#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016866.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016866_Fobs loop_ _publ_author_name 'Foces-Foces, C.' 'L\'opez-Rodr\'iguez, M.' _publ_section_title ; Hydrogen-bonded layered structures in two bis(tert-butyldimethylsilyloxy)-substituted cyclic diol derivatives ; _journal_coeditor_code GD3255 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o657 _journal_page_last o660 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.676 _cell_angle_gamma 90.000 _cell_length_a 15.0964 _cell_length_b 13.6368 _cell_length_c 24.2908 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.7827 _[local]_cod_data_source_file gd3255IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' mi25, CCD : Mo at 150K, mosaicity = 0.650(7)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 224.55 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 15269.39 16150.33 207.02 o 6 0 0 4164.61 4508.95 78.88 o 8 0 0 19.51 11.16 26.41 o 10 0 0 334.68 370.27 20.74 o 12 0 0 1111.41 1101.02 91.22 o 14 0 0 400.46 483.92 30.86 o 16 0 0 5.17 60.51 30.37 o 18 0 0 3116.99 3270.30 120.09 o 4 1 0 1567.92 1618.08 19.46 o 5 1 0 3305.73 3578.41 34.88 o 6 1 0 9401.53 10211.08 94.57 o 7 1 0 2455.89 3040.50 33.82 o 8 1 0 538.00 624.42 17.24 o 9 1 0 229.50 198.03 11.03 o 10 1 0 15.89 38.46 17.99 o 11 1 0 281.38 300.83 16.16 o 12 1 0 49.04 86.99 13.64 o 13 1 0 437.45 378.85 30.70 o 14 1 0 341.94 376.89 20.06 o 15 1 0 1407.80 1369.57 34.24 o 16 1 0 1074.80 1046.56 33.42 o 17 1 0 256.79 267.32 31.97 o 18 1 0 1180.73 1178.23 44.23 o 3 2 0 24269.49 25049.27 260.04 o 4 2 0 5240.44 5903.27 63.85 o 5 2 0 629.19 678.49 9.42 o 6 2 0 43901.57 46601.84 491.30 o 7 2 0 583.99 791.10 12.60 o 8 2 0 547.58 474.69 19.21 o 9 2 0 2171.81 2247.67 78.42 o 10 2 0 1517.48 1655.94 45.38 o 11 2 0 1120.70 1150.50 25.75 o 12 2 0 3134.58 2943.76 49.22 o 13 2 0 3943.46 3755.39 145.89 o 14 2 0 1025.85 1043.66 55.56 o 15 2 0 245.15 249.55 21.90 o 16 2 0 442.10 490.48 34.31 o 17 2 0 36.34 72.82 33.20 o 18 2 0 1041.38 1107.81 48.83 o 2 3 0 2217.41 2309.73 31.30 o 3 3 0 2025.08 2040.51 26.32 o 4 3 0 201.19 231.79 11.86 o 5 3 0 544.40 643.60 11.49 o 6 3 0 22.74 44.18 10.64 o 7 3 0 739.25 607.42 12.29 o 8 3 0 1943.55 1980.04 39.37 o 9 3 0 3795.22 4180.48 75.56 o 10 3 0 151.83 182.05 10.62 o 11 3 0 835.36 856.54 19.12 o 12 3 0 173.61 206.00 14.63 o 13 3 0 424.52 351.36 23.98 o 14 3 0 2.81 24.99 16.64 o 15 3 0 144.92 173.22 32.60 o 16 3 0 164.06 129.40 21.92 o 17 3 0 1047.65 950.73 40.58 o 18 3 0 27.86 -32.37 32.37 o 0 4 0 732.02 632.95 13.19 o 1 4 0 21860.50 22877.70 260.56 o 2 4 0 7505.43 7959.11 72.57 o 3 4 0 674.76 634.89 11.03 o 4 4 0 1407.88 1459.48 21.21 o 5 4 0 471.24 512.64 11.66 o 6 4 0 3351.72 3194.51 58.94 o 7 4 0 6498.85 6526.14 111.98 o 8 4 0 1730.69 1555.74 33.38 o 9 4 0 1445.90 1434.10 38.60 o 10 4 0 561.01 483.77 21.04 o 11 4 0 46.42 54.39 10.72 o 12 4 0 2258.05 2165.87 56.82 o 13 4 0 466.66 433.51 26.34 o 14 4 0 2849.94 2665.31 159.88 o 15 4 0 23.84 39.12 27.47 o 16 4 0 2.93 22.07 29.10 o 17 4 0 0.74 50.64 25.39 o 1 5 0 3450.45 3867.89 42.97 o 2 5 0 16429.77 15347.15 179.52 o 3 5 0 12786.47 13640.01 157.04 o 4 5 0 635.10 753.31 13.82 o 5 5 0 123.79 188.11 9.49 o 6 5 0 2436.89 2510.79 39.21 o 7 5 0 8603.90 8796.22 179.30 o 8 5 0 9.87 -6.76 13.27 o 9 5 0 2652.91 2747.16 64.40 o 10 5 0 302.91 299.86 33.35 o 11 5 0 3171.19 2966.56 157.71 o 12 5 0 356.27 326.52 17.30 o 13 5 0 444.10 387.66 28.73 o 14 5 0 39.09 68.04 23.25 o 15 5 0 98.14 104.40 32.69 o 16 5 0 1082.27 992.54 63.62 o 17 5 0 95.13 101.47 46.35 o 0 6 0 2433.08 2537.15 42.65 o 1 6 0 3985.29 4283.51 56.14 o 2 6 0 855.67 814.66 11.29 o 3 6 0 1255.55 1269.18 23.48 o 4 6 0 15243.33 15356.35 177.85 o 5 6 0 3872.51 4075.29 57.57 o 6 6 0 87.06 139.54 10.38 o 7 6 0 216.86 216.94 17.68 o 8 6 0 1878.73 1722.58 111.26 o 9 6 0 396.22 366.11 27.02 o 10 6 0 0.04 -7.70 28.14 o 11 6 0 3027.14 2894.96 71.90 o 12 6 0 120.46 105.07 54.40 o 13 6 0 4.03 22.75 27.56 o 14 6 0 446.17 414.49 43.33 o 15 6 0 813.28 809.53 72.57 o 16 6 0 0.69 35.43 31.15 o 17 6 0 1.24 -13.09 35.83 o 1 7 0 1.25 16.48 7.57 o 2 7 0 3116.92 3174.14 47.20 o 3 7 0 0.16 4.68 6.16 o 4 7 0 17932.75 17457.32 185.57 o 5 7 0 786.37 771.52 17.36 o 6 7 0 2822.26 2761.89 51.31 o 7 7 0 3654.14 3399.99 74.33 o 8 7 0 6166.12 5680.22 116.39 o 9 7 0 1003.41 1104.41 53.63 o 10 7 0 4287.27 4512.47 98.89 o 11 7 0 1912.29 1626.99 57.47 o 12 7 0 2083.60 2062.81 62.75 o 13 7 0 22.67 -18.32 33.65 o 14 7 0 150.55 180.57 30.49 o 15 7 0 384.64 489.96 35.44 o 16 7 0 5.64 15.31 36.25 o 0 8 0 5083.79 4801.62 108.43 o 1 8 0 230.51 291.05 9.11 o 2 8 0 275.25 321.88 9.28 o 3 8 0 2413.31 2311.67 30.17 o 4 8 0 165.90 176.99 6.57 o 5 8 0 526.34 572.37 21.33 o 6 8 0 72.77 96.29 11.95 o 7 8 0 256.24 244.91 20.31 o 8 8 0 2894.93 2888.87 78.15 o 9 8 0 1326.93 1301.49 42.96 o 10 8 0 1.65 -37.02 37.02 o 11 8 0 577.50 655.75 57.15 o 12 8 0 1917.24 1761.27 79.60 o 13 8 0 1088.92 1088.75 41.31 o 14 8 0 189.93 242.93 31.27 o 15 8 0 855.03 876.76 42.29 o 16 8 0 2.09 -28.58 38.01 o 1 9 0 3512.73 3345.75 40.80 o 2 9 0 1524.38 1280.74 31.40 o 3 9 0 337.43 302.81 10.81 o 4 9 0 71.57 74.09 7.96 o 5 9 0 3649.28 1045.87 1627.15 o 6 9 0 882.39 867.08 19.57 o 7 9 0 777.64 745.66 33.47 o 8 9 0 719.86 661.38 36.71 o 9 9 0 715.17 670.07 27.37 o 10 9 0 290.52 238.28 22.52 o 11 9 0 1547.72 1405.65 41.94 o 12 9 0 998.05 927.43 36.41 o 13 9 0 10.21 0.40 35.34 o 14 9 0 378.00 318.34 35.22 o 15 9 0 6.77 55.11 34.88 o 0 10 0 4291.54 4418.88 74.59 o 1 10 0 575.62 583.02 14.24 o 2 10 0 1280.96 1287.83 35.54 o 3 10 0 415.69 435.82 29.73 o 4 10 0 685.05 649.05 14.67 o 5 10 0 1767.48 1599.15 23.14 o 6 10 0 824.12 799.68 25.90 o 7 10 0 70.76 73.10 18.75 o 8 10 0 7.14 11.16 18.57 o 9 10 0 357.88 373.10 24.19 o 10 10 0 195.48 165.80 30.05 o 11 10 0 86.34 85.81 23.87 o 12 10 0 373.23 364.43 31.69 o 13 10 0 97.81 97.69 43.83 o 14 10 0 824.17 851.49 54.79 o 15 10 0 227.68 295.03 54.10 o 1 11 0 547.45 665.57 18.31 o 2 11 0 2.61 33.66 13.54 o 3 11 0 1394.76 1375.48 24.34 o 4 11 0 8.28 48.44 8.82 o 5 11 0 3.69 -2.80 9.81 o 6 11 0 43.61 79.32 14.30 o 7 11 0 256.11 271.73 47.99 o 8 11 0 6.31 42.87 20.17 o 9 11 0 14.72 9.07 21.55 o 10 11 0 726.94 662.82 31.08 o 11 11 0 1307.60 1370.10 44.45 o 12 11 0 281.29 276.42 38.98 o 13 11 0 315.84 416.55 38.22 o 14 11 0 1.92 19.29 39.77 o 0 12 0 467.79 464.18 26.72 o 1 12 0 933.95 1028.64 57.49 o 2 12 0 3837.86 3710.80 80.37 o 3 12 0 1889.00 1851.05 36.13 o 4 12 0 2134.51 2191.19 56.73 o 5 12 0 579.19 589.83 27.46 o 6 12 0 52.41 37.28 17.24 o 7 12 0 681.27 638.85 49.66 o 8 12 0 806.29 813.82 39.63 o 9 12 0 480.96 566.71 31.79 o 10 12 0 11.11 -6.70 42.50 o 11 12 0 92.83 147.86 34.00 o 12 12 0 244.06 286.16 103.59 o 13 12 0 6.65 150.96 51.53 o 1 13 0 382.80 383.48 28.31 o 2 13 0 773.48 817.17 31.59 o 3 13 0 338.25 327.36 22.22 o 4 13 0 503.63 536.16 30.88 o 5 13 0 13.78 22.11 19.76 o 6 13 0 21.98 47.98 22.04 o 7 13 0 169.24 153.68 29.81 o 8 13 0 355.45 348.23 38.41 o 9 13 0 37.75 2.64 39.72 o 10 13 0 36.65 -43.37 43.37 o 11 13 0 4.49 -45.36 45.36 o 12 13 0 2.48 -67.93 67.93 o 0 14 0 304.39 298.47 89.43 o 1 14 0 94.22 151.37 22.54 o 2 14 0 155.31 193.29 23.19 o 3 14 0 1308.39 1358.16 37.81 o 4 14 0 2071.40 2184.62 49.37 o 5 14 0 246.11 285.45 24.24 o 6 14 0 1076.55 1045.25 56.96 o 7 14 0 272.83 378.76 40.91 o 8 14 0 82.46 234.24 58.30 o 9 14 0 921.77 994.10 58.04 o 10 14 0 3.11 7.12 74.80 o 1 15 0 116.95 123.59 27.31 o 2 15 0 203.98 209.07 26.91 o 3 15 0 249.26 274.38 27.87 o 4 15 0 0.11 -10.58 26.97 o 5 15 0 295.00 335.33 27.52 o 6 15 0 792.96 828.91 59.96 o 7 15 0 158.47 127.68 50.57 o 8 15 0 182.78 227.34 48.17 o 9 15 0 488.65 425.39 52.71 o 0 16 0 0.60 24.14 45.09 o 1 16 0 1599.38 1687.69 147.29 o 2 16 0 270.89 272.53 48.81 o 3 16 0 189.11 232.35 34.19 o 4 16 0 188.07 252.55 50.94 o 5 16 0 915.67 907.60 36.01 o 6 16 0 963.28 1091.61 133.81 o 7 16 0 69.16 79.28 47.12 o 1 17 0 36.87 -10.69 35.55 o 2 17 0 1.82 42.62 36.35 o 3 17 0 134.05 121.65 49.41 o 4 17 0 494.28 474.64 54.92 o -17 0 1 1.41 -28.93 31.88 o -15 0 1 102.07 187.61 38.20 o -13 0 1 363.93 392.47 70.26 o -11 0 1 1578.19 1515.09 41.47 o -9 0 1 3865.48 3871.86 121.75 o -7 0 1 1622.81 1487.97 25.04 o -5 0 1 28756.27 29966.97 444.08 o 5 0 1 1369.75 1643.25 25.45 o 7 0 1 38378.70 38845.82 850.28 o 9 0 1 2552.90 2588.19 158.73 o 11 0 1 1792.27 1739.11 57.50 o 13 0 1 3846.38 3633.01 126.21 o 15 0 1 14.34 -6.48 28.70 o 17 0 1 300.13 360.04 49.97 o -18 1 1 736.96 721.20 63.35 o -17 1 1 1357.32 1322.15 40.51 o -16 1 1 254.05 235.38 24.36 o -15 1 1 28.69 28.41 23.61 o -14 1 1 5.24 32.49 15.75 o -13 1 1 2001.86 1924.00 44.27 o -12 1 1 2533.16 2388.68 41.92 o -11 1 1 221.42 175.58 12.93 o -10 1 1 0.10 9.30 9.78 o -9 1 1 3458.33 3520.99 52.68 o -8 1 1 14427.95 15029.59 258.03 o -7 1 1 5209.68 5338.78 51.68 o -6 1 1 1922.19 2010.64 22.10 o -5 1 1 446.93 456.67 13.95 o -4 1 1 1285.56 1266.13 13.65 o 4 1 1 135.79 140.83 4.12 o 5 1 1 531.09 493.76 8.01 o 6 1 1 117.74 71.62 6.66 o 7 1 1 1935.03 2246.08 26.64 o 8 1 1 566.67 624.51 15.82 o 9 1 1 22.72 63.82 10.18 o 10 1 1 25.14 11.60 12.48 o 11 1 1 285.96 381.47 16.96 o 12 1 1 429.85 382.02 18.58 o 13 1 1 239.83 241.90 17.61 o 14 1 1 18.14 51.20 17.80 o 15 1 1 119.77 108.60 20.22 o 16 1 1 1.45 -25.20 25.20 o 17 1 1 427.37 405.94 36.86 o 18 1 1 93.07 21.11 35.86 o -18 2 1 12.87 -14.67 34.20 o -17 2 1 451.33 478.50 39.63 o -16 2 1 1636.62 1548.86 53.73 o -15 2 1 319.85 329.62 20.93 o -14 2 1 1471.29 1349.02 36.03 o -13 2 1 26.55 26.38 15.45 o -12 2 1 1881.02 1785.67 43.04 o -11 2 1 486.31 458.94 16.85 o -10 2 1 2010.76 1945.31 48.74 o -9 2 1 127.48 138.14 13.54 o -8 2 1 7047.79 6943.89 107.63 o -7 2 1 3311.71 2905.72 43.73 o -6 2 1 351.32 422.18 7.50 o -5 2 1 391.72 477.95 9.42 o -4 2 1 863.99 998.04 13.75 o -3 2 1 9514.81 10325.91 108.09 o 3 2 1 1484.43 1363.07 26.99 o 4 2 1 2596.40 2938.84 31.84 o 5 2 1 671.92 712.71 9.17 o 6 2 1 3439.54 3972.01 41.03 o 7 2 1 3320.21 3425.79 49.17 o 8 2 1 516.21 689.95 30.77 o 9 2 1 969.28 1084.63 23.14 o 10 2 1 6723.79 6398.61 98.23 o 11 2 1 54.79 60.21 13.40 o 12 2 1 607.31 592.06 20.44 o 13 2 1 16.50 45.71 15.27 o 14 2 1 177.80 152.93 18.10 o 15 2 1 2734.03 2588.02 115.15 o 16 2 1 239.45 255.99 36.76 o 17 2 1 539.51 479.44 47.44 o 18 2 1 103.00 58.02 52.82 o -18 3 1 94.80 110.57 29.43 o -17 3 1 2413.88 2295.45 99.67 o -16 3 1 1.93 42.40 24.97 o -15 3 1 1009.72 936.78 27.98 o -14 3 1 1877.75 1881.99 39.44 o -13 3 1 4.91 5.38 12.86 o -12 3 1 417.69 466.12 20.82 o -11 3 1 134.68 152.92 11.22 o -10 3 1 3245.29 3280.67 44.43 o -9 3 1 36.34 32.89 6.77 o -8 3 1 259.20 238.27 21.30 o -7 3 1 8548.08 9570.09 114.85 o -6 3 1 10671.36 11287.20 120.70 o -5 3 1 390.18 509.62 10.17 o -4 3 1 2208.21 2115.45 25.41 o -3 3 1 1100.47 1148.97 14.80 o -2 3 1 4576.12 4352.27 43.34 o 2 3 1 1601.45 1657.08 17.66 o 3 3 1 144.34 164.53 4.96 o 4 3 1 28.26 54.72 5.65 o 5 3 1 136.68 118.23 5.73 o 6 3 1 1043.44 1204.95 14.64 o 7 3 1 1216.96 1277.42 16.01 o 8 3 1 99.87 161.96 8.33 o 9 3 1 936.62 1079.17 19.37 o 10 3 1 44.52 60.85 10.58 o 11 3 1 58.64 64.27 11.07 o 12 3 1 3842.21 3781.84 73.15 o 13 3 1 82.89 82.07 21.57 o 14 3 1 239.72 270.73 21.05 o 15 3 1 4.39 3.78 23.82 o 16 3 1 209.08 225.46 29.93 o 17 3 1 0.62 -0.90 27.56 o 18 3 1 2.05 21.95 33.25 o -18 4 1 101.31 37.25 44.11 o -17 4 1 6.10 40.41 26.05 o -16 4 1 566.14 515.50 41.13 o -15 4 1 2629.66 2424.84 52.66 o -14 4 1 2429.73 2455.15 46.48 o -13 4 1 21.92 23.90 14.71 o -12 4 1 148.43 166.07 23.15 o -11 4 1 1470.98 640.01 643.99 o -10 4 1 2478.10 2463.99 49.24 o -9 4 1 0.70 9.83 16.31 o -8 4 1 98.28 116.01 18.82 o -7 4 1 0.31 24.98 8.50 o -6 4 1 217.37 206.46 9.34 o -5 4 1 2563.33 2690.31 32.46 o -4 4 1 2293.78 2493.25 29.56 o -3 4 1 1612.73 1641.38 22.21 o -2 4 1 26872.28 28001.17 319.11 o -1 4 1 1141.86 1228.01 14.04 o 0 4 1 1195.11 1305.06 16.30 o 1 4 1 2217.96 2276.24 26.01 o 2 4 1 1455.82 1620.19 16.54 o 3 4 1 393.78 445.38 6.55 o 4 4 1 15141.34 15961.85 183.73 o 5 4 1 1132.97 1432.36 21.98 o 6 4 1 4027.13 4062.97 83.76 o 7 4 1 375.07 423.10 10.39 o 8 4 1 475.37 540.21 11.71 o 9 4 1 776.83 607.90 15.35 o 10 4 1 64.96 55.51 9.46 o 11 4 1 0.04 13.89 19.98 o 12 4 1 419.39 402.41 21.37 o 13 4 1 439.95 435.84 22.84 o 14 4 1 217.17 245.25 21.76 o 15 4 1 38.24 20.16 20.63 o 16 4 1 1073.43 1077.38 72.81 o 17 4 1 106.36 102.87 30.74 o -17 5 1 313.15 242.22 108.00 o -16 5 1 1753.31 1786.52 66.77 o -15 5 1 43.09 32.30 15.86 o -14 5 1 643.92 600.47 31.73 o -13 5 1 504.52 408.44 40.94 o -12 5 1 0.15 50.71 21.26 o -11 5 1 6.59 30.31 17.68 o -10 5 1 218.09 177.38 17.21 o -9 5 1 3057.48 3198.57 58.74 o -8 5 1 135.57 133.30 14.14 o -7 5 1 347.68 434.55 12.97 o -6 5 1 331.47 490.86 12.63 o -5 5 1 9530.76 9401.39 123.71 o -4 5 1 14879.21 15815.45 182.04 o -3 5 1 10783.85 11852.57 125.54 o -2 5 1 4615.22 4678.00 54.00 o -1 5 1 579.55 666.20 10.53 o 0 5 1 4297.27 4535.41 54.59 o 1 5 1 145.64 124.19 5.17 o 2 5 1 62.83 87.04 7.14 o 3 5 1 67.73 58.72 3.25 o 4 5 1 1771.41 1719.62 24.56 o 5 5 1 663.81 638.30 14.78 o 6 5 1 284.49 387.91 14.00 o 7 5 1 1077.73 1066.17 41.11 o 8 5 1 14.75 19.98 18.08 o 9 5 1 799.26 784.07 22.07 o 10 5 1 518.17 488.53 33.94 o 11 5 1 2748.70 2607.44 80.30 o 12 5 1 93.02 62.32 15.40 o 13 5 1 109.52 101.00 19.42 o 14 5 1 428.47 442.01 31.41 o 15 5 1 13.40 35.01 21.70 o 16 5 1 0.50 -20.67 20.67 o 17 5 1 2.33 -59.34 59.34 o -17 6 1 489.06 476.71 40.18 o -16 6 1 565.12 558.49 48.59 o -15 6 1 6.19 24.10 28.90 o -14 6 1 1.73 26.15 35.49 o -13 6 1 4.42 -13.21 32.29 o -12 6 1 393.77 428.79 58.55 o -11 6 1 433.50 423.64 28.96 o -10 6 1 168.70 181.80 22.94 o -9 6 1 42.37 63.53 36.26 o -8 6 1 1422.31 1475.77 41.26 o -7 6 1 2828.91 2733.66 50.27 o -6 6 1 1846.29 1977.51 32.71 o -5 6 1 3890.51 4080.13 57.66 o -4 6 1 2889.88 2626.60 36.00 o -3 6 1 19.51 31.58 3.60 o -2 6 1 2114.76 2388.72 26.21 o -1 6 1 4460.94 4449.20 49.61 o 0 6 1 789.55 786.55 12.48 o 1 6 1 1402.88 1351.11 34.89 o 2 6 1 2981.22 3233.40 37.08 o 3 6 1 1991.42 2044.12 21.50 o 4 6 1 2453.47 2361.61 28.20 o 5 6 1 2711.61 3014.92 44.59 o 6 6 1 16.11 17.38 9.97 o 7 6 1 0.98 24.87 29.01 o 8 6 1 633.88 576.55 78.71 o 9 6 1 2391.28 2389.00 221.12 o 10 6 1 805.50 800.39 35.16 o 11 6 1 2322.46 2161.30 59.70 o 12 6 1 413.23 394.09 37.89 o 13 6 1 372.67 390.60 41.54 o 14 6 1 1014.34 967.89 67.75 o 15 6 1 771.29 749.90 132.19 o 16 6 1 4.98 -38.98 38.98 o 17 6 1 324.12 338.96 51.82 o -17 7 1 375.91 409.32 39.03 o -16 7 1 227.57 238.24 37.07 o -15 7 1 1980.08 1955.48 62.26 o -14 7 1 53.31 90.15 28.67 o -13 7 1 11.23 20.85 25.97 o -12 7 1 104.73 126.60 26.31 o -11 7 1 0.05 24.08 19.89 o -10 7 1 1504.99 1514.01 47.41 o -9 7 1 100.70 101.31 26.93 o -8 7 1 223.96 253.82 22.37 o -7 7 1 1837.57 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