#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:16:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180842 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/73/2017309.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017309_Fobs loop_ _publ_author_name 'Omondi, Bernard' 'Levendis, Demetrius C.' 'Layh, Marcus' 'Fernandes, Manuel A.' _publ_section_title ; Two polymorphs of N-(2,6-difluorophenyl)formamide ; _journal_coeditor_code GZ3168 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o470 _journal_page_last o475 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.698 _cell_angle_gamma 90.000 _cell_length_a 4.4680 _cell_length_b 8.4860 _cell_length_c 8.8810 _exptl_crystal_F_000 160.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file gz3168Ibsup3.hkl _cod_data_source_block Ib #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6b_bo12_s in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 67.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 802.30 747.70 5.91 o 2 0 0 552.51 581.75 4.65 o 3 0 0 405.08 427.81 3.73 o 4 0 0 10.19 10.00 0.85 o 5 0 0 0.45 -0.53 1.65 o 1 1 0 36.70 31.37 0.93 o 2 1 0 11.42 9.79 0.33 o 3 1 0 44.85 46.22 0.70 o 4 1 0 44.33 42.69 0.98 o 5 1 0 3.88 3.18 1.10 o 0 2 0 275.29 294.40 2.89 o 1 2 0 250.94 242.11 1.46 o 2 2 0 79.34 78.42 0.85 o 3 2 0 13.93 14.66 0.56 o 4 2 0 3.44 1.64 0.69 o 5 2 0 1.33 -0.85 1.22 o 1 3 0 414.80 415.32 2.64 o 2 3 0 115.89 117.36 1.20 o 3 3 0 151.80 144.63 1.53 o 4 3 0 60.92 59.99 1.36 o 5 3 0 17.34 17.37 1.60 o 0 4 0 286.53 297.08 4.07 o 1 4 0 178.88 197.95 1.60 o 2 4 0 167.19 175.67 1.67 o 3 4 0 28.88 26.77 0.96 o 4 4 0 50.09 51.27 1.31 o 5 4 0 17.65 20.67 1.93 o 1 5 0 182.17 194.43 1.74 o 2 5 0 57.37 60.41 0.85 o 3 5 0 19.75 20.52 0.98 o 4 5 0 17.37 18.37 1.16 o 5 5 0 42.11 41.43 1.69 o 0 6 0 90.13 91.54 2.19 o 1 6 0 5.95 7.16 0.66 o 2 6 0 25.76 25.75 0.74 o 3 6 0 1.72 1.49 0.71 o 4 6 0 0.62 -0.47 0.89 o 1 7 0 26.63 25.45 1.05 o 2 7 0 48.41 44.67 1.29 o 3 7 0 1.94 1.63 0.78 o 4 7 0 28.26 29.19 1.42 o 0 8 0 148.14 144.21 3.46 o 1 8 0 13.69 12.26 0.87 o 2 8 0 57.33 57.28 1.55 o 3 8 0 7.48 6.74 0.90 o 4 8 0 22.76 27.43 1.77 o 1 9 0 25.62 21.80 1.74 o 2 9 0 25.70 28.12 1.48 o 3 9 0 8.36 9.63 1.20 o 0 10 0 3.24 5.85 1.04 o 1 10 0 11.60 11.12 1.30 o 2 10 0 1.73 0.93 1.13 o 1 11 0 9.28 12.61 2.53 o -5 0 1 18.01 17.21 2.19 o -4 0 1 65.14 61.39 1.26 o -3 0 1 102.93 96.02 1.31 o -2 0 1 311.08 298.96 3.82 o -1 0 1 95.34 78.14 0.80 o 0 0 1 2.88 3.25 0.17 o 1 0 1 145.27 152.29 1.44 o 2 0 1 464.48 453.70 3.84 o 3 0 1 30.94 30.47 1.08 o 4 0 1 8.49 7.82 0.88 o 5 0 1 28.76 27.88 5.37 o -5 1 1 2.68 2.14 1.15 o -4 1 1 43.68 41.97 0.90 o -3 1 1 39.70 41.30 0.70 o -2 1 1 49.18 50.51 0.60 o -1 1 1 1231.52 1203.02 5.65 o 0 1 1 722.78 713.47 3.24 o 1 1 1 659.75 621.44 3.08 o 2 1 1 17.88 19.75 0.46 o 3 1 1 15.24 18.66 0.57 o 4 1 1 32.57 30.90 0.96 o 5 1 1 28.42 29.52 2.38 o -5 2 1 15.83 15.57 1.43 o -4 2 1 43.94 42.64 1.07 o -3 2 1 116.40 110.37 1.15 o -2 2 1 49.55 40.86 0.63 o -1 2 1 860.97 884.16 4.30 o 0 2 1 227.08 224.07 1.65 o 1 2 1 313.67 316.06 2.04 o 2 2 1 97.14 100.14 0.89 o 3 2 1 20.75 19.25 0.60 o 4 2 1 23.95 24.09 1.02 o 5 2 1 0.90 0.10 1.75 o -5 3 1 3.53 3.23 1.04 o -4 3 1 102.97 100.25 1.56 o -3 3 1 24.34 24.24 0.70 o -2 3 1 67.59 70.78 0.86 o -1 3 1 491.45 513.56 2.96 o 0 3 1 298.88 310.30 2.44 o 1 3 1 100.43 109.06 0.84 o 2 3 1 38.91 41.86 0.63 o 3 3 1 124.84 122.85 1.42 o 4 3 1 37.30 35.82 1.12 o 5 3 1 11.03 10.21 1.31 o -5 4 1 6.51 7.13 1.16 o -4 4 1 150.17 149.91 2.02 o -3 4 1 158.35 153.81 1.65 o -2 4 1 13.44 13.22 0.50 o -1 4 1 451.30 486.25 3.24 o 0 4 1 560.82 577.68 5.72 o 1 4 1 66.22 73.02 0.82 o 2 4 1 139.24 139.71 1.38 o 3 4 1 286.69 280.32 2.73 o 4 4 1 21.73 21.97 1.21 o 5 4 1 24.91 25.40 1.72 o -5 5 1 11.93 13.75 1.63 o -4 5 1 3.19 2.98 0.90 o -3 5 1 61.83 60.22 1.36 o -2 5 1 9.23 9.22 0.50 o -1 5 1 34.72 35.57 0.74 o 0 5 1 173.60 193.67 2.56 o 1 5 1 37.03 39.10 0.86 o 2 5 1 12.46 13.90 0.58 o 3 5 1 154.23 149.96 2.29 o 4 5 1 6.52 7.48 1.15 o 5 5 1 12.99 11.44 1.73 o -4 6 1 1.98 1.88 0.90 o -3 6 1 21.01 21.55 0.94 o -2 6 1 7.96 7.16 0.55 o -1 6 1 1.22 0.25 0.55 o 0 6 1 43.09 44.39 1.19 o 1 6 1 95.87 96.50 1.35 o 2 6 1 1.29 0.88 0.54 o 3 6 1 14.03 14.65 1.11 o 4 6 1 19.64 22.06 1.30 o -4 7 1 4.42 4.91 1.35 o -3 7 1 20.13 19.44 1.41 o -2 7 1 2.64 0.10 0.65 o -1 7 1 25.33 25.33 1.06 o 0 7 1 141.23 137.51 1.98 o 1 7 1 162.18 162.34 2.20 o 2 7 1 23.44 23.22 0.93 o 3 7 1 13.33 14.38 1.02 o 4 7 1 10.23 9.40 1.19 o -4 8 1 5.10 5.30 1.50 o -3 8 1 5.08 4.78 0.86 o -2 8 1 145.78 143.07 2.49 o -1 8 1 26.23 27.84 1.20 o 0 8 1 23.66 24.19 1.08 o 1 8 1 207.24 197.69 3.55 o 2 8 1 22.27 22.40 1.18 o 3 8 1 0.73 -0.12 0.81 o -3 9 1 7.75 7.46 1.60 o -2 9 1 21.12 23.84 1.36 o -1 9 1 17.68 20.15 1.46 o 0 9 1 22.20 23.77 1.25 o 1 9 1 11.16 12.27 1.34 o 2 9 1 2.68 2.71 1.02 o 3 9 1 9.11 12.18 1.57 o -2 10 1 14.07 12.37 1.80 o -1 10 1 21.13 21.98 1.59 o 0 10 1 0.25 1.64 1.32 o 1 10 1 5.39 2.49 1.09 o 2 10 1 4.89 4.92 1.09 o -1 11 1 1.15 1.31 3.90 o 0 11 1 2.41 0.87 1.33 o -5 0 2 0.85 -0.30 3.89 o -4 0 2 30.75 30.61 1.01 o -3 0 2 46.20 49.33 0.95 o -2 0 2 3.23 5.94 0.40 o -1 0 2 4513.09 4116.59 24.13 o 0 0 2 881.51 825.54 5.15 o 1 0 2 17.50 17.00 0.69 o 2 0 2 291.95 328.15 2.71 o 3 0 2 13.76 18.13 0.84 o 4 0 2 0.99 -0.15 1.10 o 5 0 2 4.79 6.81 2.55 o -5 1 2 14.33 15.22 1.14 o -4 1 2 3.61 4.34 0.63 o -3 1 2 97.61 90.07 0.90 o -2 1 2 182.02 182.59 1.22 o -1 1 2 1540.03 1442.53 6.00 o 0 1 2 115.17 108.45 0.93 o 1 1 2 260.45 261.83 1.42 o 2 1 2 238.95 248.94 1.66 o 3 1 2 134.77 128.60 1.32 o 4 1 2 12.49 13.42 0.79 o 5 1 2 7.06 8.84 1.39 o -5 2 2 28.19 31.36 1.21 o -4 2 2 68.32 67.21 1.25 o -3 2 2 64.43 65.34 0.92 o -2 2 2 103.78 106.36 0.93 o -1 2 2 636.02 619.89 2.77 o 0 2 2 1456.33 1438.26 6.90 o 1 2 2 9.74 13.74 0.34 o 2 2 2 137.84 147.72 1.44 o 3 2 2 29.96 31.16 0.76 o 4 2 2 10.46 11.87 0.81 o 5 2 2 3.52 2.24 1.15 o -5 3 2 23.04 23.55 1.55 o -4 3 2 29.32 27.43 1.02 o -3 3 2 25.39 25.08 0.75 o -2 3 2 104.48 109.33 0.97 o -1 3 2 22.31 21.75 0.38 o 0 3 2 5.35 5.00 0.24 o 1 3 2 705.00 742.33 4.91 o 2 3 2 6.37 7.36 0.41 o 3 3 2 54.80 53.03 1.00 o 4 3 2 183.14 179.28 2.34 o 5 3 2 0.42 -1.50 1.50 o -5 4 2 7.75 6.77 1.43 o -4 4 2 8.68 7.17 0.86 o -3 4 2 30.68 31.07 0.87 o -2 4 2 113.83 120.11 1.20 o -1 4 2 132.11 144.10 1.00 o 0 4 2 9.96 10.70 0.38 o 1 4 2 77.12 88.61 0.92 o 2 4 2 189.41 190.43 1.89 o 3 4 2 42.28 41.35 1.09 o 4 4 2 50.83 46.69 1.43 o 5 4 2 8.39 7.89 1.73 o -5 5 2 3.16 2.37 1.40 o -4 5 2 6.62 6.84 0.90 o -3 5 2 27.36 24.46 1.04 o -2 5 2 3.58 4.15 0.45 o -1 5 2 108.39 109.51 1.11 o 0 5 2 75.62 77.94 1.34 o 1 5 2 124.62 126.69 1.25 o 2 5 2 89.44 92.09 1.42 o 3 5 2 3.13 3.60 0.90 o 4 5 2 45.10 46.13 1.74 o -4 6 2 16.87 18.85 1.10 o -3 6 2 25.44 25.96 1.18 o -2 6 2 92.70 88.26 1.46 o -1 6 2 93.50 94.04 1.51 o 0 6 2 187.37 194.93 2.43 o 1 6 2 27.68 27.54 0.76 o 2 6 2 80.23 79.88 1.49 o 3 6 2 1.36 1.84 0.90 o 4 6 2 11.35 13.86 1.35 o -4 7 2 14.57 14.97 1.51 o -3 7 2 28.43 28.00 1.21 o -2 7 2 8.82 7.28 0.79 o -1 7 2 6.55 7.14 0.75 o 0 7 2 48.58 50.61 1.36 o 1 7 2 92.92 93.45 1.49 o 2 7 2 7.78 8.67 0.79 o 3 7 2 28.57 30.88 1.47 o 4 7 2 11.56 12.70 1.98 o -4 8 2 0.61 0.72 1.13 o -3 8 2 15.05 15.36 1.37 o -2 8 2 8.56 10.61 1.25 o -1 8 2 28.61 29.60 1.36 o 0 8 2 29.48 31.24 1.46 o 1 8 2 0.33 0.94 0.70 o 2 8 2 0.03 -0.80 0.80 o 3 8 2 7.40 7.82 1.39 o -3 9 2 28.90 28.24 1.82 o -2 9 2 8.41 8.44 0.94 o -1 9 2 16.12 20.05 1.69 o 0 9 2 13.14 14.63 1.18 o 1 9 2 5.11 5.37 0.95 o 2 9 2 5.23 3.52 1.23 o 3 9 2 18.14 25.56 3.61 o -2 10 2 6.04 5.52 1.04 o -1 10 2 9.28 7.42 1.70 o 0 10 2 71.35 71.64 2.30 o 1 10 2 5.24 4.27 1.30 o 2 10 2 2.84 5.61 1.52 o 0 11 2 2.35 2.63 1.44 o -5 0 3 2.16 -1.76 1.76 o -4 0 3 34.97 33.29 1.06 o -3 0 3 0.28 -0.45 0.45 o -2 0 3 114.91 106.89 1.18 o -1 0 3 61.13 58.33 0.73 o 0 0 3 11.67 12.02 0.46 o 1 0 3 180.73 174.48 1.92 o 2 0 3 56.40 51.41 1.00 o 3 0 3 0.49 -0.36 0.56 o 4 0 3 73.37 68.10 2.25 o 5 0 3 16.07 20.66 3.36 o -5 1 3 23.62 23.93 1.42 o -4 1 3 3.70 4.34 0.60 o -3 1 3 16.50 16.59 0.53 o -2 1 3 273.84 282.16 1.55 o -1 1 3 29.29 28.81 0.43 o 0 1 3 1243.69 1186.19 5.30 o 1 1 3 362.59 376.40 1.99 o 2 1 3 29.69 30.09 0.63 o 3 1 3 44.07 47.32 0.88 o 4 1 3 36.03 33.94 1.14 o 5 1 3 6.66 8.31 2.09 o -5 2 3 49.21 50.69 1.62 o -4 2 3 87.77 88.18 1.38 o -3 2 3 26.28 24.59 0.68 o -2 2 3 903.24 903.53 4.28 o -1 2 3 239.98 239.01 1.26 o 0 2 3 243.10 233.08 1.28 o 1 2 3 180.04 181.42 1.16 o 2 2 3 9.85 9.76 0.46 o 3 2 3 52.58 46.81 1.16 o 4 2 3 26.91 27.83 1.06 o 5 2 3 5.60 8.81 3.54 o -5 3 3 20.10 22.00 1.23 o -4 3 3 11.42 10.98 0.83 o -3 3 3 23.84 24.47 0.74 o -2 3 3 28.72 29.57 0.62 o -1 3 3 209.90 209.22 1.27 o 0 3 3 100.33 108.85 0.90 o 1 3 3 338.64 367.89 2.31 o 2 3 3 60.55 60.17 0.85 o 3 3 3 114.16 112.00 1.47 o 4 3 3 23.88 26.32 1.45 o 5 3 3 2.09 4.27 3.39 o -5 4 3 1.41 0.59 1.07 o -4 4 3 23.85 22.88 1.28 o -3 4 3 80.64 77.18 1.19 o -2 4 3 10.51 12.05 0.53 o -1 4 3 33.22 34.81 0.58 o 0 4 3 108.22 111.57 1.00 o 1 4 3 17.38 16.96 0.56 o 2 4 3 6.56 7.31 0.60 o 3 4 3 29.22 27.89 0.96 o 4 4 3 6.01 5.75 0.94 o -5 5 3 2.22 0.43 1.07 o -4 5 3 36.89 36.20 1.67 o -3 5 3 6.65 7.33 0.80 o -2 5 3 2.28 2.16 0.47 o -1 5 3 46.67 48.17 0.72 o 0 5 3 38.62 37.86 0.65 o 1 5 3 63.09 63.28 0.89 o 2 5 3 236.24 232.12 2.75 o 3 5 3 9.72 12.01 0.92 o 4 5 3 10.23 14.20 1.33 o -4 6 3 22.50 22.38 1.70 o -3 6 3 1.49 0.69 0.86 o -2 6 3 2.38 2.02 0.49 o -1 6 3 92.83 100.18 1.28 o 0 6 3 278.20 283.12 2.24 o 1 6 3 6.37 7.10 0.58 o 2 6 3 97.41 95.23 1.57 o 3 6 3 29.12 29.38 1.44 o 4 6 3 1.17 0.39 1.29 o -4 7 3 2.90 1.60 1.01 o -3 7 3 27.09 22.30 1.63 o -2 7 3 29.12 25.71 1.23 o -1 7 3 41.79 40.50 1.27 o 0 7 3 280.61 277.50 2.85 o 1 7 3 23.47 25.14 0.98 o 2 7 3 2.34 0.74 0.78 o 3 7 3 33.41 31.38 2.66 o 4 7 3 5.78 5.44 2.47 o -4 8 3 4.15 6.08 1.81 o -3 8 3 12.21 11.10 0.94 o -2 8 3 6.29 5.84 1.04 o -1 8 3 7.09 6.65 0.80 o 0 8 3 34.71 32.20 1.54 o 1 8 3 4.42 4.58 0.78 o 2 8 3 5.39 6.27 0.91 o 3 8 3 0.58 0.34 1.14 o -3 9 3 7.41 6.95 1.20 o -2 9 3 3.61 3.62 1.64 o -1 9 3 2.06 1.94 0.93 o 0 9 3 2.64 1.54 1.03 o 1 9 3 18.56 16.09 1.08 o 2 9 3 18.69 19.15 1.39 o -2 10 3 7.36 6.71 1.10 o -1 10 3 7.53 8.44 1.73 o 0 10 3 0.83 0.05 1.45 o 1 10 3 19.96 22.39 1.42 o -5 0 4 0.38 -0.18 1.84 o -4 0 4 7.41 9.01 0.77 o -3 0 4 101.25 105.94 1.39 o -2 0 4 3.68 4.36 0.48 o -1 0 4 8.94 8.22 0.47 o 0 0 4 926.76 894.82 5.81 o 1 0 4 4.39 3.75 0.44 o 2 0 4 44.75 46.32 1.34 o 3 0 4 8.82 9.96 0.90 o 4 0 4 1.58 2.93 2.32 o 5 0 4 10.25 18.41 4.13 o -5 1 4 4.52 4.57 1.33 o -4 1 4 9.95 11.05 0.70 o -3 1 4 84.55 85.79 0.95 o -2 1 4 152.14 153.24 1.05 o -1 1 4 34.14 33.72 0.48 o 0 1 4 6.32 7.22 0.28 o 1 1 4 83.76 84.53 0.78 o 2 1 4 71.42 68.93 0.91 o 3 1 4 105.47 97.46 1.35 o 4 1 4 10.56 12.00 1.08 o 5 1 4 0.01 -0.94 1.54 o -5 2 4 23.57 26.76 1.91 o -4 2 4 18.67 19.91 0.89 o -3 2 4 34.41 34.16 0.75 o -2 2 4 374.42 359.21 1.99 o -1 2 4 133.12 126.73 0.90 o 0 2 4 202.40 209.82 1.25 o 1 2 4 105.46 118.02 0.95 o 2 2 4 93.51 87.99 1.03 o 3 2 4 43.34 44.23 1.08 o 4 2 4 6.50 8.07 1.07 o -5 3 4 2.83 2.82 1.11 o -4 3 4 14.03 14.60 0.82 o -3 3 4 209.26 211.56 1.81 o -2 3 4 57.58 60.59 0.74 o -1 3 4 155.14 153.02 1.10 o 0 3 4 83.53 87.54 0.83 o 1 3 4 129.53 124.84 1.18 o 2 3 4 3.90 4.25 0.47 o 3 3 4 267.10 250.05 2.44 o 4 3 4 14.72 16.05 1.11 o -5 4 4 2.09 2.40 1.30 o -4 4 4 7.95 7.31 0.81 o -3 4 4 12.65 10.88 0.75 o -2 4 4 42.16 41.66 0.87 o -1 4 4 112.27 111.36 1.10 o 0 4 4 54.11 55.74 0.81 o 1 4 4 91.61 97.24 1.27 o 2 4 4 4.25 3.53 0.56 o 3 4 4 13.74 15.10 0.83 o 4 4 4 1.66 2.71 1.62 o -5 5 4 2.83 2.89 1.01 o -4 5 4 31.07 31.31 1.34 o -3 5 4 53.71 53.59 1.52 o -2 5 4 31.80 32.64 0.94 o -1 5 4 230.33 223.66 2.00 o 0 5 4 36.70 36.09 0.75 o 1 5 4 251.92 241.76 2.31 o 2 5 4 47.41 47.18 1.34 o 3 5 4 20.70 22.01 1.21 o 4 5 4 42.01 43.82 2.59 o -4 6 4 6.24 5.78 1.28 o -3 6 4 11.30 10.22 0.88 o -2 6 4 38.75 39.45 1.32 o -1 6 4 43.37 43.16 1.00 o 0 6 4 51.17 53.04 1.06 o 1 6 4 55.52 57.96 1.32 o 2 6 4 5.20 6.65 0.97 o 3 6 4 16.39 15.57 1.40 o 4 6 4 1.89 0.91 1.35 o -4 7 4 18.69 18.26 1.76 o -3 7 4 3.36 2.17 0.78 o -2 7 4 5.09 6.47 0.83 o -1 7 4 56.88 57.12 1.47 o 0 7 4 8.89 9.10 0.81 o 1 7 4 73.88 72.43 1.36 o 2 7 4 17.98 16.27 1.09 o 3 7 4 0.10 0.22 1.11 o -3 8 4 8.29 7.78 1.00 o -2 8 4 3.47 3.35 0.95 o -1 8 4 9.77 7.98 0.89 o 0 8 4 44.58 43.90 1.91 o 1 8 4 10.04 10.20 1.03 o 2 8 4 0.73 -0.48 0.76 o 3 8 4 1.02 0.96 1.42 o -3 9 4 2.53 1.24 1.15 o -2 9 4 0.18 -0.88 0.88 o -1 9 4 1.78 1.43 0.88 o 0 9 4 1.85 1.08 0.78 o 1 9 4 7.79 6.66 1.01 o 2 9 4 2.22 2.75 1.17 o -2 10 4 7.87 7.82 1.20 o -1 10 4 51.36 51.41 2.55 o 0 10 4 5.76 4.05 1.15 o 1 10 4 15.96 17.08 1.27 o -5 0 5 16.62 18.92 2.41 o -4 0 5 47.12 47.68 2.57 o -3 0 5 33.12 34.17 1.01 o -2 0 5 112.45 111.51 1.35 o -1 0 5 75.38 69.33 1.07 o 0 0 5 39.90 39.10 0.80 o 1 0 5 49.31 50.53 0.97 o 2 0 5 30.17 28.30 0.97 o 3 0 5 44.56 47.25 1.91 o 4 0 5 0.40 -0.68 1.75 o -5 1 5 0.35 -1.07 1.07 o -4 1 5 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