#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/68/2016829.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016829_Fobs loop_ _publ_author_name 'Britton, Doyle' _publ_section_title ; 2,4,6-Trifluorobenzonitrile ; _journal_coeditor_code FN3002 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o583 _journal_page_last o585 _journal_volume 64 _journal_year 2008 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.5228 _cell_length_b 13.8222 _cell_length_c 30.7552 _exptl_crystal_F_000 1560.00 _reflns_d_resolution_high 0.7695 _[local]_cod_data_source_file fn3002Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'F3PhCN in Cmcm' _shelx_refln_list_code 4 _shelx_F_calc_maximum 965.07 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, z+1/2' '-x, y, z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' '-x, -y, -z' 'x, y, -z-1/2' '-x, y, -z-1/2' 'x, -y, -z' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' '-x+1/2, y+1/2, -z-1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11752.80 13991.59 177.65 o 4 0 0 27222.33 26974.79 341.54 o 6 0 0 86914.80 87814.30 1272.51 o 8 0 0 34.79 50.12 4.90 o 1 1 0 15523.29 15578.69 168.61 o 3 1 0 363.58 336.79 4.23 o 5 1 0 0.67 2.42 2.74 o 7 1 0 1387.55 1328.36 17.55 o 9 1 0 45.62 63.49 9.91 o 0 2 0 25416.97 26210.39 300.94 o 2 2 0 51939.41 52343.61 502.28 o 4 2 0 1105.15 1085.73 11.44 o 6 2 0 3289.39 3115.69 32.72 o 8 2 0 1652.99 1641.34 23.88 o 1 3 0 19231.22 19141.10 171.71 o 3 3 0 676.99 776.65 8.37 o 5 3 0 9969.83 10530.09 102.62 o 7 3 0 283.97 298.67 7.77 o 9 3 0 401.49 376.38 10.76 o 0 4 0 7682.85 7959.54 101.94 o 2 4 0 1251.56 1101.64 11.07 o 4 4 0 394.63 528.02 7.16 o 6 4 0 175.96 143.52 3.83 o 8 4 0 249.66 226.94 7.84 o 1 5 0 445.07 390.64 4.70 o 3 5 0 33527.90 36112.30 323.07 o 5 5 0 5577.67 6085.52 60.79 o 7 5 0 3078.80 2557.93 30.96 o 9 5 0 344.95 416.02 13.41 o 0 6 0 231.17 264.59 5.35 o 2 6 0 902.62 836.85 9.07 o 4 6 0 164.10 174.88 4.18 o 6 6 0 50.62 45.84 3.45 o 8 6 0 4.47 1.72 4.69 o 1 7 0 2297.40 2902.48 27.62 o 3 7 0 13142.69 14009.27 126.75 o 5 7 0 1228.73 1373.56 17.96 o 7 7 0 1764.70 1425.83 21.56 o 0 8 0 31399.53 33987.07 430.28 o 2 8 0 0.92 9.92 1.56 o 4 8 0 19.31 35.71 3.42 o 6 8 0 3991.43 3393.91 43.89 o 8 8 0 0.39 10.13 4.79 o 1 9 0 1237.54 1266.17 13.49 o 3 9 0 4224.25 4253.20 77.84 o 5 9 0 283.73 287.52 7.50 o 7 9 0 24.08 38.81 5.18 o 0 10 0 2438.40 2207.81 31.43 o 2 10 0 1288.78 1117.26 13.69 o 4 10 0 4169.05 4161.86 52.12 o 6 10 0 297.95 262.79 7.64 o 8 10 0 6.20 4.59 6.93 o 1 11 0 3.40 4.40 2.16 o 3 11 0 22.76 53.75 6.11 o 5 11 0 2.13 -2.46 3.34 o 7 11 0 116.62 145.72 7.44 o 0 12 0 3143.96 2508.75 42.74 o 2 12 0 1936.62 1731.48 28.78 o 4 12 0 0.62 1.70 3.56 o 6 12 0 1089.52 1348.60 24.58 o 1 13 0 3335.17 2919.55 34.84 o 3 13 0 141.02 139.36 6.10 o 5 13 0 551.04 557.35 11.94 o 0 14 0 407.37 371.40 13.32 o 2 14 0 63.02 64.79 4.94 o 4 14 0 0.63 -3.75 3.75 o 1 15 0 931.05 935.19 18.13 o 3 15 0 589.65 521.98 12.87 o 5 15 0 332.52 383.75 23.12 o 0 16 0 76.09 71.24 10.08 o 2 16 0 5.34 4.05 4.19 o 4 16 0 13.12 19.99 6.86 o 1 17 0 12.24 30.94 6.42 o 3 17 0 1048.54 1283.49 28.17 o 1 1 1 18931.08 19137.11 126.21 o 3 1 1 1825.53 2170.40 14.61 o 5 1 1 74.71 56.01 1.70 o 7 1 1 1089.52 1065.64 10.50 o 9 1 1 404.11 384.23 8.93 o 0 2 1 4881.27 4920.13 44.80 o 2 2 1 6601.58 6554.09 43.39 o 4 2 1 62.04 45.04 1.33 o 6 2 1 617.86 595.52 6.06 o 8 2 1 349.32 353.70 6.40 o 1 3 1 3327.48 3290.56 21.38 o 3 3 1 581.89 661.98 6.59 o 5 3 1 1909.40 2020.14 15.47 o 7 3 1 61.66 63.15 2.56 o 9 3 1 100.97 104.59 4.97 o 0 4 1 3146.37 2952.99 27.34 o 2 4 1 4616.68 4301.78 28.00 o 4 4 1 527.44 855.15 7.00 o 6 4 1 40.97 24.71 1.79 o 8 4 1 357.05 292.92 5.86 o 1 5 1 1.54 3.16 0.63 o 3 5 1 5.00 21.22 1.57 o 5 5 1 8.97 13.57 2.07 o 7 5 1 3.63 20.30 2.38 o 9 5 1 0.02 -0.84 3.80 o 0 6 1 9072.42 9356.96 84.84 o 2 6 1 798.09 784.10 6.18 o 4 6 1 1940.02 1943.88 14.92 o 6 6 1 175.33 218.20 3.97 o 8 6 1 119.32 110.47 4.91 o 1 7 1 231.57 317.66 3.12 o 3 7 1 3048.92 3037.72 20.66 o 5 7 1 234.39 274.83 4.28 o 7 7 1 313.61 258.98 5.58 o 0 8 1 7780.28 8422.90 76.95 o 2 8 1 17.54 33.43 1.26 o 4 8 1 36.50 39.01 1.92 o 6 8 1 1083.71 938.49 10.54 o 8 8 1 0.01 2.10 3.22 o 1 9 1 2952.50 3160.43 21.53 o 3 9 1 15508.05 15091.68 112.24 o 5 9 1 1326.80 1191.08 13.00 o 7 9 1 0.91 4.99 2.94 o 0 10 1 35.70 39.56 2.32 o 2 10 1 15.12 16.62 1.98 o 4 10 1 54.03 66.17 4.74 o 6 10 1 5.90 3.58 2.63 o 8 10 1 0.08 -1.00 4.64 o 1 11 1 183.41 146.76 2.84 o 3 11 1 6085.40 5899.22 50.60 o 5 11 1 18.12 22.49 2.72 o 7 11 1 696.39 695.06 11.22 o 0 12 1 438.29 346.88 7.15 o 2 12 1 294.64 262.44 5.19 o 4 12 1 0.08 -2.14 2.23 o 6 12 1 156.42 202.59 5.75 o 1 13 1 813.58 688.40 8.02 o 3 13 1 43.94 48.64 3.26 o 5 13 1 120.35 126.64 4.52 o 0 14 1 1623.63 1548.49 20.85 o 2 14 1 234.84 213.89 5.29 o 4 14 1 1.03 6.25 3.25 o 1 15 1 2.34 0.84 2.94 o 3 15 1 8.53 11.77 3.17 o 5 15 1 0.33 15.25 10.82 o 0 16 1 984.48 933.09 18.57 o 2 16 1 47.86 70.02 4.04 o 4 16 1 401.50 417.05 10.00 o 1 17 1 0.00 -2.50 3.30 o 3 17 1 168.20 224.42 10.63 o 0 0 2 746.55 425.39 8.56 o 2 0 2 18.50 19.62 0.91 o 4 0 2 147.46 156.19 3.65 o 6 0 2 509.63 544.19 9.22 o 8 0 2 4.02 10.00 3.16 o 1 1 2 3648.39 3717.43 24.80 o 3 1 2 1800.79 1846.84 12.18 o 5 1 2 64.53 66.13 1.54 o 7 1 2 677.06 640.84 7.34 o 9 1 2 13.60 20.24 3.88 o 0 2 2 165.77 142.86 1.85 o 2 2 2 3153.10 3249.16 21.89 o 4 2 2 592.11 676.47 5.45 o 6 2 2 42.66 48.90 2.58 o 8 2 2 5.49 14.76 2.85 o 1 3 2 79.93 86.11 1.07 o 3 3 2 1703.99 1890.26 13.44 o 5 3 2 59.07 59.32 1.85 o 7 3 2 9.85 11.44 2.12 o 9 3 2 24.75 44.73 4.46 o 0 4 2 4665.43 4956.48 45.22 o 2 4 2 72.78 86.02 1.24 o 4 4 2 116.93 119.38 2.13 o 6 4 2 186.57 181.20 3.20 o 8 4 2 36.30 42.95 3.35 o 1 5 2 15.18 18.91 0.66 o 3 5 2 112.04 126.33 1.92 o 5 5 2 21.81 28.47 1.61 o 7 5 2 13.71 11.87 2.39 o 9 5 2 9.19 9.33 4.07 o 0 6 2 4944.25 5292.78 48.68 o 2 6 2 546.36 493.14 4.19 o 4 6 2 42.84 48.04 1.60 o 6 6 2 331.32 286.80 4.53 o 8 6 2 23.33 30.04 4.27 o 1 7 2 465.08 476.91 4.18 o 3 7 2 267.90 235.96 3.06 o 5 7 2 64.50 61.79 2.12 o 7 7 2 2.21 1.36 2.61 o 0 8 2 50.95 70.45 4.01 o 2 8 2 208.19 197.87 2.50 o 4 8 2 4.82 2.66 1.68 o 6 8 2 3.22 11.75 2.67 o 8 8 2 18.09 15.17 3.56 o 1 9 2 23.64 31.18 1.46 o 3 9 2 447.25 442.40 5.85 o 5 9 2 16.35 16.69 2.89 o 7 9 2 16.37 10.38 3.02 o 0 10 2 176.20 183.70 4.11 o 2 10 2 124.94 115.02 2.55 o 4 10 2 79.41 74.43 6.00 o 6 10 2 12.26 9.22 2.91 o 8 10 2 5.12 3.45 6.67 o 1 11 2 58.01 54.08 1.97 o 3 11 2 1247.56 1216.18 13.14 o 5 11 2 0.27 -0.30 2.19 o 7 11 2 0.58 0.85 3.24 o 0 12 2 16.79 21.66 3.59 o 2 12 2 229.43 218.05 4.45 o 4 12 2 33.08 25.17 2.70 o 6 12 2 3.28 9.03 3.55 o 1 13 2 98.21 97.61 3.24 o 3 13 2 2.87 2.10 2.56 o 5 13 2 38.69 48.46 4.23 o 0 14 2 172.59 150.16 5.15 o 2 14 2 17.30 21.01 2.92 o 4 14 2 0.14 -3.00 3.00 o 1 15 2 0.51 1.10 2.45 o 3 15 2 11.16 15.91 3.44 o 5 15 2 11.90 7.34 6.12 o 0 16 2 0.29 3.38 5.06 o 2 16 2 0.00 -1.96 3.16 o 4 16 2 6.39 1.10 4.76 o 1 17 2 19.61 11.65 3.59 o 3 17 2 150.84 161.07 6.57 o 1 1 3 1353.55 1341.86 8.98 o 3 1 3 695.44 771.54 5.78 o 5 1 3 10.11 15.37 1.30 o 7 1 3 46.77 66.90 3.28 o 9 1 3 40.26 53.18 4.32 o 0 2 3 709.25 709.18 7.11 o 2 2 3 700.48 664.33 5.86 o 4 2 3 10.80 11.38 1.56 o 6 2 3 138.48 127.35 3.20 o 8 2 3 43.67 53.15 3.05 o 1 3 3 5.14 8.48 0.44 o 3 3 3 1.93 11.41 1.85 o 5 3 3 34.56 40.31 1.66 o 7 3 3 17.60 18.41 2.21 o 9 3 3 0.00 6.43 3.70 o 0 4 3 433.99 397.69 4.49 o 2 4 3 220.56 194.10 2.15 o 4 4 3 168.18 217.85 2.71 o 6 4 3 11.72 10.52 1.75 o 8 4 3 27.07 32.38 3.19 o 1 5 3 0.22 0.08 0.48 o 3 5 3 158.51 152.85 2.10 o 5 5 3 0.28 1.94 1.51 o 7 5 3 0.63 0.89 2.51 o 9 5 3 3.88 2.95 4.47 o 0 6 3 1420.60 1377.03 13.80 o 2 6 3 27.92 33.18 1.03 o 4 6 3 162.45 168.07 2.60 o 6 6 3 11.18 23.16 2.33 o 8 6 3 17.08 14.97 3.23 o 1 7 3 226.21 249.52 2.68 o 3 7 3 537.43 531.35 4.75 o 5 7 3 1.76 7.01 1.78 o 7 7 3 67.12 53.88 3.22 o 0 8 3 333.42 349.19 5.55 o 2 8 3 0.05 0.88 1.02 o 4 8 3 36.83 40.41 1.95 o 6 8 3 14.46 17.08 3.00 o 8 8 3 1.61 7.64 3.43 o 1 9 3 744.41 750.95 6.55 o 3 9 3 1027.53 1048.24 10.01 o 5 9 3 158.56 133.69 3.69 o 7 9 3 1.60 -2.80 2.80 o 0 10 3 36.51 46.79 2.52 o 2 10 3 26.18 33.45 1.96 o 4 10 3 47.18 64.13 5.38 o 6 10 3 4.91 -0.07 2.78 o 8 10 3 6.40 8.09 5.03 o 1 11 3 80.21 70.29 2.15 o 3 11 3 996.46 1021.27 12.08 o 5 11 3 0.33 -2.53 2.53 o 7 11 3 50.06 58.08 4.31 o 0 12 3 61.88 51.01 3.15 o 2 12 3 26.46 28.89 3.96 o 4 12 3 64.29 52.64 3.01 o 6 12 3 23.44 40.63 4.02 o 1 13 3 8.54 6.67 2.36 o 3 13 3 0.00 -2.45 2.45 o 5 13 3 1.23 4.94 3.31 o 0 14 3 76.85 79.03 4.57 o 2 14 3 13.80 14.71 2.91 o 4 14 3 1.80 -0.87 3.52 o 6 14 3 1.51 -9.84 9.84 o 1 15 3 18.00 18.34 3.09 o 3 15 3 0.59 2.55 2.93 o 5 15 3 8.90 8.51 6.14 o 0 16 3 50.87 49.31 4.88 o 2 16 3 8.04 5.09 2.98 o 4 16 3 36.46 36.47 6.30 o 1 17 3 0.38 -3.31 3.31 o 3 17 3 1.40 3.31 5.02 o 0 0 4 534.56 520.19 17.73 o 2 0 4 0.15 2.96 1.35 o 4 0 4 84.34 97.57 2.20 o 6 0 4 160.52 158.97 5.62 o 8 0 4 1.90 -1.51 3.55 o 1 1 4 11480.76 11920.45 76.16 o 3 1 4 5033.17 5186.31 33.63 o 5 1 4 563.66 618.38 5.58 o 7 1 4 4543.28 4298.07 35.66 o 9 1 4 11.29 17.35 3.87 o 0 2 4 2112.71 2135.66 19.79 o 2 2 4 19150.27 19445.67 127.18 o 4 2 4 4890.83 5442.40 35.53 o 6 2 4 313.29 302.88 3.95 o 8 2 4 284.38 322.19 6.07 o 1 3 4 44.25 53.52 0.82 o 3 3 4 16177.94 17280.64 113.33 o 5 3 4 486.73 457.22 4.64 o 7 3 4 53.01 59.82 2.51 o 9 3 4 228.03 284.14 7.26 o 0 4 4 26180.70 26944.05 241.85 o 2 4 4 1106.99 1246.33 9.97 o 4 4 4 1597.94 1583.84 11.84 o 6 4 4 1391.43 1320.17 11.69 o 8 4 4 177.21 157.23 4.51 o 1 5 4 157.14 178.91 2.24 o 3 5 4 126.11 118.23 2.03 o 5 5 4 0.66 5.66 2.13 o 7 5 4 11.05 9.26 2.30 o 9 5 4 0.40 8.55 4.82 o 0 6 4 35847.80 38804.78 347.10 o 2 6 4 3678.32 3259.89 21.75 o 4 6 4 157.15 178.18 2.84 o 6 6 4 2957.67 2427.00 20.61 o 8 6 4 228.62 251.13 6.01 o 1 7 4 2468.58 2575.91 18.20 o 3 7 4 288.98 236.19 2.93 o 5 7 4 336.42 283.94 4.29 o 7 7 4 157.64 132.01 3.94 o 0 8 4 0.61 1.38 1.27 o 2 8 4 2853.47 2822.51 20.07 o 4 8 4 12.42 19.31 1.86 o 6 8 4 0.35 2.79 2.74 o 8 8 4 335.06 344.53 7.34 o 1 9 4 1376.89 1420.93 11.02 o 3 9 4 1803.20 1777.99 14.76 o 5 9 4 105.71 119.90 3.53 o 7 9 4 8.85 5.39 3.04 o 0 10 4 14.72 42.16 3.78 o 2 10 4 0.81 10.38 2.72 o 4 10 4 6.38 61.08 9.61 o 6 10 4 2.27 3.06 2.67 o 8 10 4 0.38 6.75 5.19 o 1 11 4 456.07 512.37 5.83 o 3 11 4 14580.05 14509.71 113.52 o 5 11 4 0.15 -2.34 2.34 o 7 11 4 0.06 -0.08 3.15 o 0 12 4 328.33 295.67 6.47 o 2 12 4 478.42 481.05 7.54 o 4 12 4 67.98 68.45 3.17 o 6 12 4 121.10 144.76 4.92 o 1 13 4 812.22 785.80 8.84 o 3 13 4 1.48 5.39 2.37 o 5 13 4 582.66 599.09 10.16 o 0 14 4 256.37 191.85 6.28 o 2 14 4 93.58 94.72 3.84 o 4 14 4 0.07 -3.28 3.28 o 6 14 4 100.56 116.36 10.09 o 1 15 4 0.35 -0.49 2.48 o 3 15 4 0.00 11.43 4.71 o 5 15 4 6.98 2.87 5.04 o 0 16 4 10.74 21.39 4.89 o 2 16 4 4.38 -2.88 2.88 o 4 16 4 49.98 64.48 10.02 o 1 17 4 58.82 58.23 4.42 o 3 17 4 214.67 239.99 24.35 o 1 1 5 355.27 405.69 3.35 o 3 1 5 4023.80 4038.05 26.41 o 5 1 5 97.04 94.28 1.93 o 7 1 5 1047.24 1118.43 12.20 o 9 1 5 49.77 54.39 3.89 o 0 2 5 24729.84 25439.47 229.31 o 2 2 5 78537.50 81529.45 517.69 o 4 2 5 20910.30 23466.69 149.00 o 6 2 5 1382.21 1317.07 11.44 o 8 2 5 1631.02 1682.95 18.13 o 1 3 5 1489.56 1652.68 11.12 o 3 3 5 60598.66 64500.30 421.69 o 5 3 5 3992.50 3700.89 25.86 o 7 3 5 168.92 188.19 3.85 o 9 3 5 759.67 902.65 13.95 o 0 4 5 5734.05 5906.77 53.92 o 2 4 5 118.03 144.99 2.59 o 4 4 5 65.35 44.62 1.65 o 6 4 5 367.24 371.35 4.86 o 8 4 5 45.31 47.67 3.72 o 1 5 5 5863.16 5321.58 35.77 o 3 5 5 4406.55 4857.17 32.96 o 5 5 5 3445.98 3365.47 25.80 o 7 5 5 138.54 104.55 3.06 o 9 5 5 114.76 181.88 5.99 o 0 6 5 12673.70 12895.08 109.45 o 2 6 5 507.75 431.90 3.82 o 4 6 5 182.02 197.90 2.88 o 6 6 5 646.57 568.99 7.20 o 8 6 5 95.47 113.60 4.07 o 1 7 5 5161.95 5618.11 38.03 o 3 7 5 2966.52 2630.46 19.53 o 5 7 5 956.15 851.96 8.78 o 7 7 5 814.81 680.66 9.10 o 0 8 5 91.65 110.64 2.48 o 2 8 5 10399.28 10514.25 79.31 o 4 8 5 2.18 4.35 1.65 o 6 8 5 8.94 10.63 2.50 o 8 8 5 1034.90 998.21 13.86 o 1 9 5 46.19 40.57 1.42 o 3 9 5 1354.59 1412.20 12.23 o 5 9 5 6.54 1.02 2.79 o 7 9 5 36.08 12.49 3.56 o 0 10 5 20101.67 20059.81 182.33 o 2 10 5 14642.45 14161.65 94.54 o 4 10 5 21748.08 21447.49 166.28 o 6 10 5 983.78 1079.36 13.42 o 8 10 5 368.53 503.87 15.52 o 1 11 5 125.12 130.55 2.61 o 3 11 5 3965.19 3928.52 34.99 o 5 11 5 3.44 8.64 2.62 o 7 11 5 19.71 17.20 3.52 o 0 12 5 3382.20 3069.07 35.99 o 2 12 5 796.41 838.38 9.46 o 4 12 5 4.84 4.77 2.43 o 6 12 5 1146.52 1273.30 15.66 o 1 13 5 2377.26 2197.94 20.33 o 3 13 5 3.95 4.24 2.36 o 5 13 5 1927.95 1910.83 22.51 o 0 14 5 241.12 209.49 6.63 o 2 14 5 78.90 83.65 3.43 o 4 14 5 8.62 11.24 3.43 o 1 15 5 10.46 20.25 2.91 o 3 15 5 939.63 1094.44 16.27 o 5 15 5 31.18 54.99 8.04 o 0 16 5 3.18 -2.68 4.05 o 2 16 5 3.21 -1.37 2.90 o 4 16 5 36.27 62.52 10.26 o 1 17 5 412.03 390.68 8.59 o 0 0 6 335.76 313.97 6.25 o 2 0 6 76.47 63.60 1.77 o 4 0 6 12.49 19.72 1.49 o 6 0 6 11.36 22.78 3.03 o 8 0 6 0.40 3.19 4.27 o 1 1 6 22310.82 23734.39 156.47 o 3 1 6 21744.28 22529.89 142.75 o 5 1 6 577.53 584.07 5.37 o 7 1 6 8082.13 7858.97 68.96 o 9 1 6 136.93 142.33 4.92 o 0 2 6 15646.10 15402.35 138.31 o 2 2 6 20401.81 20326.67 128.95 o 4 2 6 3917.91 4306.95 28.49 o 6 2 6 781.81 751.10 7.82 o 8 2 6 597.22 636.39 9.03 o 1 3 6 2624.20 2699.32 18.35 o 3 3 6 12616.62 13316.01 84.99 o 5 3 6 2570.69 2489.67 18.02 o 7 3 6 137.10 133.73 3.35 o 9 3 6 144.35 206.10 6.36 o 0 4 6 37804.57 38162.43 342.94 o 2 4 6 983.62 837.60 6.49 o 4 4 6 482.22 457.31 4.39 o 6 4 6 2363.67 2156.74 17.66 o 8 4 6 515.00 461.37 8.09 o 1 5 6 256.52 265.42 2.69 o 3 5 6 264.62 278.73 3.04 o 5 5 6 0.02 5.91 1.75 o 7 5 6 20.54 24.23 2.53 o 9 5 6 0.54 4.30 3.79 o 0 6 6 57562.33 62626.79 807.72 o 2 6 6 3147.23 2812.58 18.98 o 4 6 6 637.46 646.51 6.18 o 6 6 6 4464.36 3663.66 31.02 o 8 6 6 414.33 468.49 8.34 o 1 7 6 180.68 233.91 2.76 o 3 7 6 581.74 508.90 5.38 o 5 7 6 30.54 19.57 2.18 o 7 7 6 171.95 145.55 4.08 o 0 8 6 102.40 105.78 2.65 o 2 8 6 3680.28 3656.78 24.74 o 4 8 6 11.58 13.46 1.82 o 6 8 6 15.06 19.67 2.67 o 8 8 6 361.95 346.49 7.37 o 1 9 6 87.90 79.87 1.95 o 3 9 6 20.61 35.53 2.68 o 5 9 6 17.11 12.91 2.27 o 7 9 6 231.51 196.03 5.18 o 0 10 6 340.59 372.86 6.39 o 2 10 6 80.06 101.20 4.07 o 4 10 6 153.74 233.02 8.80 o 6 10 6 26.20 37.54 3.49 o 1 11 6 32.85 19.01 1.82 o 3 11 6 11485.60 11027.41 101.59 o 5 11 6 171.34 192.87 4.85 o 7 11 6 3.98 16.84 3.47 o 0 12 6 1263.18 1139.70 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56.98 4.46 o 0 10 28 0.02 9.80 4.68 o 2 10 28 39.42 47.11 4.45 o 4 10 28 26.16 36.76 6.93 o 1 11 28 23.60 35.11 4.14 o 3 11 28 9.23 18.85 5.57 o 0 12 28 159.89 175.20 11.65 o 2 12 28 117.14 127.90 7.53 o 1 1 29 3240.21 3037.44 26.11 o 3 1 29 12.33 24.61 2.50 o 5 1 29 633.98 640.86 9.46 o 0 2 29 746.85 826.42 14.20 o 2 2 29 293.34 296.00 5.29 o 4 2 29 114.81 116.02 3.69 o 6 2 29 94.03 104.08 4.40 o 1 3 29 0.53 3.06 2.19 o 3 3 29 0.06 3.20 2.38 o 5 3 29 2.20 3.81 2.89 o 0 4 29 105.88 103.35 5.46 o 2 4 29 147.71 132.26 3.52 o 4 4 29 151.54 142.48 4.09 o 6 4 29 5.64 12.13 3.80 o 1 5 29 98.53 89.36 3.52 o 3 5 29 66.06 71.33 3.47 o 5 5 29 19.00 24.29 3.37 o 0 6 29 312.97 290.20 8.79 o 2 6 29 1.45 0.86 3.20 o 4 6 29 7.65 10.04 2.84 o 1 7 29 115.24 107.88 3.93 o 3 7 29 116.86 123.48 4.64 o 5 7 29 22.02 32.11 3.82 o 0 8 29 656.45 678.19 14.98 o 2 8 29 2.12 1.99 3.07 o 4 8 29 2.87 3.42 3.52 o 1 9 29 256.93 239.85 6.12 o 3 9 29 463.40 448.17 8.82 o 0 10 29 65.13 74.26 5.73 o 2 10 29 9.16 2.65 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11 30 30.07 21.76 4.32 o 1 1 31 308.51 308.18 5.54 o 3 1 31 220.91 203.93 5.17 o 5 1 31 38.54 51.75 4.14 o 0 2 31 846.47 811.03 14.00 o 2 2 31 57.10 64.18 3.25 o 4 2 31 9.22 14.11 3.02 o 6 2 31 213.12 221.08 10.94 o 1 3 31 23.33 29.55 3.12 o 3 3 31 108.98 100.74 3.85 o 5 3 31 100.78 92.68 4.07 o 0 4 31 79.67 95.88 7.02 o 2 4 31 18.35 17.06 4.40 o 4 4 31 375.40 361.18 6.53 o 1 5 31 50.84 48.80 3.77 o 3 5 31 56.76 69.94 3.90 o 5 5 31 5.82 0.81 3.58 o 0 6 31 103.47 84.96 5.74 o 2 6 31 0.67 -1.09 3.24 o 4 6 31 177.17 155.88 5.37 o 1 7 31 30.69 17.30 3.62 o 3 7 31 574.60 535.17 9.52 o 0 8 31 156.40 176.90 7.73 o 2 8 31 132.97 128.61 4.82 o 4 8 31 168.38 152.82 8.28 o 1 9 31 8.44 8.97 3.43 o 3 9 31 2869.01 2877.07 34.26 o 0 10 31 2.13 -4.29 5.36 o 2 10 31 46.03 51.79 6.64 o 1 11 31 10.30 3.86 7.47 o 0 0 32 5277.55 5361.55 104.77 o 2 0 32 267.60 219.06 7.84 o 4 0 32 583.58 535.92 12.71 o 1 1 32 21.87 39.51 3.09 o 3 1 32 32.86 34.71 3.38 o 5 1 32 7.63 7.44 3.21 o 0 2 32 502.85 563.79 12.57 o 2 2 32 22.71 41.41 3.30 o 4 2 32 44.29 41.58 3.50 o 1 3 32 22.40 27.15 3.38 o 3 3 32 23.17 16.40 3.03 o 5 3 32 35.26 34.17 4.85 o 0 4 32 206.56 224.68 8.05 o 2 4 32 10.38 10.35 3.21 o 4 4 32 30.95 46.48 3.83 o 1 5 32 1.96 0.33 3.28 o 3 5 32 83.96 99.37 4.71 o 5 5 32 40.17 49.99 5.82 o 0 6 32 20.06 23.12 5.40 o 2 6 32 12.74 10.23 4.17 o 4 6 32 4.90 1.11 3.36 o 1 7 32 6.62 3.69 3.42 o 3 7 32 687.18 677.74 11.11 o 0 8 32 156.22 146.41 7.12 o 2 8 32 17.36 18.43 3.82 o 1 9 32 12.22 16.28 3.92 o 3 9 32 178.72 199.25 9.52 o 0 10 32 110.70 113.65 17.46 o 2 10 32 49.67 66.15 8.75 o 1 1 33 59.60 52.64 3.54 o 3 1 33 4.00 5.87 3.09 o 5 1 33 43.56 41.09 4.51 o 0 2 33 216.67 228.77 8.10 o 2 2 33 127.42 117.32 4.08 o 4 2 33 100.30 97.70 4.32 o 1 3 33 101.69 112.70 4.38 o 3 3 33 71.17 76.44 3.70 o 5 3 33 35.60 40.40 4.86 o 0 4 33 7.25 17.62 4.81 o 2 4 33 129.58 123.20 5.36 o 4 4 33 70.23 61.87 4.13 o 1 5 33 1.72 1.89 3.11 o 3 5 33 303.64 293.04 7.47 o 0 6 33 7.45 7.73 4.77 o 2 6 33 3.93 -1.58 3.52 o 4 6 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