#------------------------------------------------------------------------------ #$Date: 2009-06-07 09:06:07 +0300 (Sun, 07 Jun 2009) $ #$Revision: 754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017100.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017100_Fobs loop_ _publ_author_name 'Minkov, Vasily S.' 'Boldyreva, Elena V.' _publ_section_title ; DL-Cysteinium semioxalate ; _journal_coeditor_code GZ3159 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o245 _journal_page_last o247 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 109.349 _cell_angle_beta 102.282 _cell_angle_gamma 100.119 _cell_length_a 5.6664 _cell_length_b 9.0149 _cell_length_c 9.7749 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.7001 _[local]_cod_data_source_file gz3159Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EXPERIMENT2 DL-CYSOX' _shelx_refln_list_code 4 _shelx_F_calc_maximum 88.03 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 88.50 107.46 1.41 o 2 0 0 443.74 483.55 3.27 o 3 0 0 105.70 102.49 1.73 o 4 0 0 109.80 97.14 0.68 o 5 0 0 61.24 59.93 0.88 o 6 0 0 1.66 1.41 0.40 o 7 0 0 25.34 22.72 0.97 o -7 1 0 21.90 20.90 0.91 o -6 1 0 8.28 8.22 0.48 o -5 1 0 382.84 378.38 2.01 o -4 1 0 732.98 750.10 3.21 o -3 1 0 89.93 96.25 1.23 o -2 1 0 173.79 184.26 1.76 o -1 1 0 22.59 23.43 1.28 o 2 1 0 98.06 99.85 1.41 o 3 1 0 742.70 739.96 3.32 o 4 1 0 0.08 0.54 0.31 o 5 1 0 516.55 548.52 6.38 o 6 1 0 44.20 43.92 1.07 o 7 1 0 4.91 5.65 0.76 o -7 2 0 13.43 12.09 0.76 o -6 2 0 2.66 2.73 0.35 o -5 2 0 37.74 36.97 0.73 o -4 2 0 154.14 149.57 1.01 o -3 2 0 27.54 38.95 0.49 o -2 2 0 419.59 394.34 2.62 o -1 2 0 119.55 125.21 0.82 o 0 2 0 2689.88 2779.66 56.74 o 1 2 0 1215.58 1265.95 8.75 o 2 2 0 7.25 5.94 0.35 o 3 2 0 218.19 213.20 1.33 o 4 2 0 3.04 3.62 0.38 o 5 2 0 0.17 0.34 0.56 o 6 2 0 21.33 21.05 0.89 o 7 2 0 2.35 3.14 0.81 o -7 3 0 0.36 0.78 0.55 o -6 3 0 7.25 6.40 0.38 o -5 3 0 32.64 31.94 0.76 o -4 3 0 131.68 137.96 1.16 o -3 3 0 579.03 594.32 2.99 o -2 3 0 178.36 184.84 1.84 o -1 3 0 1455.58 1456.94 14.60 o 0 3 0 892.46 1017.93 16.98 o 1 3 0 328.98 308.53 2.58 o 2 3 0 3.26 4.86 0.39 o 3 3 0 0.10 0.80 0.31 o 4 3 0 1.74 1.68 0.29 o 5 3 0 29.98 28.38 0.99 o 6 3 0 16.25 15.27 0.94 o -7 4 0 21.38 20.95 0.96 o -6 4 0 34.81 31.39 0.72 o -5 4 0 195.02 204.01 1.78 o -4 4 0 6.86 7.60 0.39 o -3 4 0 34.64 29.29 0.87 o -2 4 0 8.26 9.94 0.60 o -1 4 0 225.77 262.79 3.24 o 0 4 0 9.40 7.02 0.30 o 1 4 0 311.24 299.43 3.66 o 2 4 0 424.00 409.82 3.37 o 3 4 0 82.21 84.81 1.04 o 4 4 0 221.96 236.61 2.86 o 5 4 0 159.70 166.27 2.14 o 6 4 0 2.35 3.32 0.91 o -7 5 0 12.90 12.54 0.94 o -6 5 0 0.23 0.60 0.49 o -5 5 0 35.27 35.54 0.77 o -4 5 0 571.80 585.36 3.72 o -3 5 0 2.63 1.54 0.25 o -2 5 0 81.00 87.50 1.08 o -1 5 0 699.80 734.73 8.25 o 0 5 0 1906.06 1948.08 9.69 o 1 5 0 29.84 28.61 0.94 o 2 5 0 15.18 17.51 0.61 o 3 5 0 1.62 1.68 0.48 o 4 5 0 115.89 117.27 2.04 o 5 5 0 3.63 3.45 0.82 o 6 5 0 0.91 1.25 0.95 o -7 6 0 5.70 5.65 0.81 o -6 6 0 0.04 0.28 0.49 o -5 6 0 169.45 173.65 2.06 o -4 6 0 135.55 142.06 1.76 o -3 6 0 23.51 24.15 0.74 o -2 6 0 172.84 169.07 1.55 o -1 6 0 9.29 7.27 0.36 o 0 6 0 5.10 4.47 0.40 o 1 6 0 76.82 73.65 1.85 o 2 6 0 21.24 21.15 0.42 o 3 6 0 121.75 123.88 1.72 o 4 6 0 6.36 5.63 0.80 o 5 6 0 52.22 49.28 1.67 o -7 7 0 4.35 5.47 0.80 o -6 7 0 3.47 4.42 0.69 o -5 7 0 55.78 52.20 1.23 o -4 7 0 19.74 18.91 0.80 o -3 7 0 0.03 0.39 0.48 o -2 7 0 0.50 0.41 0.41 o -1 7 0 230.88 225.37 2.00 o 0 7 0 72.04 68.55 1.19 o 1 7 0 38.09 39.51 1.04 o 2 7 0 86.38 83.03 1.39 o 3 7 0 6.44 7.30 0.71 o 4 7 0 4.37 5.73 0.88 o 5 7 0 0.69 0.63 1.07 o -7 8 0 9.78 10.58 1.24 o -6 8 0 1.51 2.07 0.69 o -5 8 0 57.68 60.23 1.38 o -4 8 0 0.84 1.24 0.58 o -3 8 0 89.31 88.90 1.54 o -2 8 0 4.56 5.17 0.53 o -1 8 0 14.45 13.96 0.68 o 0 8 0 39.48 36.02 1.26 o 1 8 0 0.01 0.34 0.55 o 2 8 0 12.22 12.00 0.98 o 3 8 0 18.62 18.49 1.43 o 4 8 0 1.39 1.71 1.09 o -6 9 0 13.42 13.68 1.06 o -5 9 0 24.83 20.99 1.02 o -4 9 0 1.12 1.67 0.60 o -3 9 0 13.30 14.32 0.75 o -2 9 0 30.56 32.79 1.15 o -1 9 0 0.00 0.25 0.63 o 0 9 0 42.37 41.77 1.43 o 1 9 0 40.84 39.78 1.22 o 2 9 0 0.67 1.95 0.76 o 3 9 0 5.15 4.10 1.22 o -6 10 0 0.02 0.52 1.00 o -5 10 0 3.69 3.09 0.77 o -4 10 0 58.26 63.20 1.46 o -3 10 0 6.09 5.95 0.80 o -2 10 0 3.27 4.31 0.82 o -1 10 0 32.63 28.54 1.12 o 0 10 0 112.16 115.43 2.36 o 1 10 0 0.87 1.44 0.91 o 2 10 0 1.54 2.43 1.10 o -5 11 0 11.79 14.32 1.67 o -4 11 0 7.64 7.57 0.92 o -3 11 0 2.92 3.40 0.90 o -2 11 0 0.02 1.00 0.83 o -1 11 0 5.50 5.96 0.88 o 0 11 0 0.04 0.45 0.78 o 1 11 0 0.11 -0.37 0.88 o -3 12 0 0.25 0.88 1.00 o -2 12 0 10.85 11.58 1.25 o -1 12 0 1.20 4.03 1.05 o 0 -12 1 13.50 14.33 1.12 o 1 -12 1 0.62 1.22 0.93 o 2 -12 1 1.74 2.99 0.89 o 3 -12 1 5.87 8.40 0.92 o -1 -11 1 0.61 1.19 0.93 o 0 -11 1 0.02 0.17 0.80 o 1 -11 1 5.69 5.25 0.82 o 2 -11 1 20.97 24.25 1.17 o 3 -11 1 2.77 2.98 0.83 o 4 -11 1 15.71 16.33 1.15 o 5 -11 1 16.42 18.64 1.78 o -3 -10 1 3.26 3.54 1.21 o -2 -10 1 15.07 15.21 1.18 o -1 -10 1 1.15 0.26 0.83 o 0 -10 1 23.49 21.65 1.19 o 1 -10 1 5.38 7.94 0.99 o 2 -10 1 15.15 16.09 0.89 o 3 -10 1 1.55 1.83 0.72 o 4 -10 1 0.17 0.71 0.66 o 5 -10 1 17.03 18.18 1.30 o 6 -10 1 0.82 1.11 1.02 o -3 -9 1 27.13 30.50 1.36 o -2 -9 1 9.30 10.24 0.84 o -1 -9 1 19.50 19.77 1.24 o 0 -9 1 11.00 12.31 0.95 o 1 -9 1 4.19 4.01 0.63 o 2 -9 1 2.66 2.99 0.53 o 3 -9 1 5.45 5.64 0.59 o 4 -9 1 3.95 3.58 0.60 o 5 -9 1 71.10 74.65 1.70 o 6 -9 1 0.02 0.04 0.95 o -4 -8 1 18.06 16.54 1.11 o -3 -8 1 5.13 7.05 0.80 o -2 -8 1 29.03 28.95 0.93 o -1 -8 1 0.02 0.46 0.47 o 0 -8 1 117.82 123.75 1.49 o 1 -8 1 589.43 623.26 7.95 o 2 -8 1 0.02 0.33 0.38 o 3 -8 1 8.55 10.34 0.62 o 4 -8 1 88.26 89.17 1.49 o 5 -8 1 24.04 26.38 1.00 o 6 -8 1 0.03 0.39 0.91 o 7 -8 1 1.16 0.94 0.97 o -5 -7 1 26.75 25.35 1.34 o -4 -7 1 103.99 108.70 2.12 o -3 -7 1 100.16 109.55 1.68 o -2 -7 1 20.45 19.15 0.73 o -1 -7 1 99.42 98.32 1.32 o 0 -7 1 71.12 70.94 1.42 o 1 -7 1 14.12 13.45 0.70 o 2 -7 1 19.08 16.78 0.55 o 3 -7 1 51.80 52.77 0.98 o 4 -7 1 44.33 44.37 0.97 o 5 -7 1 41.39 42.13 1.11 o 6 -7 1 15.43 13.89 0.94 o 7 -7 1 27.84 28.02 1.52 o -5 -6 1 0.04 0.31 0.84 o -4 -6 1 4.27 5.31 0.79 o -3 -6 1 7.38 7.52 0.60 o -2 -6 1 141.12 126.95 1.43 o -1 -6 1 34.83 31.11 0.84 o 0 -6 1 9.84 12.60 0.54 o 1 -6 1 394.09 413.36 2.29 o 2 -6 1 245.02 259.91 1.69 o 3 -6 1 92.82 84.60 1.26 o 4 -6 1 3.84 3.17 0.37 o 5 -6 1 23.95 21.89 0.73 o 6 -6 1 7.86 7.91 0.67 o 7 -6 1 7.63 7.52 1.04 o -6 -5 1 2.02 2.20 0.92 o -5 -5 1 0.17 0.32 0.76 o -4 -5 1 1.91 2.88 0.53 o -3 -5 1 12.40 10.99 0.89 o -2 -5 1 108.16 112.62 1.58 o -1 -5 1 237.01 230.66 4.11 o 0 -5 1 277.29 300.28 2.34 o 1 -5 1 16.53 11.99 0.74 o 2 -5 1 351.31 355.72 2.71 o 3 -5 1 176.67 194.54 1.61 o 4 -5 1 4.41 2.85 0.39 o 5 -5 1 13.18 12.04 0.55 o 6 -5 1 1.06 0.98 0.48 o 7 -5 1 0.03 -0.31 0.70 o -6 -4 1 14.52 14.13 1.10 o -5 -4 1 177.47 187.68 2.55 o -4 -4 1 15.31 14.40 0.70 o -3 -4 1 100.39 93.24 1.10 o -2 -4 1 59.03 62.97 0.77 o -1 -4 1 11.00 14.57 0.50 o 0 -4 1 432.60 462.39 2.15 o 1 -4 1 61.50 49.17 0.71 o 2 -4 1 24.93 34.16 0.77 o 3 -4 1 442.17 465.16 1.70 o 4 -4 1 280.60 290.02 1.98 o 5 -4 1 239.29 245.65 1.77 o 6 -4 1 20.65 22.00 0.71 o 7 -4 1 5.74 4.56 0.82 o -7 -3 1 3.78 4.38 0.93 o -6 -3 1 37.65 33.66 1.33 o -5 -3 1 9.26 7.81 0.68 o -4 -3 1 36.28 34.32 0.93 o -3 -3 1 546.29 547.23 3.16 o -2 -3 1 137.76 143.20 1.60 o -1 -3 1 0.02 2.16 0.60 o 0 -3 1 7748.83 5946.14 59.41 o 1 -3 1 1266.13 1344.91 14.90 o 2 -3 1 25.09 22.96 0.42 o 3 -3 1 11.06 12.37 0.29 o 4 -3 1 62.41 59.03 0.75 o 5 -3 1 116.64 115.58 0.99 o 6 -3 1 0.28 0.44 0.43 o 7 -3 1 8.33 8.41 0.80 o -7 -2 1 39.34 41.04 1.31 o -6 -2 1 2.24 1.51 0.56 o -5 -2 1 131.55 129.65 1.54 o -4 -2 1 577.48 584.27 2.82 o -3 -2 1 218.01 216.37 3.19 o -2 -2 1 285.86 322.84 3.23 o -1 -2 1 1902.51 1942.57 20.22 o 1 -2 1 26.29 39.02 0.34 o 2 -2 1 228.39 228.44 1.31 o 3 -2 1 586.96 602.31 2.75 o 4 -2 1 44.66 45.32 0.72 o 5 -2 1 143.73 149.24 1.25 o 6 -2 1 30.29 29.11 0.72 o 7 -2 1 74.11 75.93 1.42 o -7 -1 1 1.22 1.65 0.79 o -6 -1 1 44.59 42.37 0.86 o -5 -1 1 0.13 0.41 0.42 o -4 -1 1 44.79 40.68 0.74 o -3 -1 1 300.28 292.99 3.28 o -2 -1 1 1226.23 1305.32 9.97 o -1 -1 1 781.35 766.23 14.67 o 1 -1 1 808.09 825.75 7.56 o 2 -1 1 1008.80 1090.02 3.17 o 3 -1 1 1028.15 1033.53 7.12 o 4 -1 1 2.50 3.82 0.41 o 5 -1 1 98.66 102.09 1.22 o 6 -1 1 0.43 0.55 0.39 o 7 -1 1 9.31 9.65 0.82 o -7 0 1 11.66 9.92 0.76 o -6 0 1 11.74 11.17 0.59 o -5 0 1 0.15 0.54 0.28 o -4 0 1 183.13 189.49 1.22 o -3 0 1 220.71 194.11 1.98 o -2 0 1 1504.00 1532.74 13.34 o -1 0 1 310.75 316.13 2.85 o 1 0 1 43.17 39.09 1.19 o 2 0 1 645.01 686.13 2.77 o 3 0 1 147.47 156.05 2.30 o 4 0 1 112.98 112.49 1.25 o 5 0 1 7.35 6.25 0.45 o 6 0 1 64.50 63.16 1.06 o 7 0 1 11.55 10.19 0.87 o -7 1 1 1.71 1.49 0.55 o -6 1 1 26.73 25.18 0.78 o -5 1 1 497.16 499.15 2.98 o -4 1 1 36.67 35.93 0.55 o -3 1 1 11.26 13.48 0.52 o -2 1 1 798.14 925.98 6.91 o 1 1 1 1136.90 1138.73 12.61 o 2 1 1 366.22 333.35 3.22 o 3 1 1 27.23 32.69 0.78 o 4 1 1 204.67 206.43 1.55 o 5 1 1 64.24 66.25 1.35 o 6 1 1 4.18 4.22 0.64 o 7 1 1 9.82 11.38 0.93 o -7 2 1 20.29 19.36 0.77 o -6 2 1 0.41 0.72 0.38 o -5 2 1 8.38 6.56 0.37 o -4 2 1 185.27 173.30 1.17 o -3 2 1 571.10 599.17 3.66 o -2 2 1 1031.45 1112.05 13.08 o -1 2 1 325.35 332.10 4.94 o 0 2 1 3481.35 3540.27 50.98 o 1 2 1 1543.49 1566.58 17.35 o 2 2 1 32.81 31.58 0.65 o 3 2 1 123.93 126.48 1.25 o 4 2 1 444.43 466.62 5.18 o 5 2 1 18.33 16.55 0.79 o 6 2 1 4.32 5.08 0.66 o -8 3 1 18.44 18.70 0.93 o -7 3 1 90.92 93.17 1.46 o -6 3 1 23.75 24.08 0.55 o -5 3 1 607.93 617.80 3.12 o -4 3 1 441.79 440.29 2.10 o -3 3 1 105.79 100.48 1.08 o -2 3 1 178.49 161.81 1.41 o -1 3 1 155.14 168.12 2.51 o 0 3 1 134.92 112.05 1.09 o 1 3 1 330.24 350.46 1.22 o 2 3 1 7.45 7.12 0.59 o 3 3 1 393.82 386.26 2.91 o 4 3 1 1.42 0.88 0.52 o 5 3 1 3.86 3.68 0.65 o 6 3 1 28.96 29.61 1.47 o -7 4 1 6.79 6.84 0.64 o -6 4 1 17.77 17.02 0.70 o -5 4 1 170.88 176.22 1.64 o -4 4 1 55.97 60.18 1.24 o -3 4 1 162.71 169.75 1.60 o -2 4 1 354.21 342.50 3.43 o -1 4 1 465.10 440.96 3.59 o 0 4 1 14.50 14.99 0.46 o 1 4 1 252.96 262.13 1.75 o 2 4 1 314.72 335.49 2.00 o 3 4 1 91.81 87.14 1.33 o 4 4 1 19.74 19.91 0.80 o 5 4 1 18.65 20.69 0.96 o 6 4 1 5.20 5.22 1.08 o -7 5 1 39.46 42.35 1.17 o -6 5 1 18.67 17.54 0.67 o -5 5 1 3.15 3.16 0.54 o -4 5 1 1.37 1.64 0.38 o -3 5 1 0.06 0.40 0.18 o -2 5 1 76.96 73.28 0.83 o -1 5 1 31.83 31.32 0.52 o 0 5 1 160.41 160.11 1.54 o 1 5 1 10.01 6.17 0.26 o 2 5 1 0.03 0.20 0.43 o 3 5 1 0.19 0.77 0.48 o 4 5 1 13.53 12.63 0.92 o 5 5 1 8.77 10.35 1.15 o -7 6 1 3.02 3.56 0.83 o -6 6 1 30.39 30.24 1.04 o -5 6 1 227.34 232.58 1.98 o -4 6 1 19.94 20.14 0.85 o -3 6 1 29.37 23.03 0.81 o -2 6 1 82.58 76.92 1.19 o -1 6 1 93.96 106.71 1.46 o 0 6 1 2.04 1.11 0.38 o 1 6 1 110.47 121.44 1.78 o 2 6 1 59.69 52.82 1.34 o 3 6 1 0.33 0.31 0.85 o 4 6 1 70.90 75.35 2.10 o 5 6 1 2.70 2.19 1.04 o -7 7 1 4.14 4.51 0.78 o -6 7 1 2.70 2.41 0.68 o -5 7 1 2.28 2.62 0.64 o -4 7 1 32.55 31.52 1.04 o -3 7 1 377.55 385.02 3.42 o -2 7 1 97.08 99.56 1.64 o -1 7 1 92.82 89.78 1.34 o 0 7 1 547.78 550.91 5.62 o 1 7 1 1.60 1.76 0.56 o 2 7 1 2.87 2.18 0.65 o 3 7 1 0.00 0.37 0.94 o 4 7 1 38.10 39.44 2.00 o -7 8 1 40.97 43.08 1.50 o -6 8 1 0.69 0.43 0.72 o -5 8 1 107.33 109.09 1.97 o -4 8 1 37.64 34.16 1.13 o -3 8 1 15.38 12.50 0.98 o -2 8 1 19.20 18.80 0.93 o -1 8 1 27.71 27.99 0.92 o 0 8 1 19.69 23.06 1.09 o 1 8 1 13.67 12.24 0.79 o 2 8 1 49.10 44.14 1.45 o 3 8 1 43.40 44.86 2.10 o -6 9 1 1.03 0.05 0.76 o -5 9 1 1.97 1.92 0.70 o -4 9 1 5.93 6.48 0.92 o -3 9 1 20.49 17.40 0.96 o -2 9 1 69.87 70.81 1.57 o -1 9 1 3.17 3.57 0.64 o 0 9 1 2.45 1.15 0.78 o 1 9 1 24.44 22.41 1.11 o 2 9 1 0.01 1.65 1.03 o 3 9 1 23.12 27.29 1.80 o -5 10 1 0.20 1.28 0.85 o -4 10 1 5.15 4.92 0.91 o -3 10 1 7.58 7.27 0.89 o -2 10 1 3.11 3.16 0.75 o -1 10 1 20.29 21.39 0.94 o 0 10 1 0.05 -0.51 0.71 o 1 10 1 1.26 2.54 1.04 o 2 10 1 1.08 1.60 1.51 o -4 11 1 1.17 3.02 1.06 o -3 11 1 0.47 0.07 0.90 o -2 11 1 2.41 2.87 0.89 o -1 11 1 8.79 8.17 1.30 o 0 11 1 3.78 3.24 1.00 o 0 -12 2 0.55 0.79 0.80 o 1 -12 2 0.50 1.18 0.85 o 2 -12 2 1.97 1.91 0.88 o 3 -12 2 3.57 5.36 1.12 o 4 -12 2 2.99 3.00 1.12 o -2 -11 2 19.02 19.66 1.64 o -1 -11 2 1.13 1.33 0.87 o 0 -11 2 18.67 17.95 1.23 o 1 -11 2 49.24 47.84 1.31 o 2 -11 2 6.56 6.03 0.84 o 3 -11 2 0.84 0.76 0.76 o 4 -11 2 26.04 24.67 1.55 o 5 -11 2 5.56 6.47 1.18 o -3 -10 2 37.53 36.43 1.38 o -2 -10 2 0.92 0.85 0.66 o -1 -10 2 0.04 0.65 0.85 o 0 -10 2 58.90 61.03 1.73 o 1 -10 2 28.90 29.21 1.10 o 2 -10 2 8.53 8.16 0.83 o 3 -10 2 3.66 3.98 0.62 o 4 -10 2 5.31 5.76 0.85 o 5 -10 2 1.85 1.88 0.83 o 6 -10 2 0.84 1.33 1.10 o -4 -9 2 11.14 14.58 1.24 o -3 -9 2 0.27 1.06 0.73 o -2 -9 2 82.83 84.59 1.52 o -1 -9 2 23.64 22.39 0.82 o 0 -9 2 27.19 24.06 0.80 o 1 -9 2 1.83 1.26 0.51 o 2 -9 2 24.43 23.44 0.82 o 3 -9 2 93.23 101.20 1.56 o 4 -9 2 18.47 15.14 0.90 o 5 -9 2 2.08 1.68 0.79 o 6 -9 2 21.55 21.50 1.42 o -4 -8 2 1.27 1.91 0.86 o -3 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