#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/70/2017094.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017094_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Kubiak, Maria' _publ_section_title ; Products of the interaction of (1-diaminomethylene)thiourea with hydrofluoric acid ; _journal_coeditor_code GD3281 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o191 _journal_page_last o194 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.650 _cell_angle_beta 83.440 _cell_angle_gamma 66.150 _cell_length_a 6.5370 _cell_length_b 7.3900 _cell_length_c 7.8840 _exptl_crystal_F_000 194.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file gd3281IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' hatfdc in P1 New: P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 85.22 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 54.30 44.56 0.81 o 2 0 0 124.40 127.64 1.25 o 3 0 0 319.29 317.53 2.39 o 4 0 0 4.45 4.68 1.11 o 5 0 0 571.06 576.14 3.00 o 6 0 0 241.19 240.98 4.74 o 7 0 0 3.63 4.21 3.23 o -7 1 0 166.90 175.13 3.07 o -6 1 0 185.82 181.65 2.71 o -5 1 0 57.38 55.68 3.85 o -4 1 0 583.68 591.88 6.41 o -3 1 0 54.94 46.40 1.59 o -2 1 0 277.46 311.74 5.85 o -1 1 0 1354.63 1441.64 24.89 o 1 1 0 441.88 447.66 2.56 o 2 1 0 2390.69 2521.22 41.32 o 3 1 0 16.01 17.73 0.68 o 4 1 0 244.04 254.43 2.72 o 5 1 0 251.06 249.51 2.12 o 6 1 0 195.64 194.15 4.64 o 7 1 0 10.83 10.78 2.70 o 8 1 0 259.40 253.11 7.64 o -7 2 0 3.97 2.97 2.80 o -6 2 0 23.48 23.05 2.21 o -5 2 0 289.71 293.81 4.36 o -4 2 0 297.24 299.18 2.84 o -3 2 0 581.61 582.51 3.49 o -2 2 0 197.13 185.90 2.88 o -1 2 0 178.70 193.77 1.48 o 0 2 0 393.46 365.65 4.31 o 1 2 0 6935.86 7070.71 239.22 o 2 2 0 7262.27 7700.38 118.70 o 3 2 0 0.49 1.25 0.62 o 4 2 0 818.07 834.02 5.97 o 5 2 0 18.53 18.93 1.00 o 6 2 0 5.32 5.21 1.50 o 7 2 0 565.59 594.83 5.33 o 8 2 0 5.65 5.47 3.21 o -6 3 0 9.09 9.40 2.32 o -5 3 0 101.26 98.21 2.65 o -4 3 0 340.10 346.87 3.43 o -3 3 0 1496.79 1521.30 6.98 o -2 3 0 33.98 34.24 1.37 o -1 3 0 182.35 164.17 1.65 o 0 3 0 1160.54 1184.27 6.04 o 1 3 0 51.66 56.87 1.55 o 2 3 0 36.26 47.02 3.27 o 3 3 0 30.34 27.27 1.26 o 4 3 0 502.82 523.35 5.27 o 5 3 0 112.40 114.04 1.86 o 6 3 0 57.97 54.37 1.45 o 7 3 0 5.81 6.03 1.76 o 8 3 0 166.63 170.49 3.42 o -6 4 0 18.30 15.89 3.70 o -5 4 0 0.94 1.89 2.12 o -4 4 0 73.06 70.59 3.91 o -3 4 0 84.63 80.69 4.66 o -2 4 0 1534.26 1553.68 15.09 o -1 4 0 331.27 327.73 2.73 o 0 4 0 79.00 80.70 1.08 o 1 4 0 939.51 965.56 6.41 o 2 4 0 256.75 268.97 17.41 o 3 4 0 3367.00 3545.41 11.73 o 4 4 0 516.56 514.49 4.03 o 5 4 0 192.54 181.95 2.04 o 6 4 0 90.42 88.68 1.68 o 7 4 0 3.02 5.12 1.60 o 8 4 0 265.44 278.13 6.74 o 9 4 0 20.64 30.38 4.47 o -5 5 0 0.02 0.00 3.65 o -4 5 0 17.80 11.64 2.96 o -3 5 0 314.58 319.09 3.96 o -2 5 0 125.31 119.52 2.73 o -1 5 0 417.78 430.76 3.91 o 0 5 0 587.41 602.99 4.14 o 1 5 0 525.99 496.95 24.31 o 2 5 0 4.24 6.47 1.92 o 3 5 0 82.84 80.86 3.57 o 4 5 0 146.30 137.48 1.68 o 5 5 0 78.90 82.76 2.45 o 6 5 0 216.58 215.91 2.42 o 7 5 0 4.48 6.25 1.68 o 8 5 0 0.01 0.84 1.66 o 9 5 0 70.71 73.16 5.02 o -4 6 0 80.30 83.68 4.04 o -3 6 0 69.60 72.96 5.01 o -2 6 0 23.49 22.18 1.80 o -1 6 0 529.10 569.23 4.86 o 0 6 0 125.12 122.66 7.64 o 1 6 0 58.74 51.44 2.68 o 2 6 0 137.44 131.80 2.95 o 3 6 0 0.22 2.42 1.18 o 4 6 0 157.72 161.66 3.59 o 5 6 0 1534.42 1551.92 7.57 o 6 6 0 51.58 52.38 2.04 o 7 6 0 24.92 22.41 2.15 o 8 6 0 66.76 67.18 4.63 o -3 7 0 51.37 46.99 3.39 o -2 7 0 294.13 311.40 7.07 o -1 7 0 0.07 0.49 1.60 o 0 7 0 174.08 183.70 5.52 o 1 7 0 433.90 465.30 6.44 o 2 7 0 31.69 30.81 3.00 o 3 7 0 154.91 149.33 4.76 o 4 7 0 41.28 44.61 2.22 o 5 7 0 61.20 58.17 1.90 o 6 7 0 0.18 0.43 1.52 o 7 7 0 322.22 346.11 7.51 o 8 7 0 4.83 4.94 2.00 o -2 8 0 47.03 49.17 4.24 o -1 8 0 6.36 8.43 2.24 o 0 8 0 329.10 323.73 5.06 o 1 8 0 111.25 110.72 7.46 o 2 8 0 4.63 8.87 3.37 o 3 8 0 92.17 90.24 3.48 o 4 8 0 21.44 21.48 2.16 o 5 8 0 3.00 1.01 1.40 o 6 8 0 433.14 444.37 5.16 o 7 8 0 65.39 62.69 3.23 o 8 8 0 1.48 2.88 2.42 o 1 9 0 1.66 2.30 3.42 o 2 9 0 476.10 483.05 39.44 o 3 9 0 43.95 38.65 3.57 o 4 9 0 3.72 2.93 1.50 o 5 9 0 112.41 119.83 5.85 o 6 9 0 11.86 8.50 2.30 o 7 9 0 2.97 2.88 2.33 o 4 10 0 114.53 109.53 4.76 o 5 10 0 0.37 1.02 2.27 o -5 -10 1 104.32 122.54 4.00 o -4 -10 1 0.34 0.25 2.97 o -6 -9 1 16.82 17.23 2.65 o -5 -9 1 60.48 57.04 2.56 o -4 -9 1 0.09 0.44 1.67 o -3 -9 1 37.46 31.19 5.00 o -2 -9 1 6.14 6.11 3.64 o 0 -9 1 27.53 27.29 3.24 o -7 -8 1 5.95 4.08 2.48 o -6 -8 1 46.44 43.91 2.65 o -5 -8 1 13.80 10.86 1.61 o -4 -8 1 39.03 39.01 2.58 o -3 -8 1 34.76 28.68 2.22 o -2 -8 1 4.21 3.17 2.72 o -1 -8 1 312.08 309.75 16.95 o 0 -8 1 10.55 10.27 1.94 o 1 -8 1 0.64 2.06 2.09 o 2 -8 1 224.43 236.84 5.83 o -8 -7 1 57.07 59.67 3.33 o -7 -7 1 0.50 0.27 1.95 o -6 -7 1 148.73 140.81 3.12 o -5 -7 1 6.15 5.37 1.36 o -4 -7 1 1.98 2.26 1.39 o -3 -7 1 171.26 163.58 2.57 o -2 -7 1 13.91 10.04 2.30 o -1 -7 1 0.11 2.49 1.63 o 0 -7 1 246.07 266.03 3.73 o 1 -7 1 68.56 68.59 2.77 o 2 -7 1 68.99 71.17 3.57 o 3 -7 1 7.16 7.77 2.93 o -8 -6 1 10.50 8.69 2.13 o -7 -6 1 116.15 119.30 2.58 o -6 -6 1 1.80 2.38 1.49 o -5 -6 1 0.03 1.51 1.31 o -4 -6 1 256.73 253.90 2.98 o -3 -6 1 20.98 18.11 1.39 o -2 -6 1 109.13 98.24 4.53 o -1 -6 1 30.28 24.96 2.34 o 0 -6 1 237.07 237.52 3.24 o 1 -6 1 90.48 87.67 2.58 o 2 -6 1 22.55 20.28 2.30 o 3 -6 1 397.14 402.53 24.26 o 4 -6 1 6.03 6.06 3.05 o -8 -5 1 66.10 66.35 2.38 o -7 -5 1 7.71 10.38 1.81 o -6 -5 1 14.74 13.96 1.50 o -5 -5 1 235.00 233.79 4.35 o -4 -5 1 0.25 1.58 0.92 o -3 -5 1 21.53 19.60 1.43 o -2 -5 1 2.31 3.44 1.72 o -1 -5 1 986.62 1028.33 10.38 o 0 -5 1 92.64 96.20 1.51 o 1 -5 1 140.44 137.83 2.93 o 2 -5 1 14.67 14.10 1.51 o 3 -5 1 0.51 2.28 1.99 o 4 -5 1 1.27 4.53 2.18 o 5 -5 1 82.23 80.18 4.00 o -8 -4 1 10.04 9.24 1.73 o -7 -4 1 4.23 6.10 1.59 o -6 -4 1 1.96 3.04 1.29 o -5 -4 1 62.26 61.73 1.95 o -4 -4 1 6.37 6.46 0.90 o -3 -4 1 428.29 424.15 3.68 o -2 -4 1 10.86 7.44 1.34 o -1 -4 1 118.39 128.83 1.70 o 0 -4 1 1259.56 1280.66 5.57 o 1 -4 1 722.64 748.94 3.62 o 2 -4 1 96.72 87.83 2.98 o 3 -4 1 205.87 204.62 3.08 o 4 -4 1 75.92 80.29 2.88 o 5 -4 1 194.43 185.65 3.67 o 6 -4 1 42.36 41.43 4.40 o -8 -3 1 136.32 131.19 4.80 o -7 -3 1 98.42 106.83 3.89 o -6 -3 1 13.06 13.31 1.30 o -5 -3 1 97.95 94.60 1.65 o -4 -3 1 46.67 45.11 1.05 o -3 -3 1 294.48 309.17 6.18 o -2 -3 1 52.84 51.13 5.01 o -1 -3 1 193.43 183.54 3.69 o 0 -3 1 2919.89 3153.82 28.04 o 1 -3 1 24.33 23.52 0.88 o 2 -3 1 167.59 153.87 2.58 o 3 -3 1 18.61 19.22 1.05 o 4 -3 1 61.27 56.29 2.14 o 5 -3 1 13.03 10.93 2.42 o 6 -3 1 34.85 33.88 2.86 o -8 -2 1 106.82 115.51 5.93 o -7 -2 1 73.38 71.20 3.97 o -6 -2 1 47.26 49.16 2.48 o -5 -2 1 154.48 153.80 2.30 o -4 -2 1 63.81 69.31 1.32 o -3 -2 1 170.52 160.82 3.22 o -2 -2 1 103.45 100.57 2.32 o -1 -2 1 493.59 501.77 10.04 o 0 -2 1 115.53 119.74 4.54 o 1 -2 1 581.86 571.13 6.83 o 2 -2 1 36.43 42.49 1.08 o 3 -2 1 212.49 211.89 3.11 o 4 -2 1 631.42 624.22 3.60 o 5 -2 1 15.57 13.71 1.49 o 6 -2 1 46.42 48.97 4.85 o 7 -2 1 89.56 94.58 4.12 o -7 -1 1 97.94 92.78 3.61 o -6 -1 1 0.05 1.61 2.19 o -5 -1 1 15.82 12.82 1.09 o -4 -1 1 105.78 107.93 1.32 o -3 -1 1 1531.72 1580.58 13.37 o -2 -1 1 346.22 339.98 6.82 o -1 -1 1 2201.78 2321.98 26.02 o 0 -1 1 286.11 336.36 8.05 o 1 -1 1 446.47 445.19 4.53 o 2 -1 1 2281.25 2589.09 5.83 o 3 -1 1 12.60 17.45 0.96 o 4 -1 1 1.40 2.71 0.87 o 5 -1 1 35.44 34.62 1.37 o 6 -1 1 38.47 34.68 1.89 o 7 -1 1 68.93 70.81 4.40 o -7 0 1 4.34 3.81 2.91 o -6 0 1 277.60 268.91 14.14 o -5 0 1 154.15 152.55 3.22 o -4 0 1 150.28 142.46 2.68 o -3 0 1 233.89 247.61 3.41 o -2 0 1 456.58 467.70 2.22 o -1 0 1 1346.04 1507.04 3.70 o 1 0 1 2635.56 2792.32 19.19 o 2 0 1 148.05 130.35 1.85 o 3 0 1 248.69 242.82 2.09 o 4 0 1 405.24 417.01 3.47 o 5 0 1 353.49 347.75 3.06 o 6 0 1 69.11 66.66 1.95 o 7 0 1 0.26 1.32 3.18 o -7 1 1 8.42 7.87 1.93 o -6 1 1 51.83 54.16 2.42 o -5 1 1 67.69 64.87 5.85 o -4 1 1 3.76 5.09 1.81 o -3 1 1 222.78 202.03 6.99 o -2 1 1 911.47 928.94 27.70 o -1 1 1 21.23 18.82 0.63 o 0 1 1 897.37 930.48 14.68 o 1 1 1 121.58 144.11 1.37 o 2 1 1 159.41 140.73 2.79 o 3 1 1 406.11 417.44 3.05 o 4 1 1 835.99 846.69 5.51 o 5 1 1 63.75 65.55 1.63 o 6 1 1 1.00 2.64 1.50 o 7 1 1 9.75 9.02 1.78 o 8 1 1 14.12 10.25 3.29 o -7 2 1 145.36 148.15 4.99 o -6 2 1 0.00 0.48 1.72 o -5 2 1 0.10 1.57 1.49 o -4 2 1 866.86 892.30 4.66 o -3 2 1 23.57 21.59 2.02 o -2 2 1 0.91 1.91 1.06 o -1 2 1 37.72 48.49 0.92 o 0 2 1 182.52 167.90 3.08 o 1 2 1 56.96 69.36 1.30 o 2 2 1 412.72 383.68 1.82 o 3 2 1 33.02 47.72 2.41 o 4 2 1 0.27 1.40 0.86 o 5 2 1 104.65 99.89 1.89 o 6 2 1 860.40 880.68 11.83 o 7 2 1 21.82 20.72 2.92 o 8 2 1 66.15 64.93 2.84 o -6 3 1 12.61 12.90 3.43 o -5 3 1 168.56 182.52 2.98 o -4 3 1 60.34 56.78 2.77 o -3 3 1 563.23 574.08 4.86 o -2 3 1 716.98 704.45 3.36 o -1 3 1 136.30 147.21 2.22 o 0 3 1 452.49 441.45 2.16 o 1 3 1 50.35 56.13 1.32 o 2 3 1 176.51 203.63 2.39 o 3 3 1 109.22 108.23 1.75 o 4 3 1 0.93 1.73 0.75 o 5 3 1 955.71 983.60 9.36 o 6 3 1 11.86 18.10 3.36 o 7 3 1 25.35 24.36 2.22 o 8 3 1 107.51 107.44 3.12 o 9 3 1 30.77 26.21 4.30 o -6 4 1 51.50 47.21 4.48 o -5 4 1 11.34 8.30 3.18 o -4 4 1 59.59 59.10 3.73 o -3 4 1 760.45 760.47 6.06 o -2 4 1 0.03 0.87 0.84 o -1 4 1 171.48 175.06 1.48 o 0 4 1 221.55 192.58 1.46 o 1 4 1 363.88 371.97 5.20 o 2 4 1 219.04 215.25 2.19 o 3 4 1 5.85 4.80 0.78 o 4 4 1 121.92 133.71 1.57 o 5 4 1 14.19 15.68 1.05 o 6 4 1 110.24 103.29 2.47 o 7 4 1 277.03 288.71 2.75 o 8 4 1 55.79 58.95 2.94 o 9 4 1 96.67 102.55 5.11 o -5 5 1 5.46 4.29 3.64 o -4 5 1 136.74 145.83 4.51 o -3 5 1 10.97 12.05 2.60 o -2 5 1 107.84 99.86 2.72 o -1 5 1 37.78 38.21 1.71 o 0 5 1 0.22 1.55 0.97 o 1 5 1 0.41 1.20 1.09 o 2 5 1 391.27 378.39 6.83 o 3 5 1 141.04 129.09 2.53 o 4 5 1 20.63 19.86 1.50 o 5 5 1 137.83 130.99 4.60 o 6 5 1 166.09 163.75 3.01 o 7 5 1 72.98 73.58 1.92 o 8 5 1 3.93 4.41 1.64 o 9 5 1 46.33 54.69 4.80 o -4 6 1 1.54 5.53 2.82 o -3 6 1 46.77 40.36 3.66 o -2 6 1 66.99 69.12 2.91 o -1 6 1 259.34 250.47 8.19 o 0 6 1 22.58 24.30 1.69 o 1 6 1 22.93 22.00 1.54 o 2 6 1 54.83 56.87 2.96 o 3 6 1 19.75 22.04 1.61 o 4 6 1 446.01 442.41 6.44 o 5 6 1 77.66 76.31 5.62 o 6 6 1 196.35 193.88 3.23 o 7 6 1 54.02 53.31 2.49 o 8 6 1 20.90 18.09 2.42 o 9 6 1 92.40 99.57 6.34 o -3 7 1 241.27 250.53 5.70 o -2 7 1 1.42 2.35 1.74 o -1 7 1 0.12 3.13 1.87 o 0 7 1 16.90 14.60 1.88 o 1 7 1 37.91 32.93 3.09 o 2 7 1 0.06 1.30 2.01 o 3 7 1 125.75 118.07 5.23 o 4 7 1 28.31 23.61 2.00 o 5 7 1 18.53 17.53 2.48 o 6 7 1 172.15 176.33 4.65 o 7 7 1 46.98 44.71 2.31 o 8 7 1 6.32 7.24 2.07 o -2 8 1 93.71 85.28 4.90 o -1 8 1 52.58 55.64 2.88 o 0 8 1 22.15 19.24 2.06 o 1 8 1 153.52 141.83 8.54 o 2 8 1 1.46 2.17 2.38 o 3 8 1 0.25 1.15 2.57 o 4 8 1 13.18 11.44 1.93 o 5 8 1 199.18 205.28 9.94 o 6 8 1 0.24 1.65 1.73 o 7 8 1 31.33 27.92 3.10 o 8 8 1 0.50 3.98 2.77 o 1 9 1 52.77 57.64 5.03 o 2 9 1 53.89 54.02 6.22 o 3 9 1 89.15 87.51 4.48 o 4 9 1 62.35 62.67 4.51 o 5 9 1 0.42 0.00 2.15 o 6 9 1 1.55 1.53 2.03 o 7 9 1 22.59 23.15 2.86 o 5 10 1 20.78 18.20 3.30 o -6 -9 2 8.15 8.26 2.64 o -5 -9 2 16.13 16.02 2.22 o -4 -9 2 173.57 178.38 3.56 o -3 -9 2 5.62 2.18 2.90 o -2 -9 2 11.86 9.97 5.70 o 0 -9 2 10.28 6.64 3.28 o -7 -8 2 49.00 46.10 4.67 o -6 -8 2 5.34 5.38 2.25 o -5 -8 2 37.19 35.45 2.33 o -4 -8 2 125.47 127.68 3.15 o -3 -8 2 38.35 40.00 2.85 o -2 -8 2 189.88 177.83 6.59 o -1 -8 2 32.20 33.23 3.92 o 0 -8 2 111.10 113.07 4.06 o 1 -8 2 206.30 224.52 7.70 o 2 -8 2 47.02 53.37 4.84 o -8 -7 2 6.74 7.60 2.84 o -7 -7 2 14.90 13.19 2.37 o -6 -7 2 13.06 11.73 3.12 o -5 -7 2 36.06 36.12 2.25 o -4 -7 2 36.00 33.36 2.30 o -3 -7 2 33.32 31.61 3.00 o -2 -7 2 151.70 143.96 3.58 o -1 -7 2 147.38 148.34 2.62 o 0 -7 2 255.70 262.24 3.31 o 1 -7 2 46.35 42.62 2.44 o 2 -7 2 26.54 27.27 3.20 o 3 -7 2 147.48 159.35 5.13 o -8 -6 2 206.91 226.22 3.93 o -7 -6 2 15.78 12.41 2.00 o -6 -6 2 73.14 70.35 2.43 o -5 -6 2 182.82 177.36 2.53 o -4 -6 2 44.60 41.79 1.83 o -3 -6 2 154.52 147.60 3.11 o -2 -6 2 309.77 322.53 3.83 o -1 -6 2 104.83 106.32 4.26 o 0 -6 2 14.73 12.03 1.69 o 1 -6 2 47.72 52.18 4.06 o 2 -6 2 51.59 49.15 2.31 o 3 -6 2 50.55 50.65 5.24 o 4 -6 2 136.31 139.14 4.99 o -8 -5 2 4.23 3.73 1.82 o -7 -5 2 89.80 88.98 2.35 o -6 -5 2 119.58 119.93 2.18 o -5 -5 2 80.73 76.91 2.18 o -4 -5 2 25.02 24.56 1.94 o -3 -5 2 494.92 494.45 3.05 o -2 -5 2 86.28 89.07 1.75 o -1 -5 2 26.46 28.09 1.61 o 0 -5 2 688.99 710.93 10.26 o 1 -5 2 21.32 20.38 1.43 o 2 -5 2 86.48 82.71 1.96 o 3 -5 2 9.35 7.57 1.86 o 4 -5 2 51.54 48.13 2.92 o 5 -5 2 43.72 48.05 4.97 o -8 -4 2 5.02 6.08 1.85 o -7 -4 2 90.16 92.45 2.95 o -6 -4 2 252.49 248.78 3.70 o -5 -4 2 89.62 94.15 1.47 o -4 -4 2 784.67 806.04 8.85 o -3 -4 2 95.12 88.20 2.45 o -2 -4 2 54.85 51.63 1.53 o -1 -4 2 2482.88 2648.76 41.69 o 0 -4 2 148.45 145.48 2.48 o 1 -4 2 23.57 20.26 1.25 o 2 -4 2 67.92 72.23 1.76 o 3 -4 2 0.90 3.33 1.92 o 4 -4 2 84.41 84.21 5.39 o 5 -4 2 108.59 111.37 5.39 o 6 -4 2 2.01 4.92 3.52 o -8 -3 2 188.22 198.11 5.50 o -7 -3 2 14.28 12.67 1.59 o -6 -3 2 83.30 82.68 2.46 o -5 -3 2 333.78 343.54 5.87 o -4 -3 2 4.52 3.88 0.89 o -3 -3 2 14.20 14.01 0.89 o -2 -3 2 296.55 276.91 7.58 o -1 -3 2 51.56 54.93 1.70 o 0 -3 2 185.35 176.07 2.99 o 1 -3 2 1947.58 2082.33 6.66 o 2 -3 2 16.46 18.45 1.07 o 3 -3 2 25.51 23.51 2.25 o 4 -3 2 53.04 52.90 1.77 o 5 -3 2 95.42 92.06 2.90 o 6 -3 2 43.85 45.36 3.13 o -7 -2 2 57.03 56.70 3.81 o -6 -2 2 89.75 93.91 3.32 o -5 -2 2 190.28 185.81 4.25 o -4 -2 2 439.00 429.62 4.97 o -3 -2 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