#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/63/2016342.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016342_Fobs loop_ _publ_author_name 'Hatert, Fr\'ed\'eric' _publ_section_title ; Fe^II^~2~(PO~4~)(OH), a synthetic analogue of wolfeite ; _journal_coeditor_code IZ3034 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i119 _journal_page_last i121 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.625 _cell_angle_gamma 90.000 _cell_length_a 12.2651 _cell_length_b 13.1973 _cell_length_c 9.7385 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.5367 _[local]_cod_data_source_file iz3034Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' h288BC in P2(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 750.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 492.78 760.36 36.34 o 4 0 0 62345.36 60218.14 428.82 o 6 0 0 39363.66 40004.71 288.75 o 8 0 0 123027.84 119667.28 712.73 o 10 0 0 55454.36 56305.77 660.52 o 12 0 0 14820.90 14814.07 348.83 o 14 0 0 2943.84 3134.87 229.81 o 16 0 0 1598.27 1759.47 295.24 o 18 0 0 11219.48 11761.69 566.54 o 2 1 0 559.05 619.71 26.62 o 3 1 0 3799.99 3862.22 67.20 o 4 1 0 5510.14 5723.20 68.81 o 5 1 0 1451.77 1698.51 67.92 o 6 1 0 853.09 892.11 61.83 o 7 1 0 268.69 271.07 52.62 o 8 1 0 2569.69 2540.75 90.96 o 9 1 0 8444.62 8337.48 113.01 o 10 1 0 7711.16 7999.35 124.53 o 11 1 0 62.71 106.19 51.67 o 12 1 0 3194.66 3249.88 117.89 o 13 1 0 3619.16 3691.29 155.57 o 14 1 0 2402.26 2402.84 153.00 o 15 1 0 56.57 139.47 130.36 o 16 1 0 113.52 158.45 124.48 o 17 1 0 191.40 253.35 163.63 o 18 1 0 2126.41 2050.61 229.87 o 19 1 0 1940.58 2037.49 277.79 o 1 2 0 40.64 257.85 26.19 o 2 2 0 16.02 61.34 20.38 o 3 2 0 6118.01 6469.37 91.09 o 4 2 0 92.46 130.19 30.82 o 5 2 0 1109.78 1348.46 72.20 o 6 2 0 505.20 560.41 70.34 o 7 2 0 43360.69 43925.66 477.12 o 8 2 0 42.70 86.78 43.53 o 9 2 0 439.86 497.94 56.46 o 10 2 0 492.45 518.89 67.72 o 11 2 0 15388.41 15037.11 171.42 o 12 2 0 7.16 108.60 60.92 o 13 2 0 2059.84 2056.47 147.05 o 14 2 0 90.51 68.07 98.92 o 15 2 0 247.49 352.48 169.82 o 16 2 0 142.04 175.22 138.15 o 17 2 0 2774.74 2741.87 209.93 o 18 2 0 345.55 374.68 191.59 o 19 2 0 2714.25 2712.09 293.36 o 1 3 0 421.65 446.32 31.08 o 2 3 0 3276.04 3357.68 47.78 o 3 3 0 6962.84 7438.71 70.04 o 4 3 0 3549.20 3717.93 76.63 o 5 3 0 709.71 749.87 64.94 o 6 3 0 135.60 188.38 56.84 o 7 3 0 3256.32 3434.49 89.85 o 8 3 0 1456.29 1446.66 75.57 o 9 3 0 142.79 202.22 58.55 o 10 3 0 337.51 350.80 66.88 o 11 3 0 453.38 473.18 60.22 o 12 3 0 869.85 900.19 83.04 o 13 3 0 4599.00 4566.29 176.71 o 14 3 0 790.82 802.06 134.39 o 15 3 0 3361.08 3280.29 255.02 o 16 3 0 1582.24 1634.38 217.17 o 17 3 0 1659.10 1710.39 216.60 o 18 3 0 151.29 257.47 205.89 o 19 3 0 382.35 371.30 195.69 o 0 4 0 27859.28 28445.40 223.42 o 1 4 0 4.59 229.11 30.87 o 2 4 0 71557.93 70910.73 272.22 o 3 4 0 224.67 402.02 39.50 o 4 4 0 5633.45 5671.18 82.03 o 5 4 0 5.25 35.30 22.46 o 6 4 0 31645.77 32389.30 590.15 o 7 4 0 79.48 206.86 72.15 o 8 4 0 1704.64 1670.16 85.79 o 9 4 0 510.24 541.36 61.73 o 10 4 0 7897.22 7782.56 131.11 o 11 4 0 125.29 108.30 54.37 o 12 4 0 8670.74 8554.95 147.17 o 13 4 0 1345.96 1404.21 134.68 o 14 4 0 5280.49 5344.63 216.19 o 15 4 0 412.24 450.84 174.96 o 16 4 0 6707.66 6720.66 307.16 o 17 4 0 121.90 193.62 160.16 o 18 4 0 1696.27 1696.71 231.13 o 19 4 0 694.37 740.83 214.35 o 1 5 0 439.49 519.97 33.33 o 2 5 0 425.36 425.85 33.17 o 3 5 0 2723.95 2863.32 56.55 o 4 5 0 1812.74 1861.84 59.23 o 5 5 0 1511.03 1505.78 68.99 o 6 5 0 4338.75 4417.28 97.23 o 7 5 0 587.22 572.44 74.29 o 8 5 0 2.83 40.30 46.70 o 9 5 0 443.84 462.88 60.96 o 10 5 0 266.55 275.67 55.50 o 11 5 0 7.33 76.98 48.47 o 12 5 0 800.41 791.71 87.49 o 13 5 0 1702.49 1761.12 144.08 o 14 5 0 268.24 329.47 101.09 o 15 5 0 191.52 150.67 119.28 o 16 5 0 1281.76 1262.62 212.65 o 17 5 0 68.82 94.48 131.79 o 18 5 0 64.71 191.25 173.82 o 19 5 0 640.56 518.74 226.20 o 0 6 0 14.73 154.05 60.12 o 1 6 0 3893.34 4601.07 72.36 o 2 6 0 236.92 257.01 38.48 o 3 6 0 21558.12 22829.94 136.92 o 4 6 0 78.24 115.93 35.03 o 5 6 0 5888.53 6236.36 91.52 o 6 6 0 0.79 57.27 47.07 o 7 6 0 9338.20 9098.22 138.60 o 8 6 0 267.08 254.37 63.62 o 9 6 0 7124.91 6838.48 138.09 o 10 6 0 2.54 78.13 45.85 o 11 6 0 449.48 387.50 64.24 o 12 6 0 999.96 1087.85 113.49 o 13 6 0 715.23 799.89 124.16 o 14 6 0 99.14 132.49 98.88 o 15 6 0 113.68 207.14 153.58 o 16 6 0 359.00 319.70 145.65 o 17 6 0 1875.59 1679.29 237.77 o 18 6 0 85.63 173.36 165.26 o 19 6 0 80.15 243.65 181.82 o 1 7 0 55.55 80.21 28.59 o 2 7 0 1172.07 1219.77 53.56 o 3 7 0 615.79 690.74 51.28 o 4 7 0 924.61 876.73 50.84 o 5 7 0 40.94 91.91 34.13 o 6 7 0 2180.63 2285.44 80.01 o 7 7 0 788.74 776.69 66.20 o 8 7 0 66.35 134.77 57.61 o 9 7 0 449.75 402.17 64.87 o 10 7 0 23.94 74.26 44.15 o 11 7 0 1883.50 1826.77 112.54 o 12 7 0 2127.75 2273.71 136.57 o 13 7 0 33.27 95.90 79.12 o 14 7 0 9.79 69.09 114.79 o 15 7 0 526.28 505.92 143.63 o 16 7 0 2600.02 2506.67 248.07 o 17 7 0 756.22 858.77 207.00 o 18 7 0 377.74 451.84 227.02 o 0 8 0 20609.03 21476.40 192.61 o 1 8 0 21.81 46.53 24.96 o 2 8 0 115495.58 115015.39 656.45 o 3 8 0 126.79 158.31 44.67 o 4 8 0 13587.10 13258.10 117.27 o 5 8 0 79.45 120.30 50.19 o 6 8 0 112734.05 110622.71 1403.60 o 7 8 0 169.82 148.64 42.88 o 8 8 0 384.42 378.59 57.33 o 9 8 0 357.50 432.81 75.73 o 10 8 0 15.65 71.69 49.76 o 11 8 0 148.44 159.90 109.92 o 12 8 0 17262.17 17383.41 247.17 o 13 8 0 34.58 62.09 87.32 o 14 8 0 4011.97 4072.21 207.68 o 15 8 0 59.99 197.64 145.97 o 16 8 0 10015.84 10554.36 355.33 o 17 8 0 136.29 139.64 150.44 o 18 8 0 700.43 614.47 207.34 o 1 9 0 1222.59 1248.07 64.29 o 2 9 0 2989.87 3017.56 80.84 o 3 9 0 542.39 621.25 58.38 o 4 9 0 21.04 55.13 32.74 o 5 9 0 2031.80 2110.06 82.58 o 6 9 0 5633.73 5871.57 106.95 o 7 9 0 6048.60 6165.99 121.56 o 8 9 0 1148.17 1069.19 89.72 o 9 9 0 6503.29 6327.88 156.01 o 10 9 0 4792.11 4963.34 162.77 o 11 9 0 1025.48 1120.47 141.71 o 12 9 0 88.80 231.33 161.32 o 13 9 0 1398.89 1455.25 148.28 o 14 9 0 67.84 62.77 95.27 o 15 9 0 3760.78 3895.41 285.50 o 16 9 0 4333.57 4544.95 286.34 o 17 9 0 43.57 108.46 143.08 o 18 9 0 1069.95 1112.64 221.54 o 0 10 0 226.31 282.13 82.34 o 1 10 0 20133.89 20966.13 142.77 o 2 10 0 70.80 128.91 47.53 o 3 10 0 61.34 191.10 58.04 o 4 10 0 112.90 117.36 42.58 o 5 10 0 10457.53 10813.53 183.44 o 6 10 0 33.43 88.18 38.14 o 7 10 0 1510.46 1317.84 77.94 o 8 10 0 0.08 54.21 49.46 o 9 10 0 17518.93 17329.73 215.78 o 10 10 0 143.19 125.60 108.49 o 11 10 0 6023.41 5922.30 260.03 o 12 10 0 41.98 56.21 95.79 o 13 10 0 9680.38 10190.13 341.72 o 14 10 0 313.28 227.94 113.39 o 15 10 0 1203.20 1063.71 217.54 o 16 10 0 0.76 81.46 118.39 o 17 10 0 762.37 693.80 216.73 o 1 11 0 1.92 117.31 42.90 o 2 11 0 1791.21 1754.78 77.00 o 3 11 0 805.62 828.90 68.27 o 4 11 0 20.67 52.95 36.54 o 5 11 0 13.95 36.77 32.60 o 6 11 0 121.75 123.24 45.04 o 7 11 0 38.50 99.28 58.98 o 8 11 0 3496.64 3446.96 123.17 o 9 11 0 4890.90 4824.24 204.93 o 10 11 0 1075.88 1061.88 170.36 o 11 11 0 468.41 259.33 171.56 o 12 11 0 569.32 625.35 191.67 o 13 11 0 2495.18 2659.80 232.92 o 14 11 0 226.35 209.01 118.46 o 15 11 0 46.81 66.57 127.49 o 16 11 0 1.29 155.12 176.17 o 17 11 0 17.17 129.58 151.11 o 0 12 0 92543.80 92896.34 352.07 o 1 12 0 167.61 164.58 48.57 o 2 12 0 688.40 708.85 65.81 o 3 12 0 29.03 51.19 39.56 o 4 12 0 11903.23 12109.08 192.68 o 5 12 0 135.57 112.16 46.14 o 6 12 0 18544.56 18665.17 192.16 o 7 12 0 137.33 123.18 62.52 o 8 12 0 18990.88 18782.87 308.13 o 9 12 0 436.48 327.16 207.47 o 10 12 0 15714.06 15775.35 534.62 o 11 12 0 384.59 231.40 171.56 o 12 12 0 1843.46 1825.93 253.86 o 13 12 0 9.65 101.74 143.88 o 14 12 0 2399.84 2483.07 248.71 o 15 12 0 150.46 130.92 101.14 o 16 12 0 101.82 215.05 165.68 o 1 13 0 682.03 672.26 75.18 o 2 13 0 1953.77 1946.15 95.74 o 3 13 0 6708.94 6839.99 139.29 o 4 13 0 9571.00 9770.31 152.24 o 5 13 0 4051.87 3936.75 116.97 o 6 13 0 405.48 423.25 91.92 o 7 13 0 339.62 258.73 110.77 o 8 13 0 11.76 40.59 64.24 o 9 13 0 0.87 23.94 139.64 o 10 13 0 298.64 255.34 179.54 o 11 13 0 912.85 1109.14 291.25 o 12 13 0 2798.66 2864.62 375.03 o 13 13 0 2185.24 2328.09 248.23 o 14 13 0 2275.17 2281.92 277.62 o 15 13 0 25.26 143.86 117.76 o 16 13 0 818.23 733.03 239.38 o 0 14 0 53.95 102.43 115.03 o 1 14 0 3980.11 4062.47 126.28 o 2 14 0 20.52 98.02 56.34 o 3 14 0 22.87 101.84 52.65 o 4 14 0 5.34 67.60 90.96 o 5 14 0 444.46 510.33 118.46 o 6 14 0 41.83 65.38 66.95 o 7 14 0 17554.61 17500.27 339.65 o 8 14 0 4.00 37.93 91.66 o 9 14 0 2800.59 2294.09 279.28 o 10 14 0 28.34 55.86 159.59 o 11 14 0 696.15 718.15 291.25 o 12 14 0 75.44 95.75 183.53 o 13 14 0 415.04 498.51 189.80 o 14 14 0 2.03 73.73 110.13 o 15 14 0 634.17 698.20 211.08 o 1 15 0 12.15 70.75 60.77 o 2 15 0 88.24 127.41 64.55 o 3 15 0 175.16 148.84 89.61 o 4 15 0 282.40 263.68 84.02 o 5 15 0 157.17 157.06 81.33 o 6 15 0 54.21 95.20 75.30 o 7 15 0 392.63 377.75 140.72 o 8 15 0 220.67 187.74 128.15 o 9 15 0 111.55 123.68 159.59 o 10 15 0 594.91 478.77 215.44 o 11 15 0 22.99 99.74 171.56 o 12 15 0 498.16 259.33 179.54 o 13 15 0 1.03 23.94 138.60 o 14 15 0 88.00 133.46 179.33 o 15 15 0 580.72 658.30 359.07 o 0 16 0 4524.93 4360.55 241.56 o 1 16 0 36.66 83.81 83.41 o 2 16 0 578.79 490.24 115.38 o 3 16 0 2.76 69.55 75.16 o 4 16 0 1393.67 1315.55 142.54 o 5 16 0 1.93 69.29 78.29 o 6 16 0 3709.12 3592.02 171.43 o 7 16 0 8.20 55.29 95.75 o 8 16 0 1542.32 1456.55 225.69 o 9 16 0 0.82 59.85 179.54 o 10 16 0 5897.50 6092.30 450.84 o 11 16 0 155.82 183.53 239.38 o 12 16 0 146.57 131.66 259.33 o 13 16 0 369.52 313.19 172.09 o 14 16 0 906.85 921.63 402.96 o 15 16 0 204.22 195.50 279.28 o 1 17 0 538.26 422.78 108.45 o 2 17 0 727.10 633.30 98.68 o 3 17 0 5863.70 5667.08 200.34 o 4 17 0 4505.19 4491.55 217.10 o 5 17 0 1602.13 1646.49 173.22 o 6 17 0 494.22 447.15 106.34 o 7 17 0 316.40 292.26 167.57 o 8 17 0 316.94 303.67 168.58 o 9 17 0 467.57 387.00 251.35 o 10 17 0 0.70 79.79 179.54 o 11 17 0 971.54 881.73 323.17 o 12 17 0 1714.86 1775.43 331.15 o 13 17 0 4026.71 4488.43 430.89 o 14 17 0 979.32 901.68 303.22 o 15 17 0 796.94 989.45 430.89 o 0 18 0 0.53 107.57 109.59 o 1 18 0 78.98 116.67 81.72 o 2 18 0 11.24 100.07 87.54 o 3 18 0 6304.27 6383.43 208.41 o 4 18 0 37.50 84.07 91.85 o 5 18 0 50.56 179.62 104.33 o 6 18 0 5.80 98.98 144.74 o 7 18 0 9549.00 9525.07 342.55 o 8 18 0 319.69 220.70 127.80 o 9 18 0 169.95 135.65 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221.43 o 7 21 0 1163.25 1068.07 215.58 o 0 22 0 54.11 87.95 158.12 o 1 22 0 1807.42 1697.83 191.13 o 2 22 0 4.26 115.34 106.07 o 3 22 0 380.73 293.35 143.57 o 4 22 0 8.77 107.28 161.81 o 1 23 0 123.30 172.21 197.08 o 2 23 0 875.81 837.84 430.89 o -20 0 1 514.30 514.67 311.20 o -18 0 1 3.01 111.71 163.58 o -16 0 1 1634.32 1643.76 267.31 o -14 0 1 43.13 74.51 106.41 o -12 0 1 901.28 867.07 89.88 o -10 0 1 12.86 68.04 55.93 o -8 0 1 690.37 710.89 87.91 o -6 0 1 755.42 818.96 109.77 o -4 0 1 114.37 419.75 61.42 o -2 0 1 4.39 1353.92 56.43 o 2 0 1 10.18 81.35 57.37 o 4 0 1 6.04 40.72 36.19 o 6 0 1 93.54 152.35 60.17 o 8 0 1 1946.45 1968.75 131.80 o 10 0 1 487.07 485.80 106.24 o 12 0 1 734.04 703.45 138.88 o 14 0 1 151.31 233.61 159.62 o 16 0 1 157.26 179.54 191.51 o 18 0 1 618.49 478.77 231.40 o -20 1 1 2639.86 2756.86 269.78 o -19 1 1 29.33 146.95 165.72 o -18 1 1 354.94 359.00 212.98 o -17 1 1 21.56 75.04 122.03 o -16 1 1 1313.37 1085.98 190.29 o -15 1 1 1117.58 900.43 157.98 o -14 1 1 125.95 116.68 89.26 o -13 1 1 857.15 744.96 78.30 o -12 1 1 4.63 72.53 48.48 o -11 1 1 36.85 88.95 38.74 o -10 1 1 1765.41 1715.91 76.36 o -9 1 1 646.23 627.31 60.46 o -8 1 1 258.65 306.89 50.26 o -7 1 1 343.86 405.53 55.46 o -6 1 1 10413.62 10803.74 112.88 o -5 1 1 1477.70 1503.67 57.19 o -4 1 1 157.03 196.02 41.26 o -3 1 1 166.66 164.17 27.61 o -2 1 1 40.86 74.77 20.56 o -1 1 1 140.68 15.96 15.96 o 1 1 1 2.22 27.00 11.90 o 2 1 1 1088.71 1084.04 31.64 o 3 1 1 1823.53 1865.08 60.89 o 4 1 1 1983.75 2004.89 52.96 o 5 1 1 239.70 244.29 45.80 o 6 1 1 677.02 760.71 63.47 o 7 1 1 2003.64 2121.20 97.98 o 8 1 1 490.47 608.35 69.12 o 9 1 1 0.52 84.94 55.24 o 10 1 1 20.25 83.53 54.07 o 11 1 1 1988.91 1973.78 103.83 o 12 1 1 4264.88 4285.28 131.75 o 13 1 1 134.36 136.53 74.16 o 14 1 1 354.75 390.08 114.56 o 15 1 1 776.72 744.07 154.86 o 16 1 1 590.27 546.15 202.18 o 17 1 1 4.60 59.96 100.12 o 18 1 1 139.52 172.87 164.87 o 19 1 1 95.58 123.60 129.26 o -20 2 1 7398.89 8606.64 392.14 o -19 2 1 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