#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016865.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016865_Fobs loop_ _publ_author_name 'Foces-Foces, C.' 'L\'opez-Rodr\'iguez, M.' _publ_section_title ; Hydrogen-bonded layered structures in two bis(tert-butyldimethylsilyloxy)-substituted cyclic diol derivatives ; _journal_coeditor_code GD3255 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o657 _journal_page_last o660 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.491 _cell_angle_gamma 90.000 _cell_length_a 27.7623 _cell_length_b 14.3663 _cell_length_c 12.6076 _exptl_crystal_F_000 1840.00 _reflns_d_resolution_high 0.7827 _[local]_cod_data_source_file gd3255Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound mi23lt at 150K.MOSAICITY 0.669(7). ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 261.73 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 68504.99 -1.23 1.23 o 4 0 0 9249.01 9405.83 574.25 o 5 0 0 127.65 147.14 11.00 o 8 0 0 4614.41 4442.42 192.90 o 9 0 0 124.34 179.15 15.04 o 10 0 0 7446.48 9064.91 551.12 o 11 0 0 4234.06 3960.02 172.05 o 15 0 0 8.36 30.44 9.73 o 20 0 0 780.77 750.36 53.56 o 21 0 0 787.39 713.50 52.33 o 22 0 0 7168.83 6741.69 419.14 o 23 0 0 1057.69 909.85 65.72 o 24 0 0 374.40 325.64 30.82 o 25 0 0 5.49 -12.16 17.05 o 26 0 0 5895.91 5448.33 395.09 o 27 0 0 163.72 155.49 26.40 o 28 0 0 309.95 375.66 43.48 o 29 0 0 633.05 605.03 59.76 o 30 0 0 7.64 45.94 27.24 o 31 0 0 118.12 114.74 32.98 o 32 0 0 4390.31 4049.96 497.25 o 33 0 0 127.42 171.96 37.90 o 34 0 0 0.03 69.72 29.78 o 35 0 0 121.33 176.34 38.79 o 1 1 0 621.68 37.05 11.62 o 2 1 0 1343.86 511.00 80.59 o 3 1 0 787.57 711.73 26.41 o 4 1 0 23969.55 24773.01 1508.07 o 5 1 0 808.08 767.06 49.98 o 6 1 0 19228.75 18798.92 1143.45 o 7 1 0 123.26 93.74 5.77 o 8 1 0 1224.30 1498.58 47.02 o 9 1 0 210.78 200.46 7.96 o 10 1 0 3041.96 3156.79 113.17 o 11 1 0 213.29 202.80 11.91 o 12 1 0 395.99 783.76 51.98 o 13 1 0 6.82 8.12 8.12 o 14 1 0 2805.88 2545.55 159.30 o 16 1 0 790.47 1282.20 82.00 o 18 1 0 16596.77 15393.54 941.21 o 19 1 0 104.23 243.95 29.97 o 20 1 0 866.27 818.73 56.76 o 21 1 0 255.34 244.38 18.19 o 22 1 0 1131.56 1090.25 62.91 o 23 1 0 899.23 803.96 34.17 o 24 1 0 2082.06 1888.83 101.10 o 25 1 0 326.36 336.09 25.70 o 26 1 0 3940.33 3742.38 193.72 o 27 1 0 25.63 43.25 15.42 o 28 1 0 170.49 128.64 22.78 o 29 1 0 9.29 49.94 21.59 o 30 1 0 332.65 488.03 40.00 o 31 1 0 2.80 11.97 25.30 o 32 1 0 16.87 35.25 19.91 o 33 1 0 41.77 110.43 46.69 o 34 1 0 188.28 274.59 97.23 o 35 1 0 46.06 28.42 20.38 o 0 2 0 19534.25 19219.91 520.47 o 1 2 0 3555.86 3364.17 68.68 o 2 2 0 17993.84 18403.77 456.50 o 3 2 0 1052.09 1027.63 26.35 o 5 2 0 1029.52 1089.08 30.99 o 6 2 0 5089.68 5961.62 212.61 o 7 2 0 26.07 15.30 4.90 o 8 2 0 5619.55 6348.05 226.04 o 9 2 0 82.75 105.45 6.20 o 10 2 0 2574.79 2683.66 83.53 o 11 2 0 2168.51 2094.21 75.94 o 12 2 0 695.67 859.58 39.72 o 13 2 0 305.72 302.47 16.39 o 14 2 0 569.03 629.69 43.21 o 15 2 0 272.33 280.43 23.63 o 16 2 0 202.22 149.29 12.54 o 17 2 0 459.18 585.33 41.48 o 19 2 0 306.22 221.67 21.51 o 20 2 0 986.42 961.72 46.52 o 21 2 0 122.46 148.53 13.62 o 22 2 0 43.82 68.55 27.74 o 23 2 0 313.06 260.57 21.34 o 24 2 0 6298.37 6105.10 339.63 o 25 2 0 7.14 40.15 13.40 o 26 2 0 142.22 197.34 18.57 o 27 2 0 61.70 53.48 17.22 o 28 2 0 39.46 63.29 16.64 o 29 2 0 11.53 67.43 17.40 o 30 2 0 650.24 768.01 57.50 o 31 2 0 130.30 159.53 22.80 o 32 2 0 109.70 161.86 24.38 o 33 2 0 13.97 47.68 21.33 o 34 2 0 92.76 105.01 25.48 o 35 2 0 48.53 88.69 22.74 o 1 3 0 3685.66 3759.91 69.55 o 2 3 0 1752.71 1752.29 36.23 o 3 3 0 223.33 277.93 6.38 o 4 3 0 87.84 124.40 7.50 o 5 3 0 226.42 228.80 6.25 o 6 3 0 13642.39 15001.24 458.03 o 7 3 0 927.04 1003.70 37.58 o 8 3 0 4204.44 4676.83 129.27 o 9 3 0 1068.55 1325.08 42.49 o 10 3 0 449.28 626.97 24.07 o 11 3 0 471.22 493.58 28.51 o 12 3 0 6150.41 6966.54 296.75 o 13 3 0 555.97 643.29 31.13 o 14 3 0 2114.00 1896.87 84.77 o 15 3 0 20.86 55.67 12.24 o 16 3 0 1774.08 2236.46 142.37 o 17 3 0 294.37 366.31 30.24 o 18 3 0 2433.98 2160.42 138.44 o 19 3 0 0.04 12.24 12.24 o 20 3 0 541.28 585.90 43.21 o 21 3 0 103.09 121.75 15.89 o 22 3 0 1517.95 1432.53 67.01 o 23 3 0 183.17 201.10 20.66 o 24 3 0 597.89 436.53 29.23 o 25 3 0 295.06 295.06 49.37 o 26 3 0 80.86 141.52 18.18 o 27 3 0 11.06 40.35 17.06 o 28 3 0 1567.55 1592.01 98.83 o 29 3 0 211.78 264.67 27.51 o 30 3 0 429.04 474.38 47.44 o 31 3 0 27.58 17.94 25.05 o 32 3 0 25.33 78.70 20.85 o 33 3 0 35.80 42.74 23.25 o 34 3 0 38.29 85.14 57.66 o 0 4 0 11744.82 12379.28 306.28 o 1 4 0 625.16 574.80 10.91 o 2 4 0 16.42 31.39 4.16 o 3 4 0 5178.84 5308.25 115.42 o 4 4 0 5321.66 5426.77 126.25 o 5 4 0 77.46 100.59 3.70 o 6 4 0 17077.50 19098.93 520.54 o 7 4 0 4431.84 4822.59 121.38 o 8 4 0 2258.34 2257.13 70.70 o 9 4 0 1941.94 2025.08 63.50 o 10 4 0 2646.86 2677.58 87.05 o 11 4 0 0.84 0.95 3.88 o 12 4 0 935.02 992.38 37.89 o 13 4 0 763.31 970.93 31.78 o 14 4 0 446.29 534.46 21.89 o 15 4 0 251.82 248.33 15.21 o 16 4 0 378.93 413.25 32.09 o 17 4 0 731.62 777.60 53.02 o 18 4 0 5031.35 5372.10 332.33 o 19 4 0 1888.87 1845.60 119.01 o 20 4 0 20.59 65.39 10.91 o 21 4 0 154.70 156.91 14.65 o 22 4 0 1614.32 1486.60 70.12 o 23 4 0 309.92 291.85 18.16 o 24 4 0 100.27 118.39 19.45 o 25 4 0 1326.13 1352.88 74.66 o 26 4 0 439.11 472.85 34.48 o 27 4 0 71.19 94.54 16.87 o 28 4 0 1388.18 1403.23 86.96 o 29 4 0 201.43 238.39 25.11 o 30 4 0 174.48 127.62 19.67 o 31 4 0 599.18 637.53 61.24 o 32 4 0 601.87 657.64 63.32 o 33 4 0 4.32 -6.62 29.40 o 34 4 0 90.77 120.75 24.11 o 1 5 0 21.25 45.81 3.13 o 2 5 0 8374.42 8220.32 158.87 o 3 5 0 1331.56 1322.73 28.71 o 4 5 0 259.58 347.92 9.30 o 5 5 0 525.20 793.12 21.07 o 6 5 0 322.19 493.70 12.71 o 7 5 0 557.39 606.21 20.61 o 8 5 0 1869.58 2121.57 54.54 o 9 5 0 2475.45 2661.67 68.02 o 10 5 0 4748.56 5590.61 173.27 o 11 5 0 17.75 3.53 4.10 o 12 5 0 5.24 13.33 6.40 o 13 5 0 120.20 95.03 6.16 o 14 5 0 2151.12 2183.94 81.85 o 15 5 0 358.12 310.29 24.47 o 16 5 0 35.37 39.32 11.16 o 17 5 0 52.14 69.88 15.31 o 18 5 0 43.45 80.53 14.47 o 19 5 0 3.20 10.31 15.28 o 20 5 0 518.43 521.31 28.06 o 21 5 0 416.08 406.63 24.55 o 22 5 0 3981.35 3827.73 140.36 o 23 5 0 414.63 371.52 44.35 o 24 5 0 1402.47 1379.92 98.45 o 25 5 0 3.78 17.97 12.82 o 26 5 0 591.14 567.39 44.59 o 27 5 0 126.49 68.56 19.16 o 28 5 0 998.08 1069.01 75.49 o 29 5 0 43.00 44.91 22.76 o 30 5 0 11.24 6.61 15.81 o 31 5 0 65.80 160.52 24.47 o 32 5 0 1.24 20.73 17.59 o 33 5 0 119.73 161.63 23.85 o 34 5 0 2639.91 2808.75 285.39 o 0 6 0 14874.53 15436.91 545.67 o 1 6 0 381.73 451.34 9.87 o 2 6 0 3229.94 3338.36 57.34 o 3 6 0 0.09 9.09 2.56 o 4 6 0 4564.75 5329.00 109.05 o 5 6 0 2435.66 2743.91 56.56 o 6 6 0 6319.46 7004.34 151.64 o 7 6 0 2145.04 2476.40 58.32 o 8 6 0 4527.41 4148.90 97.30 o 9 6 0 872.98 963.93 28.16 o 10 6 0 2143.45 2118.82 59.81 o 11 6 0 507.56 521.78 18.33 o 12 6 0 1994.37 1775.68 56.54 o 13 6 0 1016.47 1087.27 41.23 o 14 6 0 133.36 126.46 13.16 o 15 6 0 8.19 27.05 13.31 o 16 6 0 18423.04 18507.60 1130.60 o 17 6 0 203.76 207.22 15.55 o 18 6 0 365.34 354.57 28.67 o 19 6 0 2581.11 2425.77 154.07 o 20 6 0 4530.75 4083.25 257.69 o 21 6 0 225.00 181.41 13.00 o 22 6 0 912.90 849.25 48.55 o 23 6 0 825.86 881.30 50.02 o 24 6 0 9.42 10.18 10.83 o 25 6 0 188.04 156.57 18.65 o 26 6 0 14.29 21.55 13.93 o 27 6 0 196.82 256.39 25.09 o 28 6 0 25.09 69.47 22.91 o 29 6 0 106.66 161.21 20.35 o 30 6 0 0.22 58.59 18.89 o 31 6 0 18.71 22.47 17.54 o 32 6 0 401.93 349.54 25.61 o 33 6 0 436.56 477.63 72.07 o 1 7 0 346.56 452.86 13.43 o 2 7 0 14214.37 14139.96 286.88 o 3 7 0 241.90 251.82 7.39 o 4 7 0 1766.01 2139.60 82.94 o 5 7 0 1548.90 1403.39 31.67 o 6 7 0 1783.84 2231.32 56.76 o 7 7 0 2193.15 2428.61 61.77 o 8 7 0 4150.72 4355.21 120.80 o 9 7 0 73.54 68.89 4.26 o 10 7 0 1288.35 1229.32 35.49 o 11 7 0 1725.94 1812.35 51.56 o 12 7 0 1378.27 1468.75 47.21 o 13 7 0 235.22 183.12 18.54 o 14 7 0 67.90 80.78 7.20 o 15 7 0 19.62 38.04 7.39 o 16 7 0 236.60 292.64 17.03 o 17 7 0 1454.18 1366.69 64.02 o 18 7 0 3352.98 2938.04 132.76 o 19 7 0 7.86 0.00 8.80 o 20 7 0 5242.00 5205.90 264.72 o 21 7 0 472.04 427.61 27.43 o 22 7 0 45.64 46.83 11.68 o 23 7 0 1737.67 1741.87 104.53 o 24 7 0 19.74 40.06 17.18 o 25 7 0 57.20 59.18 13.43 o 26 7 0 2423.99 2511.40 221.11 o 27 7 0 542.27 574.20 43.51 o 28 7 0 0.03 11.63 19.89 o 29 7 0 24.00 44.25 28.13 o 30 7 0 1134.06 1319.03 167.88 o 31 7 0 109.07 106.62 33.48 o 32 7 0 23.74 64.45 28.51 o 0 8 0 1700.66 1636.94 66.08 o 1 8 0 35.76 31.09 4.80 o 2 8 0 2322.20 2278.90 50.70 o 3 8 0 236.22 332.14 8.43 o 4 8 0 442.53 566.21 12.63 o 5 8 0 1289.29 1144.94 28.39 o 6 8 0 1890.62 1793.18 93.08 o 7 8 0 802.13 786.11 20.86 o 8 8 0 2701.47 2776.54 77.35 o 9 8 0 4744.12 4331.40 120.46 o 10 8 0 2.98 10.50 3.85 o 11 8 0 8.75 17.11 5.25 o 12 8 0 774.09 800.67 26.55 o 13 8 0 5101.20 4619.52 167.72 o 14 8 0 0.01 -3.82 4.97 o 15 8 0 495.73 378.30 20.64 o 16 8 0 108.30 133.58 9.12 o 17 8 0 1159.88 1249.30 57.73 o 18 8 0 974.25 934.98 48.33 o 19 8 0 1055.23 1001.99 63.91 o 20 8 0 25.12 35.15 10.02 o 21 8 0 154.24 137.92 14.46 o 22 8 0 65.04 42.11 11.52 o 23 8 0 795.74 923.56 58.18 o 24 8 0 13.98 29.01 13.92 o 25 8 0 11.16 7.04 17.01 o 26 8 0 0.69 -18.66 20.32 o 27 8 0 0.01 18.24 21.55 o 28 8 0 88.66 23.20 24.86 o 29 8 0 329.07 327.99 51.37 o 30 8 0 1068.17 1089.97 160.68 o 31 8 0 19.71 45.94 26.09 o 1 9 0 1977.71 1721.74 45.57 o 2 9 0 348.19 289.00 14.92 o 3 9 0 775.78 820.00 19.47 o 4 9 0 13.74 45.52 4.63 o 5 9 0 2693.90 2499.44 61.45 o 6 9 0 94.91 96.76 9.46 o 7 9 0 30.87 41.14 8.78 o 8 9 0 1554.31 1569.90 45.39 o 9 9 0 1543.59 1390.18 44.42 o 10 9 0 686.18 691.62 23.17 o 11 9 0 1387.20 1306.99 42.00 o 12 9 0 4563.91 4763.66 147.41 o 13 9 0 334.04 374.64 16.61 o 14 9 0 44.14 66.81 8.84 o 15 9 0 432.85 473.32 24.45 o 16 9 0 69.65 78.45 10.24 o 17 9 0 394.47 453.18 27.52 o 18 9 0 698.65 681.89 38.91 o 19 9 0 56.13 21.59 14.97 o 20 9 0 0.29 -7.89 14.93 o 21 9 0 21.70 93.35 19.51 o 22 9 0 178.13 157.61 24.05 o 23 9 0 38.69 46.44 14.93 o 24 9 0 1274.03 1299.79 126.90 o 25 9 0 3.82 17.82 20.28 o 26 9 0 8.64 -2.89 17.82 o 27 9 0 9.92 38.90 24.43 o 28 9 0 0.30 49.64 23.16 o 29 9 0 66.59 90.96 30.21 o 30 9 0 328.84 442.80 39.75 o 0 10 0 4833.06 4775.43 172.60 o 1 10 0 259.46 238.82 9.91 o 2 10 0 809.13 791.44 22.78 o 3 10 0 439.92 372.49 12.61 o 4 10 0 17.09 33.83 4.97 o 5 10 0 67.42 59.08 4.66 o 6 10 0 114.57 91.99 4.08 o 7 10 0 120.06 133.44 11.05 o 8 10 0 290.48 274.64 26.95 o 9 10 0 82.69 96.27 5.05 o 10 10 0 834.14 885.02 27.01 o 11 10 0 36.68 36.12 15.95 o 12 10 0 401.98 344.10 15.30 o 13 10 0 17.85 8.99 7.85 o 14 10 0 2.47 12.77 9.89 o 15 10 0 39.29 9.89 11.12 o 16 10 0 4669.77 4416.20 318.91 o 17 10 0 199.95 231.60 23.97 o 18 10 0 299.29 333.57 31.01 o 19 10 0 279.82 303.40 32.24 o 20 10 0 126.35 80.88 19.39 o 21 10 0 181.69 183.62 23.93 o 22 10 0 44.73 66.84 16.51 o 23 10 0 122.64 131.94 21.47 o 24 10 0 133.74 141.41 24.74 o 25 10 0 509.83 504.02 59.41 o 26 10 0 133.40 177.58 33.40 o 27 10 0 99.36 107.08 25.13 o 28 10 0 322.59 354.57 59.72 o 29 10 0 0.43 -20.16 20.16 o 1 11 0 1368.01 1267.68 35.06 o 2 11 0 2047.16 2014.48 53.55 o 3 11 0 55.25 56.96 7.25 o 4 11 0 16.95 50.68 8.91 o 5 11 0 3405.92 3234.38 83.81 o 6 11 0 1151.12 1161.71 31.77 o 7 11 0 2127.51 1945.29 60.30 o 8 11 0 227.74 248.00 11.18 o 9 11 0 242.07 276.09 14.66 o 10 11 0 372.95 332.32 14.04 o 11 11 0 348.48 348.25 24.78 o 12 11 0 33.63 28.63 10.68 o 13 11 0 15.35 33.84 12.16 o 14 11 0 172.13 185.79 14.75 o 15 11 0 1164.10 1052.83 79.46 o 16 11 0 283.66 270.27 27.82 o 17 11 0 195.79 163.22 20.05 o 18 11 0 1142.65 1083.42 93.04 o 19 11 0 783.14 773.79 69.26 o 20 11 0 734.98 681.71 61.91 o 21 11 0 185.88 189.04 24.97 o 22 11 0 985.20 896.84 95.85 o 23 11 0 122.68 126.40 24.16 o 24 11 0 518.62 463.04 63.03 o 25 11 0 0.04 29.44 20.86 o 26 11 0 404.52 416.76 66.30 o 27 11 0 999.04 1037.91 61.60 o 28 11 0 123.20 64.60 22.89 o 0 12 0 860.73 901.27 36.89 o 1 12 0 1128.93 1086.54 30.71 o 2 12 0 79.59 137.93 9.70 o 3 12 0 1758.81 1683.72 50.15 o 4 12 0 509.56 551.93 18.00 o 5 12 0 1283.46 1162.23 35.74 o 6 12 0 5.26 20.49 7.34 o 7 12 0 739.21 749.00 26.86 o 8 12 0 2353.39 2202.22 72.21 o 9 12 0 448.02 453.00 17.74 o 10 12 0 822.90 730.51 38.32 o 11 12 0 347.56 283.36 14.02 o 12 12 0 219.93 193.72 11.56 o 13 12 0 1194.64 1154.68 49.43 o 14 12 0 595.97 535.47 25.50 o 15 12 0 111.73 153.03 15.82 o 16 12 0 3398.26 3209.49 264.96 o 17 12 0 1212.46 1132.41 95.43 o 18 12 0 461.37 469.97 43.86 o 19 12 0 13.72 27.97 13.78 o 20 12 0 91.78 84.31 17.85 o 21 12 0 72.52 103.35 19.85 o 22 12 0 1.85 5.66 13.39 o 23 12 0 29.27 31.63 18.66 o 24 12 0 503.60 516.37 68.57 o 25 12 0 1.71 -19.05 20.66 o 26 12 0 403.32 413.06 59.26 o 1 13 0 62.03 83.07 12.34 o 2 13 0 308.03 347.01 14.58 o 3 13 0 9.33 25.53 8.50 o 4 13 0 166.68 161.56 11.90 o 5 13 0 700.11 700.63 26.59 o 6 13 0 67.57 90.66 10.07 o 7 13 0 9.13 7.72 8.87 o 8 13 0 12.03 33.66 9.97 o 9 13 0 943.47 946.57 36.95 o 10 13 0 64.05 94.78 8.36 o 11 13 0 3.82 5.09 6.70 o 12 13 0 359.26 318.54 28.68 o 13 13 0 1338.00 1365.58 64.85 o 14 13 0 127.19 145.93 19.44 o 15 13 0 872.62 947.15 41.56 o 16 13 0 141.98 120.92 27.59 o 17 13 0 10.61 63.46 30.96 o 18 13 0 30.74 54.08 13.37 o 19 13 0 12.51 44.84 31.59 o 20 13 0 28.46 28.42 12.38 o 21 13 0 55.79 23.70 15.66 o 22 13 0 143.37 137.40 27.32 o 23 13 0 105.30 119.74 24.93 o 24 13 0 504.79 528.84 70.03 o 0 14 0 4.04 23.67 11.45 o 1 14 0 43.80 45.20 8.97 o 2 14 0 3.76 117.09 43.00 o 3 14 0 3651.45 3494.71 118.48 o 4 14 0 157.79 183.21 18.46 o 5 14 0 660.68 603.38 26.13 o 6 14 0 157.97 191.66 17.80 o 7 14 0 1336.33 1345.79 58.29 o 8 14 0 250.83 259.54 17.21 o 9 14 0 303.97 354.52 27.62 o 10 14 0 1161.95 1143.36 68.98 o 11 14 0 85.56 96.13 14.31 o 12 14 0 1135.46 1026.99 52.08 o 13 14 0 188.90 209.52 16.35 o 14 14 0 162.90 133.87 20.53 o 15 14 0 726.05 790.27 49.60 o 16 14 0 632.68 612.00 39.71 o 17 14 0 15.63 55.95 29.87 o 18 14 0 446.42 477.39 37.06 o 19 14 0 125.46 98.76 14.85 o 20 14 0 21.25 17.87 14.12 o 21 14 0 89.86 108.89 15.47 o 22 14 0 14.96 44.98 56.25 o 1 15 0 21.00 63.32 10.06 o 2 15 0 786.19 717.34 30.39 o 3 15 0 0.31 48.45 9.34 o 4 15 0 58.09 84.87 12.12 o 5 15 0 102.84 117.72 11.57 o 6 15 0 57.65 98.30 11.29 o 7 15 0 1322.52 1316.51 63.48 o 8 15 0 58.80 120.91 13.26 o 9 15 0 270.49 285.88 23.74 o 10 15 0 19.11 55.03 19.89 o 11 15 0 548.40 571.38 39.15 o 12 15 0 289.56 310.04 25.57 o 13 15 0 752.11 705.62 46.40 o 14 15 0 180.88 244.38 27.10 o 15 15 0 1442.27 1329.57 97.06 o 16 15 0 100.14 57.80 21.06 o 17 15 0 18.95 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