#------------------------------------------------------------------------------ #$Date: 2009-06-07 09:06:07 +0300 (Sun, 07 Jun 2009) $ #$Revision: 754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017103.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017103_Fobs loop_ _publ_author_name 'Sridhar, Balasubramanian' 'Ravikumar, Krishnan' 'Varghese, Babu' _publ_section_title ; Supramolecular hydrogen-bonded networks in adeninediium hemioxalate chloride and adeninium semioxalate hemi(oxalic acid) monohydrate ; _journal_coeditor_code LN3126 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o202 _journal_page_last o206 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.558 _cell_angle_gamma 90.000 _cell_length_a 4.3758 _cell_length_b 17.1354 _cell_length_c 11.1188 _exptl_crystal_F_000 444.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file ln3126Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AC86m in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 258.14 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3.61 1.82 0.22 o 2 0 0 2654.77 2654.79 50.76 o 3 0 0 2160.42 2182.27 41.84 o 4 0 0 15.27 15.69 0.58 o 1 1 0 1074.64 1036.09 14.03 o 2 1 0 97.48 89.93 1.29 o 3 1 0 147.63 157.72 2.29 o 4 1 0 41.34 45.21 0.87 o 5 1 0 21.80 20.74 1.25 o 0 2 0 213.88 167.74 5.54 o 1 2 0 3706.41 4274.43 57.66 o 2 2 0 406.10 420.51 6.04 o 3 2 0 5.68 5.86 0.20 o 4 2 0 223.80 230.94 3.84 o 5 2 0 8.35 10.96 0.92 o 1 3 0 0.97 1.04 0.18 o 2 3 0 634.79 636.25 8.66 o 3 3 0 404.53 375.50 6.12 o 4 3 0 126.95 123.19 2.49 o 5 3 0 40.24 41.14 1.43 o 0 4 0 21.08 27.04 1.32 o 1 4 0 109.85 124.46 1.77 o 2 4 0 635.04 654.74 8.95 o 3 4 0 292.40 285.14 4.24 o 4 4 0 0.88 0.71 0.20 o 5 4 0 66.00 69.50 2.01 o 1 5 0 809.65 824.85 11.95 o 2 5 0 541.16 585.38 8.01 o 3 5 0 11.28 11.31 0.38 o 4 5 0 26.95 25.20 0.69 o 5 5 0 89.81 96.44 2.66 o 0 6 0 13762.05 9622.36 388.39 o 1 6 0 5667.43 6047.51 82.75 o 2 6 0 198.30 167.48 2.53 o 3 6 0 1040.31 1021.25 16.42 o 4 6 0 136.29 140.64 2.78 o 1 7 0 698.78 759.22 10.36 o 2 7 0 72.31 82.38 1.34 o 3 7 0 173.97 177.44 3.03 o 4 7 0 39.95 37.80 0.96 o 0 8 0 2269.91 2284.52 45.37 o 1 8 0 165.07 220.62 3.33 o 2 8 0 679.63 711.57 11.48 o 3 8 0 3.78 5.53 0.29 o 4 8 0 18.78 19.80 0.69 o 1 9 0 138.94 124.31 2.11 o 2 9 0 880.57 948.17 15.26 o 3 9 0 257.04 259.48 4.35 o 4 9 0 12.67 12.44 0.53 o 0 10 0 182.57 189.81 3.80 o 1 10 0 1.71 0.59 0.35 o 2 10 0 549.53 548.57 10.07 o 3 10 0 405.70 411.00 6.79 o 4 10 0 10.78 11.17 0.64 o 1 11 0 58.10 57.87 1.21 o 2 11 0 12.19 12.72 0.42 o 3 11 0 0.90 1.79 0.32 o 4 11 0 9.67 8.84 0.48 o 0 12 0 2182.40 2309.33 60.84 o 1 12 0 452.42 421.35 7.37 o 2 12 0 210.56 206.28 3.89 o 3 12 0 610.90 604.67 11.91 o 4 12 0 0.46 0.59 0.28 o 1 13 0 13.95 15.03 0.42 o 2 13 0 1.78 2.49 0.21 o 3 13 0 65.51 70.74 1.60 o 0 14 0 1153.04 1134.40 32.70 o 1 14 0 105.10 100.17 1.80 o 2 14 0 9.68 11.89 0.52 o 3 14 0 16.91 11.93 0.58 o 1 15 0 221.66 239.83 4.02 o 2 15 0 198.83 213.77 3.63 o 3 15 0 71.63 78.74 1.80 o 0 16 0 73.83 71.43 2.44 o 1 16 0 282.36 306.14 5.06 o 2 16 0 82.81 78.59 1.71 o 3 16 0 169.45 176.23 4.65 o 1 17 0 3.29 2.76 0.24 o 2 17 0 3.79 4.85 0.36 o 0 18 0 437.76 484.38 14.20 o 1 18 0 345.50 344.41 7.33 o 2 18 0 96.52 97.63 2.47 o 1 19 0 32.23 32.35 1.27 o 0 20 0 369.79 406.73 12.19 o -5 1 1 6.99 8.38 0.88 o -4 1 1 13.25 13.82 0.37 o -3 1 1 49.19 45.42 0.76 o -2 1 1 103.22 99.79 1.44 o -1 1 1 0.45 0.55 0.25 o 0 1 1 0.37 1.76 4.41 o 1 1 1 424.64 429.55 5.83 o 2 1 1 252.44 226.45 3.16 o 3 1 1 151.93 140.49 2.20 o 4 1 1 67.06 68.26 1.32 o 5 1 1 3.89 5.16 0.51 o -5 2 1 70.41 76.97 2.95 o -4 2 1 99.67 108.39 1.78 o -3 2 1 18.84 15.39 0.37 o -2 2 1 796.06 754.04 10.23 o -1 2 1 2947.15 3169.51 58.96 o 0 2 1 873.10 821.58 16.15 o 1 2 1 2850.57 2954.17 39.80 o 2 2 1 157.95 169.89 2.40 o 3 2 1 41.08 36.41 0.65 o 4 2 1 24.35 26.18 0.72 o 5 2 1 10.10 11.81 0.64 o -5 3 1 1.51 1.32 0.51 o -4 3 1 1.30 1.58 0.18 o -3 3 1 56.29 62.69 1.01 o -2 3 1 296.91 300.26 4.13 o -1 3 1 112.66 94.20 1.49 o 0 3 1 410.03 430.53 6.33 o 1 3 1 179.46 179.11 2.46 o 2 3 1 6.58 6.29 0.23 o 3 3 1 30.68 28.66 0.56 o 4 3 1 6.46 7.05 0.45 o 5 3 1 1.28 1.17 0.28 o -5 4 1 89.00 104.22 4.59 o -4 4 1 130.82 136.80 2.44 o -3 4 1 64.16 67.21 1.05 o -2 4 1 535.85 494.17 6.77 o -1 4 1 4172.83 4490.97 74.03 o 0 4 1 72.53 37.65 0.69 o 1 4 1 1223.93 1081.59 15.60 o 2 4 1 478.38 491.29 6.75 o 3 4 1 0.73 0.33 0.16 o 4 4 1 0.00 0.00 0.20 o 5 4 1 6.44 8.05 0.58 o -5 5 1 0.04 0.15 0.25 o -4 5 1 31.55 30.74 0.74 o -3 5 1 159.05 157.41 2.49 o -2 5 1 12.36 13.15 0.35 o -1 5 1 1.47 0.61 0.20 o 0 5 1 1111.67 1060.08 16.34 o 1 5 1 228.82 211.57 3.11 o 2 5 1 94.32 85.35 1.26 o 3 5 1 136.68 131.91 2.06 o 4 5 1 69.44 70.13 1.55 o -4 6 1 6.61 6.65 0.62 o -3 6 1 100.53 101.18 1.83 o -2 6 1 0.38 0.57 0.17 o -1 6 1 451.66 463.16 6.98 o 0 6 1 713.23 734.86 9.99 o 1 6 1 525.14 521.66 7.58 o 2 6 1 96.09 92.18 1.37 o 3 6 1 0.38 0.44 0.18 o 4 6 1 61.07 60.25 1.35 o -4 7 1 46.94 45.74 1.20 o -3 7 1 35.04 34.02 0.85 o -2 7 1 21.32 18.10 0.40 o -1 7 1 633.66 674.13 10.08 o 0 7 1 182.48 159.74 2.55 o 1 7 1 112.77 95.15 1.50 o 2 7 1 408.77 401.29 5.88 o 3 7 1 114.88 110.18 2.21 o 4 7 1 58.40 58.73 1.54 o -4 8 1 19.92 19.56 0.75 o -3 8 1 1.67 1.21 0.18 o -2 8 1 931.16 932.20 15.00 o -1 8 1 173.64 217.22 3.03 o 0 8 1 13.73 18.90 0.48 o 1 8 1 638.45 634.40 9.20 o 2 8 1 676.79 730.72 11.18 o 3 8 1 153.21 149.55 2.92 o 4 8 1 46.41 45.91 1.12 o -4 9 1 41.42 40.43 1.20 o -3 9 1 20.02 21.10 0.62 o -2 9 1 627.17 671.94 11.78 o -1 9 1 65.20 79.77 1.51 o 0 9 1 46.72 42.69 0.69 o 1 9 1 28.99 29.41 0.56 o 2 9 1 0.12 0.51 0.24 o 3 9 1 74.39 71.34 1.55 o 4 9 1 0.02 0.09 0.20 o -4 10 1 57.79 57.85 1.52 o -3 10 1 125.67 128.82 2.37 o -2 10 1 106.01 87.06 1.60 o -1 10 1 463.72 496.83 8.05 o 0 10 1 20.71 8.73 0.22 o 1 10 1 364.36 392.49 5.78 o 2 10 1 10.89 12.03 0.40 o 3 10 1 24.87 24.54 1.00 o 4 10 1 0.99 1.27 0.24 o -4 11 1 40.22 38.47 1.27 o -3 11 1 188.63 192.41 3.29 o -2 11 1 8.42 7.45 0.57 o -1 11 1 60.41 55.60 1.18 o 0 11 1 844.81 853.26 11.66 o 1 11 1 585.38 558.10 8.62 o 2 11 1 101.72 100.45 1.80 o 3 11 1 35.94 35.24 0.89 o 4 11 1 87.40 92.45 2.14 o -4 12 1 3.98 2.92 0.44 o -3 12 1 9.16 9.71 0.38 o -2 12 1 0.57 0.22 0.18 o -1 12 1 84.15 80.46 2.09 o 0 12 1 0.78 0.99 0.16 o 1 12 1 19.97 19.48 0.51 o 2 12 1 28.53 28.40 0.64 o 3 12 1 3.45 3.79 0.51 o 4 12 1 9.24 8.83 0.48 o -4 13 1 0.13 0.44 0.24 o -3 13 1 124.67 121.72 2.38 o -2 13 1 48.33 47.29 0.98 o -1 13 1 128.88 125.78 2.21 o 0 13 1 1421.20 1460.30 21.11 o 1 13 1 762.86 768.06 14.08 o 2 13 1 138.06 139.42 3.17 o 3 13 1 130.97 128.70 2.56 o -3 14 1 7.78 6.01 0.42 o -2 14 1 533.50 514.62 8.85 o -1 14 1 26.46 25.73 0.61 o 0 14 1 565.66 586.49 10.36 o 1 14 1 1466.34 1525.88 24.38 o 2 14 1 23.50 22.64 0.66 o 3 14 1 95.71 91.86 2.13 o -3 15 1 57.22 53.59 1.46 o -2 15 1 136.46 127.73 2.59 o -1 15 1 135.09 127.89 2.26 o 0 15 1 0.76 1.05 0.24 o 1 15 1 152.18 150.50 2.61 o 2 15 1 31.94 29.70 0.74 o 3 15 1 20.88 19.65 0.65 o -3 16 1 183.72 180.84 3.85 o -2 16 1 94.55 104.42 2.41 o -1 16 1 69.84 79.56 3.03 o 0 16 1 1123.49 1132.73 23.15 o 1 16 1 278.38 272.22 4.80 o 2 16 1 300.07 317.75 5.85 o 3 16 1 4.53 3.80 0.39 o -2 17 1 15.22 14.22 0.56 o -1 17 1 29.39 31.71 0.85 o 0 17 1 39.37 42.82 1.20 o 1 17 1 168.83 179.30 6.12 o 2 17 1 17.66 18.10 0.71 o -2 18 1 0.05 0.35 0.23 o -1 18 1 12.37 11.47 0.70 o 0 18 1 18.42 20.19 0.75 o 1 18 1 42.47 44.33 1.59 o 2 18 1 21.60 22.55 1.11 o -1 19 1 172.60 182.27 5.03 o 0 19 1 288.74 327.90 6.97 o 1 19 1 290.13 319.89 6.89 o 0 20 1 16.16 16.46 0.75 o -4 0 2 12.35 12.45 0.52 o -3 0 2 5.00 5.39 0.28 o -2 0 2 1517.34 1535.19 29.38 o -1 0 2 2116.57 2125.73 40.73 o 0 0 2 110.66 74.90 2.12 o 1 0 2 66638.79 61545.12 2711.68 o 2 0 2 178.73 191.40 3.80 o 3 0 2 389.48 384.61 7.55 o 4 0 2 533.77 560.99 12.84 o 5 0 2 0.68 0.00 0.88 o -5 1 2 0.01 -0.44 0.44 o -4 1 2 107.43 108.80 1.83 o -3 1 2 99.41 127.84 2.17 o -2 1 2 2378.25 2450.60 33.06 o -1 1 2 105.81 122.49 1.84 o 0 1 2 1416.15 1345.07 18.22 o 1 1 2 8326.96 8572.48 200.53 o 2 1 2 266.36 248.25 3.46 o 3 1 2 179.46 166.95 2.61 o 4 1 2 14.65 14.99 0.53 o 5 1 2 19.92 21.53 0.91 o -5 2 2 0.04 0.22 0.31 o -4 2 2 3.95 3.74 0.23 o -3 2 2 177.15 184.21 2.81 o -2 2 2 408.66 447.64 6.42 o -1 2 2 2.67 2.92 0.17 o 0 2 2 1916.56 2176.84 29.47 o 1 2 2 236.99 233.34 3.22 o 2 2 2 822.79 897.03 12.17 o 3 2 2 167.31 161.89 2.48 o 4 2 2 0.78 0.62 0.20 o -5 3 2 159.74 179.09 4.27 o -4 3 2 330.10 335.23 5.54 o -3 3 2 1230.11 1263.81 19.36 o -2 3 2 3545.27 3669.43 49.65 o -1 3 2 5899.35 6148.57 123.76 o 0 3 2 1633.15 1723.25 29.49 o 1 3 2 1928.71 1913.48 25.89 o 2 3 2 642.48 618.72 8.42 o 3 3 2 68.48 69.67 1.15 o 4 3 2 7.63 8.37 0.42 o -5 4 2 5.92 7.34 0.66 o -4 4 2 2.87 2.13 0.21 o -3 4 2 26.66 30.42 0.63 o -2 4 2 64.35 62.62 1.20 o -1 4 2 25.51 37.46 0.63 o 0 4 2 100.07 87.73 1.23 o 1 4 2 30.46 33.89 0.61 o 2 4 2 21.54 20.50 0.42 o 3 4 2 224.23 222.67 3.66 o 4 4 2 72.00 67.67 1.74 o -5 5 2 80.85 84.97 2.64 o -4 5 2 332.99 356.68 6.35 o -3 5 2 344.84 346.21 5.65 o -2 5 2 273.16 260.82 3.61 o -1 5 2 546.99 682.75 10.18 o 0 5 2 22.26 21.50 0.40 o 1 5 2 1254.74 1225.90 19.17 o 2 5 2 901.05 907.83 12.33 o 3 5 2 255.72 259.99 4.21 o 4 5 2 13.42 13.19 1.34 o -4 6 2 45.47 46.29 1.06 o -3 6 2 0.04 -0.07 0.18 o -2 6 2 409.79 400.15 6.05 o -1 6 2 13.11 9.98 0.29 o 0 6 2 2594.21 2837.17 42.92 o 1 6 2 4424.28 4698.29 67.47 o 2 6 2 1197.27 1207.25 17.43 o 3 6 2 0.66 0.79 0.20 o 4 6 2 278.40 285.44 6.01 o -4 7 2 22.24 22.95 0.65 o -3 7 2 159.82 154.99 2.67 o -2 7 2 1634.04 1788.46 27.40 o -1 7 2 36.08 69.23 1.32 o 0 7 2 3592.13 3936.11 53.37 o 1 7 2 493.47 497.65 7.22 o 2 7 2 51.69 49.24 0.86 o 3 7 2 36.66 35.75 0.89 o 4 7 2 2.55 3.18 0.44 o -4 8 2 5.21 4.82 0.39 o -3 8 2 15.44 13.85 0.45 o -2 8 2 141.73 154.42 3.50 o -1 8 2 52.99 47.15 0.82 o 0 8 2 243.57 298.21 4.14 o 1 8 2 835.59 850.71 12.33 o 2 8 2 151.76 166.19 2.55 o 3 8 2 376.25 384.79 7.08 o 4 8 2 1.42 1.01 0.24 o -4 9 2 1176.19 1235.49 21.33 o -3 9 2 138.92 137.49 2.65 o -2 9 2 1802.15 1743.80 29.90 o -1 9 2 4510.38 5019.77 78.94 o 0 9 2 867.40 776.20 10.57 o 1 9 2 1119.11 1112.02 16.05 o 2 9 2 33.36 25.33 0.80 o 3 9 2 0.82 0.69 0.21 o 4 9 2 1.78 2.54 0.44 o -4 10 2 2.70 2.92 0.44 o -3 10 2 75.39 70.08 1.48 o -2 10 2 215.05 211.39 3.85 o -1 10 2 183.34 177.08 2.98 o 0 10 2 146.70 165.20 2.65 o 1 10 2 9.37 9.52 0.28 o 2 10 2 0.08 1.18 0.44 o 3 10 2 159.91 152.06 2.99 o 4 10 2 121.69 122.82 2.77 o -4 11 2 18.45 14.04 0.66 o -3 11 2 87.77 87.49 1.75 o -2 11 2 28.99 28.49 0.72 o -1 11 2 0.40 1.54 0.17 o 0 11 2 5.88 4.25 0.16 o 1 11 2 188.36 195.30 2.96 o 2 11 2 159.18 160.87 2.74 o 3 11 2 23.66 22.62 0.69 o 4 11 2 4.84 5.94 0.51 o -4 12 2 58.11 59.51 1.83 o -3 12 2 67.28 66.60 1.40 o -2 12 2 250.86 232.91 3.94 o -1 12 2 18.91 16.85 0.52 o 0 12 2 63.59 57.46 0.96 o 1 12 2 700.10 748.13 12.07 o 2 12 2 54.90 51.59 1.28 o 3 12 2 24.28 25.21 0.79 o 4 12 2 187.38 198.80 4.40 o -3 13 2 31.58 25.40 0.69 o -2 13 2 691.94 694.33 12.03 o -1 13 2 104.87 107.03 1.89 o 0 13 2 196.12 201.95 3.37 o 1 13 2 642.90 628.24 11.47 o 2 13 2 33.62 31.66 0.85 o 3 13 2 14.46 14.75 0.59 o -3 14 2 0.19 0.71 0.20 o -2 14 2 86.53 72.65 1.59 o -1 14 2 34.36 28.68 0.79 o 0 14 2 2.08 1.87 0.31 o 1 14 2 900.25 889.44 14.29 o 2 14 2 52.91 53.71 1.25 o 3 14 2 8.38 9.83 0.45 o -3 15 2 186.71 190.26 3.55 o -2 15 2 491.37 546.84 9.57 o -1 15 2 765.14 825.10 13.30 o 0 15 2 1216.32 1278.43 26.06 o 1 15 2 43.56 46.46 0.99 o 2 15 2 34.69 33.90 1.03 o 3 15 2 0.59 0.81 0.28 o -3 16 2 0.06 0.20 0.21 o -2 16 2 68.42 74.29 1.57 o -1 16 2 7.02 5.99 0.39 o 0 16 2 78.58 84.96 2.09 o 1 16 2 9.01 8.98 0.42 o 2 16 2 107.60 111.78 2.33 o 3 16 2 28.48 27.87 1.24 o -2 17 2 0.03 0.18 0.20 o -1 17 2 24.96 26.55 0.73 o 0 17 2 63.08 55.05 1.42 o 1 17 2 15.09 16.37 0.62 o 2 17 2 15.62 16.01 0.62 o -2 18 2 67.60 63.89 1.55 o -1 18 2 13.86 11.82 0.58 o 0 18 2 123.85 118.10 2.84 o 1 18 2 128.57 146.65 3.89 o 2 18 2 79.80 77.94 2.15 o -1 19 2 17.82 15.15 0.76 o 0 19 2 3.69 3.97 0.51 o 1 19 2 196.06 212.02 5.16 o 0 20 2 0.74 2.00 0.33 o -5 1 3 3.85 4.88 0.51 o -4 1 3 317.17 334.58 5.93 o -3 1 3 609.52 630.97 12.59 o -2 1 3 187.03 172.13 2.76 o -1 1 3 423.27 372.34 5.30 o 0 1 3 2234.47 2321.07 31.50 o 1 1 3 48.11 53.68 0.87 o 2 1 3 1020.61 1044.77 14.21 o 3 1 3 15.78 15.95 0.42 o 4 1 3 6.69 6.90 0.39 o -5 2 3 11.98 13.30 0.76 o -4 2 3 80.46 80.52 1.60 o -3 2 3 49.25 46.11 1.07 o -2 2 3 39.45 29.17 0.51 o -1 2 3 811.99 771.55 11.59 o 0 2 3 2669.03 2878.44 41.70 o 1 2 3 1.14 2.48 0.17 o 2 2 3 938.43 952.76 12.97 o 3 2 3 5.85 4.89 0.23 o 4 2 3 2.36 2.77 0.24 o -5 3 3 5.82 6.68 0.51 o -4 3 3 4.76 4.63 0.36 o -3 3 3 1.35 0.92 0.16 o -2 3 3 199.80 228.47 3.20 o -1 3 3 676.76 750.39 10.74 o 0 3 3 231.72 205.96 2.85 o 1 3 3 208.62 234.43 3.46 o 2 3 3 19.08 17.02 0.48 o 3 3 3 0.07 0.22 0.18 o 4 3 3 0.09 -0.09 0.20 o -5 4 3 41.51 43.31 1.43 o -4 4 3 126.34 131.35 2.56 o -3 4 3 136.99 136.00 2.37 o -2 4 3 30.97 20.47 0.46 o -1 4 3 1020.03 961.85 13.73 o 0 4 3 3405.22 3653.58 49.36 o 1 4 3 96.43 98.30 1.50 o 2 4 3 537.39 499.67 6.84 o 3 4 3 2.60 2.51 0.19 o 4 4 3 23.44 26.19 0.93 o -5 5 3 4.26 5.79 0.95 o -4 5 3 60.79 62.94 1.40 o -3 5 3 744.45 776.67 12.41 o -2 5 3 11.56 17.34 0.34 o -1 5 3 851.12 838.51 12.00 o 0 5 3 833.52 880.60 12.00 o 1 5 3 147.44 138.09 2.26 o 2 5 3 114.46 104.75 1.52 o 3 5 3 0.66 0.74 0.18 o 4 5 3 15.99 15.15 0.66 o -4 6 3 52.64 52.95 1.25 o -3 6 3 8.76 8.91 0.67 o -2 6 3 48.59 51.46 0.92 o -1 6 3 33.01 34.30 0.61 o 0 6 3 561.53 593.47 8.11 o 1 6 3 234.60 240.69 3.36 o 2 6 3 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