#------------------------------------------------------------------------------ #$Date: 2009-06-07 09:06:07 +0300 (Sun, 07 Jun 2009) $ #$Revision: 754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017115.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017115_Fobs loop_ _publ_author_name 'Meng, Xiang-Gao' 'Cheng, Cui-Xia' 'Yan, Gang' _publ_section_title ; A two-dimensional network in the molecular salt 2-methylimidazolium hydrogen glutarate, and three-dimensional networks in the salts 2-methylimidazolium hydrogen succinate and 2-methylimidazolium hydrogen adipate monohydrate ; _journal_coeditor_code SK3296 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o217 _journal_page_last o221 _journal_volume 65 _journal_year 2009 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8017 _cell_length_b 8.1580 _cell_length_c 17.4380 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.7509 _[local]_cod_data_source_file sk3296Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Succ+2-MeIm in C m c 21' _shelx_refln_list_code 4 _shelx_F_calc_maximum 159.37 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25399.78 26617.64 237.38 o 4 0 0 7352.79 7723.24 82.34 o 6 0 0 605.85 604.84 9.92 o 8 0 0 35.77 28.94 3.41 o 1 1 0 4377.73 4768.52 30.40 o 3 1 0 318.67 285.35 3.77 o 5 1 0 87.79 78.69 2.26 o 7 1 0 59.93 52.27 2.46 o 9 1 0 9.28 10.71 5.35 o 2 2 0 2.55 2.07 0.36 o 4 2 0 104.65 98.56 3.66 o 6 2 0 81.43 70.86 3.03 o 8 2 0 12.87 16.04 2.14 o 1 3 0 10.68 11.68 0.73 o 3 3 0 265.82 272.87 3.01 o 5 3 0 97.67 93.81 3.73 o 7 3 0 0.02 2.09 1.30 o 0 4 0 55.01 54.81 3.49 o 2 4 0 543.31 566.04 4.89 o 4 4 0 6.60 6.34 0.94 o 6 4 0 0.05 -0.37 0.98 o 8 4 0 0.28 1.63 2.31 o 1 5 0 26.10 27.68 1.36 o 3 5 0 22.62 19.37 1.14 o 5 5 0 0.03 -0.36 0.84 o 7 5 0 1.01 -1.09 1.85 o 0 6 0 820.36 832.79 9.90 o 2 6 0 303.76 287.61 3.95 o 4 6 0 130.35 122.67 2.84 o 6 6 0 76.24 78.12 3.96 o 1 7 0 867.18 856.83 8.13 o 3 7 0 636.31 614.26 7.87 o 5 7 0 106.80 105.58 3.80 o 0 8 0 292.57 271.87 5.79 o 2 8 0 309.36 286.80 4.34 o 4 8 0 79.49 88.18 4.08 o 1 9 0 1.38 0.70 1.16 o 3 9 0 3.15 2.50 1.74 o 5 9 0 0.00 -0.87 4.50 o 0 10 0 217.31 205.08 14.51 o 2 10 0 173.46 184.25 5.99 o 1 1 1 70.02 63.97 0.62 o 3 1 1 122.59 117.06 1.46 o 5 1 1 4.46 5.89 0.63 o 7 1 1 11.70 12.51 1.08 o 9 1 1 1.52 -0.33 3.98 o 0 2 1 3639.35 4155.14 22.89 o 2 2 1 1788.79 1957.94 8.28 o 4 2 1 350.99 321.71 2.62 o 6 2 1 46.54 44.09 1.64 o 8 2 1 14.58 13.00 1.44 o 1 3 1 2769.56 3053.85 18.68 o 3 3 1 588.85 626.97 3.92 o 5 3 1 41.14 39.82 1.31 o 7 3 1 2.52 3.26 0.96 o 0 4 1 146.03 120.44 1.85 o 2 4 1 691.23 723.80 4.41 o 4 4 1 52.03 54.69 1.35 o 6 4 1 18.64 18.74 1.59 o 8 4 1 7.35 2.96 1.63 o 1 5 1 247.19 250.67 2.26 o 3 5 1 217.52 209.27 2.15 o 5 5 1 2.51 2.00 0.66 o 7 5 1 2.02 0.41 1.21 o 0 6 1 618.59 566.63 5.42 o 2 6 1 360.73 335.36 3.53 o 4 6 1 148.91 142.41 2.18 o 6 6 1 57.01 55.43 2.50 o 1 7 1 171.29 165.16 2.17 o 3 7 1 113.09 112.24 2.02 o 5 7 1 12.50 13.92 1.47 o 0 8 1 20.49 20.97 1.58 o 2 8 1 30.07 31.75 1.49 o 4 8 1 1.53 1.20 1.06 o 1 9 1 26.94 29.25 1.58 o 3 9 1 8.24 7.56 1.51 o 5 9 1 9.47 9.62 3.66 o 0 10 1 239.86 245.05 14.07 o 2 10 1 153.79 160.01 3.86 o 0 0 2 2610.64 3051.96 37.89 o 2 0 2 16952.15 17393.65 95.98 o 4 0 2 1147.97 1249.42 9.12 o 6 0 2 529.72 495.90 6.79 o 8 0 2 184.65 161.51 4.24 o 1 1 2 4020.79 3955.63 16.08 o 3 1 2 79.25 80.28 0.97 o 5 1 2 74.08 84.53 1.75 o 7 1 2 8.70 10.54 1.08 o 0 2 2 3802.37 4184.20 23.09 o 2 2 2 2901.65 2973.52 12.08 o 4 2 2 359.81 333.58 2.69 o 6 2 2 5.05 5.72 0.80 o 8 2 2 0.58 -0.20 1.19 o 1 3 2 2796.51 3205.71 13.44 o 3 3 2 1421.28 1463.81 6.92 o 5 3 2 109.33 108.35 1.87 o 7 3 2 29.83 29.53 1.54 o 0 4 2 607.14 700.30 5.91 o 2 4 2 804.47 841.53 4.72 o 4 4 2 40.73 43.77 1.17 o 6 4 2 3.93 5.02 0.89 o 8 4 2 1.71 1.10 1.74 o 1 5 2 1065.38 1094.88 5.75 o 3 5 2 449.08 415.93 3.25 o 5 5 2 45.55 46.34 1.67 o 7 5 2 2.83 1.08 1.35 o 0 6 2 277.00 269.98 3.49 o 2 6 2 254.47 255.34 2.46 o 4 6 2 99.93 97.95 2.22 o 6 6 2 19.92 16.61 2.22 o 1 7 2 992.83 940.75 6.45 o 3 7 2 347.80 328.64 4.14 o 5 7 2 214.10 209.96 3.47 o 0 8 2 282.65 260.58 4.29 o 2 8 2 134.42 137.65 2.53 o 4 8 2 73.07 74.90 2.34 o 6 8 2 7.00 7.32 6.53 o 1 9 2 8.32 8.08 1.18 o 3 9 2 5.31 5.16 1.41 o 5 9 2 0.92 0.78 3.43 o 0 10 2 77.37 85.29 5.77 o 2 10 2 55.74 62.34 3.54 o 1 1 3 1111.88 1190.13 5.58 o 3 1 3 139.67 132.17 1.22 o 5 1 3 84.98 77.22 1.54 o 7 1 3 2.38 2.41 0.87 o 0 2 3 193.69 200.87 1.86 o 2 2 3 18.65 20.01 0.52 o 4 2 3 64.05 63.01 1.13 o 6 2 3 20.95 23.64 1.19 o 8 2 3 6.31 5.86 1.51 o 1 3 3 652.94 710.71 4.42 o 3 3 3 173.48 162.38 1.87 o 5 3 3 79.58 79.90 1.65 o 7 3 3 9.60 9.34 1.26 o 0 4 3 113.34 123.01 1.86 o 2 4 3 172.30 171.65 1.71 o 4 4 3 8.99 8.43 0.67 o 6 4 3 5.01 5.25 0.97 o 8 4 3 3.04 2.53 2.04 o 1 5 3 92.39 97.36 1.45 o 3 5 3 24.37 26.04 0.96 o 5 5 3 35.87 33.71 1.49 o 7 5 3 0.10 0.62 1.33 o 0 6 3 179.51 163.60 2.80 o 2 6 3 241.83 219.85 2.28 o 4 6 3 65.25 65.53 1.97 o 6 6 3 20.39 24.65 1.90 o 1 7 3 284.43 284.02 2.95 o 3 7 3 53.43 58.23 1.71 o 5 7 3 69.42 73.61 2.58 o 0 8 3 183.24 188.76 6.09 o 2 8 3 42.79 44.19 1.64 o 4 8 3 26.10 28.06 2.07 o 6 8 3 1.44 2.17 3.86 o 1 9 3 46.50 49.54 2.17 o 3 9 3 23.37 27.48 1.87 o 0 10 3 44.78 44.10 3.37 o 2 10 3 62.16 66.62 2.93 o 0 0 4 18948.96 19555.23 231.13 o 2 0 4 1676.20 1695.27 10.14 o 4 0 4 1324.85 1326.85 9.69 o 6 0 4 158.10 149.49 8.42 o 8 0 4 20.63 10.70 3.45 o 1 1 4 236.44 256.15 2.02 o 3 1 4 20.85 21.36 0.60 o 5 1 4 5.61 4.57 0.61 o 7 1 4 27.47 26.91 1.43 o 0 2 4 481.13 572.15 3.98 o 2 2 4 291.83 291.47 1.92 o 4 2 4 64.50 58.39 1.06 o 6 2 4 12.41 12.37 0.96 o 8 2 4 3.09 1.44 1.38 o 1 3 4 5680.80 6178.42 24.85 o 3 3 4 1392.65 1514.26 7.36 o 5 3 4 297.81 295.16 3.14 o 7 3 4 33.61 34.89 1.81 o 0 4 4 354.94 371.21 3.53 o 2 4 4 301.91 323.70 2.41 o 4 4 4 42.10 42.58 1.31 o 6 4 4 35.83 35.37 1.69 o 8 4 4 8.13 8.36 2.49 o 1 5 4 504.56 495.29 3.30 o 3 5 4 228.18 227.06 2.49 o 5 5 4 85.03 78.69 2.14 o 7 5 4 7.82 9.07 1.68 o 0 6 4 121.80 115.87 2.23 o 2 6 4 70.99 65.91 1.52 o 4 6 4 32.31 36.57 1.72 o 6 6 4 26.91 32.90 2.12 o 1 7 4 331.62 306.60 3.99 o 3 7 4 243.01 222.04 2.97 o 5 7 4 64.65 69.46 2.29 o 0 8 4 15.99 16.42 1.89 o 2 8 4 2.30 1.79 0.83 o 4 8 4 0.23 0.80 1.08 o 1 9 4 11.08 12.56 1.45 o 3 9 4 6.33 7.84 1.58 o 0 10 4 146.13 157.89 6.32 o 2 10 4 84.90 94.28 3.50 o 1 1 5 19.52 20.78 0.52 o 3 1 5 35.29 31.10 0.68 o 5 1 5 2.02 1.89 0.53 o 7 1 5 0.37 -0.37 0.94 o 0 2 5 331.54 364.59 2.84 o 2 2 5 69.93 67.43 0.84 o 4 2 5 21.33 20.38 0.86 o 6 2 5 4.47 3.36 0.84 o 8 2 5 1.53 2.14 1.41 o 1 3 5 361.70 357.37 2.77 o 3 3 5 243.76 227.25 1.94 o 5 3 5 22.85 24.90 1.27 o 7 3 5 17.29 19.36 1.60 o 0 4 5 535.39 562.10 4.66 o 2 4 5 477.09 465.43 3.03 o 4 4 5 20.75 21.99 1.10 o 6 4 5 1.93 1.61 0.93 o 8 4 5 2.70 1.25 2.56 o 1 5 5 46.55 48.21 1.00 o 3 5 5 51.25 52.44 1.39 o 5 5 5 6.45 7.01 1.01 o 7 5 5 4.07 3.62 1.54 o 0 6 5 175.39 159.62 2.84 o 2 6 5 118.52 120.12 2.12 o 4 6 5 21.68 22.73 1.41 o 6 6 5 16.03 19.07 1.89 o 1 7 5 153.52 152.05 2.45 o 3 7 5 153.06 150.45 2.48 o 5 7 5 3.67 2.93 1.18 o 0 8 5 35.08 37.47 2.59 o 2 8 5 93.16 90.90 2.57 o 4 8 5 6.52 8.31 1.30 o 1 9 5 58.07 58.80 2.41 o 3 9 5 14.36 17.19 1.85 o 0 10 5 105.67 104.76 4.74 o 2 10 5 42.67 45.42 2.89 o 0 0 6 208.19 194.45 2.97 o 2 0 6 676.63 674.31 6.15 o 4 0 6 73.82 81.64 2.22 o 6 0 6 57.15 59.05 2.31 o 8 0 6 18.16 11.92 3.96 o 1 1 6 129.09 141.63 1.29 o 3 1 6 21.65 22.37 0.62 o 5 1 6 32.24 34.03 1.17 o 7 1 6 0.51 -0.26 0.89 o 0 2 6 346.14 366.02 3.18 o 2 2 6 393.36 416.43 2.71 o 4 2 6 43.00 37.69 0.94 o 6 2 6 1.28 1.69 0.79 o 8 2 6 0.50 1.08 1.46 o 1 3 6 1303.05 1438.04 7.16 o 3 3 6 594.84 567.13 3.87 o 5 3 6 117.76 122.33 2.30 o 7 3 6 50.20 45.85 2.16 o 0 4 6 1062.78 1162.03 8.01 o 2 4 6 728.56 693.38 4.45 o 4 4 6 163.72 162.70 4.54 o 6 4 6 27.45 25.32 1.66 o 1 5 6 343.56 367.18 3.64 o 3 5 6 180.53 177.30 2.35 o 5 5 6 10.33 11.43 1.14 o 7 5 6 1.53 1.09 1.50 o 0 6 6 356.56 333.48 6.72 o 2 6 6 196.50 198.55 3.81 o 4 6 6 26.74 33.07 1.62 o 6 6 6 6.10 7.15 1.51 o 1 7 6 381.41 332.73 4.25 o 3 7 6 182.53 172.65 2.81 o 5 7 6 52.07 52.93 2.85 o 0 8 6 4.45 3.21 1.43 o 2 8 6 3.78 5.18 1.15 o 4 8 6 0.34 -0.93 1.10 o 1 9 6 4.19 4.29 1.29 o 3 9 6 1.92 1.41 1.50 o 0 10 6 40.49 41.85 3.55 o 2 10 6 41.58 47.12 3.77 o 1 1 7 2410.02 2629.93 10.74 o 3 1 7 580.67 566.62 3.41 o 5 1 7 71.55 78.13 1.65 o 7 1 7 0.71 0.42 0.97 o 0 2 7 1467.98 1614.12 10.58 o 2 2 7 365.67 402.65 3.41 o 4 2 7 103.07 91.13 1.88 o 6 2 7 0.26 0.42 0.75 o 8 2 7 2.62 1.52 1.55 o 1 3 7 716.15 766.15 4.66 o 3 3 7 122.63 124.13 1.64 o 5 3 7 51.67 49.73 1.78 o 7 3 7 2.62 4.04 1.26 o 0 4 7 718.79 740.97 6.20 o 2 4 7 96.49 93.25 1.68 o 4 4 7 44.72 40.62 1.37 o 6 4 7 3.10 4.11 1.10 o 1 5 7 153.08 164.70 2.21 o 3 5 7 83.84 83.49 1.66 o 5 5 7 2.27 3.93 0.95 o 7 5 7 0.38 1.05 1.56 o 0 6 7 195.52 208.93 4.43 o 2 6 7 238.33 219.41 3.02 o 4 6 7 32.04 38.21 1.81 o 6 6 7 4.92 6.10 1.55 o 1 7 7 14.21 10.10 1.12 o 3 7 7 11.31 12.49 1.15 o 5 7 7 17.33 15.30 1.61 o 0 8 7 101.82 84.08 3.62 o 2 8 7 65.13 62.44 2.35 o 4 8 7 26.22 19.35 3.37 o 1 9 7 19.24 19.15 1.78 o 3 9 7 10.07 9.84 1.82 o 0 10 7 90.82 93.86 5.81 o 2 10 7 77.57 73.43 8.59 o 0 0 8 935.06 892.96 10.36 o 2 0 8 161.79 146.92 1.91 o 4 0 8 16.72 17.45 1.06 o 6 0 8 14.30 17.73 2.05 o 8 0 8 14.53 2.45 2.63 o 1 1 8 591.64 648.83 3.32 o 3 1 8 234.02 248.23 1.99 o 5 1 8 23.97 23.10 1.19 o 7 1 8 4.44 4.43 1.38 o 0 2 8 167.58 155.61 1.91 o 2 2 8 83.50 74.15 1.28 o 4 2 8 6.59 7.81 0.66 o 6 2 8 1.66 1.21 0.88 o 8 2 8 2.74 -1.95 3.67 o 1 3 8 248.57 244.35 2.22 o 3 3 8 82.42 77.39 1.43 o 5 3 8 95.88 95.07 2.44 o 7 3 8 20.47 17.38 1.76 o 0 4 8 689.99 677.54 13.12 o 2 4 8 552.37 546.19 4.11 o 4 4 8 147.68 144.35 2.28 o 6 4 8 56.67 58.64 2.30 o 1 5 8 75.29 81.94 1.89 o 3 5 8 21.29 21.18 1.12 o 5 5 8 0.96 0.23 0.85 o 7 5 8 0.33 -0.01 1.55 o 0 6 8 190.06 182.20 4.22 o 2 6 8 186.11 174.05 3.11 o 4 6 8 37.15 40.73 1.80 o 6 6 8 6.68 5.32 1.64 o 1 7 8 35.98 39.23 1.86 o 3 7 8 20.86 21.81 1.69 o 5 7 8 11.20 9.28 1.55 o 0 8 8 50.86 54.77 3.23 o 2 8 8 51.47 51.19 2.24 o 4 8 8 4.73 2.25 1.68 o 1 9 8 51.04 48.50 2.55 o 3 9 8 17.01 14.72 1.97 o 1 1 9 1125.06 1153.27 5.36 o 3 1 9 647.38 661.00 4.22 o 5 1 9 39.82 37.72 1.60 o 7 1 9 13.44 15.09 1.78 o 0 2 9 160.51 159.44 2.02 o 2 2 9 88.28 84.18 1.42 o 4 2 9 3.29 3.59 0.60 o 6 2 9 13.02 18.42 1.45 o 8 2 9 5.06 9.62 6.45 o 1 3 9 328.96 356.84 3.07 o 3 3 9 20.95 20.49 0.92 o 5 3 9 26.40 31.03 2.37 o 7 3 9 16.66 13.73 2.84 o 0 4 9 705.24 667.02 7.88 o 2 4 9 169.45 160.53 2.18 o 4 4 9 129.33 134.47 2.26 o 6 4 9 19.57 18.67 1.90 o 1 5 9 34.24 36.68 1.51 o 3 5 9 40.17 42.42 1.45 o 5 5 9 6.19 6.34 1.18 o 7 5 9 1.45 3.15 2.40 o 0 6 9 144.93 129.69 3.64 o 2 6 9 8.70 7.08 1.01 o 4 6 9 43.01 45.66 1.94 o 6 6 9 12.76 15.97 2.04 o 1 7 9 26.42 29.92 1.71 o 3 7 9 11.54 9.14 1.39 o 5 7 9 4.14 5.45 1.85 o 0 8 9 70.81 69.24 3.54 o 2 8 9 30.12 24.59 1.83 o 4 8 9 11.53 9.15 1.90 o 1 9 9 35.49 30.80 3.26 o 3 9 9 3.68 5.84 2.68 o 0 0 10 750.50 796.50 8.12 o 2 0 10 70.39 83.38 1.61 o 4 0 10 93.74 101.55 3.80 o 6 0 10 22.20 27.76 2.91 o 1 1 10 260.28 277.90 1.94 o 3 1 10 75.00 74.18 1.46 o 5 1 10 28.33 31.66 1.75 o 7 1 10 1.36 1.88 1.35 o 0 2 10 378.71 344.47 3.55 o 2 2 10 114.14 107.77 1.54 o 4 2 10 52.84 50.47 1.40 o 6 2 10 19.74 25.56 1.90 o 8 2 10 3.14 6.48 6.18 o 1 3 10 205.29 206.04 2.27 o 3 3 10 274.77 261.32 3.13 o 5 3 10 47.87 46.83 1.75 o 7 3 10 28.40 21.60 4.84 o 0 4 10 310.25 303.36 4.98 o 2 4 10 108.05 96.62 1.82 o 4 4 10 151.43 140.95 2.43 o 6 4 10 44.38 44.57 2.30 o 1 5 10 87.74 89.40 2.08 o 3 5 10 24.13 24.09 1.50 o 5 5 10 2.31 2.20 1.09 o 7 5 10 3.83 4.01 4.18 o 0 6 10 49.08 45.07 2.59 o 2 6 10 3.41 2.14 0.89 o 4 6 10 24.68 25.18 1.88 o 6 6 10 12.92 11.94 2.08 o 1 7 10 0.54 -0.13 0.93 o 3 7 10 8.53 7.39 1.38 o 5 7 10 1.61 4.07 1.84 o 0 8 10 66.91 64.56 3.92 o 2 8 10 68.38 60.45 3.95 o 4 8 10 15.32 11.64 2.19 o 1 9 10 1.12 -0.39 1.53 o 3 9 10 1.43 0.92 5.64 o 1 1 11 572.20 657.12 4.23 o 3 1 11 71.38 72.24 1.51 o 5 1 11 56.06 60.97 2.30 o 7 1 11 1.89 2.49 1.61 o 0 2 11 1126.85 1077.16 24.48 o 2 2 11 259.46 242.14 2.87 o 4 2 11 126.58 125.38 2.09 o 6 2 11 9.21 12.75 1.50 o 1 3 11 230.32 219.99 3.25 o 3 3 11 136.36 134.02 2.18 o 5 3 11 46.32 47.91 1.82 o 7 3 11 12.92 8.62 2.79 o 0 4 11 708.26 611.63 7.75 o 2 4 11 959.62 920.00 7.66 o 4 4 11 213.31 213.67 3.09 o 6 4 11 71.46 76.90 3.47 o 1 5 11 15.02 14.62 1.15 o 3 5 11 44.83 51.99 1.93 o 5 5 11 4.01 3.82 1.20 o 0 6 11 59.19 51.81 2.83 o 2 6 11 171.26 162.75 4.87 o 4 6 11 27.13 30.08 2.92 o 6 6 11 8.06 10.14 4.29 o 1 7 11 13.55 13.74 1.45 o 3 7 11 3.84 6.29 1.42 o 5 7 11 0.62 -2.71 2.82 o 0 8 11 42.35 39.86 5.39 o 2 8 11 9.90 7.32 1.56 o 4 8 11 5.68 6.59 3.99 o 1 9 11 23.38 14.26 5.24 o 0 0 12 117.16 101.83 2.81 o 2 0 12 212.96 215.30 5.42 o 4 0 12 13.26 13.93 1.62 o 6 0 12 0.12 -0.64 1.74 o 1 1 12 23.63 26.72 0.87 o 3 1 12 6.07 5.43 0.69 o 5 1 12 13.59 15.74 1.77 o 7 1 12 1.78 2.55 1.87 o 0 2 12 241.85 212.56 3.82 o 2 2 12 287.96 262.33 2.97 o 4 2 12 86.48 88.40 1.84 o 6 2 12 23.08 23.57 2.06 o 1 3 12 232.72 220.21 3.34 o 3 3 12 95.92 89.90 1.87 o 5 3 12 154.95 155.66 3.87 o 7 3 12 32.86 35.79 4.14 o 0 4 12 396.42 391.07 6.11 o 2 4 12 539.09 515.65 5.42 o 4 4 12 115.06 110.29 2.56 o 6 4 12 26.73 21.96 2.69 o 1 5 12 183.94 176.04 3.01 o 3 5 12 63.88 68.09 2.18 o 5 5 12 7.37 7.55 1.63 o 0 6 12 179.61 168.68 4.47 o 2 6 12 229.69 209.12 3.55 o 4 6 12 39.70 35.71 2.34 o 1 7 12 90.46 97.89 2.85 o 3 7 12 68.40 78.61 3.30 o 5 7 12 2.24 5.80 5.69 o 0 8 12 55.49 53.85 4.74 o 2 8 12 28.57 27.80 3.32 o 1 9 12 18.38 13.53 6.97 o 1 1 13 84.65 67.72 1.35 o 3 1 13 0.35 1.60 0.64 o 5 1 13 51.44 62.90 2.65 o 7 1 13 1.49 2.03 1.87 o 0 2 13 177.18 183.89 3.66 o 2 2 13 226.08 229.85 3.67 o 4 2 13 49.62 50.12 1.83 o 6 2 13 30.40 33.06 2.40 o 1 3 13 371.45 349.80 3.93 o 3 3 13 175.14 178.11 2.90 o 5 3 13 46.49 52.13 2.42 o 7 3 13 8.91 7.02 3.40 o 0 4 13 1223.38 1197.27 12.63 o 2 4 13 507.06 474.33 5.69 o 4 4 13 262.16 259.83 4.15 o 6 4 13 49.58 55.33 3.34 o 1 5 13 58.07 57.67 2.03 o 3 5 13 9.49 8.10 1.19 o 5 5 13 19.36 20.61 2.15 o 0 6 13 210.69 203.46 5.05 o 2 6 13 94.42 98.19 2.66 o 4 6 13 33.18 39.05 2.71 o 1 7 13 152.41 158.97 3.46 o 3 7 13 45.35 48.21 2.56 o 0 8 13 45.84 33.28 7.48 o 2 8 13 3.47 2.78 1.60 o 0 0 14 253.51 221.64 10.30 o 2 0 14 421.40 344.39 5.70 o 4 0 14 36.86 36.39 2.49 o 6 0 14 0.65 0.50 2.08 o 1 1 14 92.81 92.38 2.14 o 3 1 14 65.63 75.98 2.01 o 5 1 14 8.64 9.01 1.52 o 7 1 14 8.14 12.40 3.69 o 0 2 14 447.16 412.67 11.50 o 2 2 14 193.90 194.75 2.86 o 4 2 14 72.91 72.19 2.52 o 6 2 14 14.45 16.18 2.26 o 1 3 14 856.33 828.19 6.81 o 3 3 14 616.68 599.56 6.59 o 5 3 14 99.58 94.77 3.00 o 0 4 14 66.72 70.62 2.88 o 2 4 14 7.63 6.67 1.02 o 4 4 14 40.62 40.86 2.05 o 6 4 14 18.95 22.42 4.77 o 1 5 14 32.52 33.51 1.73 o 3 5 14 15.93 19.07 1.52 o 5 5 14 23.01 26.64 2.51 o 0 6 14 121.14 115.74 4.09 o 2 6 14 26.24 26.49 1.76 o 4 6 14 10.21 9.39 1.89 o 1 7 14 194.82 196.77 4.60 o 3 7 14 59.30 70.15 2.98 o 0 8 14 21.95 15.34 4.38 o 2 8 14 21.00 17.24 5.21 o 1 1 15 447.75 368.50 6.40 o 3 1 15 335.82 318.82 4.60 o 5 1 15 27.38 30.83 2.49 o 0 2 15 23.99 24.86 1.80 o 2 2 15 120.29 129.85 3.05 o 4 2 15 20.87 20.58 1.92 o 6 2 15 1.54 3.76 2.02 o 1 3 15 150.14 155.88 2.72 o 3 3 15 93.93 102.97 2.79 o 5 3 15 35.46 39.30 3.51 o 0 4 15 338.36 329.75 6.01 o 2 4 15 290.78 297.55 4.05 o 4 4 15 77.41 83.58 3.13 o 1 5 15 1.63 3.28 1.07 o 3 5 15 12.85 15.98 1.70 o 5 5 15 2.09 0.88 2.85 o 0 6 15 26.55 27.41 2.67 o 2 6 15 6.07 9.91 1.44 o 4 6 15 8.11 9.73 2.00 o 1 7 15 118.01 117.08 3.93 o 3 7 15 102.08 111.40 4.98 o 0 0 16 402.96 366.45 14.64 o 2 0 16 26.35 26.40 3.57 o 4 0 16 124.55 134.54 4.96 o 6 0 16 39.43 44.44 5.16 o 1 1 16 320.72 312.78 5.66 o 3 1 16 123.86 113.60 3.65 o 5 1 16 26.22 28.56 2.67 o 0 2 16 179.42 182.28 7.42 o 2 2 16 57.55 59.90 3.22 o 4 2 16 10.26 13.07 1.91 o 6 2 16 3.22 6.54 2.31 o 1 3 16 232.98 234.95 3.47 o 3 3 16 73.15 82.50 2.94 o 5 3 16 93.67 99.48 4.69 o 0 4 16 45.44 46.69 3.32 o 2 4 16 105.83 104.09 2.57 o 4 4 16 15.02 12.39 2.01 o 1 5 16 128.71 127.26 3.48 o 3 5 16 83.59 86.14 4.32 o 5 5 16 11.62 12.72 4.37 o 0 6 16 20.28 20.78 2.60 o 2 6 16 2.78 2.66 1.40 o 4 6 16 2.93 6.12 3.22 o 1 7 16 79.92 91.78 4.99 o 3 7 16 73.78 74.32 10.30 o 1 1 17 168.17 147.04 4.74 o 3 1 17 70.13 65.20 3.37 o 5 1 17 60.81 71.77 7.16 o 0 2 17 0.64 0.28 2.32 o 2 2 17 7.49 6.08 1.38 o 4 2 17 1.66 1.53 1.48 o 1 3 17 154.24 150.15 3.54 o 3 3 17 63.72 70.67 3.09 o 5 3 17 19.27 19.52 3.03 o 0 4 17 83.12 82.42 4.59 o 2 4 17 8.82 8.34 1.47 o 4 4 17 11.68 12.32 2.56 o 1 5 17 58.84 56.59 2.37 o 3 5 17 21.91 19.50 2.24 o 0 6 17 19.91 21.39 2.79 o 2 6 17 11.72 13.39 1.86 o 1 7 17 67.18 71.28 5.41 o 0 0 18 908.81 857.73 25.68 o 2 0 18 848.41 834.59 28.17 o 4 0 18 194.56 196.86 12.20 o 1 1 18 35.08 38.15 3.13 o 3 1 18 11.77 12.84 3.98 o 5 1 18 5.60 6.54 3.23 o 0 2 18 18.93 25.14 4.53 o 2 2 18 4.88 6.25 1.52 o 4 2 18 1.95 2.81 1.87 o 1 3 18 68.47 68.56 3.09 o 3 3 18 50.02 47.33 2.75 o 5 3 18 8.78 14.15 7.13 o 0 4 18 17.74 17.65 2.46 o 2 4 18 7.00 9.36 1.70 o 4 4 18 2.14 3.80 2.29 o 1 5 18 2.62 3.59 1.43 o 3 5 18 0.32 0.29 1.95 o 0 6 18 21.94 29.28 3.31 o 2 6 18 33.23 45.82 3.78 o 1 1 19 76.52 69.74 4.07 o 3 1 19 50.56 46.09 5.07 o 5 1 19 20.01 20.70 4.50 o 0 2 19 74.80 66.09 11.01 o 2 2 19 41.45 37.16 3.39 o 4 2 19 5.32 1.56 2.21 o 1 3 19 75.63 77.10 5.93 o 3 3 19 24.13 24.85 3.16 o 0 4 19 18.92 18.29 4.42 o 2 4 19 1.85 0.91 1.80 o 4 4 19 2.56 2.23 4.48 o 1 5 19 9.19 8.93 2.21 o 3 5 19 3.44 3.90 6.59 o 0 6 19 48.13 46.71 4.76 o 0 0 20 194.14 194.61 12.99 o 2 0 20 89.77 105.12 7.21 o 4 0 20 67.63 67.46 9.19 o 1 1 20 62.42 62.78 4.14 o 3 1 20 29.32 27.03 3.59 o 0 2 20 41.25 45.35 5.51 o 2 2 20 15.21 12.60 2.89 o 4 2 20 3.02 4.74 3.98 o 1 3 20 26.15 29.66 4.59 o 3 3 20 10.78 11.63 3.63 o 0 4 20 21.08 4.65 6.24 o 2 4 20 5.10 7.22 2.22 o 1 5 20 34.41 35.53 5.40 o 1 1 21 14.63 18.76 3.17 o 3 1 21 21.15 31.90 3.96 o 0 2 21 3.00 2.76 3.86 o 2 2 21 21.76 22.95 3.46 o 1 3 21 13.25 8.51 4.97 o 0 0 22 4.22 2.90 5.42 o 2 0 22 3.01 1.79 6.02 o 1 1 22 21.50 23.64 4.02 o 2 2 22 7.94 11.03 7.51 o