#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016852.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016852_Fobs loop_ _publ_author_name 'Ravikumar, K.' 'Sridhar, B.' 'Krishnan, Harihara' 'Singh, A. N.' _publ_section_title ; Halide salts of antimigraine agents eletriptan and naratriptan ; _journal_coeditor_code DN3101 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o653 _journal_page_last o656 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4019 _cell_length_b 13.4089 _cell_length_c 18.0173 _exptl_crystal_F_000 1000.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file dn3101Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AB52 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 233.80 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17879.44 17774.04 1027.60 o 4 0 0 7180.44 6250.20 255.54 o 6 0 0 3362.20 3517.77 149.04 o 8 0 0 275.95 254.17 18.89 o 10 0 0 166.97 158.33 13.12 o 1 1 0 1305.52 1373.06 46.57 o 2 1 0 20988.68 20624.69 826.33 o 3 1 0 7319.73 7152.65 214.94 o 4 1 0 3959.61 3802.60 103.70 o 5 1 0 1276.03 1223.78 29.19 o 6 1 0 1254.92 1256.46 32.99 o 7 1 0 383.34 369.09 7.82 o 8 1 0 9.52 6.42 4.32 o 9 1 0 0.88 4.77 5.81 o 10 1 0 45.42 47.40 7.30 o 11 1 0 0.28 -1.49 7.42 o 0 2 0 32274.38 30418.17 1448.44 o 1 2 0 1212.98 1349.20 33.24 o 2 2 0 54660.49 51271.64 2219.87 o 3 2 0 2299.64 2170.32 66.49 o 4 2 0 1789.85 1776.72 52.12 o 5 2 0 2599.32 2743.68 69.16 o 6 2 0 360.48 351.42 7.64 o 7 2 0 1809.55 1707.31 50.57 o 8 2 0 606.37 600.32 18.79 o 9 2 0 787.54 775.41 32.16 o 10 2 0 8.61 11.17 6.67 o 11 2 0 168.37 181.29 15.19 o 1 3 0 2691.13 2570.01 71.37 o 2 3 0 4088.37 4264.50 122.68 o 3 3 0 10586.25 10892.04 403.65 o 4 3 0 0.28 1.56 1.37 o 5 3 0 994.04 966.56 28.59 o 6 3 0 22.70 17.59 3.32 o 7 3 0 107.54 106.04 5.12 o 8 3 0 179.68 165.75 7.36 o 9 3 0 67.56 74.17 6.20 o 10 3 0 107.42 116.88 8.56 o 0 4 0 38.32 45.51 4.16 o 1 4 0 833.52 787.56 17.55 o 2 4 0 1541.44 1441.41 30.16 o 3 4 0 4231.09 4256.95 125.93 o 4 4 0 1090.27 1099.11 38.07 o 5 4 0 1779.39 1786.22 69.14 o 6 4 0 64.83 61.73 3.84 o 7 4 0 888.43 844.68 28.69 o 8 4 0 34.89 41.97 4.48 o 9 4 0 94.40 103.66 6.87 o 10 4 0 106.21 130.72 8.36 o 1 5 0 137.25 122.42 3.84 o 2 5 0 7309.63 7732.73 144.99 o 3 5 0 107.96 113.75 5.52 o 4 5 0 605.32 739.48 23.72 o 5 5 0 11.98 9.41 2.73 o 6 5 0 1360.86 1327.89 45.66 o 7 5 0 467.91 427.49 13.38 o 8 5 0 322.14 334.29 12.26 o 9 5 0 3.14 0.33 5.48 o 10 5 0 362.99 408.84 11.46 o 0 6 0 814.96 759.01 29.27 o 1 6 0 599.20 604.38 14.17 o 2 6 0 61.06 50.50 2.46 o 3 6 0 120.32 121.42 3.62 o 4 6 0 81.81 73.25 3.67 o 5 6 0 458.14 387.97 16.70 o 6 6 0 718.08 727.29 31.16 o 7 6 0 140.43 131.21 6.60 o 8 6 0 423.25 420.95 15.66 o 9 6 0 20.68 19.13 6.02 o 10 6 0 56.38 73.91 7.56 o 1 7 0 7445.25 7191.02 173.92 o 2 7 0 6.46 4.07 1.72 o 3 7 0 2212.03 2218.63 48.55 o 4 7 0 1007.36 985.95 45.50 o 5 7 0 783.41 762.24 22.82 o 6 7 0 578.10 539.29 19.66 o 7 7 0 1216.44 1189.16 49.42 o 8 7 0 388.74 368.47 11.75 o 9 7 0 173.63 152.88 7.87 o 10 7 0 182.75 196.36 10.18 o 0 8 0 748.14 796.84 29.07 o 1 8 0 438.64 424.91 8.56 o 2 8 0 244.03 237.69 5.20 o 3 8 0 25.16 28.55 2.76 o 4 8 0 26.02 29.73 3.46 o 5 8 0 98.98 115.12 5.31 o 6 8 0 20.86 17.55 4.06 o 7 8 0 8.08 8.24 4.22 o 8 8 0 143.11 129.33 7.82 o 9 8 0 8.55 4.88 6.24 o 1 9 0 6150.89 6004.20 126.91 o 2 9 0 22.20 25.07 3.02 o 3 9 0 3346.69 3374.40 56.62 o 4 9 0 50.26 51.84 4.10 o 5 9 0 1616.35 1536.83 47.77 o 6 9 0 184.84 207.94 7.69 o 7 9 0 152.65 173.90 7.60 o 8 9 0 53.94 51.33 5.92 o 9 9 0 88.30 91.84 7.15 o 0 10 0 806.64 784.65 13.41 o 1 10 0 47.75 45.59 3.01 o 2 10 0 233.45 255.87 6.01 o 3 10 0 61.06 59.37 4.29 o 4 10 0 755.67 761.44 26.80 o 5 10 0 68.62 72.44 5.09 o 6 10 0 139.17 135.14 6.54 o 7 10 0 11.74 10.30 4.93 o 8 10 0 0.70 -3.66 5.72 o 1 11 0 985.68 930.05 11.95 o 2 11 0 3.65 5.70 3.22 o 3 11 0 181.25 156.60 6.56 o 4 11 0 384.71 409.14 11.46 o 5 11 0 255.14 241.54 10.29 o 6 11 0 209.00 229.31 13.35 o 7 11 0 110.74 109.96 7.45 o 8 11 0 376.83 409.38 16.34 o 0 12 0 12.42 11.31 4.49 o 1 12 0 218.99 226.39 6.33 o 2 12 0 612.59 638.91 12.45 o 3 12 0 286.96 292.82 8.58 o 4 12 0 19.51 18.51 5.14 o 5 12 0 48.28 57.59 6.22 o 6 12 0 53.23 57.86 6.68 o 7 12 0 110.46 120.48 7.81 o 1 13 0 122.52 128.60 6.73 o 2 13 0 84.32 86.40 6.13 o 3 13 0 4.54 8.41 5.22 o 4 13 0 75.84 79.60 6.56 o 5 13 0 7.82 7.93 5.99 o 6 13 0 79.95 92.10 7.64 o 0 14 0 2.74 6.15 8.74 o 1 14 0 20.63 18.56 6.31 o 2 14 0 106.10 121.25 7.91 o 3 14 0 112.18 124.41 8.13 o 4 14 0 61.38 85.05 8.22 o 5 14 0 104.57 104.52 9.08 o 1 15 0 10.10 12.73 7.73 o 2 15 0 20.73 27.43 7.09 o 3 15 0 14.75 7.87 6.90 o 1 0 1 79.68 91.95 1.30 o 2 0 1 3.78 9.10 1.46 o 3 0 1 1914.85 1919.04 52.30 o 4 0 1 1445.92 1364.51 32.51 o 5 0 1 462.26 453.47 13.14 o 6 0 1 220.89 194.01 6.57 o 7 0 1 1245.76 1331.77 25.68 o 8 0 1 1600.53 1617.96 68.92 o 9 0 1 201.95 194.67 9.39 o 10 0 1 269.94 245.55 12.55 o 11 0 1 217.56 234.91 12.04 o -11 1 1 44.40 57.86 8.36 o -10 1 1 186.14 184.18 10.50 o -9 1 1 87.88 97.42 7.15 o -8 1 1 592.98 584.09 18.95 o -7 1 1 1871.87 1911.64 65.18 o -6 1 1 208.07 188.69 5.86 o -5 1 1 3512.57 3582.07 83.80 o -4 1 1 1128.18 1064.97 22.34 o -3 1 1 7492.92 7406.24 195.26 o -2 1 1 6332.35 6536.32 172.09 o -1 1 1 2550.69 2881.42 63.43 o 0 1 1 518.33 523.27 3.54 o 1 1 1 1819.51 2108.96 33.01 o 2 1 1 6072.36 6525.77 161.01 o 3 1 1 7353.70 7322.74 190.67 o 4 1 1 965.06 859.62 29.99 o 5 1 1 3690.65 3722.17 111.95 o 6 1 1 150.08 138.53 3.73 o 7 1 1 1652.52 1741.03 64.56 o 8 1 1 483.54 478.34 20.31 o 9 1 1 56.40 58.73 6.31 o 10 1 1 173.73 168.35 9.83 o 11 1 1 34.45 34.76 7.98 o -11 2 1 35.64 36.18 8.05 o -10 2 1 320.34 310.79 18.48 o -9 2 1 61.38 65.25 7.02 o -8 2 1 1689.44 1764.98 67.60 o -7 2 1 45.36 43.93 3.88 o -6 2 1 2289.82 2283.80 76.32 o -5 2 1 316.00 307.46 7.87 o -4 2 1 5964.01 5723.75 151.38 o -3 2 1 2357.13 2439.13 68.45 o -2 2 1 36189.92 36714.43 1157.50 o -1 2 1 3766.83 3895.00 114.63 o 0 2 1 2514.05 2627.20 49.58 o 1 2 1 3466.13 3504.93 86.05 o 2 2 1 31297.14 33027.74 1001.14 o 3 2 1 2164.36 2344.64 50.49 o 4 2 1 5866.23 5616.56 175.48 o 5 2 1 331.58 321.14 8.76 o 6 2 1 1796.05 1781.98 44.47 o 7 2 1 24.78 28.25 3.60 o 8 2 1 1480.88 1495.42 49.84 o 9 2 1 46.51 51.22 6.58 o 10 2 1 268.39 266.90 18.99 o 11 2 1 30.57 38.16 7.85 o -10 3 1 652.77 672.42 38.27 o -9 3 1 18.97 18.32 5.69 o -8 3 1 706.03 720.72 18.06 o -7 3 1 2.02 3.25 3.26 o -6 3 1 3145.86 3140.24 84.21 o -5 3 1 426.41 445.54 16.01 o -4 3 1 1504.63 1553.15 54.49 o -3 3 1 2471.92 2529.34 90.83 o -2 3 1 3519.79 3806.93 125.41 o -1 3 1 4962.06 4929.89 102.98 o 0 3 1 2538.21 2688.96 36.44 o 1 3 1 5143.81 5219.72 50.90 o 2 3 1 4026.39 4475.06 75.84 o 3 3 1 2626.67 2806.47 70.36 o 4 3 1 1106.06 1118.33 24.30 o 5 3 1 382.71 401.54 17.64 o 6 3 1 2522.38 2332.29 94.10 o 7 3 1 3.10 5.31 3.36 o 8 3 1 653.54 651.53 20.36 o 9 3 1 23.11 28.92 5.67 o 10 3 1 572.44 582.80 16.41 o -10 4 1 162.93 177.62 9.42 o -9 4 1 305.34 302.42 12.49 o -8 4 1 582.25 582.96 26.00 o -7 4 1 619.45 602.24 17.92 o -6 4 1 897.97 802.53 34.69 o -5 4 1 2571.14 2522.91 92.09 o -4 4 1 8892.70 9244.36 325.38 o -3 4 1 7134.80 7283.33 239.97 o -2 4 1 2490.21 2436.61 71.74 o -1 4 1 2278.69 2154.42 43.42 o 0 4 1 10024.07 9960.31 112.02 o 1 4 1 2513.26 2422.18 16.85 o 2 4 1 2259.08 2301.12 34.99 o 3 4 1 7348.12 7597.25 186.30 o 4 4 1 7301.47 7870.52 233.87 o 5 4 1 2925.71 2919.14 91.85 o 6 4 1 715.14 641.26 18.08 o 7 4 1 687.84 644.05 20.48 o 8 4 1 490.72 487.53 12.98 o 9 4 1 269.83 259.13 8.92 o 10 4 1 140.73 152.25 8.24 o -10 5 1 78.00 74.49 7.36 o -9 5 1 192.49 196.25 9.02 o -8 5 1 404.82 375.67 12.80 o -7 5 1 339.20 340.12 13.85 o -6 5 1 979.43 930.66 42.04 o -5 5 1 1317.24 1270.78 45.82 o -4 5 1 61.57 57.85 3.16 o -3 5 1 7111.98 7198.63 221.43 o -2 5 1 3294.13 3156.63 98.48 o -1 5 1 8566.97 8342.57 176.71 o 0 5 1 718.21 736.26 10.95 o 1 5 1 9804.97 9773.02 97.41 o 2 5 1 3323.27 3354.28 52.72 o 3 5 1 8321.03 8576.86 209.38 o 4 5 1 60.34 62.05 4.18 o 5 5 1 1355.56 1329.52 38.47 o 6 5 1 833.16 807.15 28.87 o 7 5 1 337.17 341.02 18.80 o 8 5 1 337.51 302.84 15.45 o 9 5 1 259.57 273.60 9.41 o 10 5 1 86.90 86.01 7.58 o -10 6 1 2.98 3.33 6.21 o -9 6 1 347.98 357.65 12.99 o -8 6 1 55.41 53.88 4.77 o -7 6 1 1206.04 1174.91 40.59 o -6 6 1 173.18 156.20 6.36 o -5 6 1 1239.27 1201.60 50.91 o -4 6 1 760.72 750.95 18.19 o -3 6 1 517.26 497.07 14.61 o -2 6 1 723.72 746.43 20.43 o -1 6 1 1290.19 1230.83 30.92 o 0 6 1 2.20 3.46 1.44 o 1 6 1 1404.90 1366.06 15.12 o 2 6 1 844.65 913.24 9.66 o 3 6 1 580.97 555.36 12.90 o 4 6 1 800.32 778.22 19.94 o 5 6 1 1589.73 1524.83 57.48 o 6 6 1 217.31 203.41 6.53 o 7 6 1 1332.01 1302.96 47.29 o 8 6 1 72.78 70.33 5.97 o 9 6 1 378.05 390.40 10.65 o 10 6 1 2.32 -0.37 6.27 o -10 7 1 47.36 51.50 7.42 o -9 7 1 211.35 235.85 11.05 o -8 7 1 32.01 29.03 5.05 o -7 7 1 345.22 321.26 11.51 o -6 7 1 615.25 569.28 21.90 o -5 7 1 1469.71 1444.83 56.78 o -4 7 1 475.04 452.38 21.27 o -3 7 1 2076.96 2086.38 45.55 o -2 7 1 63.61 55.38 2.31 o -1 7 1 1775.23 1635.54 43.67 o 0 7 1 1464.92 1501.21 28.05 o 1 7 1 1882.29 1772.40 30.41 o 2 7 1 42.14 37.26 2.15 o 3 7 1 2286.97 2345.83 42.04 o 4 7 1 459.14 440.41 17.50 o 5 7 1 1742.13 1729.29 53.34 o 6 7 1 668.49 637.43 19.28 o 7 7 1 437.01 404.66 16.81 o 8 7 1 64.47 60.91 5.89 o 9 7 1 250.11 270.22 16.66 o 10 7 1 39.49 35.44 7.08 o -9 8 1 19.34 18.97 5.23 o -8 8 1 99.31 96.06 6.14 o -7 8 1 246.17 217.16 9.74 o -6 8 1 531.91 489.09 12.45 o -5 8 1 321.53 305.77 10.36 o -4 8 1 1567.28 1564.26 40.36 o -3 8 1 197.53 182.44 5.19 o -2 8 1 2391.07 2455.26 62.21 o -1 8 1 1026.25 921.94 23.59 o 0 8 1 5486.16 5351.43 107.02 o 1 8 1 1065.30 967.47 17.03 o 2 8 1 2645.89 2794.92 50.98 o 3 8 1 220.13 202.01 4.77 o 4 8 1 1542.75 1558.53 16.31 o 5 8 1 339.94 323.05 9.36 o 6 8 1 748.54 704.45 20.02 o 7 8 1 287.43 261.81 10.52 o 8 8 1 103.65 98.50 6.21 o 9 8 1 21.84 22.46 6.25 o -9 9 1 198.22 214.51 9.08 o -8 9 1 85.41 85.75 6.39 o -7 9 1 523.75 532.26 19.06 o -6 9 1 387.41 389.60 8.45 o -5 9 1 60.54 66.92 4.62 o -4 9 1 764.84 745.30 16.36 o -3 9 1 93.78 103.12 4.44 o -2 9 1 569.10 579.98 11.62 o -1 9 1 267.05 266.83 5.92 o 0 9 1 395.64 423.09 10.08 o 1 9 1 195.69 196.17 7.36 o 2 9 1 566.55 585.77 12.75 o 3 9 1 77.41 88.15 4.08 o 4 9 1 709.68 704.57 13.96 o 5 9 1 38.93 39.45 4.30 o 6 9 1 345.06 346.11 12.33 o 7 9 1 495.17 499.47 22.07 o 8 9 1 144.43 137.84 7.35 o 9 9 1 180.12 178.99 9.23 o -8 10 1 80.93 66.90 6.44 o -7 10 1 109.85 114.84 6.42 o -6 10 1 115.44 95.55 5.80 o -5 10 1 59.62 66.98 4.99 o -4 10 1 149.47 141.36 6.02 o -3 10 1 145.20 141.04 5.71 o -2 10 1 637.39 620.23 10.16 o -1 10 1 1624.23 1589.02 31.30 o 0 10 1 2576.41 2531.06 52.82 o 1 10 1 1573.53 1531.89 35.37 o 2 10 1 655.20 641.04 14.74 o 3 10 1 110.76 111.54 5.21 o 4 10 1 214.08 217.45 9.30 o 5 10 1 36.99 42.37 4.48 o 6 10 1 94.37 83.99 7.72 o 7 10 1 74.68 74.82 7.38 o 8 10 1 103.40 87.97 8.99 o -8 11 1 11.83 8.93 6.34 o -7 11 1 330.25 338.63 11.44 o -6 11 1 6.13 2.58 4.83 o -5 11 1 291.23 285.45 11.16 o -4 11 1 154.73 146.73 6.70 o -3 11 1 281.48 291.55 8.33 o -2 11 1 300.52 298.55 7.02 o -1 11 1 601.58 634.34 12.19 o 0 11 1 112.67 102.44 4.03 o 1 11 1 651.85 692.82 12.78 o 2 11 1 310.40 314.31 7.19 o 3 11 1 268.92 269.26 10.50 o 4 11 1 163.48 152.20 7.61 o 5 11 1 231.13 230.61 12.47 o 6 11 1 4.86 2.40 5.25 o 7 11 1 265.31 278.91 17.91 o 8 11 1 10.00 7.07 7.33 o -7 12 1 85.85 102.68 7.82 o -6 12 1 11.32 13.98 5.87 o -5 12 1 86.26 101.70 6.88 o -4 12 1 151.73 158.63 7.10 o -3 12 1 128.56 128.88 6.15 o -2 12 1 32.03 19.97 3.82 o -1 12 1 304.53 318.55 7.62 o 0 12 1 56.02 70.52 4.18 o 1 12 1 300.79 321.28 8.97 o 2 12 1 33.82 31.86 4.90 o 3 12 1 112.98 124.10 6.55 o 4 12 1 165.92 162.03 7.76 o 5 12 1 67.68 77.39 6.47 o 6 12 1 10.80 14.03 6.05 o 7 12 1 60.53 67.26 7.11 o -6 13 1 47.67 58.29 7.00 o -5 13 1 32.66 36.50 7.28 o -4 13 1 80.08 78.93 7.52 o -3 13 1 175.84 165.59 10.25 o -2 13 1 184.75 181.42 9.04 o -1 13 1 210.85 205.75 7.33 o 0 13 1 17.70 17.50 4.90 o 1 13 1 184.09 183.35 7.13 o 2 13 1 204.76 213.32 9.71 o 3 13 1 130.22 130.93 7.07 o 4 13 1 102.46 118.85 7.72 o 5 13 1 20.85 20.97 5.72 o 6 13 1 59.09 64.14 7.25 o -5 14 1 47.69 41.75 7.79 o -4 14 1 62.22 65.54 7.85 o -3 14 1 4.01 5.57 6.28 o -2 14 1 198.08 210.25 15.04 o -1 14 1 91.03 91.42 6.45 o 0 14 1 4.55 -2.55 6.01 o 1 14 1 94.42 97.18 6.66 o 2 14 1 241.33 263.39 10.60 o 3 14 1 6.40 6.87 5.51 o 4 14 1 74.18 79.25 7.10 o 5 14 1 47.85 49.40 7.12 o -3 15 1 8.11 6.50 6.80 o -2 15 1 11.28 12.83 6.65 o -1 15 1 35.89 41.82 8.63 o 0 15 1 169.99 178.68 10.22 o 1 15 1 32.26 39.86 8.22 o 2 15 1 15.04 16.64 6.68 o 3 15 1 4.03 5.61 6.89 o 0 0 2 2751.49 2870.34 115.05 o 1 0 2 4303.91 4316.88 82.18 o 2 0 2 954.09 1208.54 10.91 o 3 0 2 6251.37 6862.82 79.40 o 4 0 2 3641.36 3642.73 74.54 o 5 0 2 559.58 578.76 11.91 o 6 0 2 18.89 19.87 2.25 o 7 0 2 11.37 5.57 3.33 o 8 0 2 283.06 316.99 9.84 o 9 0 2 0.23 -0.40 5.81 o 10 0 2 37.33 54.40 7.15 o 11 0 2 1.93 3.41 7.11 o -11 1 2 27.97 26.25 7.56 o -10 1 2 691.42 698.16 47.39 o -9 1 2 288.44 278.71 10.48 o -8 1 2 1841.15 1853.33 59.81 o -7 1 2 853.76 855.95 36.19 o -6 1 2 3378.48 3240.08 114.17 o -5 1 2 893.15 852.91 20.26 o -4 1 2 903.81 836.52 16.67 o -3 1 2 2970.74 3189.70 50.19 o -2 1 2 1497.41 1578.08 17.54 o -1 1 2 9930.07 10753.84 147.38 o 0 1 2 326.51 313.61 7.67 o 1 1 2 9800.94 10636.75 167.74 o 2 1 2 1331.43 1384.04 34.13 o 3 1 2 3821.26 4216.17 61.57 o 4 1 2 1056.19 989.17 21.62 o 5 1 2 842.14 785.89 24.36 o 6 1 2 3537.00 3363.37 98.22 o 7 1 2 722.98 760.76 11.19 o 8 1 2 1839.56 1815.29 63.06 o 9 1 2 255.08 250.11 14.39 o 10 1 2 676.00 694.01 31.59 o 11 1 2 37.64 33.62 8.18 o -11 2 2 88.31 102.12 9.18 o -10 2 2 22.81 25.55 6.93 o -9 2 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7291.50 133.52 o 4 3 2 1773.11 1873.55 41.41 o 5 3 2 5955.34 6140.47 141.95 o 6 3 2 316.62 317.75 13.11 o 7 3 2 1312.37 1293.84 34.75 o 8 3 2 609.56 604.55 14.33 o 9 3 2 52.55 52.10 5.99 o 10 3 2 31.71 23.36 7.03 o -10 4 2 72.99 73.46 7.36 o -9 4 2 191.33 180.24 8.34 o -8 4 2 505.68 470.92 18.60 o -7 4 2 672.88 620.28 18.51 o -6 4 2 1716.29 1595.91 63.29 o -5 4 2 1843.90 1809.33 53.85 o -4 4 2 4094.42 4027.91 132.34 o -3 4 2 1501.21 1563.19 49.56 o -2 4 2 3942.28 3843.30 86.43 o -1 4 2 681.52 708.48 14.84 o 0 4 2 22722.70 23868.00 339.04 o 1 4 2 598.37 616.19 4.96 o 2 4 2 4069.32 3973.30 55.04 o 3 4 2 1878.19 1961.10 30.45 o 4 4 2 4273.68 4423.32 113.64 o 5 4 2 1543.61 1514.10 45.84 o 6 4 2 1739.39 1657.48 73.39 o 7 4 2 594.48 541.26 15.51 o 8 4 2 545.08 512.11 14.75 o 9 4 2 178.70 177.13 8.62 o 10 4 2 56.10 53.60 7.00 o -10 5 2 128.39 145.78 8.61 o -9 5 2 41.06 45.91 6.27 o -8 5 2 140.38 137.07 6.09 o -7 5 2 405.15 380.77 14.12 o -6 5 2 423.79 390.04 15.03 o -5 5 2 862.07 825.62 26.46 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