#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:15:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180839 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/70/2017093.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017093_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Kubiak, Maria' _publ_section_title ; Products of the interaction of (1-diaminomethylene)thiourea with hydrofluoric acid ; _journal_coeditor_code GD3281 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o191 _journal_page_last o194 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.780 _cell_angle_beta 93.870 _cell_angle_gamma 104.500 _cell_length_a 8.1990 _cell_length_b 12.2030 _cell_length_c 14.1580 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.7107 _cod_data_source_file gd3281Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mas9dc in P1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 362.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 109.33 90.44 10.67 o 3 0 0 122.94 125.06 9.01 o 4 0 0 4172.34 4212.11 20.46 o 5 0 0 948.32 975.20 20.95 o 6 0 0 54.56 70.25 10.80 o 7 0 0 661.74 682.24 49.70 o 8 0 0 293.38 305.11 17.75 o 9 0 0 15.62 24.73 19.66 o 10 0 0 0.05 10.76 24.53 o 11 0 0 39.39 77.06 43.14 o -11 1 0 56.54 16.59 30.95 o -10 1 0 210.50 247.94 25.66 o -9 1 0 58.15 54.57 17.04 o -8 1 0 1536.20 1550.20 27.14 o -7 1 0 529.78 504.36 15.55 o -6 1 0 62.88 86.42 20.61 o -5 1 0 6761.90 6746.21 65.29 o -4 1 0 3436.50 3572.01 46.25 o -3 1 0 13.89 18.09 5.84 o -2 1 0 2527.01 2338.01 20.39 o 1 1 0 310.70 281.81 8.11 o 2 1 0 1807.90 1743.01 32.32 o 3 1 0 1051.14 1091.92 22.36 o 4 1 0 196.49 180.46 16.99 o 5 1 0 783.44 758.53 23.03 o 6 1 0 128.08 111.11 11.56 o 7 1 0 10.66 26.60 10.54 o 8 1 0 211.59 207.86 21.57 o 9 1 0 518.85 473.16 43.44 o 10 1 0 279.88 343.19 50.89 o -10 2 0 4.49 36.82 19.33 o -9 2 0 77.14 92.00 15.30 o -8 2 0 356.45 361.90 19.89 o -7 2 0 56.24 65.62 13.85 o -6 2 0 57.80 67.44 11.42 o -5 2 0 1757.44 1732.26 16.37 o -4 2 0 137.33 159.11 11.65 o -3 2 0 811.14 801.29 19.86 o -2 2 0 2562.48 2738.07 56.13 o -1 2 0 199.92 188.81 7.24 o 0 2 0 3046.07 2759.33 26.75 o 1 2 0 2.09 13.82 9.75 o 2 2 0 200.74 228.59 14.92 o 3 2 0 5.29 36.74 15.47 o 4 2 0 3575.06 3855.08 51.27 o 5 2 0 121.84 108.52 23.05 o 6 2 0 1045.41 1065.54 18.86 o 7 2 0 139.68 130.54 14.84 o 8 2 0 684.71 663.15 28.89 o 9 2 0 2.07 25.59 22.41 o 10 2 0 46.09 76.25 44.29 o -10 3 0 659.21 665.26 35.85 o -9 3 0 416.38 412.63 21.38 o -8 3 0 87.14 99.33 23.78 o -7 3 0 226.53 240.09 16.05 o -6 3 0 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1471.66 27.15 o -4 8 0 1287.45 1408.66 27.74 o -3 8 0 614.32 656.84 15.34 o -2 8 0 531.51 516.39 10.98 o -1 8 0 567.24 588.30 11.80 o 0 8 0 1635.04 1721.39 17.79 o 1 8 0 773.54 824.69 14.58 o 2 8 0 57.30 59.99 15.45 o 3 8 0 104.02 85.23 16.69 o 4 8 0 378.28 370.44 29.08 o 5 8 0 1049.46 1045.22 28.95 o 6 8 0 219.24 204.77 29.53 o 7 8 0 226.23 209.54 34.34 o 8 8 0 579.99 551.26 54.05 o -11 9 0 0.18 28.90 41.75 o -10 9 0 80.11 81.82 26.01 o -9 9 0 26.26 36.19 18.40 o -8 9 0 187.76 182.76 39.21 o -7 9 0 258.33 227.13 23.25 o -6 9 0 98.57 101.47 19.49 o -5 9 0 811.60 879.28 25.61 o -4 9 0 732.99 679.91 38.94 o -3 9 0 14.71 17.51 12.52 o -2 9 0 778.31 748.27 23.38 o -1 9 0 1246.33 1227.23 14.16 o 0 9 0 804.38 750.22 16.47 o 1 9 0 799.21 832.09 19.83 o 2 9 0 591.82 617.28 23.06 o 3 9 0 1437.48 1456.00 30.97 o 4 9 0 92.13 79.53 18.03 o 5 9 0 126.44 141.85 26.44 o 6 9 0 12.17 35.79 25.32 o 7 9 0 27.30 43.09 33.09 o -10 10 0 3.32 0.00 31.71 o -9 10 0 375.73 332.40 27.18 o -8 10 0 158.91 203.11 35.61 o -7 10 0 1.05 33.40 18.60 o -6 10 0 55.41 31.83 15.23 o -5 10 0 513.07 508.49 20.79 o -4 10 0 59.47 61.66 19.53 o -3 10 0 1.96 24.62 9.44 o -2 10 0 249.71 285.23 12.00 o -1 10 0 452.15 437.94 11.93 o 0 10 0 116.33 124.41 9.66 o 1 10 0 29.61 23.67 11.32 o 2 10 0 340.38 328.78 21.07 o 3 10 0 56.83 64.51 17.05 o 4 10 0 1101.72 1123.73 74.28 o 5 10 0 52.28 38.39 27.38 o 6 10 0 208.64 185.23 45.53 o 7 10 0 1.19 53.19 32.52 o -10 11 0 5.68 11.72 32.92 o -9 11 0 39.08 80.71 30.28 o -8 11 0 29.35 59.87 26.19 o -7 11 0 60.89 79.56 22.52 o -6 11 0 822.75 812.77 29.15 o -5 11 0 137.44 101.81 17.85 o -4 11 0 377.27 359.88 23.47 o -3 11 0 791.50 809.05 22.57 o -2 11 0 1940.72 1969.29 22.52 o -1 11 0 823.36 813.94 15.28 o 0 11 0 1030.65 980.41 28.11 o 1 11 0 1212.39 1206.78 23.56 o 2 11 0 1219.32 1245.07 49.65 o 3 11 0 128.28 127.97 26.56 o 4 11 0 47.48 19.71 24.64 o 5 11 0 71.48 91.93 29.05 o 6 11 0 509.97 607.15 59.06 o -9 12 0 2.21 10.34 33.08 o -8 12 0 0.60 0.00 23.52 o -7 12 0 95.73 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37.53 13.70 o 5 -8 2 378.92 407.66 20.83 o 6 -8 2 28.00 50.88 16.38 o 7 -8 2 1538.11 1594.02 37.21 o 8 -8 2 15.76 39.84 17.64 o 9 -8 2 950.15 929.08 33.03 o 10 -8 2 7.85 47.91 21.91 o 11 -8 2 514.14 459.70 60.73 o -8 -7 2 58.61 45.18 25.01 o -7 -7 2 346.07 345.54 35.70 o -6 -7 2 137.61 111.83 26.24 o -5 -7 2 1229.25 1227.79 47.42 o -4 -7 2 150.45 153.83 16.91 o -3 -7 2 2847.46 2861.22 46.72 o -2 -7 2 22.55 20.61 11.61 o -1 -7 2 1608.06 1525.08 19.31 o 0 -7 2 2372.40 2292.88 43.59 o 1 -7 2 565.48 543.76 13.39 o 2 -7 2 3683.98 3463.59 66.32 o 3 -7 2 5582.35 5839.59 36.89 o 4 -7 2 28.20 3.27 11.07 o 5 -7 2 1410.32 1442.04 58.32 o 6 -7 2 1054.67 1066.18 23.71 o 7 -7 2 109.01 134.64 18.48 o 8 -7 2 95.15 101.19 18.45 o 9 -7 2 4.48 25.19 20.79 o 10 -7 2 9.07 37.51 27.75 o 11 -7 2 23.74 76.36 38.36 o -9 -6 2 102.39 50.35 33.09 o -8 -6 2 326.65 353.83 37.98 o -7 -6 2 151.82 159.52 25.40 o -6 -6 2 440.00 440.05 21.68 o -5 -6 2 143.77 163.64 17.54 o -4 -6 2 0.66 20.89 14.80 o -3 -6 2 1337.63 1365.17 41.92 o -2 -6 2 2116.11 2211.32 36.49 o -1 -6 2 9.79 33.10 8.27 o 0 -6 2 33.25 42.64 8.51 o 1 -6 2 289.63 318.88 14.70 o 2 -6 2 4782.69 4836.08 33.63 o 3 -6 2 2.36 10.04 8.22 o 4 -6 2 3617.81 3628.22 52.22 o 5 -6 2 327.04 344.86 19.60 o 6 -6 2 5.09 25.07 14.97 o 7 -6 2 137.85 122.66 16.02 o 8 -6 2 319.43 312.89 23.90 o 9 -6 2 656.01 626.31 37.45 o 10 -6 2 73.93 51.81 24.56 o 11 -6 2 171.83 172.29 33.59 o -9 -5 2 232.44 299.51 49.63 o -8 -5 2 140.56 160.59 27.82 o -7 -5 2 440.85 394.72 22.01 o -6 -5 2 168.55 208.36 22.12 o -5 -5 2 1901.99 1928.50 31.66 o -4 -5 2 617.28 595.64 29.66 o -3 -5 2 1965.85 1908.35 35.50 o -2 -5 2 0.64 15.18 8.90 o -1 -5 2 335.39 350.94 12.54 o 0 -5 2 4213.99 4103.73 27.43 o 1 -5 2 1064.53 1097.55 13.74 o 2 -5 2 762.96 843.38 13.74 o 3 -5 2 1504.65 1544.09 56.84 o 4 -5 2 33.11 45.76 17.50 o 5 -5 2 8.84 21.34 10.96 o 6 -5 2 400.41 395.24 22.64 o 7 -5 2 13.92 47.73 13.13 o 8 -5 2 643.05 664.49 35.44 o 9 -5 2 136.98 122.57 26.44 o 10 -5 2 0.12 22.24 21.09 o -10 -4 2 7.09 55.83 41.12 o -9 -4 2 1.04 17.60 27.17 o -8 -4 2 45.74 43.78 16.56 o -7 -4 2 449.54 453.72 18.33 o -6 -4 2 444.36 450.01 18.15 o -5 -4 2 25.68 27.32 14.67 o -4 -4 2 235.18 251.55 14.12 o -3 -4 2 31.22 56.79 9.22 o -2 -4 2 557.85 563.10 15.37 o -1 -4 2 175.90 191.84 11.48 o 0 -4 2 54.42 72.75 7.28 o 1 -4 2 732.21 704.10 18.52 o 2 -4 2 2837.44 2824.32 27.51 o 3 -4 2 244.57 232.51 18.65 o 4 -4 2 4788.79 5049.17 74.67 o 5 -4 2 3006.91 2987.15 44.52 o 6 -4 2 37.45 43.47 13.94 o 7 -4 2 120.24 119.43 15.46 o 8 -4 2 11.41 20.57 21.23 o 9 -4 2 452.67 430.73 27.78 o 10 -4 2 160.11 141.80 35.17 o -10 -3 2 46.45 50.95 33.28 o -9 -3 2 166.99 150.04 26.59 o -8 -3 2 2.06 22.94 14.61 o -7 -3 2 90.39 78.75 14.64 o -6 -3 2 231.28 228.14 17.54 o -5 -3 2 628.53 594.24 18.78 o -4 -3 2 927.97 1005.20 32.90 o -3 -3 2 850.69 831.39 22.87 o -2 -3 2 76.02 92.99 22.69 o -1 -3 2 1992.86 1981.86 15.32 o 0 -3 2 5205.98 5060.90 55.94 o 1 -3 2 96.48 85.84 9.89 o 2 -3 2 825.44 782.82 16.62 o 3 -3 2 9.44 22.39 11.02 o 4 -3 2 4.96 15.88 10.85 o 5 -3 2 93.75 113.28 16.82 o 6 -3 2 439.10 425.46 12.74 o 7 -3 2 189.81 176.24 12.49 o 8 -3 2 667.99 662.80 34.55 o 9 -3 2 76.61 117.75 34.59 o 10 -3 2 65.76 112.73 48.57 o -10 -2 2 319.44 287.28 39.59 o -9 -2 2 0.11 31.40 22.21 o -8 -2 2 0.10 11.36 14.29 o -7 -2 2 16.87 34.90 11.69 o -6 -2 2 3.41 38.31 14.49 o -5 -2 2 79.17 100.47 14.62 o -4 -2 2 45.53 49.82 8.85 o -3 -2 2 2243.40 2454.65 18.39 o -2 -2 2 32.99 36.43 9.44 o -1 -2 2 133.23 126.35 11.31 o 0 -2 2 1517.61 2005.79 67.95 o 1 -2 2 257.88 248.67 30.97 o 2 -2 2 3161.06 3216.24 19.83 o 3 -2 2 76.89 94.97 12.51 o 4 -2 2 544.56 534.43 16.05 o 5 -2 2 17.48 30.35 8.32 o 6 -2 2 1428.15 1343.32 35.06 o 7 -2 2 684.83 670.04 20.28 o 8 -2 2 285.06 277.39 28.86 o 9 -2 2 0.54 89.99 31.74 o 10 -2 2 60.13 60.27 31.09 o -10 -1 2 0.26 0.00 22.72 o -9 -1 2 5.15 4.14 16.07 o -8 -1 2 557.09 520.62 25.36 o -7 -1 2 291.54 285.84 15.77 o -6 -1 2 67.43 103.40 18.10 o -5 -1 2 5330.24 5331.06 48.07 o -4 -1 2 7488.03 7667.19 35.13 o -3 -1 2 11.14 24.08 10.40 o -2 -1 2 1.55 24.56 8.76 o -1 -1 2 2486.11 2184.96 22.64 o 0 -1 2 4249.17 3676.20 25.59 o 1 -1 2 2.53 15.49 7.70 o 2 -1 2 331.33 318.73 14.56 o 3 -1 2 612.39 605.35 9.94 o 4 -1 2 914.22 942.43 13.47 o 6 -1 2 1835.91 1816.97 28.86 o 7 -1 2 2084.44 2085.56 25.34 o 8 -1 2 146.56 148.66 32.31 o 9 -1 2 3.01 37.33 19.68 o 10 -1 2 179.32 127.96 33.45 o -11 0 2 8.96 9.07 42.35 o -10 0 2 560.73 606.88 26.62 o -9 0 2 20.38 48.52 16.97 o -8 0 2 578.22 594.34 60.27 o -7 0 2 149.71 174.52 15.99 o -6 0 2 1264.34 1377.36 36.74 o -5 0 2 1006.21 974.29 12.45 o -4 0 2 2474.83 2552.26 21.62 o -3 0 2 1020.84 1187.34 14.99 o -2 0 2 31626.73 34868.89 216.00 o -1 0 2 80.51 73.70 7.92 o 0 0 2 139.45 120.23 11.74 o 1 0 2 6.01 3.43 8.09 o 3 0 2 1568.64 1544.09 35.21 o 4 0 2 162.44 164.98 13.79 o 5 0 2 17.31 48.29 19.73 o 6 0 2 58.72 76.87 19.44 o 7 0 2 0.05 20.43 17.75 o 8 0 2 151.09 181.62 22.55 o 9 0 2 147.26 163.40 26.93 o 10 0 2 90.14 104.27 31.68 o -11 1 2 0.12 6.30 23.29 o -10 1 2 883.92 915.74 27.82 o -9 1 2 1.17 36.78 15.70 o -8 1 2 4.12 22.71 13.81 o -7 1 2 571.55 593.83 56.19 o -6 1 2 812.86 853.17 14.08 o -5 1 2 203.17 205.63 9.09 o -4 1 2 685.97 699.69 17.12 o -3 1 2 74.34 80.23 16.22 o -2 1 2 73.82 87.50 14.45 o -1 1 2 0.00 6.46 8.17 o 0 1 2 4.89 0.22 6.42 o 1 1 2 15.39 8.94 10.04 o 2 1 2 7456.93 7774.71 64.00 o 3 1 2 13597.36 14649.30 71.56 o 4 1 2 5.09 23.83 17.51 o 5 1 2 9.31 39.90 10.95 o 6 1 2 599.37 585.48 20.09 o 7 1 2 714.17 708.35 45.46 o 8 1 2 149.58 138.60 21.03 o 9 1 2 264.73 261.33 27.36 o 10 1 2 123.98 98.33 38.35 o -11 2 2 26.21 22.17 25.04 o -10 2 2 79.97 88.99 19.59 o -9 2 2 159.37 171.42 17.41 o -8 2 2 153.10 181.59 19.36 o -7 2 2 7.36 27.05 11.64 o -6 2 2 406.63 433.36 14.75 o -5 2 2 637.14 551.62 10.19 o -4 2 2 541.88 502.84 18.40 o -3 2 2 2194.83 2187.75 47.73 o -2 2 2 131488.05 136820.89 524.04 o -1 2 2 636.27 570.01 19.67 o 0 2 2 147.46 135.89 8.52 o 1 2 2 994.31 931.43 20.46 o 2 2 2 5847.23 6119.19 129.74 o 3 2 2 13.21 45.66 37.90 o 4 2 2 53.07 60.07 12.72 o 5 2 2 235.17 269.58 14.93 o 6 2 2 151.86 145.45 14.47 o 7 2 2 0.09 11.60 16.65 o 8 2 2 80.50 76.15 18.90 o 9 2 2 30.59 58.98 26.56 o 10 2 2 204.14 195.56 41.43 o -11 3 2 47.10 46.30 26.11 o -10 3 2 203.75 234.51 20.93 o -9 3 2 279.91 270.49 18.70 o -8 3 2 222.69 229.22 14.50 o -7 3 2 714.56 746.87 17.07 o -6 3 2 1261.06 1300.99 23.95 o -5 3 2 213.85 202.45 17.30 o -4 3 2 1477.66 1477.97 16.73 o -3 3 2 113.37 138.38 15.93 o -2 3 2 36.08 50.37 10.01 o -1 3 2 2056.94 1877.96 15.89 o 0 3 2 275.54 259.33 9.53 o 1 3 2 1011.08 1054.42 30.77 o 2 3 2 3963.34 3818.70 34.90 o 3 3 2 565.39 602.37 49.99 o 4 3 2 37.93 53.83 13.15 o 5 3 2 4.48 46.83 15.16 o 6 3 2 49.60 63.30 14.55 o 7 3 2 2169.64 2313.03 34.09 o 8 3 2 4.94 34.20 19.04 o 9 3 2 126.63 129.74 26.53 o 10 3 2 136.07 198.35 39.67 o -11 4 2 2.43 0.00 30.15 o -10 4 2 83.83 81.88 16.77 o -9 4 2 0.41 24.32 14.42 o -8 4 2 3.07 28.05 16.30 o -7 4 2 1726.40 1746.09 21.82 o -6 4 2 460.33 450.14 15.77 o -5 4 2 67.13 84.17 12.71 o -4 4 2 512.87 543.70 25.37 o -3 4 2 107.45 79.38 15.08 o -2 4 2 19.60 44.75 10.29 o -1 4 2 834.08 999.92 12.55 o 0 4 2 1187.95 1255.10 30.12 o 1 4 2 1.25 21.62 8.20 o 2 4 2 2574.08 2866.73 26.43 o 3 4 2 41.15 41.35 11.37 o 4 4 2 625.88 664.00 19.40 o 5 4 2 869.84 952.26 44.78 o 6 4 2 480.69 461.34 19.72 o 7 4 2 10.29 19.75 15.89 o 8 4 2 53.07 40.05 19.76 o 9 4 2 412.48 382.67 42.20 o -11 5 2 18.67 16.92 39.07 o -10 5 2 2.14 37.28 20.44 o -9 5 2 4.68 6.11 15.29 o -8 5 2 78.26 73.08 15.52 o -7 5 2 43.50 39.57 12.94 o -6 5 2 162.19 177.81 20.94 o -5 5 2 58.63 54.84 12.54 o -4 5 2 4310.24 4281.42 27.64 o -3 5 2 4075.38 3937.04 71.49 o -2 5 2 249.34 207.46 11.03 o -1 5 2 2397.74 2372.70 20.85 o 0 5 2 5942.57 6128.52 26.42 o 1 5 2 815.33 787.21 16.05 o 2 5 2 2308.26 2246.83 25.01 o 3 5 2 95.41 79.30 13.52 o 4 5 2 60.32 71.67 17.92 o 5 5 2 3600.51 3593.29 42.92 o 6 5 2 8.77 32.27 17.05 o 7 5 2 136.01 145.84 21.90 o 8 5 2 18.03 24.03 21.28 o 9 5 2 190.89 201.91 55.15 o -11 6 2 0.36 45.62 39.84 o -10 6 2 11.46 19.81 22.29 o -9 6 2 1285.62 1361.11 35.49 o -8 6 2 83.24 70.62 13.49 o -7 6 2 72.25 63.25 11.67 o -6 6 2 87.17 68.03 16.94 o -5 6 2 1219.04 1306.86 20.33 o -4 6 2 1437.22 1425.03 20.26 o -3 6 2 7185.76 7378.37 30.79 o -2 6 2 199.62 194.19 20.19 o -1 6 2 285.05 294.14 11.22 o 0 6 2 27.27 27.48 8.69 o 1 6 2 612.60 636.47 12.74 o 2 6 2 13.96 23.26 11.59 o 3 6 2 0.20 35.80 16.52 o 4 6 2 752.30 690.34 22.00 o 5 6 2 37.95 66.74 19.07 o 6 6 2 83.98 86.27 20.69 o 7 6 2 98.25 87.40 22.91 o 8 6 2 384.80 337.45 26.45 o -11 7 2 2.24 11.24 32.87 o -10 7 2 81.11 90.49 23.30 o -9 7 2 1.19 9.23 24.21 o -8 7 2 136.05 142.68 15.16 o -7 7 2 44.80 56.41 15.51 o -6 7 2 176.18 172.35 30.02 o -5 7 2 0.26 13.58 10.81 o -4 7 2 557.25 514.51 15.51 o -3 7 2 0.15 28.51 9.04 o -2 7 2 34.87 29.37 8.46 o -1 7 2 16.74 23.26 6.80 o 0 7 2 2181.75 2171.40 24.30 o 1 7 2 218.02 215.29 11.44 o 2 7 2 187.00 193.14 15.57 o 3 7 2 3458.36 3465.41 39.22 o 4 7 2 214.98 200.75 20.56 o 5 7 2 10.92 7.49 15.59 o 6 7 2 0.58 15.78 20.16 o 7 7 2 11.63 32.69 23.25 o 8 7 2 235.35 159.12 31.00 o -11 8 2 110.96 74.00 38.19 o -10 8 2 14.09 39.09 29.16 o -9 8 2 18.84 24.61 18.93 o -8 8 2 43.15 27.34 18.32 o -7 8 2 34.21 56.69 19.25 o -6 8 2 5.32 16.36 13.36 o -5 8 2 1741.58 1794.41 24.12 o -4 8 2 193.36 193.69 14.50 o -3 8 2 138.96 146.95 11.24 o -2 8 2 0.13 10.08 7.16 o -1 8 2 12.41 19.26 7.25 o 0 8 2 504.51 494.75 11.69 o 1 8 2 0.11 14.89 9.68 o 2 8 2 503.91 538.99 21.97 o 3 8 2 214.99 248.85 21.08 o 4 8 2 27.16 42.42 17.14 o 5 8 2 32.21 26.08 17.44 o 6 8 2 332.95 388.24 31.13 o 7 8 2 461.38 439.42 35.81 o -10 9 2 7.06 3.87 30.82 o -9 9 2 10.86 47.80 23.72 o -8 9 2 18.18 42.01 29.59 o -7 9 2 211.59 218.61 25.54 o -6 9 2 32.88 34.56 19.34 o -5 9 2 44.37 42.27 12.99 o -4 9 2 199.20 194.64 14.18 o -3 9 2 480.76 454.03 23.10 o -2 9 2 938.96 856.54 13.83 o -1 9 2 321.88 331.48 11.04 o 0 9 2 934.64 925.12 15.93 o 1 9 2 2883.19 2855.45 26.49 o 2 9 2 51.90 53.90 14.20 o 3 9 2 107.07 79.75 15.98 o 4 9 2 2.69 16.18 18.56 o 5 9 2 53.33 76.34 19.76 o 6 9 2 41.53 23.89 22.29 o 7 9 2 99.83 63.13 45.62 o -10 10 2 27.19 64.59 44.92 o -9 10 2 1.15 53.23 28.42 o -8 10 2 0.43 8.13 22.67 o -7 10 2 1483.71 1521.20 45.18 o -6 10 2 359.63 354.10 29.69 o -5 10 2 7.92 26.21 13.50 o -4 10 2 88.94 93.10 14.37 o -3 10 2 626.43 622.70 17.32 o -2 10 2 733.74 768.27 16.70 o -1 10 2 385.27 381.24 14.57 o 0 10 2 13.91 24.54 10.61 o 1 10 2 88.00 107.70 17.95 o 2 10 2 585.07 582.27 32.32 o 3 10 2 1422.87 1472.18 48.15 o 4 10 2 47.25 52.90 19.61 o 5 10 2 15.26 20.51 21.24 o 6 10 2 617.10 613.43 49.82 o -10 11 2 20.35 43.35 33.79 o -9 11 2 0.18 0.00 30.49 o -8 11 2 279.51 258.50 32.43 o -7 11 2 40.17 29.67 21.57 o -6 11 2 171.81 193.38 25.77 o -5 11 2 73.34 73.75 18.35 o -4 11 2 426.25 413.33 22.67 o -3 11 2 33.09 33.84 11.81 o -2 11 2 1111.38 1137.95 21.82 o -1 11 2 4.43 23.98 10.65 o 0 11 2 604.35 596.98 19.52 o 1 11 2 18.61 41.36 17.37 o 2 11 2 744.06 687.54 26.29 o 3 11 2 66.43 61.89 19.04 o 4 11 2 289.77 278.77 26.44 o 5 11 2 70.74 126.55 35.17 o -9 12 2 133.78 186.69 47.98 o -8 12 2 62.13 65.95 24.72 o -7 12 2 23.75 77.75 29.14 o -6 12 2 60.58 47.97 23.69 o -5 12 2 1.75 22.55 16.54 o -4 12 2 285.97 345.98 24.90 o -3 12 2 115.63 119.19 16.35 o -2 12 2 32.18 45.20 17.54 o -1 12 2 74.09 71.50 15.61 o 0 12 2 348.99 355.76 26.61 o 1 12 2 203.61 215.39 22.19 o 2 12 2 237.31 237.55 24.43 o 3 12 2 16.63 30.92 27.32 o 4 12 2 145.50 158.26 41.42 o 5 12 2 9.79 87.41 50.16 o -9 13 2 0.06 17.78 35.15 o -8 13 2 245.05 231.40 39.27 o -7 13 2 0.28 8.58 25.14 o -6 13 2 31.40 25.20 23.38 o -5 13 2 291.48 351.34 27.94 o -4 13 2 708.89 677.17 23.98 o -3 13 2 152.71 125.32 16.20 o -2 13 2 267.86 236.50 24.58 o -1 13 2 150.42 167.06 18.16 o 0 13 2 129.71 140.62 23.44 o 1 13 2 217.83 185.08 23.80 o 2 13 2 234.14 216.36 29.74 o 3 13 2 93.04 96.33 36.24 o 4 13 2 455.92 544.15 64.41 o -8 14 2 28.76 35.65 38.91 o -7 14 2 91.56 187.76 49.39 o -6 14 2 7.94 21.45 30.09 o -5 14 2 130.24 152.64 33.60 o -4 14 2 80.29 72.51 25.91 o -3 14 2 146.94 132.70 22.13 o -2 14 2 60.33 47.25 25.84 o -1 14 2 241.66 231.98 32.68 o 0 14 2 13.28 18.90 25.38 o 1 14 2 370.39 413.98 34.28 o 2 14 2 7.35 6.95 38.06 o 3 14 2 21.15 36.34 32.33 o -7 15 2 2.60 0.00 33.99 o -6 15 2 163.21 146.91 39.27 o -5 15 2 0.08 35.14 33.50 o -4 15 2 298.84 307.88 35.06 o -3 15 2 22.97 43.43 24.96 o -2 15 2 130.02 160.93 40.04 o 0 15 2 9.72 29.75 28.78 o 1 15 2 0.21 13.34 37.70 o -3 16 2 180.41 199.83 34.14 o 3 -17 3 30.92 62.02 40.50 o 4 -17 3 43.27 39.99 33.45 o 1 -16 3 0.86 14.77 49.77 o 2 -16 3 85.34 111.69 27.73 o 3 -16 3 41.41 62.13 30.32 o 4 -16 3 6.39 34.19 32.00 o 5 -16 3 485.00 487.03 45.84 o 6 -16 3 1.31 48.94 40.55 o -1 -15 3 10.55 19.38 35.06 o 0 -15 3 44.77 48.07 39.81 o 1 -15 3 177.01 180.32 58.04 o 2 -15 3 75.48 90.63 23.55 o 3 -15 3 301.83 271.94 24.02 o 4 -15 3 532.72 634.12 35.32 o 5 -15 3 13.69 22.51 23.68 o 6 -15 3 0.02 18.81 29.79 o 7 -15 3 165.67 237.04 50.16 o -4 -14 3 203.13 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