#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/69/2016997.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016997_Fobs loop_ _publ_author_name 'Hori, Kayako' 'Kouno, Naomi' _publ_section_title ; Two crystal forms of mesogenic bis(4'-cyanobiphenyl-4-yl) butanedioate ; _journal_coeditor_code EG3008 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o108 _journal_page_last o110 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.058 _cell_angle_gamma 90.000 _cell_length_a 10.4777 _cell_length_b 11.6064 _cell_length_c 9.5897 _exptl_crystal_F_000 492.00 _reflns_d_resolution_high 0.8314 _[local]_cod_data_source_file eg3008Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' twin-ester-2-1 (Rigaku Master for Cu)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 135.31 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13.27 13.37 0.13 o 2 0 0 876.75 976.55 3.89 o 3 0 0 5.07 10.30 0.30 o 4 0 0 653.54 765.28 6.91 o 5 0 0 477.39 513.93 7.72 o 6 0 0 270.55 305.64 6.16 o 7 0 0 475.15 494.48 12.11 o 8 0 0 1599.02 1674.93 42.01 o 9 0 0 3334.25 3858.31 99.80 o 10 0 0 9.09 9.37 0.33 o 11 0 0 5.41 4.68 0.25 o 12 0 0 5.42 6.41 0.29 o 1 1 0 518.40 533.04 2.07 o 2 1 0 2.82 2.58 0.09 o 3 1 0 190.63 190.08 1.36 o 4 1 0 16.09 20.22 0.35 o 5 1 0 266.47 284.41 1.04 o 6 1 0 50.12 76.80 7.53 o 7 1 0 1.77 2.01 0.23 o 8 1 0 0.00 2.38 1.32 o 9 1 0 1.09 1.34 0.11 o 10 1 0 239.76 254.37 2.79 o 11 1 0 27.48 26.03 0.44 o 12 1 0 0.79 0.68 0.07 o 0 2 0 2075.35 1825.36 6.59 o 1 2 0 122.21 94.65 1.97 o 2 2 0 289.20 309.81 7.28 o 3 2 0 3283.26 3770.55 29.44 o 4 2 0 203.61 244.58 2.89 o 5 2 0 71.03 83.37 1.05 o 6 2 0 721.64 782.85 4.97 o 7 2 0 105.86 115.89 0.86 o 8 2 0 295.35 306.36 1.51 o 9 2 0 34.30 40.46 1.75 o 10 2 0 4.90 4.20 0.26 o 11 2 0 3.01 2.54 0.25 o 12 2 0 121.29 121.91 4.24 o 1 3 0 1981.37 2092.13 75.16 o 2 3 0 243.40 229.91 5.56 o 3 3 0 701.84 767.07 34.75 o 4 3 0 59.81 51.09 1.80 o 5 3 0 24.83 33.95 2.54 o 6 3 0 173.68 214.18 2.97 o 7 3 0 106.59 105.04 1.38 o 8 3 0 2.08 2.45 0.15 o 9 3 0 172.38 176.33 1.20 o 10 3 0 7.03 21.24 11.18 o 11 3 0 65.51 66.45 2.00 o 0 4 0 4687.92 4765.43 15.83 o 1 4 0 296.10 387.52 70.24 o 2 4 0 156.61 164.77 5.17 o 3 4 0 506.14 565.63 18.68 o 4 4 0 0.59 0.82 0.06 o 5 4 0 285.88 314.76 8.29 o 6 4 0 2.42 0.99 0.07 o 7 4 0 52.66 45.49 0.60 o 8 4 0 133.16 149.45 2.56 o 9 4 0 0.02 1.61 0.38 o 10 4 0 13.49 11.74 0.77 o 11 4 0 6.38 5.23 0.22 o 1 5 0 460.55 470.41 3.97 o 2 5 0 1272.01 1336.68 43.28 o 3 5 0 92.70 122.72 4.53 o 4 5 0 902.71 944.28 45.47 o 5 5 0 174.42 197.50 6.20 o 6 5 0 17.35 19.46 0.38 o 7 5 0 25.21 30.10 0.50 o 8 5 0 4.36 4.26 0.46 o 9 5 0 122.80 125.38 2.11 o 10 5 0 70.71 70.52 3.75 o 11 5 0 59.11 60.34 1.46 o 0 6 0 2.11 4.71 0.26 o 1 6 0 0.64 0.80 0.05 o 2 6 0 1383.29 1529.96 72.60 o 3 6 0 57.43 56.42 2.45 o 4 6 0 167.16 207.55 8.16 o 5 6 0 86.91 98.64 3.74 o 6 6 0 168.18 156.05 5.69 o 7 6 0 11.07 7.97 0.34 o 8 6 0 0.62 0.29 0.20 o 9 6 0 0.01 0.09 0.18 o 10 6 0 48.94 46.50 1.65 o 11 6 0 13.82 13.33 0.25 o 1 7 0 1260.37 1391.64 20.76 o 2 7 0 30.44 41.40 2.01 o 3 7 0 24.70 22.31 1.44 o 4 7 0 101.58 102.28 4.56 o 5 7 0 43.40 46.22 1.86 o 6 7 0 55.93 64.37 0.72 o 7 7 0 89.38 68.60 2.87 o 8 7 0 103.40 93.97 2.23 o 9 7 0 98.17 85.27 7.20 o 10 7 0 37.10 32.29 0.42 o 0 8 0 388.68 401.14 2.22 o 1 8 0 749.15 802.66 5.78 o 2 8 0 906.33 959.10 27.72 o 3 8 0 87.17 95.56 0.82 o 4 8 0 2.98 15.76 9.34 o 5 8 0 7.93 9.74 1.18 o 6 8 0 70.04 72.54 1.55 o 7 8 0 232.77 230.18 8.35 o 8 8 0 294.97 262.90 20.00 o 9 8 0 36.71 32.02 3.42 o 10 8 0 160.21 169.84 0.88 o 1 9 0 8.54 6.94 0.29 o 2 9 0 1020.69 1090.77 23.97 o 3 9 0 0.14 1.01 0.32 o 4 9 0 154.35 149.65 6.37 o 5 9 0 85.39 95.77 5.30 o 6 9 0 82.88 84.27 3.61 o 7 9 0 379.51 374.12 36.13 o 8 9 0 3.21 4.32 0.24 o 9 9 0 1.98 2.01 0.15 o 0 10 0 0.80 1.06 0.11 o 1 10 0 22.60 28.60 0.51 o 2 10 0 736.19 817.94 21.99 o 3 10 0 83.90 84.98 2.44 o 4 10 0 9.29 8.50 0.31 o 5 10 0 48.01 52.91 2.44 o 6 10 0 49.82 46.79 3.55 o 7 10 0 40.09 43.76 2.82 o 8 10 0 24.87 27.19 0.53 o 1 11 0 64.92 72.11 1.40 o 2 11 0 16.65 19.65 0.45 o 3 11 0 25.37 28.32 0.51 o 4 11 0 28.03 26.45 1.18 o 5 11 0 28.86 29.53 0.47 o 6 11 0 0.57 0.12 0.21 o 0 12 0 2.57 3.47 0.32 o 1 12 0 0.61 0.55 0.12 o 2 12 0 161.39 160.91 4.66 o 3 12 0 91.96 88.23 4.71 o 4 12 0 19.28 17.01 0.82 o 5 12 0 2.40 3.12 0.28 o 6 12 0 5.52 4.71 0.18 o 1 13 0 23.77 26.27 0.41 o 2 13 0 54.09 57.78 1.15 o 3 13 0 2.01 1.71 0.22 o -12 1 1 55.83 59.61 0.78 o -11 1 1 52.34 48.18 0.84 o -10 1 1 7.67 8.35 0.44 o -9 1 1 160.32 185.87 1.74 o -8 1 1 9.52 12.58 0.35 o -7 1 1 0.66 0.92 0.17 o -6 1 1 20.29 23.23 0.35 o -5 1 1 1626.64 1889.93 21.70 o -4 1 1 890.88 971.71 5.06 o -3 1 1 90.65 89.84 1.20 o -2 1 1 67.76 71.04 0.34 o -1 1 1 72.02 72.05 0.32 o 0 1 1 102.18 102.49 23.43 o 1 1 1 7441.39 8136.44 471.50 o 2 1 1 0.56 0.62 0.08 o 3 1 1 384.28 420.68 3.55 o 4 1 1 19.91 28.42 0.52 o 5 1 1 11.09 12.20 0.25 o 6 1 1 129.61 140.06 1.33 o 7 1 1 48.42 49.99 0.59 o 8 1 1 506.72 521.12 12.88 o 9 1 1 993.70 1008.88 4.06 o 10 1 1 205.32 204.33 1.77 o 11 1 1 14.58 15.17 0.47 o -11 2 1 19.69 21.91 0.58 o -10 2 1 0.29 0.65 0.11 o -9 2 1 231.28 259.45 2.05 o -8 2 1 420.77 431.13 1.77 o -7 2 1 165.69 182.32 1.74 o -6 2 1 183.86 223.60 1.05 o -5 2 1 1204.91 1444.37 9.49 o -4 2 1 286.12 283.75 7.00 o -3 2 1 583.63 623.18 9.95 o -2 2 1 8.00 8.93 0.24 o -1 2 1 412.02 380.20 8.41 o 0 2 1 6715.46 5783.09 424.86 o 1 2 1 9956.48 10831.86 31.29 o 2 2 1 3506.44 3670.15 32.92 o 3 2 1 265.68 269.45 5.16 o 4 2 1 647.10 726.03 9.81 o 5 2 1 46.94 48.31 0.47 o 6 2 1 2.38 9.03 2.89 o 7 2 1 147.61 154.90 1.02 o 8 2 1 29.78 30.12 0.51 o 9 2 1 670.73 720.47 3.42 o 10 2 1 149.19 158.12 1.54 o 11 2 1 80.35 85.29 1.00 o -11 3 1 42.13 38.76 0.73 o -10 3 1 1.53 1.99 0.18 o -9 3 1 853.78 877.37 3.78 o -8 3 1 96.26 92.48 0.84 o -7 3 1 3.75 6.36 1.37 o -6 3 1 2.67 4.53 0.20 o -5 3 1 2401.07 2911.61 78.23 o -4 3 1 66.64 65.75 1.39 o -3 3 1 297.61 323.83 6.16 o -2 3 1 57.19 57.97 2.90 o -1 3 1 333.74 306.06 7.28 o 0 3 1 12218.12 12194.84 505.51 o 1 3 1 1122.32 1026.98 14.44 o 2 3 1 395.44 395.20 9.42 o 3 3 1 868.44 944.40 31.48 o 4 3 1 451.24 523.30 9.81 o 5 3 1 64.27 74.52 0.61 o 6 3 1 310.87 325.16 1.94 o 7 3 1 70.53 62.57 0.68 o 8 3 1 202.73 204.31 1.80 o 9 3 1 0.01 2.24 0.19 o 10 3 1 9.30 9.16 0.44 o 11 3 1 0.70 1.33 0.13 o -11 4 1 4.59 8.44 0.37 o -10 4 1 62.74 68.47 1.03 o -9 4 1 66.11 72.06 1.09 o -8 4 1 31.04 30.98 0.73 o -7 4 1 0.53 0.73 0.28 o -6 4 1 96.50 90.04 0.73 o -5 4 1 0.48 -0.13 0.14 o -4 4 1 0.14 4.94 2.45 o -3 4 1 2991.81 3382.81 92.59 o -2 4 1 95.63 89.82 2.41 o -1 4 1 7385.29 7805.66 282.46 o 0 4 1 2491.18 2414.39 7.85 o 1 4 1 56.58 59.20 4.79 o 2 4 1 4.13 2.39 0.20 o 3 4 1 46.86 51.54 1.94 o 4 4 1 224.68 254.46 6.57 o 5 4 1 508.22 539.69 9.47 o 6 4 1 650.22 688.17 10.29 o 7 4 1 300.33 276.32 3.54 o 8 4 1 37.64 43.72 0.88 o 9 4 1 307.57 321.86 2.26 o 10 4 1 172.20 170.77 1.53 o 11 4 1 0.10 0.56 0.07 o -11 5 1 2.64 3.69 0.29 o -10 5 1 164.99 163.42 1.51 o -9 5 1 12.77 15.29 0.58 o -8 5 1 11.37 21.32 0.63 o -7 5 1 152.73 157.73 3.47 o -6 5 1 46.33 45.30 3.35 o -5 5 1 38.70 41.43 1.09 o -4 5 1 343.90 409.87 19.91 o -3 5 1 742.79 781.87 2.33 o -2 5 1 75.21 86.14 4.02 o -1 5 1 817.87 844.77 5.02 o 0 5 1 65.50 65.55 0.98 o 1 5 1 279.72 270.18 12.96 o 2 5 1 146.88 139.14 6.03 o 3 5 1 11.41 15.83 0.95 o 4 5 1 5.18 3.18 0.23 o 5 5 1 218.02 228.78 4.45 o 6 5 1 319.10 326.73 5.79 o 7 5 1 36.85 44.76 0.87 o 8 5 1 130.37 127.38 1.45 o 9 5 1 29.32 29.11 0.71 o 10 5 1 22.65 21.72 0.56 o 11 5 1 68.81 65.21 0.75 o -10 6 1 2.11 2.74 0.27 o -9 6 1 0.30 0.29 0.10 o -8 6 1 0.04 0.20 0.27 o -7 6 1 287.67 262.33 2.03 o -6 6 1 0.54 0.33 0.33 o -5 6 1 58.96 51.58 1.40 o -4 6 1 291.69 272.16 5.74 o -3 6 1 1010.79 973.15 21.38 o -2 6 1 2.53 2.04 0.11 o -1 6 1 355.38 359.18 7.08 o 0 6 1 159.65 150.99 0.79 o 1 6 1 553.85 594.93 34.93 o 2 6 1 2167.58 2213.53 117.96 o 3 6 1 16.20 19.40 3.54 o 4 6 1 39.72 50.38 0.93 o 5 6 1 22.61 25.18 0.44 o 6 6 1 77.48 72.95 2.23 o 7 6 1 215.64 228.33 1.92 o 8 6 1 2.44 3.91 0.38 o 9 6 1 97.38 98.46 1.20 o 10 6 1 0.95 1.14 0.10 o -10 7 1 0.04 0.02 0.20 o -9 7 1 119.22 108.11 1.24 o -8 7 1 6.37 6.06 0.41 o -7 7 1 7.25 7.88 0.46 o -6 7 1 8.84 10.13 0.79 o -5 7 1 5.76 7.43 0.45 o -4 7 1 20.42 17.98 1.72 o -3 7 1 199.33 205.08 9.97 o -2 7 1 152.35 154.96 2.78 o -1 7 1 432.39 464.59 8.34 o 0 7 1 152.23 181.69 4.14 o 1 7 1 230.04 265.98 3.26 o 2 7 1 134.11 116.82 1.66 o 3 7 1 199.28 210.41 7.33 o 4 7 1 0.38 1.73 0.79 o 5 7 1 141.23 142.59 3.50 o 6 7 1 134.21 127.69 1.44 o 7 7 1 191.22 169.74 1.66 o 8 7 1 51.44 47.79 0.88 o 9 7 1 0.12 0.32 0.09 o 10 7 1 2.47 2.91 0.24 o -9 8 1 0.12 0.25 0.08 o -8 8 1 35.13 33.73 0.73 o -7 8 1 3.22 3.43 0.27 o -6 8 1 56.03 52.27 0.95 o -5 8 1 8.23 9.18 0.45 o -4 8 1 22.46 24.28 0.67 o -3 8 1 3.22 2.46 0.61 o -2 8 1 164.44 193.66 6.95 o -1 8 1 215.06 191.81 1.10 o 0 8 1 257.51 294.42 4.91 o 1 8 1 2.46 3.10 0.46 o 2 8 1 17.43 15.27 1.01 o 3 8 1 37.87 41.50 1.74 o 4 8 1 8.53 11.53 5.91 o 5 8 1 0.10 0.13 0.27 o 6 8 1 106.16 112.97 1.37 o 7 8 1 10.50 14.67 0.53 o 8 8 1 3.41 10.57 0.45 o 9 8 1 59.20 54.80 0.78 o -9 9 1 0.13 0.16 0.11 o -8 9 1 7.46 6.26 0.36 o -7 9 1 316.48 317.45 2.18 o -6 9 1 25.19 28.32 0.72 o -5 9 1 15.82 17.35 0.60 o -4 9 1 7.61 8.66 0.45 o -3 9 1 10.20 11.33 0.34 o -2 9 1 94.89 100.65 2.60 o -1 9 1 120.38 135.84 1.69 o 0 9 1 25.04 28.62 0.87 o 1 9 1 0.25 0.86 0.10 o 2 9 1 156.84 149.04 5.66 o 3 9 1 129.22 133.28 1.46 o 4 9 1 0.11 0.10 0.27 o 5 9 1 2.80 2.36 0.19 o 6 9 1 119.73 121.75 1.39 o 7 9 1 47.51 46.27 0.83 o 8 9 1 152.62 149.01 1.31 o 9 9 1 2.95 4.35 0.23 o -8 10 1 4.34 2.31 0.18 o -7 10 1 423.55 393.71 2.24 o -6 10 1 155.64 157.77 1.53 o -5 10 1 38.06 41.01 0.82 o -4 10 1 0.60 1.15 0.11 o -3 10 1 55.56 58.18 0.99 o -2 10 1 5.60 6.99 0.44 o -1 10 1 81.91 94.96 1.25 o 0 10 1 0.00 0.19 0.14 o 1 10 1 4.61 6.22 0.40 o 2 10 1 680.04 736.47 3.46 o 3 10 1 572.79 634.22 3.21 o 4 10 1 27.29 25.34 0.68 o 5 10 1 32.04 30.94 0.73 o 6 10 1 67.39 70.75 1.01 o 7 10 1 3.71 4.95 0.33 o 8 10 1 32.44 32.62 0.55 o -7 11 1 0.38 1.02 0.10 o -6 11 1 50.13 48.83 0.79 o -5 11 1 6.11 6.27 0.39 o -4 11 1 46.73 46.65 0.86 o -3 11 1 183.83 188.78 1.73 o -2 11 1 666.92 708.32 3.37 o -1 11 1 193.43 217.66 1.88 o 0 11 1 45.70 45.27 0.88 o 1 11 1 9.94 11.62 0.51 o 2 11 1 0.41 0.52 0.11 o 3 11 1 287.78 307.27 2.17 o 4 11 1 49.01 50.02 0.88 o 5 11 1 117.94 133.36 1.33 o 6 11 1 15.03 12.25 0.41 o 7 11 1 105.48 108.57 0.96 o -5 12 1 10.01 11.69 0.40 o -4 12 1 8.78 8.94 0.40 o -3 12 1 31.10 30.68 0.68 o -2 12 1 357.49 375.85 2.30 o -1 12 1 155.04 171.71 1.58 o 0 12 1 0.18 0.29 0.10 o 1 12 1 1.34 2.13 0.21 o 2 12 1 46.72 44.55 0.81 o 3 12 1 30.76 31.22 0.66 o 4 12 1 3.73 4.77 0.33 o 5 12 1 0.45 0.58 0.08 o -3 13 1 43.20 38.90 0.65 o -2 13 1 178.43 166.79 1.35 o -1 13 1 24.47 24.80 0.58 o 0 13 1 0.11 0.38 0.08 o 1 13 1 2.75 2.97 0.27 o 2 13 1 12.03 9.90 0.37 o 4 13 1 121.24 125.27 0.99 o -12 0 2 0.00 0.25 0.07 o -11 0 2 0.17 0.27 0.23 o -10 0 2 154.56 154.55 1.58 o -9 0 2 12.73 11.71 0.51 o -8 0 2 130.98 127.70 2.18 o -7 0 2 298.77 313.13 4.15 o -6 0 2 313.00 328.82 2.73 o -5 0 2 5077.08 6192.34 94.77 o -4 0 2 1.03 6.45 0.16 o -3 0 2 245.96 259.97 6.85 o -2 0 2 3109.07 3226.38 78.77 o -1 0 2 1028.01 908.01 13.42 o 0 0 2 823.50 677.45 4.48 o 1 0 2 2300.58 2033.72 23.95 o 2 0 2 12.34 22.06 0.34 o 3 0 2 470.74 488.46 2.37 o 4 0 2 183.32 193.43 0.85 o 5 0 2 84.64 101.17 0.70 o 6 0 2 77.74 76.90 2.20 o 7 0 2 18.22 20.44 0.41 o 8 0 2 159.24 162.09 1.61 o 9 0 2 330.67 339.44 2.34 o 10 0 2 23.95 26.10 0.68 o 11 0 2 8.90 7.96 0.36 o -12 1 2 18.24 19.09 0.47 o -11 1 2 12.48 14.08 0.49 o -10 1 2 0.08 0.33 0.11 o -9 1 2 0.04 1.41 0.14 o -8 1 2 1405.04 1475.52 3.26 o -7 1 2 0.87 4.73 5.30 o -6 1 2 31.00 33.43 0.43 o -5 1 2 18.15 17.86 0.66 o -4 1 2 166.88 197.68 0.77 o -3 1 2 2.82 6.01 0.37 o -2 1 2 548.12 520.18 0.97 o -1 1 2 79.57 73.72 2.23 o 0 1 2 149.49 149.34 27.73 o 1 1 2 18307.45 20084.14 2480.65 o 2 1 2 110.01 121.37 1.17 o 3 1 2 223.99 229.83 2.00 o 4 1 2 179.23 184.59 2.78 o 5 1 2 64.16 66.22 0.57 o 6 1 2 1.73 1.58 0.09 o 7 1 2 28.86 27.48 0.47 o 8 1 2 54.74 57.12 0.98 o 9 1 2 95.98 96.76 1.26 o 10 1 2 815.02 859.42 3.49 o 11 1 2 0.26 -0.04 0.20 o -12 2 2 16.47 19.41 0.47 o -11 2 2 12.06 8.86 0.40 o -10 2 2 166.42 171.84 1.66 o -9 2 2 725.26 785.07 3.55 o -8 2 2 997.68 1009.55 19.47 o -7 2 2 93.20 94.71 3.82 o -6 2 2 14.70 12.44 0.28 o -5 2 2 283.12 266.73 4.74 o -4 2 2 1391.22 1502.17 53.95 o -3 2 2 91.16 97.77 3.90 o -2 2 2 53.72 46.38 1.60 o -1 2 2 328.17 287.40 10.52 o 0 2 2 3449.87 2831.99 67.15 o 1 2 2 14166.14 13878.03 669.62 o 2 2 2 23.63 24.51 0.50 o 3 2 2 52.93 58.47 0.48 o 4 2 2 605.15 639.18 7.28 o 5 2 2 4.50 4.34 0.63 o 6 2 2 273.55 293.60 1.34 o 7 2 2 2.11 1.77 0.11 o 8 2 2 158.53 165.64 1.63 o 9 2 2 630.29 677.63 3.29 o 10 2 2 78.45 96.96 1.17 o 11 2 2 37.82 36.19 0.61 o -11 3 2 2.21 2.58 0.21 o -10 3 2 46.93 42.39 0.86 o -9 3 2 335.51 342.79 2.36 o -8 3 2 306.45 316.59 4.83 o -7 3 2 102.58 113.19 1.04 o -6 3 2 433.03 461.49 26.77 o -5 3 2 843.63 921.34 35.61 o -4 3 2 1033.49 1171.85 71.34 o -3 3 2 392.03 403.70 14.96 o -2 3 2 497.70 481.55 20.14 o -1 3 2 36.80 38.28 2.51 o 0 3 2 3251.80 2945.92 109.89 o 1 3 2 102.36 97.60 1.03 o 2 3 2 191.20 207.72 36.98 o 3 3 2 36.35 34.36 0.36 o 4 3 2 1417.37 1556.21 31.29 o 5 3 2 48.50 38.98 0.47 o 6 3 2 260.06 256.93 1.29 o 7 3 2 274.24 302.84 3.79 o 8 3 2 30.07 32.52 0.76 o 9 3 2 39.53 43.86 0.87 o 10 3 2 53.11 46.58 0.81 o 11 3 2 21.50 21.00 0.48 o -12 4 2 15.94 13.62 0.36 o -11 4 2 18.67 19.89 0.53 o -10 4 2 82.20 71.34 1.06 o -9 4 2 0.49 1.13 0.11 o -8 4 2 0.14 0.71 0.11 o -7 4 2 12.02 10.97 0.31 o -6 4 2 119.38 112.24 6.46 o -5 4 2 9.99 13.32 0.82 o -4 4 2 146.40 164.28 8.94 o -3 4 2 392.85 440.80 21.47 o -2 4 2 1005.04 1046.94 38.19 o -1 4 2 279.09 281.32 1.91 o 0 4 2 0.00 0.31 0.21 o 1 4 2 5.87 6.05 0.43 o 2 4 2 59.91 55.69 0.88 o 3 4 2 474.93 491.73 5.77 o 4 4 2 409.18 441.08 10.80 o 5 4 2 43.62 54.57 1.05 o 6 4 2 163.26 172.04 4.05 o 7 4 2 254.50 249.49 1.97 o 8 4 2 41.89 42.95 0.85 o 9 4 2 67.66 71.97 1.07 o 10 4 2 41.29 39.09 0.71 o 11 4 2 14.28 13.04 0.36 o -11 5 2 23.90 22.25 0.51 o -10 5 2 132.88 106.58 1.25 o -9 5 2 115.65 110.79 1.35 o -8 5 2 2.06 1.98 0.19 o -7 5 2 2.90 3.35 0.50 o -6 5 2 265.16 266.68 22.18 o -5 5 2 42.89 37.07 1.97 o -4 5 2 166.35 180.87 14.35 o -3 5 2 96.97 82.42 6.52 o -2 5 2 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