#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017028.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017028_Fobs loop_ _publ_author_name 'Gavilan, Elisabeth' 'Audebrand, Nathalie' _publ_section_title ; A monoclinic pseudopolymorph of manganese squarate dihydrate, Mn(\m-C~4~O~4~)(H~2~O)~2~, built from cubic units ; _journal_coeditor_code DN3102 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m156 _journal_page_last m159 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.084 _cell_angle_gamma 90.000 _cell_length_a 11.5921 _cell_length_b 11.8471 _cell_length_c 16.5666 _exptl_crystal_F_000 1212.00 _reflns_d_resolution_high 0.6189 _[local]_cod_data_source_file dn3102Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mnsq-07 in C 1 2/c 1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 429.21 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 53372.96 40676.76 710.40 o 4 0 0 16093.04 17046.80 177.76 o 6 0 0 15368.52 15579.29 131.81 o 8 0 0 4576.22 4434.93 50.64 o 10 0 0 989.53 939.71 29.96 o 12 0 0 14071.93 14296.92 138.52 o 14 0 0 1693.33 1714.77 64.86 o 16 0 0 3746.65 3697.78 118.21 o 18 0 0 1054.61 1164.81 202.60 o 3 1 0 1741.25 2439.52 21.57 o 5 1 0 914.40 729.84 11.02 o 7 1 0 3243.96 2932.00 26.34 o 9 1 0 7468.31 7350.59 51.85 o 11 1 0 1414.06 1434.45 23.70 o 13 1 0 724.17 705.03 27.31 o 15 1 0 789.99 780.85 35.48 o 17 1 0 577.78 579.59 58.05 o 4 2 0 21132.57 22464.89 135.18 o 6 2 0 39113.59 39704.83 224.01 o 8 2 0 1969.04 1893.18 20.22 o 10 2 0 7510.50 7415.96 54.17 o 12 2 0 346.28 321.83 22.22 o 14 2 0 5563.14 5747.20 82.41 o 16 2 0 399.09 418.33 122.10 o 18 2 0 2271.62 2112.61 109.62 o 1 3 0 227.91 422.00 8.48 o 3 3 0 54219.62 59018.57 363.46 o 5 3 0 44.29 21.66 6.22 o 7 3 0 5790.39 6401.33 44.57 o 9 3 0 9.35 22.60 10.19 o 11 3 0 427.31 463.00 18.18 o 13 3 0 3416.67 3157.53 71.95 o 15 3 0 987.46 996.03 56.12 o 17 3 0 279.24 225.74 60.95 o 0 4 0 39979.20 41081.41 319.38 o 2 4 0 13579.37 14510.35 84.63 o 4 4 0 89091.80 87206.88 573.47 o 6 4 0 7185.27 8126.36 56.10 o 8 4 0 10909.85 10814.10 68.52 o 10 4 0 1778.63 1701.66 23.93 o 12 4 0 10977.64 10975.11 91.83 o 14 4 0 4.70 29.96 43.25 o 16 4 0 3353.24 3485.96 120.01 o 18 4 0 476.22 574.44 89.30 o 1 5 0 11839.97 12096.79 76.35 o 3 5 0 550.59 615.70 11.88 o 5 5 0 27501.78 29739.86 181.85 o 7 5 0 908.84 897.35 18.23 o 9 5 0 1519.05 1550.43 24.91 o 11 5 0 2444.23 2300.94 32.57 o 13 5 0 58.01 73.92 22.89 o 15 5 0 219.19 88.44 100.81 o 17 5 0 201.42 488.76 173.11 o 0 6 0 1456.41 1275.35 21.13 o 2 6 0 63473.13 65696.59 405.32 o 4 6 0 8715.81 9816.65 66.97 o 6 6 0 1490.66 1412.08 19.55 o 8 6 0 3095.25 2884.80 33.68 o 10 6 0 21123.10 20718.75 167.09 o 12 6 0 84.28 66.50 23.71 o 14 6 0 8789.89 9010.64 152.07 o 16 6 0 627.25 540.58 139.16 o 1 7 0 11741.03 11712.31 81.55 o 3 7 0 7663.69 8333.36 59.79 o 5 7 0 809.71 866.23 15.50 o 7 7 0 1890.45 2196.40 42.50 o 9 7 0 1204.28 1170.02 45.79 o 11 7 0 1150.51 1021.76 53.23 o 13 7 0 139.53 134.50 61.56 o 15 7 0 104.07 231.69 83.83 o 0 8 0 11722.84 11844.78 118.97 o 2 8 0 1020.52 971.48 18.92 o 4 8 0 11728.76 11754.11 81.34 o 6 8 0 3923.26 3698.16 56.62 o 8 8 0 25077.52 24801.41 291.60 o 10 8 0 2415.48 2318.52 83.25 o 12 8 0 4215.26 4285.34 92.45 o 14 8 0 289.68 262.18 64.50 o 1 9 0 9534.67 9690.12 77.89 o 3 9 0 4.47 7.48 11.29 o 5 9 0 1507.67 1498.09 40.99 o 7 9 0 474.42 409.88 57.88 o 9 9 0 196.50 196.06 53.01 o 11 9 0 826.33 745.18 57.68 o 13 9 0 730.53 700.80 119.68 o 15 9 0 240.59 439.71 124.96 o 0 10 0 88.46 73.93 23.22 o 2 10 0 8153.80 8022.40 70.98 o 4 10 0 1987.65 1907.61 30.09 o 6 10 0 17747.39 18351.29 230.14 o 8 10 0 3915.89 3927.75 100.48 o 10 10 0 5109.00 4991.50 100.39 o 12 10 0 591.39 622.19 71.87 o 14 10 0 2143.72 2369.92 148.10 o 1 11 0 801.03 777.64 30.35 o 3 11 0 495.19 487.34 21.01 o 5 11 0 943.84 858.01 38.79 o 7 11 0 284.64 286.16 50.51 o 9 11 0 285.44 315.79 66.72 o 11 11 0 882.27 796.53 102.08 o 13 11 0 559.54 670.69 102.85 o 15 11 0 801.03 856.97 111.11 o 0 12 0 13886.56 13596.98 224.70 o 2 12 0 660.21 569.38 26.24 o 4 12 0 8593.53 8707.12 94.02 o 6 12 0 1529.96 1424.43 128.75 o 8 12 0 2590.19 2747.23 92.89 o 10 12 0 879.90 913.25 97.40 o 12 12 0 3769.95 3867.76 174.21 o 14 12 0 235.64 19.77 97.67 o 1 13 0 434.72 387.01 30.67 o 3 13 0 1775.78 1630.94 54.16 o 5 13 0 142.69 160.51 27.96 o 7 13 0 4.16 -22.09 60.04 o 9 13 0 540.85 496.70 66.48 o 11 13 0 314.71 457.33 112.81 o 13 13 0 2193.58 2336.50 98.22 o 0 14 0 1611.04 1724.71 80.90 o 2 14 0 4816.45 4775.48 118.44 o 4 14 0 462.98 421.92 55.78 o 6 14 0 6685.78 6661.83 160.20 o 8 14 0 687.45 541.86 92.48 o 10 14 0 2041.06 1842.01 156.36 o 12 14 0 593.56 435.70 148.97 o 1 15 0 738.29 735.81 47.71 o 3 15 0 478.17 421.20 48.94 o 5 15 0 34.43 5.31 81.60 o 7 15 0 1.61 -94.80 94.80 o 9 15 0 287.53 286.38 98.91 o 11 15 0 603.04 681.87 108.72 o 0 16 0 3494.17 3278.62 122.04 o 2 16 0 708.64 860.35 70.11 o 4 16 0 2973.06 3015.07 116.69 o 6 16 0 1143.55 1020.62 112.10 o 8 16 0 2356.85 2267.75 199.09 o 10 16 0 123.41 -154.88 158.15 o 1 17 0 368.71 259.31 74.30 o 3 17 0 185.94 214.09 201.86 o 5 17 0 79.97 50.92 117.04 o 7 17 0 42.04 77.59 204.58 o 0 18 0 1128.41 1404.07 228.79 o 2 18 0 2179.64 2058.49 104.34 o 4 18 0 839.31 956.36 139.27 o 6 18 0 1009.85 1276.69 227.69 o 1 19 0 585.96 1173.24 233.43 o -17 1 1 9.01 -50.96 50.96 o -15 1 1 16.15 40.49 35.84 o -13 1 1 25.29 54.38 23.90 o -11 1 1 596.98 583.14 19.06 o -9 1 1 787.00 757.73 16.46 o -7 1 1 2.77 -1.94 11.56 o -5 1 1 36.08 46.58 8.00 o -3 1 1 373.23 394.30 7.65 o 3 1 1 465.16 463.47 7.52 o 5 1 1 1413.12 1550.53 14.56 o 7 1 1 267.88 215.36 8.69 o 9 1 1 52.85 44.55 11.24 o 11 1 1 0.92 -2.26 16.31 o 13 1 1 76.33 97.73 21.69 o 15 1 1 2.13 7.81 41.26 o 17 1 1 37.14 -19.99 91.31 o -18 2 1 50.32 121.88 105.74 o -16 2 1 179.93 113.21 51.95 o -14 2 1 6.03 24.89 32.54 o -12 2 1 61.44 96.76 19.99 o -10 2 1 177.16 134.67 17.05 o -8 2 1 992.87 1064.20 18.50 o -6 2 1 161.85 166.70 16.82 o -4 2 1 19134.81 20337.57 133.48 o -2 2 1 885.32 1105.15 13.50 o 0 2 1 341.11 156.62 4.23 o 2 2 1 876.85 1121.42 13.59 o 4 2 1 25162.26 26892.14 144.09 o 6 2 1 1019.16 1136.69 18.72 o 8 2 1 938.67 935.48 21.10 o 10 2 1 115.58 121.97 13.16 o 12 2 1 164.83 209.11 21.17 o 14 2 1 51.35 53.26 32.39 o 16 2 1 72.08 108.39 97.60 o 18 2 1 286.28 442.55 106.43 o -17 3 1 320.98 280.83 268.63 o -15 3 1 1.07 17.37 34.54 o -13 3 1 234.73 198.94 26.39 o -11 3 1 23.05 13.90 15.13 o -9 3 1 581.39 471.10 15.29 o -7 3 1 191.17 180.61 10.44 o -5 3 1 5.89 5.50 7.24 o -3 3 1 1820.53 1922.56 25.76 o -1 3 1 0.93 1.10 3.87 o 1 3 1 93.49 5.98 2.84 o 3 3 1 992.27 1048.36 16.71 o 5 3 1 18.68 11.67 4.87 o 7 3 1 1207.34 1171.33 14.81 o 9 3 1 920.97 840.18 15.19 o 11 3 1 303.82 262.97 22.29 o 13 3 1 27.14 -19.02 23.21 o 15 3 1 2.73 -0.80 37.15 o 17 3 1 180.18 156.83 73.40 o -18 4 1 97.68 263.01 122.21 o -16 4 1 98.53 173.65 89.07 o -14 4 1 41.19 68.44 34.62 o -12 4 1 21.61 33.90 18.98 o -10 4 1 5338.40 5134.07 44.22 o -8 4 1 1226.29 1107.30 19.73 o -6 4 1 4.32 42.03 10.50 o -4 4 1 1676.60 1629.41 24.28 o -2 4 1 16940.76 18671.38 128.59 o 0 4 1 2158.17 2547.35 20.44 o 2 4 1 14277.60 15088.52 84.49 o 4 4 1 1766.74 1682.00 30.94 o 6 4 1 106.88 282.42 54.37 o 8 4 1 511.79 441.01 10.95 o 10 4 1 2882.08 2775.60 28.50 o 12 4 1 489.19 486.72 20.00 o 14 4 1 807.98 806.73 35.50 o 16 4 1 118.68 276.84 87.84 o 18 4 1 137.27 63.42 95.31 o -17 5 1 172.25 141.53 166.95 o -15 5 1 236.81 225.97 47.87 o -13 5 1 43.77 100.19 34.86 o -11 5 1 4.97 9.56 14.38 o -9 5 1 433.89 381.13 14.50 o -7 5 1 37.51 37.94 10.23 o -5 5 1 2370.77 2774.98 29.76 o -3 5 1 112.39 93.49 7.17 o -1 5 1 7698.31 8157.39 57.37 o 1 5 1 225.79 340.76 8.74 o 3 5 1 154.15 136.01 5.80 o 5 5 1 2463.28 2743.01 32.52 o 7 5 1 386.59 364.74 16.72 o 9 5 1 2011.58 1911.97 25.04 o 11 5 1 593.70 564.80 21.10 o 13 5 1 60.99 85.73 28.91 o 15 5 1 2.40 69.88 57.51 o 17 5 1 87.62 -146.59 146.59 o -14 6 1 25.50 55.60 40.01 o -12 6 1 133.49 139.36 21.46 o -10 6 1 178.14 210.69 14.69 o -8 6 1 98.41 112.49 12.44 o -6 6 1 768.05 826.13 17.29 o -4 6 1 20.99 24.96 8.55 o -2 6 1 1773.22 1973.10 21.03 o 0 6 1 656.01 753.56 12.26 o 2 6 1 131.48 130.67 7.11 o 4 6 1 62.95 63.45 15.76 o 6 6 1 664.05 651.92 22.99 o 8 6 1 101.15 139.31 28.25 o 10 6 1 432.14 457.50 23.07 o 12 6 1 40.35 47.96 15.48 o 14 6 1 45.42 80.71 107.35 o 16 6 1 125.27 239.78 89.43 o -15 7 1 106.16 -38.33 99.10 o -13 7 1 498.01 531.61 33.48 o -11 7 1 22.65 46.41 20.65 o -9 7 1 80.25 209.34 43.06 o -7 7 1 1189.73 1248.49 22.04 o -5 7 1 812.38 860.67 15.35 o -3 7 1 6167.89 6265.10 48.09 o -1 7 1 559.12 477.00 12.81 o 1 7 1 337.80 310.63 10.01 o 3 7 1 180.23 241.78 17.27 o 5 7 1 213.00 255.53 21.47 o 7 7 1 1094.68 1053.86 31.13 o 9 7 1 127.50 119.25 37.82 o 11 7 1 324.86 255.51 49.08 o 13 7 1 38.19 24.30 101.59 o 15 7 1 35.16 32.88 97.07 o -16 8 1 3.67 104.23 137.11 o -14 8 1 389.41 352.00 83.99 o -12 8 1 207.46 245.73 49.87 o -10 8 1 468.77 527.03 50.48 o -8 8 1 1701.95 1781.56 29.28 o -6 8 1 215.22 188.99 16.54 o -4 8 1 112.76 108.40 15.75 o -2 8 1 5449.48 5777.68 51.02 o 0 8 1 241.57 299.61 13.10 o 2 8 1 180.13 202.10 12.60 o 4 8 1 894.47 822.46 19.18 o 6 8 1 0.96 15.54 25.32 o 8 8 1 1674.97 1608.72 63.94 o 10 8 1 973.65 1155.01 53.99 o 12 8 1 22.29 -50.54 57.83 o 14 8 1 0.49 58.10 69.85 o 16 8 1 141.21 46.59 155.03 o -15 9 1 546.58 557.87 105.81 o -13 9 1 91.27 36.57 106.96 o -11 9 1 14.19 33.01 42.45 o -9 9 1 783.30 673.69 48.40 o -7 9 1 37.36 38.29 12.58 o -5 9 1 2290.51 2195.24 26.62 o -3 9 1 1219.53 1062.57 20.32 o -1 9 1 2852.06 2773.19 32.12 o 1 9 1 490.18 432.02 16.33 o 3 9 1 235.64 179.39 13.09 o 5 9 1 186.45 174.54 28.43 o 7 9 1 7.79 10.38 38.69 o 9 9 1 1047.82 1019.56 54.21 o 11 9 1 175.15 227.51 54.11 o 13 9 1 296.09 254.80 55.43 o 15 9 1 34.97 122.15 112.49 o -14 10 1 15.51 -2.03 93.64 o -12 10 1 296.98 323.95 79.16 o -10 10 1 645.06 709.10 88.20 o -8 10 1 124.38 224.84 76.35 o -6 10 1 1040.71 1057.17 28.55 o -4 10 1 1900.70 1729.32 26.89 o -2 10 1 69.08 46.75 15.20 o 0 10 1 3070.99 3225.78 37.57 o 2 10 1 423.21 363.44 16.74 o 4 10 1 6883.36 6793.35 63.37 o 6 10 1 374.04 402.86 40.80 o 8 10 1 305.39 336.26 57.40 o 10 10 1 608.44 709.36 55.95 o 12 10 1 6.87 -15.11 100.50 o 14 10 1 658.43 845.86 125.91 o -15 11 1 531.82 390.97 182.16 o -13 11 1 9.79 11.53 94.42 o -11 11 1 686.39 632.85 84.78 o -9 11 1 4.82 -4.47 57.56 o -7 11 1 28.18 140.66 56.53 o -5 11 1 2330.77 2275.65 37.79 o -3 11 1 1905.29 1877.12 37.17 o -1 11 1 88.61 89.70 18.43 o 1 11 1 1098.90 1124.28 25.63 o 3 11 1 24.66 24.15 16.52 o 5 11 1 32.29 2.84 32.10 o 7 11 1 538.99 542.51 77.42 o 9 11 1 15.45 25.85 65.38 o 11 11 1 513.97 610.85 95.68 o 13 11 1 193.31 136.03 80.10 o 15 11 1 61.93 199.75 126.98 o -14 12 1 246.65 57.03 142.57 o -12 12 1 368.10 292.33 82.78 o -10 12 1 1.21 -85.54 85.54 o -8 12 1 1.48 -17.76 43.22 o -6 12 1 37.31 91.47 34.01 o -4 12 1 2095.29 2079.29 41.71 o -2 12 1 1251.69 1269.40 43.84 o 0 12 1 5.14 -15.90 47.72 o 2 12 1 770.46 788.30 33.39 o 4 12 1 31.40 45.13 17.56 o 6 12 1 501.75 554.10 45.59 o 8 12 1 644.87 579.48 65.22 o 10 12 1 73.27 98.94 80.55 o 12 12 1 412.58 438.94 78.42 o 14 12 1 213.94 99.57 118.26 o -13 13 1 729.51 784.79 168.30 o -11 13 1 83.61 132.91 81.45 o -9 13 1 377.15 229.07 89.16 o -7 13 1 14.34 39.63 98.31 o -5 13 1 225.17 188.41 27.04 o -3 13 1 1254.12 1054.14 33.58 o -1 13 1 57.86 -5.42 27.85 o 1 13 1 474.50 481.35 35.07 o 3 13 1 935.09 883.66 33.47 o 5 13 1 62.56 133.22 84.14 o 7 13 1 691.02 704.72 59.15 o 9 13 1 128.82 130.73 128.23 o 11 13 1 4.74 194.45 118.72 o 13 13 1 658.29 680.52 147.42 o -12 14 1 309.35 323.01 141.17 o -8 14 1 50.22 79.32 117.71 o -6 14 1 175.58 224.70 80.77 o -4 14 1 1188.75 1187.77 44.17 o -2 14 1 401.73 420.83 41.10 o 0 14 1 915.15 934.76 80.81 o 2 14 1 232.51 238.37 32.73 o 4 14 1 5.70 -7.67 31.27 o 6 14 1 47.58 100.03 62.48 o 8 14 1 387.35 541.49 74.27 o 10 14 1 90.17 -10.44 96.13 o 12 14 1 344.11 446.27 132.45 o -11 15 1 397.13 331.12 140.01 o -9 15 1 38.70 12.39 104.08 o -7 15 1 287.58 165.01 115.15 o -5 15 1 73.05 -19.93 88.89 o -3 15 1 7.35 79.16 46.39 o -1 15 1 1518.28 1562.36 61.52 o 1 15 1 629.62 679.02 58.27 o 3 15 1 28.54 94.29 71.64 o 5 15 1 418.91 340.15 87.35 o 7 15 1 56.25 178.15 60.67 o 9 15 1 781.15 880.33 164.72 o 11 15 1 1157.60 1419.81 169.26 o -8 16 1 339.07 441.93 180.13 o -6 16 1 426.56 558.26 105.96 o -4 16 1 147.73 152.89 125.27 o -2 16 1 72.48 85.76 56.32 o 0 16 1 1007.48 989.26 64.02 o 2 16 1 745.85 778.23 81.22 o 4 16 1 6.39 -10.96 126.44 o 6 16 1 74.54 117.17 91.59 o 8 16 1 1.62 162.97 183.70 o 10 16 1 147.42 -24.31 167.50 o -7 17 1 193.32 213.28 116.92 o -5 17 1 2.68 -7.29 104.68 o -3 17 1 57.49 199.64 93.62 o -1 17 1 666.05 747.81 109.67 o 1 17 1 132.29 81.05 67.12 o 3 17 1 683.18 772.67 233.60 o 5 17 1 342.22 552.93 108.51 o 7 17 1 58.45 -185.57 204.27 o -6 18 1 24.34 146.00 113.15 o -4 18 1 1153.25 1084.25 113.98 o -2 18 1 1183.86 1167.25 128.38 o 0 18 1 81.95 42.74 156.35 o 2 18 1 4.63 156.48 158.69 o 4 18 1 5.28 -97.14 128.06 o 6 18 1 17.02 184.77 268.77 o -1 19 1 183.18 76.46 140.26 o 1 19 1 79.29 323.81 127.22 o -18 0 2 4806.67 4868.57 233.22 o -16 0 2 49.17 66.09 55.19 o -14 0 2 6399.23 6232.04 136.56 o -12 0 2 9700.91 9924.76 109.74 o -10 0 2 17397.85 18191.05 240.93 o -8 0 2 124.16 109.86 19.17 o -6 0 2 90483.22 92742.67 1335.37 o -4 0 2 11481.07 10279.78 159.15 o -2 0 2 16818.80 21014.76 570.77 o 2 0 2 17075.03 21594.93 155.18 o 4 0 2 160.06 300.79 8.16 o 6 0 2 8620.43 8671.55 79.24 o 8 0 2 3803.99 4470.21 51.50 o 10 0 2 17277.49 17831.12 158.18 o 12 0 2 3586.53 3533.52 60.65 o 14 0 2 5737.67 5950.42 130.21 o 16 0 2 171.90 119.73 71.15 o 18 0 2 4280.82 4532.56 219.93 o -17 1 2 580.99 617.22 75.21 o -15 1 2 1162.49 1130.54 49.90 o -13 1 2 69.82 21.41 23.47 o -11 1 2 1359.77 1275.52 22.85 o -9 1 2 998.89 873.44 21.26 o -7 1 2 1171.11 956.02 17.57 o -5 1 2 10564.38 11566.57 83.96 o -3 1 2 1975.99 1154.65 13.37 o 3 1 2 4283.62 3212.21 22.97 o 5 1 2 34.93 96.29 11.89 o 7 1 2 694.24 558.29 11.54 o 9 1 2 4333.36 4312.40 35.37 o 11 1 2 3099.66 2968.37 33.61 o 13 1 2 489.18 506.83 27.33 o 15 1 2 191.01 207.97 48.89 o 17 1 2 242.58 280.43 45.61 o -18 2 2 279.09 99.76 87.36 o -16 2 2 3903.08 4044.18 71.62 o -14 2 2 17.37 -12.36 30.32 o -12 2 2 10715.92 10699.17 86.97 o -10 2 2 4788.87 4913.00 46.10 o -8 2 2 32648.91 33453.13 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