.42 25.62 o -8 5 2 15.59 13.41 24.55 o -7 5 2 18.87 1.65 21.39 o -6 5 2 4.23 -10.04 17.79 o -5 5 2 3.88 16.41 18.81 o -4 5 2 13.35 17.62 18.72 o -3 5 2 67.98 93.17 19.91 o -2 5 2 265.58 285.02 26.00 o -1 5 2 84.27 73.28 17.96 o 0 5 2 313.59 305.84 25.70 o 1 5 2 116.86 110.46 19.68 o 2 5 2 0.95 -4.07 11.36 o 3 5 2 0.04 -12.02 12.02 o 4 5 2 268.54 310.21 31.36 o 5 5 2 34.89 33.63 23.58 o 6 5 2 1.82 0.60 21.33 o 7 5 2 1.72 -2.67 21.90 o 8 5 2 2.74 32.38 25.90 o 9 5 2 50.18 43.32 27.93 o -6 6 2 34.72 68.62 28.93 o -5 6 2 1.72 12.27 23.08 o -4 6 2 19.40 34.42 23.69 o -3 6 2 2.00 12.92 23.20 o -2 6 2 159.82 191.85 29.22 o -1 6 2 2.72 -1.20 17.28 o 0 6 2 22.77 43.63 21.38 o 1 6 2 15.06 28.28 19.95 o 2 6 2 0.02 -7.53 17.46 o 3 6 2 8.83 6.35 28.36 o 4 6 2 8.90 3.56 29.15 o 5 6 2 29.51 35.87 29.74 o 6 6 2 4.08 21.88 30.69 o -13 0 3 87.63 114.92 41.42 o -11 0 3 52.66 52.00 30.50 o -9 0 3 762.21 670.21 48.74 o -7 0 3 532.27 508.05 24.47 o -5 0 3 16.03 10.11 14.50 o -3 0 3 34927.48 39738.98 1471.20 o 3 0 3 42556.07 47346.84 486.45 o 5 0 3 112.44 136.02 15.65 o 7 0 3 327.29 336.12 28.59 o 9 0 3 262.58 219.24 36.57 o 11 0 3 3.28 -22.42 22.42 o 13 0 3 327.40 279.12 50.60 o -14 1 3 0.00 6.17 23.03 o -13 1 3 29.03 49.35 24.57 o -12 1 3 109.08 106.01 26.56 o -11 1 3 416.76 414.70 36.42 o -10 1 3 36.50 38.43 19.01 o -9 1 3 1102.42 1050.99 34.08 o -8 1 3 21.92 -1.10 10.37 o -7 1 3 362.91 380.09 21.52 o -6 1 3 990.96 888.46 39.13 o -5 1 3 332.94 285.13 17.14 o -4 1 3 305.90 267.41 14.98 o -3 1 3 4317.20 4340.48 75.84 o -2 1 3 10595.66 11047.71 230.62 o -1 1 3 1552.38 1226.77 23.25 o 0 1 3 7830.19 9444.05 480.51 o 1 1 3 17809.86 19958.19 322.12 o 2 1 3 245.57 264.43 15.86 o 3 1 3 907.25 721.91 22.87 o 4 1 3 1653.39 1643.63 29.66 o 5 1 3 142.30 136.71 12.66 o 6 1 3 194.13 197.34 13.18 o 7 1 3 57.84 74.89 9.97 o 8 1 3 71.82 81.56 14.51 o 9 1 3 3.61 1.35 10.65 o 10 1 3 98.18 110.05 22.93 o 11 1 3 1.12 -9.54 17.38 o 12 1 3 0.00 0.56 18.62 o 13 1 3 10.31 5.75 20.50 o -13 2 3 286.39 294.16 36.49 o -12 2 3 7.17 15.69 19.72 o -11 2 3 5.79 11.81 15.06 o -10 2 3 30.39 41.88 15.72 o -9 2 3 4.18 0.42 12.37 o -8 2 3 11.39 17.82 12.17 o -7 2 3 801.25 699.67 27.35 o -6 2 3 1308.62 1225.36 32.53 o -5 2 3 676.18 629.71 23.40 o -4 2 3 159.60 156.44 14.82 o -3 2 3 241.97 233.17 12.98 o -2 2 3 9.90 5.23 7.65 o -1 2 3 115.95 135.00 12.09 o 0 2 3 116.97 141.37 12.04 o 1 2 3 1420.85 1258.66 39.63 o 2 2 3 1016.20 1043.48 23.58 o 3 2 3 194.66 194.36 12.94 o 4 2 3 246.22 262.85 18.17 o 5 2 3 1088.65 1116.18 25.10 o 6 2 3 476.75 477.47 17.89 o 7 2 3 588.75 595.31 26.00 o 8 2 3 257.32 306.88 23.81 o 9 2 3 77.63 83.59 17.50 o 10 2 3 248.31 222.47 23.75 o 11 2 3 99.13 117.01 23.50 o 12 2 3 155.05 150.62 35.28 o 13 2 3 42.03 57.36 30.04 o -13 3 3 17.74 35.01 26.83 o -12 3 3 47.15 65.20 20.72 o -11 3 3 5.23 13.07 16.73 o -10 3 3 0.11 -6.69 15.00 o -9 3 3 85.70 86.86 18.94 o -8 3 3 235.44 252.31 24.02 o -7 3 3 387.79 395.84 25.30 o -6 3 3 594.15 547.78 25.74 o -5 3 3 237.91 249.36 16.09 o -4 3 3 333.09 333.21 21.48 o -3 3 3 465.53 406.11 17.83 o -2 3 3 583.46 553.61 25.14 o -1 3 3 354.94 343.08 17.45 o 0 3 3 9.29 11.38 8.84 o 1 3 3 76.32 68.96 10.33 o 2 3 3 452.53 449.46 17.23 o 3 3 3 2.68 4.47 7.51 o 4 3 3 2848.44 2730.71 58.91 o 5 3 3 2.39 8.08 8.72 o 6 3 3 2.57 3.78 10.80 o 7 3 3 24.87 2.76 12.62 o 8 3 3 336.83 366.70 32.54 o 9 3 3 0.00 -5.76 15.76 o 10 3 3 107.43 82.74 23.53 o 11 3 3 116.40 132.24 26.99 o 12 3 3 0.01 -18.02 18.02 o -11 4 3 12.20 7.58 23.36 o -10 4 3 166.23 157.01 33.57 o -9 4 3 177.73 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