#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016998.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016998_Fobs loop_ _publ_author_name 'Hori, Kayako' 'Kouno, Naomi' _publ_section_title ; Two crystal forms of mesogenic bis(4'-cyanobiphenyl-4-yl) butanedioate ; _journal_coeditor_code EG3008 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o108 _journal_page_last o110 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.452 _cell_angle_gamma 90.000 _cell_length_a 9.9235 _cell_length_b 8.7879 _cell_length_c 13.4152 _exptl_crystal_F_000 492.00 _reflns_d_resolution_high 0.8317 _[local]_cod_data_source_file eg3008IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' twin-ester-2-2 (Rigaku Master for Cu)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 177.24 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 179.67 160.02 0.58 o 2 0 0 1742.08 1591.17 12.44 o 3 0 0 311.68 298.33 2.89 o 4 0 0 6.38 6.29 0.37 o 5 0 0 552.76 609.03 11.73 o 6 0 0 81.67 91.21 1.26 o 7 0 0 44.79 46.47 2.76 o 8 0 0 102.41 98.90 2.03 o 9 0 0 0.02 0.14 0.45 o 10 0 0 0.19 0.44 0.22 o 11 0 0 101.38 103.96 1.41 o 1 1 0 215.51 206.01 2.97 o 2 1 0 0.25 1.83 0.15 o 3 1 0 2173.17 2163.49 22.25 o 4 1 0 59.58 55.63 2.34 o 5 1 0 363.54 370.98 2.20 o 6 1 0 95.89 87.96 1.25 o 7 1 0 62.14 57.34 1.14 o 8 1 0 17.61 22.03 0.83 o 9 1 0 18.44 16.27 0.91 o 10 1 0 11.96 13.02 0.69 o 11 1 0 6.40 6.31 0.36 o 0 2 0 31413.85 32009.25 64.22 o 1 2 0 20.80 33.48 0.48 o 2 2 0 1862.41 1821.41 36.61 o 3 2 0 1647.19 1650.25 42.39 o 4 2 0 165.20 164.18 3.70 o 5 2 0 109.89 123.01 3.12 o 6 2 0 80.60 93.21 1.34 o 7 2 0 30.73 26.07 1.62 o 8 2 0 53.73 46.10 1.15 o 9 2 0 13.43 10.45 0.79 o 10 2 0 2.72 3.69 0.25 o 11 2 0 2.98 2.94 0.44 o 1 3 0 1613.08 1594.00 15.96 o 2 3 0 13.29 13.48 1.76 o 3 3 0 434.79 456.36 15.72 o 4 3 0 576.95 627.76 25.37 o 5 3 0 272.35 277.32 11.53 o 6 3 0 8.29 9.59 0.58 o 7 3 0 9.27 7.00 0.40 o 8 3 0 1.55 2.88 0.20 o 9 3 0 154.32 139.47 2.71 o 10 3 0 2.18 4.01 0.53 o 11 3 0 4.03 4.78 0.50 o 0 4 0 37.33 31.29 0.91 o 1 4 0 146.40 156.85 3.59 o 2 4 0 588.25 596.69 12.03 o 3 4 0 1039.19 1116.67 42.84 o 4 4 0 0.06 0.88 0.30 o 5 4 0 45.08 53.02 2.47 o 6 4 0 16.01 26.95 3.06 o 7 4 0 55.96 48.44 5.08 o 8 4 0 3.48 4.51 0.31 o 9 4 0 109.83 104.73 1.62 o 10 4 0 1.80 1.04 0.23 o 1 5 0 90.51 97.74 1.25 o 2 5 0 136.85 140.28 3.39 o 3 5 0 6.29 6.06 0.52 o 4 5 0 95.61 127.98 1.63 o 5 5 0 0.88 0.17 0.35 o 6 5 0 72.99 64.86 1.43 o 7 5 0 64.27 60.21 1.32 o 8 5 0 45.58 40.07 1.08 o 9 5 0 65.33 53.51 1.51 o 10 5 0 45.10 37.38 7.77 o 0 6 0 227.03 223.05 2.96 o 1 6 0 28.85 24.07 0.80 o 2 6 0 379.20 398.68 2.87 o 3 6 0 52.36 58.59 1.20 o 4 6 0 2.18 2.87 0.19 o 5 6 0 7.41 6.17 0.45 o 6 6 0 26.90 26.20 1.57 o 7 6 0 12.27 11.97 0.73 o 8 6 0 23.99 21.26 1.19 o 9 6 0 69.41 55.70 1.02 o 1 7 0 20.14 20.58 0.81 o 2 7 0 0.25 0.12 0.38 o 3 7 0 258.34 269.54 2.62 o 4 7 0 60.61 56.41 1.28 o 5 7 0 2.84 2.86 0.20 o 6 7 0 54.33 54.80 1.22 o 7 7 0 34.35 32.26 0.92 o 8 7 0 15.34 14.24 0.60 o 0 8 0 486.29 496.43 5.06 o 1 8 0 39.93 39.58 1.11 o 2 8 0 96.88 107.17 1.73 o 3 8 0 0.04 -0.46 0.46 o 4 8 0 14.69 14.70 0.74 o 5 8 0 27.33 24.30 1.78 o 6 8 0 12.90 12.82 1.29 o 7 8 0 1.08 1.93 0.13 o 1 9 0 176.71 174.73 2.05 o 2 9 0 42.55 47.74 1.11 o 3 9 0 28.79 28.10 0.88 o 4 9 0 67.08 67.58 1.20 o 5 9 0 23.70 27.57 0.89 o 6 9 0 2.52 2.27 0.15 o 0 10 0 72.26 68.13 1.59 o 1 10 0 1.92 1.70 0.14 o 2 10 0 1.77 1.21 0.26 o 3 10 0 1.85 1.66 0.17 o -11 1 1 88.80 82.54 1.80 o -10 1 1 119.01 118.03 2.42 o -9 1 1 0.81 1.45 0.24 o -8 1 1 32.43 32.73 1.58 o -7 1 1 35.14 35.35 0.95 o -6 1 1 1.67 1.01 0.28 o -5 1 1 2853.85 2967.22 95.88 o -4 1 1 113.01 121.72 4.20 o -3 1 1 12249.64 12084.84 581.09 o -2 1 1 23129.87 23266.76 910.26 o -1 1 1 1234.62 1275.95 80.03 o 0 1 1 369.44 335.59 15.24 o 1 1 1 31.47 33.77 1.15 o 2 1 1 169.44 159.02 3.81 o 3 1 1 480.98 428.95 6.38 o 4 1 1 223.00 187.85 1.87 o 5 1 1 20.77 21.57 0.62 o 6 1 1 17.07 17.80 0.66 o 7 1 1 0.69 1.46 0.72 o 8 1 1 1.91 2.07 0.27 o 9 1 1 50.48 47.29 1.67 o 10 1 1 80.85 87.74 2.09 o 11 1 1 24.90 26.28 1.05 o -11 2 1 0.23 0.13 0.46 o -10 2 1 1.03 0.93 0.23 o -9 2 1 2.10 3.61 0.36 o -8 2 1 64.65 64.53 1.89 o -7 2 1 80.35 83.54 2.29 o -6 2 1 26.18 31.17 0.83 o -5 2 1 572.09 619.65 23.72 o -4 2 1 615.21 589.74 16.36 o -3 2 1 1492.73 1517.20 71.86 o -2 2 1 3527.45 3722.04 226.61 o -1 2 1 10102.66 10267.26 508.11 o 0 2 1 816.83 822.80 25.69 o 1 2 1 99.55 81.96 1.36 o 2 2 1 18.03 16.28 0.43 o 3 2 1 1129.20 1119.03 28.98 o 4 2 1 24.65 15.93 0.52 o 5 2 1 355.80 336.95 2.24 o 6 2 1 105.95 96.03 1.37 o 7 2 1 143.23 137.63 2.49 o 8 2 1 15.34 14.16 1.06 o 9 2 1 216.34 216.88 3.42 o 10 2 1 4.32 4.28 0.41 o 11 2 1 11.21 9.27 0.68 o -11 3 1 41.29 36.92 1.14 o -10 3 1 0.49 -0.09 0.63 o -9 3 1 25.81 24.49 1.27 o -8 3 1 0.03 0.01 0.62 o -7 3 1 0.37 0.43 0.42 o -6 3 1 49.22 49.06 2.99 o -5 3 1 608.00 692.62 33.53 o -4 3 1 233.98 245.56 14.98 o -3 3 1 237.81 264.01 12.94 o -2 3 1 1120.39 1165.11 64.90 o -1 3 1 3182.13 3509.61 202.59 o 0 3 1 569.47 575.93 14.95 o 1 3 1 637.96 665.87 3.54 o 2 3 1 3.24 4.01 0.46 o 3 3 1 14.10 19.11 0.66 o 4 3 1 440.83 502.05 18.40 o 5 3 1 6.24 8.72 0.51 o 6 3 1 0.27 0.53 0.19 o 7 3 1 9.27 10.56 0.72 o 8 3 1 8.90 9.82 0.88 o 9 3 1 8.75 9.96 0.95 o 10 3 1 8.94 7.08 0.53 o 11 3 1 18.89 17.66 0.79 o -11 4 1 15.54 10.11 0.64 o -10 4 1 26.89 28.28 1.14 o -9 4 1 153.74 139.09 2.64 o -8 4 1 0.22 0.06 0.63 o -7 4 1 19.93 16.42 1.11 o -6 4 1 9.40 7.66 1.10 o -5 4 1 0.15 0.18 0.40 o -4 4 1 31.24 27.91 0.74 o -3 4 1 1567.21 1589.05 87.63 o -2 4 1 1040.81 1119.10 45.09 o -1 4 1 1493.08 1609.48 33.63 o 0 4 1 160.94 195.13 1.48 o 1 4 1 932.85 985.37 12.13 o 2 4 1 1439.27 1534.26 19.51 o 3 4 1 118.59 141.89 1.45 o 4 4 1 208.06 231.73 12.42 o 5 4 1 17.96 19.50 2.12 o 6 4 1 41.61 39.48 1.01 o 7 4 1 129.64 117.05 2.49 o 8 4 1 84.75 84.13 2.17 o 9 4 1 66.81 63.92 1.82 o 10 4 1 24.21 23.93 1.06 o -10 5 1 49.99 45.54 1.24 o -9 5 1 18.50 19.14 1.06 o -8 5 1 28.45 27.88 1.30 o -7 5 1 6.08 5.01 0.46 o -6 5 1 73.31 79.55 1.45 o -5 5 1 0.14 0.75 0.19 o -4 5 1 77.00 78.04 2.06 o -3 5 1 705.40 707.97 29.65 o -2 5 1 341.22 379.02 12.47 o -1 5 1 339.20 374.50 8.44 o 0 5 1 1.14 0.66 0.34 o 1 5 1 66.40 75.18 2.72 o 2 5 1 159.57 173.85 5.16 o 3 5 1 113.27 126.60 1.55 o 4 5 1 66.88 78.82 2.23 o 5 5 1 6.45 7.51 0.61 o 6 5 1 21.32 21.81 1.22 o 7 5 1 50.45 37.58 1.53 o 8 5 1 0.17 0.12 0.43 o 9 5 1 8.48 8.47 0.74 o 10 5 1 1.79 2.50 0.23 o -9 6 1 112.44 96.12 1.88 o -8 6 1 21.17 21.11 1.10 o -7 6 1 62.96 58.53 1.81 o -6 6 1 52.07 51.98 1.75 o -5 6 1 25.57 27.96 1.34 o -4 6 1 6.14 6.96 0.42 o -3 6 1 61.89 57.94 1.20 o -2 6 1 640.09 639.66 23.71 o -1 6 1 242.08 250.83 6.62 o 0 6 1 153.33 154.03 2.95 o 1 6 1 67.68 64.03 1.19 o 2 6 1 151.01 179.59 1.96 o 3 6 1 1.49 4.29 0.29 o 4 6 1 76.57 68.08 2.35 o 5 6 1 30.60 27.14 1.35 o 6 6 1 123.44 122.81 2.59 o 7 6 1 94.33 84.08 2.17 o 8 6 1 0.29 0.46 0.62 o 9 6 1 2.39 2.79 0.26 o -8 7 1 7.66 6.62 0.48 o -7 7 1 8.47 10.15 0.93 o -6 7 1 15.15 20.12 1.11 o -5 7 1 49.83 53.26 1.77 o -4 7 1 33.05 32.26 1.50 o -3 7 1 138.21 139.75 2.71 o -2 7 1 60.22 56.65 4.39 o -1 7 1 9.82 10.07 0.63 o 0 7 1 136.37 148.25 1.93 o 1 7 1 292.98 308.17 14.79 o 2 7 1 99.16 93.58 2.76 o 3 7 1 38.88 35.33 1.48 o 4 7 1 54.29 58.30 1.86 o 5 7 1 32.26 36.32 1.46 o 6 7 1 35.68 31.32 1.39 o 7 7 1 18.78 16.56 0.97 o 8 7 1 4.34 3.66 0.31 o -7 8 1 35.04 37.93 1.17 o -6 8 1 15.61 14.90 0.93 o -5 8 1 18.36 18.38 1.07 o -4 8 1 16.70 17.39 1.13 o -3 8 1 2.03 3.64 0.35 o -2 8 1 160.53 166.36 2.99 o -1 8 1 32.34 29.65 1.40 o 0 8 1 25.36 26.52 1.38 o 1 8 1 306.52 316.27 4.07 o 2 8 1 37.16 35.85 1.49 o 3 8 1 3.27 2.04 0.28 o 4 8 1 15.76 14.10 1.01 o 5 8 1 0.06 0.31 0.59 o 6 8 1 13.64 10.76 0.79 o 7 8 1 29.10 26.41 1.01 o -6 9 1 0.75 0.67 0.15 o -5 9 1 12.08 11.98 0.81 o -4 9 1 10.50 10.82 0.84 o -3 9 1 0.01 0.38 0.61 o -2 9 1 226.22 230.03 3.26 o -1 9 1 7.17 8.05 0.61 o 0 9 1 80.20 81.20 2.07 o 1 9 1 128.32 125.63 2.47 o 2 9 1 135.34 124.84 2.42 o 3 9 1 6.11 5.05 0.44 o 4 9 1 37.87 34.80 1.27 o 5 9 1 41.89 46.40 1.30 o 6 9 1 51.82 59.89 1.25 o -2 10 1 4.52 4.96 0.42 o -1 10 1 71.69 65.09 1.52 o 0 10 1 83.33 82.29 1.72 o 1 10 1 18.71 18.05 0.90 o 2 10 1 99.56 101.61 1.82 o 3 10 1 1.48 3.17 0.28 o -11 0 2 27.65 27.56 1.13 o -10 0 2 6.53 3.07 0.29 o -9 0 2 16.79 20.03 1.19 o -8 0 2 67.63 68.84 1.35 o -7 0 2 463.68 527.29 5.57 o -6 0 2 51.61 43.18 0.92 o -5 0 2 629.95 684.17 9.78 o -4 0 2 1112.92 1170.39 22.18 o -3 0 2 3400.98 3741.32 143.69 o -2 0 2 10839.42 11571.03 664.70 o -1 0 2 59.43 65.65 2.34 o 0 0 2 607.77 507.02 15.25 o 1 0 2 0.74 3.78 0.22 o 2 0 2 413.81 356.41 9.54 o 3 0 2 207.47 170.56 7.25 o 4 0 2 285.21 253.85 9.49 o 5 0 2 76.58 78.98 3.08 o 6 0 2 33.26 22.12 0.71 o 7 0 2 2.74 2.90 0.19 o 8 0 2 9.62 7.15 0.64 o 9 0 2 54.03 60.96 1.88 o 10 0 2 100.53 113.20 2.29 o 11 0 2 152.93 151.97 2.29 o -11 1 2 7.89 8.69 0.72 o -10 1 2 11.34 9.71 0.84 o -9 1 2 2.36 4.40 0.40 o -8 1 2 0.05 -0.44 0.44 o -7 1 2 22.72 21.62 0.76 o -6 1 2 815.45 812.15 23.83 o -5 1 2 67.57 70.31 2.81 o -4 1 2 52.81 58.55 0.96 o -3 1 2 545.76 554.40 25.91 o -2 1 2 4669.20 4783.31 258.03 o -1 1 2 744.14 720.94 36.78 o 0 1 2 497.41 437.99 28.84 o 1 1 2 109.41 93.93 4.28 o 2 1 2 226.02 201.82 5.73 o 3 1 2 16.34 18.16 0.48 o 4 1 2 260.73 245.53 4.28 o 5 1 2 132.20 118.63 2.88 o 6 1 2 54.38 54.29 2.37 o 7 1 2 108.23 119.87 2.42 o 8 1 2 10.52 12.33 1.00 o 9 1 2 1.29 1.55 0.26 o 10 1 2 61.81 63.23 1.79 o 11 1 2 1.07 1.03 0.18 o -11 2 2 0.63 0.20 0.45 o -10 2 2 16.32 16.10 1.01 o -9 2 2 27.91 25.09 1.28 o -8 2 2 35.34 42.91 1.51 o -7 2 2 349.13 387.20 17.62 o -6 2 2 231.59 238.04 11.11 o -5 2 2 1159.77 1182.61 51.34 o -4 2 2 17.82 22.68 0.61 o -3 2 2 170.78 159.08 8.37 o -2 2 2 3278.27 3549.32 213.26 o -1 2 2 3086.67 3141.06 197.55 o 0 2 2 203.15 174.32 5.97 o 1 2 2 440.48 380.43 1.57 o 2 2 2 136.54 137.61 3.55 o 3 2 2 73.12 86.31 3.95 o 4 2 2 123.15 111.64 3.18 o 5 2 2 63.37 63.94 1.05 o 6 2 2 38.15 45.80 1.01 o 7 2 2 129.05 134.01 1.79 o 8 2 2 62.92 66.17 1.91 o 9 2 2 66.07 69.10 1.95 o 10 2 2 23.67 25.61 1.19 o 11 2 2 93.03 88.52 1.67 o -11 3 2 94.10 89.45 1.73 o -10 3 2 0.98 0.34 0.57 o -9 3 2 13.98 12.61 0.94 o -8 3 2 8.68 8.72 0.67 o -7 3 2 0.69 0.04 0.44 o -6 3 2 856.47 896.93 38.69 o -5 3 2 14.66 16.29 1.36 o -4 3 2 818.44 816.89 48.40 o -3 3 2 754.83 816.08 46.94 o -2 3 2 1014.76 1057.38 63.51 o -1 3 2 35.90 36.59 1.80 o 0 3 2 641.17 653.00 22.97 o 1 3 2 0.01 -0.09 0.40 o 2 3 2 208.22 214.78 7.83 o 3 3 2 104.38 105.41 3.34 o 4 3 2 29.09 30.99 0.73 o 5 3 2 234.40 239.77 10.66 o 6 3 2 8.01 9.05 0.59 o 7 3 2 205.42 203.18 6.45 o 8 3 2 82.78 83.31 2.18 o 9 3 2 0.02 -0.05 0.64 o 10 3 2 47.33 43.02 1.37 o 11 3 2 22.51 24.11 0.84 o -11 4 2 32.38 33.73 1.00 o -10 4 2 18.47 15.61 0.95 o -9 4 2 12.38 10.86 0.93 o -8 4 2 20.34 21.26 1.22 o -7 4 2 159.92 176.97 3.02 o -6 4 2 1.88 2.27 0.20 o -5 4 2 84.36 87.84 4.79 o -4 4 2 52.08 58.54 4.83 o -3 4 2 124.15 156.75 7.82 o -2 4 2 20.78 24.24 1.25 o -1 4 2 330.58 370.42 9.56 o 0 4 2 52.14 60.76 0.87 o 1 4 2 168.23 170.26 2.19 o 2 4 2 889.04 959.41 14.87 o 3 4 2 67.90 79.47 1.13 o 4 4 2 52.65 49.04 1.48 o 5 4 2 14.36 12.42 1.18 o 6 4 2 81.52 76.29 5.25 o 7 4 2 1.60 3.25 0.31 o 8 4 2 113.45 113.89 2.48 o 9 4 2 229.76 234.73 3.28 o 10 4 2 40.23 39.60 1.25 o -10 5 2 19.34 18.83 0.85 o -9 5 2 52.65 51.42 1.56 o -8 5 2 29.02 30.59 1.35 o -7 5 2 6.23 5.66 0.49 o -6 5 2 15.99 16.98 0.76 o -5 5 2 36.54 36.60 1.02 o -4 5 2 167.50 169.90 9.05 o -3 5 2 586.32 630.18 37.02 o -2 5 2 19.12 18.34 0.67 o -1 5 2 870.74 918.37 34.66 o 0 5 2 152.80 178.56 5.60 o 1 5 2 449.38 487.49 11.29 o 2 5 2 647.68 717.99 16.45 o 3 5 2 127.38 117.27 1.51 o 4 5 2 74.49 69.86 1.27 o 5 5 2 4.86 4.05 0.26 o 6 5 2 11.40 10.24 0.94 o 7 5 2 51.71 46.02 1.66 o 8 5 2 16.89 15.45 1.08 o 9 5 2 38.30 40.86 1.34 o 10 5 2 6.08 7.44 0.61 o -9 6 2 1.22 1.48 0.20 o -8 6 2 4.74 5.37 0.52 o -7 6 2 0.17 0.15 0.58 o -6 6 2 124.98 135.76 2.70 o -5 6 2 29.32 30.31 1.41 o -4 6 2 265.40 262.47 13.64 o -3 6 2 55.82 54.10 1.17 o -2 6 2 735.58 726.41 21.64 o -1 6 2 68.72 74.15 1.52 o 0 6 2 7.29 5.64 0.36 o 1 6 2 56.56 71.51 1.26 o 2 6 2 0.04 1.11 0.35 o 3 6 2 145.86 153.12 1.88 o 4 6 2 4.40 3.59 0.85 o 5 6 2 20.73 16.63 1.12 o 6 6 2 4.55 3.92 0.37 o 7 6 2 50.23 41.96 1.57 o 8 6 2 0.69 0.75 0.62 o 9 6 2 55.88 54.88 1.36 o -8 7 2 1.56 1.40 0.19 o -7 7 2 16.98 13.36 0.95 o -6 7 2 0.08 0.67 0.54 o -5 7 2 9.17 8.51 0.63 o -4 7 2 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