#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:15:20 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180838 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/69/2016952.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016952_Fobs loop_ _publ_author_name 'Tafeenko, Viktor A.' 'Gurskiy, Stanislav I.' 'Baranov, Andrey N.' 'Kaisarova, Tatiana V.' 'Aslanov, Leonid A.' _publ_section_title ; Luminescence properties of three structures built from 3-cyano-4-dicyanomethylene-5-oxo-4,5-dihydro-1H-pyrrol-2-olate and alkaline metals (Na, K and Rb) ; _journal_coeditor_code FA3172 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m52 _journal_page_last m55 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.215 _cell_angle_gamma 90.000 _cell_length_a 4.2753 _cell_length_b 9.6013 _cell_length_c 21.6136 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8024 _cod_data_source_file fa3172rbsup2.hkl _cod_data_source_block rb #BEGIN Tags that were not found in dictionaries: _shelx_title ' al2 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 410.23 395.87 4.95 o 2 0 0 3186.64 3331.73 121.82 o 3 0 0 1137.94 1093.35 15.76 o 4 0 0 2230.04 2068.48 73.65 o 5 0 0 1.25 0.54 2.65 o 1 1 0 6630.34 6530.78 58.37 o 2 1 0 8685.03 9163.58 89.68 o 3 1 0 264.68 292.42 8.75 o 4 1 0 271.53 274.52 9.53 o 5 1 0 219.31 195.79 12.89 o 0 2 0 10.97 22.77 2.44 o 1 2 0 1287.29 1292.59 9.65 o 2 2 0 0.54 1.57 2.25 o 3 2 0 23.88 60.40 26.90 o 4 2 0 0.47 2.77 4.09 o 5 2 0 0.22 2.88 2.88 o 1 3 0 11119.90 10272.95 1903.14 o 2 3 0 3782.08 3908.68 89.69 o 3 3 0 760.25 803.25 57.26 o 4 3 0 187.09 200.71 7.91 o 5 3 0 358.48 433.38 38.41 o 0 4 0 16383.74 15936.34 69.84 o 1 4 0 2187.80 1955.51 55.10 o 2 4 0 136.19 128.84 11.26 o 3 4 0 2575.66 2806.60 240.64 o 4 4 0 943.81 942.35 85.98 o 5 4 0 19.51 22.79 4.55 o 1 5 0 18.65 15.07 2.48 o 2 5 0 316.96 320.62 20.85 o 3 5 0 33.71 41.14 7.62 o 4 5 0 72.72 74.75 12.38 o 0 6 0 5555.76 5668.13 46.21 o 1 6 0 1261.39 1208.56 14.82 o 2 6 0 155.55 166.58 7.50 o 3 6 0 304.38 335.37 31.37 o 4 6 0 461.80 494.53 60.74 o 1 7 0 4770.48 5101.66 34.68 o 2 7 0 4801.92 5074.85 156.45 o 3 7 0 98.31 110.90 8.21 o 4 7 0 389.74 444.40 42.94 o 0 8 0 2915.24 3034.85 39.32 o 1 8 0 1053.47 999.52 15.75 o 2 8 0 407.72 388.61 20.45 o 3 8 0 1185.51 1548.41 63.60 o 1 9 0 296.24 295.22 10.44 o 2 9 0 80.02 73.09 8.06 o 3 9 0 40.77 64.86 4.60 o 0 10 0 1601.51 1505.77 25.82 o 1 10 0 533.22 463.29 14.51 o 2 10 0 179.50 166.44 5.26 o 1 11 0 1340.88 1280.31 18.25 o 2 11 0 1155.48 835.11 126.81 o -5 1 1 37.32 30.73 4.97 o -4 1 1 111.86 108.70 9.66 o -3 1 1 2512.90 2588.81 34.98 o -2 1 1 2938.27 2714.88 26.23 o -1 1 1 6.82 10.12 2.54 o 0 1 1 1635.58 1581.90 9.88 o 1 1 1 12128.94 11564.07 240.69 o 2 1 1 1100.90 1071.92 16.76 o 3 1 1 79.39 93.89 8.38 o 4 1 1 661.92 666.90 20.20 o 5 1 1 165.53 147.02 7.82 o -5 2 1 393.73 367.61 10.24 o -4 2 1 676.58 663.04 19.65 o -3 2 1 82.24 105.00 8.37 o -2 2 1 1945.84 1897.59 22.47 o -1 2 1 17281.22 17518.23 366.64 o 0 2 1 6587.75 5664.76 31.06 o 1 2 1 22.35 28.12 2.73 o 2 2 1 1908.29 1787.69 22.75 o 3 2 1 4414.41 4437.10 48.74 o 4 2 1 8.66 10.40 5.07 o 5 2 1 296.86 289.55 9.76 o -5 3 1 19.93 16.64 3.67 o -4 3 1 32.28 44.12 5.69 o -3 3 1 372.68 399.92 13.81 o -2 3 1 3200.12 3438.78 33.41 o -1 3 1 180.32 229.67 6.92 o 0 3 1 3947.55 3728.96 26.04 o 1 3 1 3665.19 3835.27 27.25 o 2 3 1 152.43 159.37 7.91 o 3 3 1 14.71 13.56 6.25 o 4 3 1 332.17 346.05 14.53 o 5 3 1 102.05 103.65 6.61 o -5 4 1 33.40 28.22 3.74 o -4 4 1 56.64 52.19 6.70 o -3 4 1 0.26 0.43 5.13 o -2 4 1 60.21 55.30 5.46 o -1 4 1 2896.46 2902.00 26.90 o 0 4 1 2608.96 2642.65 23.45 o 1 4 1 77.61 85.95 5.03 o 2 4 1 314.68 329.61 11.45 o 3 4 1 36.43 43.50 6.36 o 4 4 1 0.19 5.23 5.23 o -4 5 1 164.99 153.56 8.46 o -3 5 1 1373.52 1445.77 27.26 o -2 5 1 3319.36 3479.45 38.82 o -1 5 1 340.04 358.34 10.62 o 0 5 1 5012.74 4997.60 38.00 o 1 5 1 6193.43 6198.15 44.74 o 2 5 1 1490.69 1327.99 25.72 o 3 5 1 560.79 577.00 19.00 o 4 5 1 556.59 540.91 16.24 o -4 6 1 642.61 646.18 14.25 o -3 6 1 97.47 89.44 8.15 o -2 6 1 793.80 837.81 20.04 o -1 6 1 2606.76 2761.42 32.71 o 0 6 1 3375.72 3509.12 35.23 o 1 6 1 251.66 248.02 9.70 o 2 6 1 2509.72 2356.89 38.63 o 3 6 1 2027.70 1973.88 35.53 o 4 6 1 51.14 56.95 5.88 o -4 7 1 9.53 16.13 2.98 o -3 7 1 44.91 44.72 6.20 o -2 7 1 320.49 346.36 14.23 o -1 7 1 82.37 84.74 8.02 o 0 7 1 6.69 5.67 5.36 o 1 7 1 471.59 488.32 14.67 o 2 7 1 101.65 119.49 9.16 o 3 7 1 141.66 136.65 10.84 o 4 7 1 56.55 57.51 5.30 o -3 8 1 85.03 73.95 6.84 o -2 8 1 207.80 200.21 10.67 o -1 8 1 4220.93 4446.60 49.32 o 0 8 1 125.88 107.61 8.27 o 1 8 1 8.00 18.90 4.71 o 2 8 1 312.65 347.52 14.00 o 3 8 1 896.74 1069.66 23.90 o -3 9 1 900.00 912.77 15.67 o -2 9 1 1219.12 1173.81 22.70 o -1 9 1 7.67 14.62 5.74 o 0 9 1 2804.12 2858.59 38.74 o 1 9 1 1569.78 1472.19 26.78 o 2 9 1 499.06 425.02 13.40 o 3 9 1 208.15 297.05 10.66 o -2 10 1 292.93 284.22 10.32 o -1 10 1 1175.80 1120.84 21.57 o 0 10 1 310.46 257.03 11.54 o 1 10 1 181.30 163.61 8.68 o 2 10 1 865.88 777.16 14.88 o -2 11 1 2.61 4.81 3.85 o -1 11 1 0.63 3.49 3.90 o 0 11 1 4.62 4.04 4.07 o 1 11 1 3.33 4.73 3.61 o 2 11 1 100.10 64.44 4.37 o -5 0 2 132.44 118.26 7.16 o -4 0 2 199.40 209.72 12.64 o -3 0 2 334.06 325.09 13.29 o -2 0 2 25565.89 25586.54 547.81 o -1 0 2 2811.15 3002.93 20.20 o 0 0 2 118.68 125.96 2.20 o 1 0 2 1492.61 1363.64 12.28 o 2 0 2 6972.97 7046.24 45.66 o 3 0 2 107.34 111.67 8.21 o 4 0 2 307.32 320.67 13.81 o 5 0 2 300.65 295.92 10.08 o -5 1 2 4.77 12.43 3.98 o -4 1 2 566.29 602.33 19.42 o -3 1 2 1142.70 1220.72 23.75 o -2 1 2 105.38 122.56 6.30 o -1 1 2 872.49 996.05 11.72 o 0 1 2 236.12 265.21 3.94 o 1 1 2 10264.11 10455.79 216.34 o 2 1 2 342.03 325.94 9.34 o 3 1 2 1957.24 1969.47 30.84 o 4 1 2 59.16 53.38 8.09 o 5 1 2 0.94 1.31 4.07 o -5 2 2 1.30 4.75 3.56 o -4 2 2 34.47 37.42 6.68 o -3 2 2 353.31 375.04 13.79 o -2 2 2 1406.19 1442.07 19.73 o -1 2 2 669.78 737.04 11.06 o 0 2 2 53.37 55.48 2.97 o 1 2 2 1496.03 1403.01 13.80 o 2 2 2 133.43 126.09 6.61 o 3 2 2 246.89 247.67 12.54 o 4 2 2 42.49 56.57 7.19 o 5 2 2 0.10 2.77 3.80 o -5 3 2 160.66 159.31 6.82 o -4 3 2 967.58 979.60 22.54 o -3 3 2 2433.36 2437.04 34.42 o -2 3 2 0.30 8.60 3.13 o -1 3 2 12735.57 12558.14 59.71 o 0 3 2 8085.54 7366.07 38.79 o 1 3 2 2323.15 2439.51 21.42 o 2 3 2 2083.64 1962.92 25.99 o 3 3 2 2302.28 2243.01 35.98 o 4 3 2 207.12 190.54 11.43 o 5 3 2 30.71 28.43 4.57 o -5 4 2 354.13 366.15 8.62 o -4 4 2 61.84 55.09 6.84 o -3 4 2 1456.48 1484.53 27.46 o -2 4 2 7633.62 7875.69 58.37 o -1 4 2 1981.37 2029.57 22.26 o 0 4 2 1636.25 1670.49 18.31 o 1 4 2 6806.57 6334.99 41.54 o 2 4 2 4425.16 4252.73 42.85 o 3 4 2 5.15 0.51 5.27 o 4 4 2 572.11 572.19 17.22 o -4 5 2 15.23 14.53 4.46 o -3 5 2 12.09 17.89 5.56 o -2 5 2 50.21 68.24 7.25 o -1 5 2 1254.19 1352.88 20.17 o 0 5 2 763.76 803.63 14.47 o 1 5 2 246.48 240.50 8.50 o 2 5 2 838.10 793.67 20.26 o 3 5 2 158.75 144.77 10.56 o 4 5 2 155.28 154.12 8.88 o -4 6 2 54.72 48.94 5.14 o -3 6 2 310.20 308.52 13.04 o -2 6 2 2057.50 2154.49 32.17 o -1 6 2 84.59 75.74 6.49 o 0 6 2 151.88 176.58 8.26 o 1 6 2 331.64 307.17 10.65 o 2 6 2 1606.71 1521.70 30.93 o 3 6 2 37.18 40.35 6.72 o 4 6 2 224.14 236.22 9.68 o -4 7 2 525.48 533.24 11.04 o -3 7 2 1054.44 1066.86 21.95 o -2 7 2 2.45 4.57 4.92 o -1 7 2 3162.98 3372.16 39.93 o 0 7 2 5648.56 5903.64 52.53 o 1 7 2 271.93 287.34 11.74 o 2 7 2 770.42 824.40 22.46 o 3 7 2 1355.75 1592.20 31.57 o 4 7 2 301.01 353.61 10.31 o -3 8 2 58.94 44.08 6.01 o -2 8 2 519.00 562.70 17.36 o -1 8 2 2141.82 2200.26 34.06 o 0 8 2 994.52 1000.81 22.37 o 1 8 2 2482.61 2541.91 36.01 o 2 8 2 280.90 294.83 12.98 o 3 8 2 309.06 361.35 14.00 o -3 9 2 28.16 28.69 4.39 o -2 9 2 14.25 4.22 5.40 o -1 9 2 245.23 214.87 11.71 o 0 9 2 239.94 223.55 12.34 o 1 9 2 550.09 509.18 16.04 o 2 9 2 3.80 16.23 4.04 o 3 9 2 7.77 16.62 3.99 o -2 10 2 1914.80 1914.66 25.21 o -1 10 2 31.34 32.13 5.33 o 0 10 2 61.91 50.28 6.63 o 1 10 2 1516.47 1406.88 23.52 o 2 10 2 1468.02 1366.38 19.99 o -2 11 2 20.01 12.99 4.28 o -1 11 2 1028.84 983.90 17.30 o 0 11 2 2602.00 2507.98 29.18 o 1 11 2 2.00 6.73 3.21 o 2 11 2 77.60 51.38 3.76 o -5 1 3 267.03 248.44 9.31 o -4 1 3 431.51 456.32 17.19 o -3 1 3 7.72 9.55 5.07 o -2 1 3 3066.48 3174.62 29.41 o -1 1 3 2997.45 3129.44 22.52 o 0 1 3 56.52 52.95 2.36 o 1 1 3 614.33 661.05 8.66 o 2 1 3 3707.23 3526.83 31.37 o 3 1 3 710.19 709.42 18.93 o 4 1 3 116.29 123.66 9.77 o 5 1 3 124.64 127.66 6.90 o -5 2 3 43.03 43.49 4.82 o -4 2 3 894.83 960.75 23.59 o -3 2 3 3253.30 3106.83 39.49 o -2 2 3 314.69 319.04 9.43 o -1 2 3 1746.71 2169.66 19.63 o 0 2 3 6544.14 6258.52 29.64 o 1 2 3 9584.66 10389.68 235.75 o 2 2 3 17.92 22.12 3.75 o 3 2 3 1607.75 1602.11 28.91 o 4 2 3 753.01 690.83 20.32 o 5 2 3 86.89 89.08 6.27 o -5 3 3 60.15 63.53 4.75 o -4 3 3 137.63 144.12 9.79 o -3 3 3 7.36 24.65 5.66 o -2 3 3 1317.50 1388.20 21.09 o -1 3 3 4802.60 4776.97 32.94 o 0 3 3 195.94 245.79 6.32 o 1 3 3 475.86 447.77 9.21 o 2 3 3 1750.67 1636.67 23.77 o 3 3 3 94.71 82.54 8.64 o 4 3 3 7.42 6.21 5.50 o 5 3 3 6.38 6.82 4.24 o -5 4 3 16.97 20.77 3.15 o -4 4 3 10.15 7.10 5.71 o -3 4 3 624.51 687.81 18.86 o -2 4 3 1151.21 1201.81 21.02 o -1 4 3 353.12 425.61 10.31 o 0 4 3 98.50 149.82 6.01 o 1 4 3 2.35 46.23 4.05 o 2 4 3 13.32 23.32 4.31 o 3 4 3 25.29 16.52 6.41 o 4 4 3 168.97 148.71 10.03 o -4 5 3 345.11 313.64 11.56 o -3 5 3 14.85 17.48 5.89 o -2 5 3 3270.21 3342.89 38.06 o -1 5 3 2674.70 2641.60 28.75 o 0 5 3 969.49 998.78 16.24 o 1 5 3 1326.61 1218.29 19.30 o 2 5 3 2338.36 2063.08 33.33 o 3 5 3 503.37 440.42 17.97 o 4 5 3 4.53 16.73 4.97 o -4 6 3 531.82 522.50 12.66 o -3 6 3 690.19 683.25 18.77 o -2 6 3 297.20 297.03 12.56 o -1 6 3 540.78 574.25 14.78 o 0 6 3 4662.37 4852.77 42.55 o 1 6 3 1929.54 1908.24 26.93 o 2 6 3 179.84 196.13 11.98 o 3 6 3 685.10 669.38 21.76 o 4 6 3 498.55 555.10 14.56 o -4 7 3 19.84 19.36 3.66 o -3 7 3 134.46 143.87 8.71 o -2 7 3 315.38 316.37 13.67 o -1 7 3 2.04 4.12 5.01 o 0 7 3 62.72 71.88 7.15 o 1 7 3 100.12 97.82 8.08 o 2 7 3 68.50 71.73 8.38 o 3 7 3 12.82 7.12 6.03 o 4 7 3 15.10 22.05 4.28 o -3 8 3 1524.39 1547.98 23.55 o -2 8 3 2.61 0.45 5.26 o -1 8 3 1.64 0.46 5.71 o 0 8 3 233.91 249.31 12.07 o 1 8 3 4118.42 4246.95 48.18 o 2 8 3 230.44 223.99 11.74 o 3 8 3 183.33 228.10 11.21 o -3 9 3 80.71 90.13 5.20 o -2 9 3 1181.20 1143.91 22.22 o -1 9 3 2076.73 2151.60 33.12 o 0 9 3 894.58 910.05 21.90 o 1 9 3 1069.69 1044.99 22.47 o 2 9 3 2591.91 2706.91 34.57 o 3 9 3 462.10 594.90 13.66 o -2 10 3 131.29 125.12 7.14 o -1 10 3 189.37 169.90 9.09 o 0 10 3 1493.25 1446.55 25.66 o 1 10 3 921.41 850.43 18.59 o 2 10 3 1.56 3.85 3.24 o -2 11 3 0.37 1.05 3.94 o -1 11 3 19.46 37.01 5.03 o 0 11 3 167.68 141.06 7.90 o 1 11 3 3.08 1.49 3.49 o -5 0 4 452.35 426.23 12.00 o -4 0 4 2466.98 2622.69 42.20 o -3 0 4 133.83 143.54 9.15 o -2 0 4 111.74 87.07 5.77 o -1 0 4 26108.07 25436.19 452.74 o 0 0 4 12235.50 12573.48 213.48 o 1 0 4 44208.50 45347.64 585.89 o 2 0 4 562.86 418.32 10.42 o 3 0 4 2013.92 1998.29 30.62 o 4 0 4 384.78 387.03 15.23 o 5 0 4 342.62 355.16 10.05 o -5 1 4 55.80 50.95 5.44 o -4 1 4 56.41 54.81 8.53 o -3 1 4 1973.97 2053.69 31.66 o -2 1 4 1352.85 1313.15 18.75 o -1 1 4 15.47 25.92 3.09 o 0 1 4 2603.28 2617.95 15.79 o 1 1 4 15310.64 16491.53 298.17 o 2 1 4 72.45 100.84 5.80 o 3 1 4 813.73 822.38 19.82 o 4 1 4 159.57 159.46 10.58 o 5 1 4 109.48 111.15 6.41 o -5 2 4 0.33 3.13 3.59 o -4 2 4 53.15 62.28 8.12 o -3 2 4 214.54 226.64 11.10 o -2 2 4 102.88 121.55 6.44 o -1 2 4 0.94 0.31 2.82 o 0 2 4 165.40 149.98 4.67 o 1 2 4 11.79 11.17 2.58 o 2 2 4 665.28 635.81 13.89 o 3 2 4 0.54 8.21 5.70 o 4 2 4 23.08 34.30 6.43 o 5 2 4 0.14 2.82 3.64 o -5 3 4 186.63 196.47 7.28 o -4 3 4 4.73 1.34 5.92 o -3 3 4 1723.54 1739.74 29.19 o -2 3 4 3085.09 3109.77 32.59 o -1 3 4 1331.50 1379.76 16.83 o 0 3 4 5210.87 5130.57 30.82 o 1 3 4 6223.08 6493.61 39.28 o 2 3 4 305.36 270.79 9.98 o 3 3 4 143.25 147.39 10.49 o 4 3 4 853.35 793.19 21.28 o 5 3 4 165.92 176.83 7.28 o -5 4 4 137.50 148.53 5.88 o -4 4 4 2068.07 1939.39 29.80 o -3 4 4 237.87 264.43 12.23 o -2 4 4 1597.85 1645.48 25.06 o -1 4 4 3778.28 3583.02 31.06 o 0 4 4 7013.10 6927.40 41.80 o 1 4 4 125.48 142.44 6.60 o 2 4 4 2043.77 1987.19 29.61 o 3 4 4 2177.29 1966.98 36.15 o 4 4 4 67.61 62.14 7.59 o -4 5 4 10.83 15.12 4.68 o -3 5 4 218.16 198.15 11.72 o -2 5 4 710.59 687.62 17.31 o -1 5 4 178.57 187.48 8.17 o 0 5 4 108.79 86.43 5.67 o 1 5 4 1395.48 1317.02 20.55 o 2 5 4 523.16 505.17 16.67 o 3 5 4 2.28 5.86 5.11 o 4 5 4 46.71 45.68 5.89 o -4 6 4 319.09 334.82 10.24 o -3 6 4 11.67 16.29 5.62 o -2 6 4 6.30 3.38 5.62 o -1 6 4 1761.52 1876.03 27.11 o 0 6 4 805.59 799.14 16.75 o 1 6 4 687.03 695.35 16.70 o 2 6 4 1347.93 1262.18 27.75 o 3 6 4 226.36 215.92 13.08 o 4 6 4 16.51 22.07 5.17 o -4 7 4 28.03 25.73 3.92 o -3 7 4 2493.95 2500.07 33.45 o -2 7 4 2812.94 2964.28 39.50 o -1 7 4 8.53 20.82 5.33 o 0 7 4 2898.37 3043.60 37.61 o 1 7 4 5255.85 5577.40 54.11 o 2 7 4 521.13 513.88 18.07 o 3 7 4 433.41 512.58 17.63 o 4 7 4 259.74 332.47 9.95 o -3 8 4 293.79 309.89 10.70 o -2 8 4 1048.51 1077.27 23.28 o -1 8 4 3744.25 3960.09 46.55 o 0 8 4 909.77 1001.69 22.66 o 1 8 4 2.71 1.41 5.46 o 2 8 4 769.66 836.06 21.73 o 3 8 4 577.26 737.26 18.40 o -3 9 4 21.79 11.10 4.16 o -2 9 4 49.55 52.62 6.34 o -1 9 4 16.51 20.98 5.20 o 0 9 4 82.66 100.54 9.01 o 1 9 4 6.83 0.44 5.87 o 2 9 4 102.53 96.41 7.65 o 3 9 4 10.59 13.27 3.68 o -2 10 4 43.89 46.01 5.23 o -1 10 4 1472.71 1484.72 24.98 o 0 10 4 1808.36 1781.16 28.29 o 1 10 4 15.10 13.36 4.82 o 2 10 4 1052.93 1005.81 16.94 o -2 11 4 1411.28 1221.06 17.07 o -1 11 4 45.72 32.72 4.93 o 0 11 4 740.41 719.21 15.33 o 1 11 4 1463.35 1369.92 19.56 o -5 1 5 1.28 2.39 3.89 o -4 1 5 715.45 804.22 22.26 o -3 1 5 1361.31 1472.08 27.14 o -2 1 5 22.14 20.09 4.17 o -1 1 5 553.72 509.14 9.26 o 0 1 5 8334.42 8676.14 185.58 o 1 1 5 3619.20 3488.78 23.00 o 2 1 5 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