#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/68/2016828.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016828_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Bhuiyan, M. Delower H.' 'Kay, Andrew J.' _publ_section_title ; Geometry and bond-length alternation in nonlinear optical materials. III. Structural parameters of two chromophores containing aromatizable donors ; _journal_coeditor_code FG3060 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o616 _journal_page_last o619 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.211 _cell_angle_gamma 90.000 _cell_length_a 12.5261 _cell_length_b 9.8849 _cell_length_c 24.3711 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file fg3060IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' KSSZ in P2(1)/n 50 2theta limit' _shelx_refln_list_code 4 _shelx_F_calc_maximum 210.64 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 664.94 695.27 30.85 o 6 0 0 139.93 110.30 32.17 o 8 0 0 2597.33 2503.99 84.79 o 10 0 0 100.28 96.91 45.12 o 12 0 0 4.46 -13.16 45.48 o 14 0 0 61.83 22.28 51.74 o 2 1 0 4741.20 3363.71 666.32 o 3 1 0 13191.50 12881.39 180.96 o 4 1 0 475.12 579.74 19.36 o 5 1 0 5.15 8.36 10.02 o 6 1 0 801.67 679.72 26.89 o 7 1 0 107.06 130.92 18.83 o 8 1 0 158.66 148.37 20.30 o 9 1 0 292.18 336.30 25.63 o 10 1 0 383.08 419.09 30.45 o 11 1 0 64.42 57.48 34.71 o 12 1 0 41.56 15.06 33.77 o 13 1 0 23.70 22.04 36.26 o 14 1 0 34.38 35.61 43.48 o 0 2 0 73.01 59.44 6.18 o 1 2 0 13229.76 11193.43 212.81 o 2 2 0 5789.16 6269.92 90.31 o 3 2 0 3609.26 3814.89 42.34 o 4 2 0 1628.53 1673.67 19.44 o 5 2 0 46.88 63.33 14.76 o 6 2 0 10287.83 10405.52 71.80 o 7 2 0 2.01 15.21 17.91 o 8 2 0 297.64 286.75 25.08 o 9 2 0 535.72 500.46 31.19 o 10 2 0 7.10 -3.93 23.75 o 11 2 0 55.95 70.70 25.81 o 12 2 0 0.55 6.38 24.97 o 13 2 0 31.89 41.54 36.02 o 14 2 0 137.84 128.44 39.89 o 1 3 0 1957.61 1859.17 17.74 o 2 3 0 5246.25 5437.20 135.19 o 3 3 0 9539.69 8820.73 181.69 o 4 3 0 875.51 736.52 21.87 o 5 3 0 335.90 344.42 22.49 o 6 3 0 12.17 32.43 18.12 o 7 3 0 55.36 50.23 18.14 o 8 3 0 92.37 89.53 23.61 o 9 3 0 1114.30 1220.14 43.70 o 10 3 0 101.91 132.36 28.10 o 11 3 0 3.21 10.11 24.84 o 12 3 0 0.38 -27.37 25.67 o 13 3 0 3.16 -14.67 35.23 o 14 3 0 16.38 8.76 53.55 o 0 4 0 11.28 5.44 10.01 o 1 4 0 38.37 10.91 7.58 o 2 4 0 825.87 876.80 19.16 o 3 4 0 729.52 993.98 19.20 o 4 4 0 135.31 145.97 14.56 o 5 4 0 1843.62 1967.49 47.12 o 6 4 0 70.62 108.04 25.18 o 7 4 0 80.06 69.20 28.29 o 8 4 0 7.08 15.83 21.51 o 9 4 0 53.87 41.16 26.86 o 10 4 0 39.59 19.68 26.54 o 11 4 0 529.59 467.43 42.45 o 12 4 0 202.99 161.20 37.88 o 13 4 0 0.75 -31.41 49.18 o 1 5 0 35.69 14.45 10.87 o 2 5 0 79.54 76.94 14.34 o 3 5 0 1534.24 1526.24 33.21 o 4 5 0 134.00 117.52 15.50 o 5 5 0 5.23 31.45 15.91 o 6 5 0 2480.68 2463.80 52.42 o 7 5 0 227.75 272.98 21.17 o 8 5 0 43.51 40.38 23.39 o 9 5 0 138.79 140.84 26.22 o 10 5 0 68.75 64.61 28.78 o 11 5 0 6.80 -4.69 28.85 o 12 5 0 95.12 83.89 32.02 o 13 5 0 36.06 15.64 31.81 o 0 6 0 167.38 137.25 19.52 o 1 6 0 1283.40 1247.35 36.62 o 2 6 0 362.09 408.05 18.68 o 3 6 0 0.00 0.65 14.75 o 4 6 0 7.67 2.13 15.78 o 5 6 0 22.42 8.62 17.57 o 6 6 0 121.61 134.83 20.72 o 7 6 0 635.29 622.48 30.31 o 8 6 0 1.78 -19.40 21.08 o 9 6 0 980.45 891.19 46.30 o 10 6 0 15.92 -20.44 24.81 o 11 6 0 4.05 -22.76 29.60 o 12 6 0 5.40 3.08 31.51 o 1 7 0 19.95 31.19 13.70 o 2 7 0 48.91 32.02 13.02 o 3 7 0 158.79 208.65 15.67 o 4 7 0 64.39 71.33 18.38 o 5 7 0 1.42 -5.20 18.66 o 6 7 0 26.36 7.92 20.05 o 7 7 0 367.09 337.20 25.19 o 8 7 0 137.89 103.02 22.55 o 9 7 0 593.41 526.42 29.57 o 10 7 0 9.40 -18.91 22.10 o 11 7 0 259.18 263.82 29.62 o 0 8 0 219.95 184.78 49.72 o 1 8 0 0.43 5.59 20.05 o 2 8 0 6.23 7.39 16.15 o 3 8 0 849.93 801.73 35.87 o 4 8 0 306.28 321.07 21.64 o 5 8 0 103.45 52.94 19.14 o 6 8 0 592.30 581.95 29.24 o 7 8 0 5.54 -1.38 20.75 o 8 8 0 224.82 214.16 24.11 o 9 8 0 115.75 115.29 23.75 o 10 8 0 122.25 145.77 29.94 o 1 9 0 27.52 -10.82 31.16 o 2 9 0 11.56 1.26 36.61 o 3 9 0 15.44 17.12 30.78 o 4 9 0 26.11 13.19 24.56 o 5 9 0 143.39 149.35 28.21 o 6 9 0 21.28 14.03 26.97 o 7 9 0 90.82 111.40 30.05 o 8 9 0 34.26 23.50 27.60 o 9 9 0 1.27 0.73 28.03 o 0 10 0 0.67 -17.85 48.85 o 1 10 0 6.11 -16.03 33.98 o 2 10 0 14.28 -1.51 38.66 o 3 10 0 0.07 -38.02 39.88 o 4 10 0 168.04 89.74 36.93 o 5 10 0 87.31 102.77 38.55 o 6 10 0 36.74 47.91 37.27 o 7 10 0 10.57 -1.51 33.10 o 1 11 0 147.58 177.25 51.63 o 2 11 0 37.63 29.79 51.18 o 3 11 0 288.50 246.92 49.96 o 4 11 0 16.92 -10.80 38.11 o 5 11 0 42.35 4.21 38.79 o -13 0 1 23.80 -1.19 47.16 o -11 0 1 1.09 -4.82 43.91 o -9 0 1 122.68 178.92 46.02 o -7 0 1 812.53 963.49 61.66 o -5 0 1 209.24 248.05 17.55 o -3 0 1 1041.22 1026.55 17.38 o 3 0 1 8863.67 7563.05 77.61 o 5 0 1 1362.20 1340.50 63.07 o 7 0 1 2271.46 2459.66 78.86 o 9 0 1 301.93 379.16 51.51 o 11 0 1 531.75 455.34 61.60 o 13 0 1 4.36 -3.80 47.99 o -14 1 1 48.92 40.41 37.21 o -13 1 1 58.15 45.31 36.39 o -12 1 1 26.21 33.03 33.86 o -11 1 1 318.49 290.52 39.46 o -10 1 1 180.54 176.76 25.46 o -9 1 1 151.22 236.89 24.64 o -8 1 1 75.91 85.06 19.59 o -7 1 1 226.88 258.05 20.52 o -6 1 1 360.90 346.02 21.82 o -5 1 1 791.54 771.59 19.08 o -4 1 1 324.79 300.05 12.67 o -3 1 1 14394.82 13642.23 143.34 o 2 1 1 349.63 229.85 41.39 o 3 1 1 252.64 226.48 10.74 o 4 1 1 65.21 89.41 10.84 o 5 1 1 1642.97 1501.23 25.85 o 6 1 1 2123.84 2011.07 34.86 o 7 1 1 702.58 706.29 27.70 o 8 1 1 7.90 14.98 17.39 o 9 1 1 143.63 128.21 21.78 o 10 1 1 5.93 21.93 31.51 o 11 1 1 35.51 14.89 31.99 o 12 1 1 1.13 -16.94 31.66 o 13 1 1 254.20 207.65 41.12 o 14 1 1 167.26 201.91 42.42 o -14 2 1 26.93 -5.70 35.88 o -13 2 1 51.64 63.80 37.00 o -12 2 1 96.68 76.76 26.50 o -11 2 1 0.10 -14.45 23.84 o -10 2 1 213.18 234.73 28.80 o -9 2 1 26.20 27.01 22.58 o -8 2 1 89.06 102.98 21.80 o -7 2 1 55.50 57.64 18.75 o -6 2 1 1484.75 1613.26 35.80 o -5 2 1 1342.97 1281.82 24.99 o -4 2 1 1577.12 1458.80 34.99 o -3 2 1 23429.77 22548.58 284.91 o -2 2 1 4528.66 4869.00 115.74 o -1 2 1 3304.18 3058.50 72.22 o 1 2 1 215.08 242.52 9.95 o 2 2 1 38088.64 37869.75 481.06 o 3 2 1 4554.31 4669.03 40.50 o 4 2 1 2619.02 2482.84 25.15 o 5 2 1 6574.33 6778.42 68.84 o 6 2 1 706.84 727.90 38.27 o 7 2 1 469.64 466.90 29.28 o 8 2 1 93.80 68.44 21.35 o 9 2 1 21.56 41.93 22.57 o 10 2 1 206.75 236.57 28.31 o 11 2 1 2.11 -32.29 22.74 o 12 2 1 77.13 67.93 34.71 o 13 2 1 0.23 -5.03 42.12 o 14 2 1 79.08 64.78 55.81 o -14 3 1 155.04 186.77 43.66 o -13 3 1 25.25 -19.15 35.66 o -12 3 1 20.44 26.83 27.64 o -11 3 1 9.55 23.67 25.96 o -10 3 1 15.18 14.93 25.81 o -9 3 1 82.10 97.93 25.89 o -8 3 1 251.41 238.20 26.48 o -7 3 1 15.07 27.00 17.74 o -6 3 1 1.56 -5.06 11.20 o -5 3 1 34.61 65.70 13.25 o -4 3 1 4581.29 4640.00 36.07 o -3 3 1 0.11 7.97 11.83 o -2 3 1 526.83 459.75 16.99 o -1 3 1 3508.15 3284.76 41.75 o 0 3 1 1203.34 1272.76 13.08 o 1 3 1 2.21 -4.30 7.43 o 2 3 1 3368.60 2904.28 65.31 o 3 3 1 1983.34 2104.34 39.62 o 4 3 1 566.31 443.01 19.97 o 5 3 1 1391.87 1324.97 40.53 o 6 3 1 201.96 202.71 21.11 o 7 3 1 232.23 252.75 24.29 o 8 3 1 34.77 35.56 22.66 o 9 3 1 97.33 54.23 25.62 o 10 3 1 413.21 394.12 54.27 o 11 3 1 492.39 467.89 34.77 o 12 3 1 433.15 386.97 39.76 o 13 3 1 15.84 -20.34 49.94 o 14 3 1 339.99 389.67 67.26 o -14 4 1 41.02 26.93 55.14 o -13 4 1 53.70 70.80 54.03 o -12 4 1 34.03 31.40 29.32 o -11 4 1 89.25 87.65 28.96 o -10 4 1 92.68 71.53 27.38 o -9 4 1 8.07 1.42 26.43 o -8 4 1 51.96 42.55 22.00 o -7 4 1 14.13 7.42 14.36 o -6 4 1 142.81 186.89 16.99 o -5 4 1 605.90 643.30 29.94 o -4 4 1 4728.04 4777.45 90.68 o -3 4 1 7844.76 7667.93 141.26 o -2 4 1 5446.95 6003.57 88.06 o -1 4 1 1654.29 1727.32 21.46 o 0 4 1 149.06 109.16 7.98 o 1 4 1 38.33 56.33 7.64 o 2 4 1 634.60 470.03 15.04 o 3 4 1 102.72 129.25 12.02 o 4 4 1 36.93 35.81 12.95 o 5 4 1 966.64 992.34 31.30 o 6 4 1 568.84 542.57 30.87 o 7 4 1 163.13 159.32 24.85 o 8 4 1 226.45 207.25 34.14 o 9 4 1 72.89 57.86 33.19 o 10 4 1 50.01 69.94 33.15 o 11 4 1 555.34 483.85 42.99 o 12 4 1 3.10 14.02 28.76 o 13 4 1 1.01 -3.78 37.57 o -13 5 1 51.49 49.76 32.98 o -12 5 1 54.19 75.45 38.36 o -11 5 1 16.76 -21.31 34.43 o -10 5 1 121.11 106.38 36.18 o -9 5 1 166.57 140.94 30.49 o -8 5 1 2.09 7.49 17.84 o -7 5 1 451.04 481.33 26.34 o -6 5 1 1585.10 1535.63 35.69 o -5 5 1 2277.41 2274.18 50.06 o -4 5 1 14.95 8.65 14.14 o -3 5 1 36.25 31.58 13.27 o -2 5 1 184.43 178.24 13.88 o -1 5 1 4.59 8.60 9.30 o 0 5 1 1049.85 1179.93 28.99 o 1 5 1 157.25 163.31 10.78 o 2 5 1 7.79 15.35 13.76 o 3 5 1 1528.00 1399.39 27.21 o 4 5 1 79.76 109.02 14.90 o 5 5 1 644.97 573.83 26.31 o 6 5 1 2093.32 1879.63 38.05 o 7 5 1 34.62 50.82 24.12 o 8 5 1 4.78 -6.17 24.99 o 9 5 1 13.68 -20.78 23.07 o 10 5 1 45.92 55.93 28.38 o 11 5 1 0.00 -16.57 28.38 o 12 5 1 1.96 4.36 30.07 o 13 5 1 11.31 17.32 38.85 o -12 6 1 138.17 110.83 34.33 o -11 6 1 3.46 -32.01 29.64 o -10 6 1 42.69 36.03 25.57 o -9 6 1 124.32 120.27 24.16 o -8 6 1 14.98 7.76 21.21 o -7 6 1 1366.87 1341.08 47.14 o -6 6 1 249.18 271.11 22.78 o -5 6 1 336.18 368.44 22.14 o -4 6 1 9.98 17.88 16.30 o -3 6 1 283.67 326.56 18.61 o -2 6 1 283.71 288.04 14.14 o -1 6 1 2648.19 2727.67 49.30 o 0 6 1 1442.00 1436.40 32.90 o 1 6 1 27.20 22.58 19.58 o 2 6 1 160.77 190.38 13.56 o 3 6 1 35.99 52.55 15.86 o 4 6 1 135.60 136.07 17.05 o 5 6 1 15.99 15.19 17.51 o 6 6 1 50.79 40.28 19.22 o 7 6 1 13.16 16.02 22.19 o 8 6 1 1300.19 1055.20 37.63 o 9 6 1 109.46 70.58 22.97 o 10 6 1 141.61 165.52 28.46 o 11 6 1 49.42 32.32 31.32 o 12 6 1 20.64 25.60 31.63 o -11 7 1 16.47 -0.58 25.69 o -10 7 1 14.21 -3.71 22.51 o -9 7 1 0.49 10.87 21.19 o -8 7 1 31.69 22.83 20.76 o -7 7 1 0.72 1.46 19.35 o -6 7 1 130.07 158.23 22.36 o -5 7 1 292.80 309.95 25.98 o -4 7 1 0.02 -8.79 18.10 o -3 7 1 910.24 883.79 24.69 o -2 7 1 234.93 215.92 15.08 o -1 7 1 82.88 49.21 14.09 o 0 7 1 218.71 189.26 21.64 o 1 7 1 980.75 969.60 41.99 o 2 7 1 17.74 41.58 20.96 o 3 7 1 7.10 5.81 14.94 o 4 7 1 45.24 23.08 22.65 o 5 7 1 112.07 96.75 19.81 o 6 7 1 20.81 17.80 19.89 o 7 7 1 33.71 66.60 21.05 o 8 7 1 126.39 112.09 19.91 o 9 7 1 1.47 -12.61 21.01 o 10 7 1 21.87 12.07 24.34 o 11 7 1 265.50 250.62 29.42 o -10 8 1 112.37 100.44 28.80 o -9 8 1 45.80 26.55 22.51 o -8 8 1 37.98 21.61 21.48 o -7 8 1 200.56 189.92 22.44 o -6 8 1 424.75 292.73 23.86 o -5 8 1 1.01 -12.08 18.69 o -4 8 1 20.34 9.16 18.55 o -3 8 1 16.23 25.37 22.71 o -2 8 1 238.52 174.90 17.97 o -1 8 1 0.00 -0.29 19.79 o 0 8 1 240.51 182.13 35.17 o 1 8 1 11.95 35.43 21.94 o 2 8 1 21.08 50.86 36.94 o 3 8 1 154.29 130.91 25.85 o 4 8 1 57.10 81.85 25.17 o 5 8 1 139.04 142.10 26.27 o 6 8 1 704.72 700.89 29.43 o 7 8 1 61.03 37.70 20.91 o 8 8 1 0.28 -13.79 18.91 o 9 8 1 117.46 98.77 28.27 o 10 8 1 0.00 11.99 27.82 o -9 9 1 134.68 102.87 29.61 o -8 9 1 5.37 -18.18 26.24 o -7 9 1 86.53 94.85 26.99 o -6 9 1 6.04 -3.83 24.50 o -5 9 1 60.70 37.17 25.91 o -4 9 1 14.91 18.91 24.02 o -3 9 1 18.04 10.85 30.76 o -2 9 1 8.66 -11.99 36.95 o -1 9 1 80.42 75.04 33.03 o 0 9 1 28.55 2.01 31.29 o 1 9 1 13.07 29.13 31.96 o 2 9 1 8.00 -39.31 36.40 o 3 9 1 113.83 161.91 34.46 o 4 9 1 0.00 21.62 25.26 o 5 9 1 186.14 138.60 28.36 o 6 9 1 0.00 -28.54 26.14 o 7 9 1 119.12 111.12 26.67 o 8 9 1 42.27 47.93 30.54 o 9 9 1 3.16 11.69 28.40 o -7 10 1 3.35 -11.88 32.56 o -6 10 1 1.64 -16.15 32.71 o -5 10 1 41.72 38.94 36.80 o -4 10 1 100.26 127.30 37.10 o -3 10 1 19.64 5.33 34.92 o -2 10 1 126.52 116.89 55.76 o -1 10 1 45.11 21.66 35.15 o 0 10 1 212.51 231.71 40.59 o 1 10 1 24.13 24.19 35.96 o 2 10 1 10.41 -30.29 38.34 o 3 10 1 47.15 32.06 35.30 o 4 10 1 100.81 71.31 36.80 o 5 10 1 12.34 -7.68 35.49 o 6 10 1 2.72 -14.76 30.84 o 7 10 1 2.47 4.54 30.76 o -5 11 1 0.04 -17.66 34.03 o -4 11 1 3.51 -10.84 33.34 o -3 11 1 197.87 214.39 48.87 o -2 11 1 2.37 -18.94 41.90 o -1 11 1 3.53 29.64 37.67 o 0 11 1 191.24 232.18 43.23 o 1 11 1 88.29 122.22 59.11 o 2 11 1 43.59 13.39 43.32 o 3 11 1 9.53 -37.11 42.55 o 4 11 1 6.95 8.11 38.02 o 5 11 1 1.55 -11.92 32.93 o -14 0 2 14.23 24.20 51.01 o -12 0 2 315.91 314.34 59.50 o -10 0 2 255.65 208.95 51.34 o -8 0 2 856.46 758.42 65.29 o -6 0 2 644.49 690.16 29.77 o -4 0 2 3.33 2.42 10.14 o 4 0 2 4894.42 4959.82 118.69 o 6 0 2 6478.10 6652.49 107.90 o 8 0 2 2210.91 2442.45 86.48 o 10 0 2 685.72 686.65 75.77 o 12 0 2 43.06 73.93 49.23 o 14 0 2 130.56 128.15 56.61 o -14 1 2 27.73 38.00 36.56 o -13 1 2 33.45 50.04 36.02 o -12 1 2 176.36 188.21 38.42 o -11 1 2 16.74 -12.32 22.68 o -10 1 2 13.58 17.21 22.93 o -9 1 2 536.46 605.18 34.58 o -8 1 2 271.74 298.33 23.89 o -7 1 2 299.33 320.56 21.86 o -6 1 2 268.65 264.34 15.54 o -5 1 2 88.00 97.57 8.82 o -4 1 2 1737.12 1636.81 34.17 o -3 1 2 6067.55 5528.55 47.67 o -2 1 2 19077.46 18284.85 175.04 o 1 1 2 4.30 -0.07 2.32 o 2 1 2 5609.91 5185.40 72.77 o 3 1 2 64.16 37.61 10.01 o 4 1 2 8641.04 8849.98 44.64 o 5 1 2 122.90 108.85 13.97 o 6 1 2 127.63 133.34 24.01 o 7 1 2 654.49 703.63 27.66 o 8 1 2 626.64 729.24 31.56 o 9 1 2 68.22 106.09 30.56 o 10 1 2 54.22 84.39 33.98 o 11 1 2 106.13 120.17 35.74 o 12 1 2 2.74 -12.47 32.02 o 13 1 2 0.59 11.34 34.78 o 14 1 2 140.12 127.81 54.80 o -14 2 2 1.17 12.61 37.11 o -13 2 2 79.92 82.52 37.70 o -12 2 2 1.91 9.35 25.58 o -11 2 2 76.85 36.74 25.44 o -10 2 2 92.35 84.35 26.86 o -9 2 2 74.46 61.48 23.91 o -8 2 2 440.44 444.12 28.78 o -7 2 2 41.77 36.72 18.57 o -6 2 2 60.34 49.82 18.15 o -5 2 2 1607.95 1646.13 32.57 o -4 2 2 1962.05 1790.58 25.07 o -3 2 2 1827.80 1858.86 19.59 o -2 2 2 7724.80 7534.36 184.31 o -1 2 2 15793.80 14019.92 266.72 o 0 2 2 4682.85 4358.95 55.83 o 1 2 2 7333.19 6519.87 192.99 o 2 2 2 44367.97 42295.24 567.16 o 3 2 2 8275.99 8347.18 123.32 o 4 2 2 659.08 654.20 19.51 o 5 2 2 2389.15 2753.63 41.47 o 6 2 2 2.25 -6.36 17.43 o 7 2 2 345.47 356.77 29.99 o 8 2 2 34.00 26.73 24.22 o 9 2 2 3.24 -1.23 21.93 o 10 2 2 47.22 42.91 24.50 o 11 2 2 17.69 32.04 23.63 o 12 2 2 65.06 4.25 33.86 o 13 2 2 358.13 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