#------------------------------------------------------------------------------ #$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $ #$Revision: 840 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017321.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017321_Fobs loop_ _publ_author_name 'Gerdes, Allison' 'Bond, Marcus R.' _publ_section_title ; Octakis(dimethylammonium) hexa-\m~2~-chlorido-hexachloridotrinickelate(II) dichloride: a linear trinickel complex with asymmetric bridging ; _journal_coeditor_code DN3125 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m398 _journal_page_last m400 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.464 _cell_angle_gamma 90.000 _cell_length_a 10.0058 _cell_length_b 20.0564 _cell_length_c 10.9787 _exptl_crystal_F_000 1076.00 _reflns_d_resolution_high 0.5001 _[local]_cod_data_source_file dn3125Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dmanicl in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 312.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 4277.24 4022.17 61.72 o 4 0 0 6584.25 6484.57 106.09 o 5 0 0 19748.44 19190.43 298.37 o 6 0 0 3336.93 3303.77 57.98 o 7 0 0 42.47 60.75 7.92 o 8 0 0 1472.40 1409.02 28.13 o 9 0 0 2658.42 2673.28 49.31 o 10 0 0 6464.99 6252.14 107.01 o 11 0 0 349.86 364.01 13.86 o 12 0 0 3235.41 3149.99 53.02 o 13 0 0 839.78 866.91 21.85 o 14 0 0 1986.32 1976.33 38.87 o 15 0 0 142.15 150.07 16.47 o 16 0 0 209.93 216.91 20.77 o 17 0 0 427.19 374.94 45.73 o 18 0 0 2711.90 3118.23 127.43 o 19 0 0 152.47 184.09 41.36 o 2 1 0 8.82 34.91 4.56 o 3 1 0 4341.41 4420.50 51.14 o 4 1 0 18.58 22.98 2.58 o 5 1 0 332.82 355.86 7.90 o 6 1 0 258.34 270.59 10.64 o 7 1 0 1332.63 1321.60 21.91 o 8 1 0 496.03 486.34 10.03 o 9 1 0 194.51 196.67 7.44 o 10 1 0 1246.79 1226.71 18.49 o 11 1 0 164.26 164.01 7.68 o 12 1 0 305.89 290.86 9.82 o 13 1 0 1113.13 1111.60 18.30 o 14 1 0 823.43 820.98 16.47 o 15 1 0 70.78 86.08 17.92 o 16 1 0 94.16 102.54 14.83 o 17 1 0 1.23 33.84 21.92 o 18 1 0 0.35 -10.33 85.66 o 19 1 0 34.16 50.82 22.05 o 3 2 0 1250.28 1225.78 15.25 o 4 2 0 14489.38 14253.69 157.44 o 5 2 0 7051.75 6847.52 78.47 o 6 2 0 2200.70 2124.75 26.25 o 7 2 0 75.21 84.77 12.46 o 8 2 0 273.56 275.29 7.15 o 9 2 0 1054.73 1056.30 16.03 o 10 2 0 34.18 56.51 10.94 o 11 2 0 1003.66 1014.87 16.79 o 12 2 0 18.00 39.49 7.30 o 13 2 0 5.08 31.69 11.24 o 14 2 0 40.42 40.61 11.38 o 15 2 0 25.86 32.70 10.90 o 16 2 0 403.23 437.74 57.43 o 17 2 0 694.42 678.03 50.75 o 18 2 0 788.26 791.00 37.69 o 19 2 0 430.30 355.65 30.15 o 2 3 0 2263.27 2286.56 29.11 o 3 3 0 3493.69 3448.03 38.93 o 4 3 0 15147.23 15131.47 213.12 o 5 3 0 8035.64 7885.82 85.53 o 6 3 0 692.91 703.69 9.86 o 7 3 0 78.72 109.54 8.51 o 8 3 0 2367.33 2335.98 30.47 o 9 3 0 352.97 352.40 7.91 o 10 3 0 1001.68 966.02 14.92 o 11 3 0 860.24 850.79 14.57 o 12 3 0 154.25 159.52 9.12 o 13 3 0 4252.35 4268.05 58.78 o 14 3 0 840.34 812.97 18.83 o 15 3 0 1381.01 1467.71 27.21 o 16 3 0 1152.76 1127.91 26.93 o 17 3 0 66.04 62.66 27.03 o 18 3 0 482.36 428.38 31.67 o 19 3 0 369.63 363.30 46.49 o 1 4 0 38.57 24.83 3.65 o 2 4 0 1811.39 1804.36 20.78 o 3 4 0 4202.30 4196.28 46.54 o 4 4 0 38679.18 37947.64 423.14 o 5 4 0 23.65 40.17 4.86 o 6 4 0 557.72 543.19 8.16 o 7 4 0 1059.09 999.06 13.70 o 8 4 0 116.71 123.49 6.99 o 9 4 0 3238.38 3208.70 39.21 o 10 4 0 836.28 810.41 13.43 o 11 4 0 169.75 192.01 31.29 o 12 4 0 32.13 43.04 16.10 o 13 4 0 41.24 50.02 11.10 o 14 4 0 5292.54 5422.27 73.85 o 15 4 0 249.96 259.57 25.22 o 16 4 0 526.10 539.62 33.43 o 17 4 0 16.24 -12.39 34.63 o 18 4 0 316.61 318.64 28.84 o 19 4 0 304.88 246.66 26.87 o 1 5 0 2407.67 2518.75 45.66 o 2 5 0 7999.68 8417.41 102.39 o 3 5 0 2307.33 2342.90 26.76 o 4 5 0 4329.94 4372.61 48.47 o 5 5 0 215.15 220.17 4.86 o 6 5 0 1903.46 1831.75 21.75 o 7 5 0 846.33 802.59 11.72 o 8 5 0 2865.18 2787.52 33.99 o 9 5 0 600.69 590.06 10.65 o 10 5 0 131.15 131.85 15.19 o 11 5 0 1970.27 2007.11 28.82 o 12 5 0 14.26 36.56 9.85 o 13 5 0 2687.61 2663.49 44.14 o 14 5 0 400.27 465.93 17.44 o 15 5 0 0.37 14.88 18.22 o 16 5 0 123.83 127.95 38.88 o 17 5 0 267.33 265.83 26.43 o 18 5 0 503.32 454.78 25.91 o 19 5 0 0.19 -12.51 27.94 o 0 6 0 5.54 14.09 1.57 o 1 6 0 3899.88 3916.21 67.64 o 2 6 0 15400.65 15697.10 171.81 o 3 6 0 25471.67 25678.04 292.66 o 4 6 0 5265.20 5346.54 59.55 o 5 6 0 1738.63 1741.44 20.61 o 6 6 0 264.58 242.19 5.47 o 7 6 0 29.54 41.87 8.81 o 8 6 0 1948.38 1896.54 24.01 o 9 6 0 76.90 87.03 10.94 o 10 6 0 1664.31 1655.73 32.25 o 11 6 0 436.39 431.39 17.62 o 12 6 0 91.62 102.69 9.47 o 13 6 0 546.40 559.16 18.35 o 14 6 0 2105.91 2196.97 59.03 o 15 6 0 2433.40 2434.42 41.11 o 16 6 0 2.03 4.53 30.07 o 17 6 0 344.42 390.12 20.81 o 18 6 0 31.75 49.02 18.42 o 19 6 0 1.29 -21.75 21.75 o 1 7 0 19226.56 19703.09 235.39 o 2 7 0 4344.42 4450.79 66.93 o 3 7 0 3023.24 2978.53 32.90 o 4 7 0 5388.97 5402.81 75.17 o 5 7 0 1743.75 1739.56 21.88 o 6 7 0 3468.28 3440.43 38.38 o 7 7 0 2274.49 2166.94 26.35 o 8 7 0 4453.75 4366.02 51.25 o 9 7 0 525.07 522.60 17.93 o 10 7 0 116.80 110.90 11.24 o 11 7 0 1386.97 1388.58 30.41 o 12 7 0 189.00 187.43 20.66 o 13 7 0 10.35 33.32 17.62 o 14 7 0 532.07 561.48 19.02 o 15 7 0 326.82 349.86 50.13 o 16 7 0 277.75 257.45 17.90 o 17 7 0 2781.34 2973.19 59.22 o 18 7 0 46.17 47.12 21.87 o 19 7 0 380.80 326.83 41.32 o 0 8 0 123.48 126.61 13.98 o 1 8 0 2701.32 2880.07 40.66 o 2 8 0 16017.58 16527.83 178.51 o 3 8 0 6116.61 6276.08 67.30 o 4 8 0 645.20 605.57 8.62 o 5 8 0 5172.04 5083.03 58.89 o 6 8 0 2108.56 2023.81 25.35 o 7 8 0 4569.71 4495.98 123.43 o 8 8 0 3334.86 3201.07 40.84 o 9 8 0 6.63 21.85 7.59 o 10 8 0 5862.34 5713.58 74.53 o 11 8 0 101.90 110.11 10.74 o 12 8 0 59.35 59.26 11.39 o 13 8 0 5.19 -11.07 11.07 o 14 8 0 96.53 107.30 30.68 o 15 8 0 1305.04 1295.76 30.27 o 16 8 0 65.54 76.11 19.14 o 17 8 0 99.67 108.69 18.90 o 18 8 0 629.76 639.69 67.77 o 19 8 0 1.15 45.60 32.20 o 1 9 0 16674.66 16683.05 309.88 o 2 9 0 11461.02 11469.62 122.22 o 3 9 0 1646.69 1569.35 25.29 o 4 9 0 481.91 440.75 10.34 o 5 9 0 4.48 21.58 3.20 o 6 9 0 4192.37 4154.03 49.00 o 7 9 0 2979.89 2904.55 35.58 o 8 9 0 157.87 178.04 6.65 o 9 9 0 820.68 785.97 13.66 o 10 9 0 964.27 959.54 19.18 o 11 9 0 152.70 163.35 10.70 o 12 9 0 6.91 10.40 9.72 o 13 9 0 70.93 74.75 12.88 o 14 9 0 112.84 131.11 13.87 o 15 9 0 27.28 28.00 23.39 o 16 9 0 287.49 234.76 20.36 o 17 9 0 407.98 438.39 22.41 o 18 9 0 18.03 4.97 22.66 o 19 9 0 55.16 74.47 21.46 o 0 10 0 4808.70 5209.02 230.93 o 1 10 0 16742.28 17022.92 287.61 o 2 10 0 2936.07 2952.30 68.11 o 3 10 0 2013.52 2028.14 24.10 o 4 10 0 6141.94 6146.49 97.84 o 5 10 0 4095.21 4068.85 47.21 o 6 10 0 7317.18 7345.33 84.01 o 7 10 0 1504.77 1549.84 34.08 o 8 10 0 72.98 60.33 14.88 o 9 10 0 198.91 180.48 8.13 o 10 10 0 2298.84 2368.38 36.71 o 11 10 0 11220.91 11392.48 150.59 o 12 10 0 2560.27 2565.53 72.45 o 13 10 0 23.41 46.83 14.28 o 14 10 0 27.11 68.54 15.31 o 15 10 0 667.99 666.98 22.89 o 16 10 0 17.70 -16.78 54.07 o 17 10 0 122.09 152.67 40.40 o 18 10 0 301.57 288.00 22.65 o 19 10 0 128.81 138.21 27.25 o 1 11 0 1891.50 1904.70 23.30 o 2 11 0 358.76 388.28 20.06 o 3 11 0 12934.77 12702.33 138.66 o 4 11 0 669.48 670.75 14.29 o 5 11 0 2067.25 1989.69 23.90 o 6 11 0 1032.45 1016.12 14.27 o 7 11 0 7212.57 7012.17 79.27 o 8 11 0 1.23 11.95 8.20 o 9 11 0 945.80 936.11 18.24 o 10 11 0 1355.85 1362.53 23.26 o 11 11 0 1482.89 1560.50 27.83 o 12 11 0 79.29 111.27 12.56 o 13 11 0 1374.56 1429.67 28.18 o 14 11 0 164.25 133.38 13.60 o 15 11 0 6.94 -3.17 15.46 o 16 11 0 253.94 239.91 52.86 o 17 11 0 264.89 305.72 21.42 o 18 11 0 0.44 -4.67 45.56 o 19 11 0 1.57 -32.46 94.77 o 0 12 0 983.98 979.89 16.17 o 1 12 0 1049.68 1072.05 46.55 o 2 12 0 180.33 174.10 15.50 o 3 12 0 1912.87 1966.83 23.04 o 4 12 0 230.63 234.28 5.47 o 5 12 0 119.92 112.80 4.92 o 6 12 0 14494.80 13934.49 154.24 o 7 12 0 9077.94 8799.41 161.72 o 8 12 0 7.43 7.00 5.51 o 9 12 0 96.04 103.27 16.10 o 10 12 0 52.97 27.86 10.33 o 11 12 0 2882.56 2879.75 40.84 o 12 12 0 3425.50 3427.81 50.17 o 13 12 0 36.07 30.37 12.15 o 14 12 0 0.93 4.16 12.19 o 15 12 0 179.33 158.51 32.20 o 16 12 0 30.22 23.26 35.54 o 17 12 0 787.07 787.78 75.37 o 18 12 0 162.81 167.84 73.21 o 19 12 0 21.63 70.47 46.78 o 1 13 0 71.42 82.90 3.95 o 2 13 0 4165.53 4104.63 56.24 o 3 13 0 179.56 201.66 10.63 o 4 13 0 2114.28 2165.61 25.78 o 5 13 0 5164.60 5047.36 56.42 o 6 13 0 313.69 320.11 18.54 o 7 13 0 4633.37 4583.81 54.97 o 8 13 0 200.74 212.14 22.18 o 9 13 0 536.45 537.49 11.62 o 10 13 0 215.10 231.33 12.76 o 11 13 0 2.95 21.40 20.05 o 12 13 0 678.53 654.68 24.01 o 13 13 0 264.84 260.57 32.81 o 14 13 0 4.08 7.46 13.04 o 15 13 0 3.66 3.04 18.83 o 16 13 0 445.04 434.50 25.89 o 17 13 0 60.33 37.37 20.43 o 18 13 0 19.91 -4.70 26.43 o 0 14 0 1430.13 1425.93 74.27 o 1 14 0 2243.67 2312.11 30.54 o 2 14 0 1215.26 1177.99 17.34 o 3 14 0 4239.64 4247.19 50.16 o 4 14 0 296.16 294.17 11.24 o 5 14 0 2746.20 2682.52 30.95 o 6 14 0 1199.86 1207.50 36.20 o 7 14 0 2936.27 2839.28 36.48 o 8 14 0 1819.98 1771.50 25.00 o 9 14 0 64.51 61.53 7.54 o 10 14 0 682.65 682.72 22.19 o 11 14 0 738.97 724.03 15.79 o 12 14 0 1591.89 1577.63 49.58 o 13 14 0 1028.13 1035.13 24.93 o 14 14 0 38.57 50.53 15.49 o 15 14 0 566.06 495.32 26.00 o 16 14 0 190.91 122.73 21.91 o 17 14 0 31.49 36.45 19.96 o 18 14 0 91.91 82.01 41.92 o 1 15 0 694.60 712.94 23.11 o 2 15 0 3483.81 3488.94 47.13 o 3 15 0 5979.67 5893.60 68.96 o 4 15 0 545.03 534.34 10.33 o 5 15 0 1916.40 1795.76 40.49 o 6 15 0 17.25 21.27 9.42 o 7 15 0 13634.57 13417.31 353.29 o 8 15 0 222.85 236.52 11.24 o 9 15 0 146.85 157.63 8.37 o 10 15 0 884.89 881.14 31.61 o 11 15 0 869.92 927.89 21.58 o 12 15 0 303.97 274.37 16.48 o 13 15 0 1033.70 1135.00 25.64 o 14 15 0 2.15 16.32 22.17 o 15 15 0 121.49 83.84 21.89 o 16 15 0 210.64 193.82 22.56 o 17 15 0 3.76 5.96 21.94 o 18 15 0 117.05 63.60 41.01 o 0 16 0 1956.65 1981.51 34.43 o 1 16 0 774.23 779.30 16.11 o 2 16 0 3023.89 3004.36 42.99 o 3 16 0 7792.04 7704.61 96.78 o 4 16 0 1177.41 1189.49 18.22 o 5 16 0 3.78 9.47 5.16 o 6 16 0 1314.30 1307.88 19.89 o 7 16 0 336.59 307.72 31.90 o 8 16 0 4794.21 4698.10 94.90 o 9 16 0 2416.94 2390.77 36.63 o 10 16 0 678.96 668.76 18.86 o 11 16 0 186.48 194.14 15.19 o 12 16 0 628.32 628.20 19.40 o 13 16 0 1615.48 1668.57 32.43 o 14 16 0 334.88 297.75 20.87 o 15 16 0 564.01 553.05 27.31 o 16 16 0 213.63 223.59 24.41 o 17 16 0 113.15 123.03 24.79 o 18 16 0 338.70 341.94 27.25 o 1 17 0 343.40 357.11 16.41 o 2 17 0 210.50 201.74 6.53 o 3 17 0 939.31 903.72 30.41 o 4 17 0 2.39 19.43 9.72 o 5 17 0 177.66 197.89 12.76 o 6 17 0 3413.44 3379.18 46.52 o 7 17 0 119.68 118.70 7.48 o 8 17 0 0.34 2.53 7.66 o 9 17 0 777.72 739.51 16.37 o 10 17 0 546.09 508.91 44.06 o 11 17 0 196.01 207.64 36.15 o 12 17 0 1039.51 1005.22 87.86 o 13 17 0 427.15 493.02 70.49 o 14 17 0 17.40 16.40 18.23 o 15 17 0 109.05 69.87 23.10 o 16 17 0 459.72 429.98 27.75 o 17 17 0 84.33 85.95 37.06 o 0 18 0 433.19 416.95 11.97 o 1 18 0 156.69 167.08 12.46 o 2 18 0 216.53 226.89 22.79 o 3 18 0 993.58 999.75 21.59 o 4 18 0 2652.80 2615.29 36.40 o 5 18 0 33.46 47.82 6.73 o 6 18 0 46.05 47.43 14.28 o 7 18 0 2140.99 2095.89 33.39 o 8 18 0 4034.07 3981.40 60.82 o 9 18 0 2774.18 2797.68 124.84 o 10 18 0 16.37 7.21 23.39 o 11 18 0 1.07 -1.42 11.41 o 12 18 0 29.83 26.65 38.27 o 13 18 0 2.60 -2.69 13.34 o 14 18 0 8.86 23.08 17.01 o 15 18 0 143.49 134.88 22.52 o 16 18 0 276.67 324.27 26.95 o 17 18 0 201.95 206.99 91.74 o 1 19 0 65.17 81.79 6.30 o 2 19 0 2941.91 2944.54 56.07 o 3 19 0 203.45 217.61 12.46 o 4 19 0 350.79 350.66 16.10 o 5 19 0 2961.54 2904.32 54.84 o 6 19 0 2282.78 2213.26 35.99 o 7 19 0 1719.56 1671.07 27.59 o 8 19 0 100.13 93.49 17.01 o 9 19 0 70.63 83.33 24.61 o 10 19 0 2462.47 2478.32 42.58 o 11 19 0 2620.89 2686.27 82.79 o 12 19 0 1342.11 1337.84 29.57 o 13 19 0 958.90 943.51 30.67 o 14 19 0 1406.59 1409.02 41.96 o 15 19 0 103.81 119.66 24.30 o 16 19 0 268.77 356.22 51.04 o 17 19 0 174.26 206.61 73.52 o 0 20 0 6318.42 6285.08 130.26 o 1 20 0 1815.48 1839.29 30.91 o 2 20 0 27.88 43.94 7.07 o 3 20 0 0.29 12.45 6.27 o 4 20 0 1.37 18.86 13.36 o 5 20 0 51.11 51.24 10.94 o 6 20 0 651.74 654.76 21.58 o 7 20 0 37.70 33.20 9.05 o 8 20 0 589.95 544.81 14.41 o 9 20 0 1692.66 1659.14 28.74 o 10 20 0 289.25 276.51 30.08 o 11 20 0 472.32 495.79 44.67 o 12 20 0 972.62 994.31 83.59 o 13 20 0 153.18 132.45 15.25 o 14 20 0 7.52 8.78 17.30 o 15 20 0 64.98 35.05 35.24 o 16 20 0 34.11 48.45 51.64 o 17 20 0 262.61 289.21 28.31 o 1 21 0 1317.36 1316.44 26.48 o 2 21 0 5835.22 5727.88 99.43 o 3 21 0 14.96 31.29 24.00 o 4 21 0 3451.15 3437.98 86.25 o 5 21 0 3059.53 2953.66 46.07 o 6 21 0 17.19 21.95 17.62 o 7 21 0 238.39 238.54 17.32 o 8 21 0 4450.22 4416.85 121.96 o 9 21 0 80.52 106.57 20.66 o 10 21 0 734.96 738.66 19.57 o 11 21 0 20.63 11.78 12.04 o 12 21 0 260.12 209.37 15.59 o 13 21 0 563.45 582.22 25.59 o 14 21 0 2.32 -18.60 18.60 o 15 21 0 5.63 -37.16 84.44 o 16 21 0 210.06 259.67 68.66 o 0 22 0 4242.68 4168.75 133.59 o 1 22 0 2325.91 2289.41 36.40 o 2 22 0 441.87 471.04 43.15 o 3 22 0 439.18 475.85 13.20 o 4 22 0 897.21 840.52 18.12 o 5 22 0 3366.39 3309.29 164.22 o 6 22 0 1989.11 1921.93 33.17 o 7 22 0 668.63 630.45 16.10 o 8 22 0 139.77 111.31 10.31 o 9 22 0 24.97 40.26 9.79 o 10 22 0 123.58 121.71 14.28 o 11 22 0 246.35 223.81 14.73 o 12 22 0 702.72 726.34 25.37 o 13 22 0 239.77 194.45 26.43 o 14 22 0 0.84 -14.15 18.43 o 15 22 0 9.20 -1.89 102.36 o 16 22 0 37.04 12.13 52.85 o 1 23 0 1492.58 1529.04 53.23 o 2 23 0 3400.01 3376.39 58.11 o 3 23 0 809.45 803.30 17.27 o 4 23 0 1.00 -0.25 31.89 o 5 23 0 801.96 829.07 17.67 o 6 23 0 95.68 99.46 8.55 o 7 23 0 490.81 513.10 15.07 o 8 23 0 283.31 298.46 13.72 o 9 23 0 89.83 107.94 21.57 o 10 23 0 48.37 47.16 18.23 o 11 23 0 504.54 491.18 19.85 o 12 23 0 0.14 19.88 13.01 o 13 23 0 35.80 33.27 15.94 o 14 23 0 3.99 31.49 64.70 o 15 23 0 62.49 59.98 48.60 o 16 23 0 524.37 543.08 33.19 o 0 24 0 2471.16 2457.88 74.89 o 1 24 0 556.69 577.20 14.05 o 2 24 0 18.39 42.09 13.06 o 3 24 0 194.53 198.86 12.46 o 4 24 0 514.92 549.69 14.64 o 5 24 0 3444.11 3455.30 53.83 o 6 24 0 1006.35 1056.49 21.22 o 7 24 0 79.30 54.86 10.31 o 8 24 0 146.30 139.95 30.68 o 9 24 0 297.30 277.53 45.27 o 10 24 0 1.59 15.99 11.90 o 11 24 0 103.44 92.66 16.43 o 12 24 0 3.58 17.01 32.80 o 13 24 0 305.67 347.27 53.17 o 14 24 0 94.97 143.54 99.33 o 15 24 0 137.36 134.28 45.26 o 1 25 0 1721.31 1683.22 38.94 o 2 25 0 676.13 699.47 16.91 o 3 25 0 330.48 313.32 12.76 o 4 25 0 2438.88 2461.08 42.82 o 5 25 0 10.42 20.70 9.89 o 6 25 0 2343.99 2436.52 42.14 o 7 25 0 350.38 381.45 16.41 o 8 25 0 2186.29 2137.73 97.37 o 9 25 0 117.45 110.66 11.93 o 10 25 0 290.93 313.93 16.85 o 11 25 0 333.23 351.75 60.76 o 12 25 0 764.15 743.59 78.11 o 13 25 0 116.18 29.05 87.18 o 14 25 0 2.08 11.59 37.06 o 15 25 0 294.94 262.64 138.54 o 0 26 0 945.31 956.97 30.71 o 1 26 0 696.67 716.92 17.55 o 2 26 0 2245.19 2283.59 46.08 o 3 26 0 1601.88 1572.87 30.75 o 4 26 0 42.75 44.33 48.91 o 5 26 0 242.55 265.57 17.01 o 6 26 0 779.14 790.88 48.33 o 7 26 0 430.29 436.10 20.36 o 8 26 0 53.16 60.59 19.74 o 9 26 0 289.23 279.86 66.54 o 10 26 0 1060.79 1072.91 40.43 o 11 26 0 25.97 0.15 84.14 o 12 26 0 208.08 219.53 23.66 o 13 26 0 75.42 88.32 63.79 o 14 26 0 217.00 155.39 114.83 o 15 26 0 614.42 498.36 65.83 o 1 27 0 444.12 448.50 25.32 o 2 27 0 5.90 44.95 12.16 o 3 27 0 76.38 94.78 15.82 o 4 27 0 63.27 53.46 13.38 o 5 27 0 8.33 -2.92 24.91 o 6 27 0 349.14 351.96 33.42 o 7 27 0 63.67 48.30 12.88 o 8 27 0 246.19 249.05 15.58 o 9 27 0 23.94 22.07 14.73 o 10 27 0 529.13 506.70 132.18 o 11 27 0 277.73 249.14 48.31 o 12 27 0 79.57 83.71 20.92 o 13 27 0 164.73 154.73 23.05 o 14 27 0 117.57 64.86 29.89 o 1 28 0 831.88 839.52 54.75 o 2 28 0 679.34 737.91 30.09 o 3 28 0 909.83 869.96 36.91 o 4 28 0 801.56 778.09 25.53 o 5 28 0 1.59 4.25 13.36 o 6 28 0 74.70 89.31 15.21 o 7 28 0 45.05 61.36 15.81 o 8 28 0 7.13 9.72 14.58 o 9 28 0 1082.25 1106.39 65.36 o 10 28 0 40.75 44.62 20.96 o 11 28 0 116.06 128.56 21.33 o 12 28 0 1110.47 1151.68 232.25 o 13 28 0 335.18 379.74 77.17 o 14 28 0 438.46 313.73 50.46 o 1 29 0 1757.07 1800.70 53.61 o 2 29 0 7.37 14.58 15.80 o 3 29 0 371.18 353.06 24.56 o 4 29 0 481.98 466.12 21.78 o 5 29 0 5.13 25.74 16.27 o 6 29 0 1175.82 1230.67 33.36 o 7 29 0 15.68 15.18 40.40 o 8 29 0 143.61 151.28 18.29 o 9 29 0 190.43 177.00 49.82 o 10 29 0 345.19 277.37 23.27 o 11 29 0 9.57 -6.69 41.61 o 12 29 0 258.62 251.34 30.05 o 13 29 0 191.99 227.03 34.02 o 0 30 0 149.91 166.47 28.60 o 1 30 0 1677.47 1671.58 60.16 o 2 30 0 775.83 753.14 30.13 o 3 30 0 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97.12 14.88 o 1 22 2 454.32 479.07 12.69 o 2 22 2 184.33 179.57 8.16 o 3 22 2 932.34 930.51 18.27 o 4 22 2 4392.28 4323.47 154.01 o 5 22 2 1114.66 1103.50 22.60 o 6 22 2 296.31 302.02 25.83 o 7 22 2 472.98 496.73 54.70 o 8 22 2 171.49 167.25 25.21 o 9 22 2 1568.34 1565.25 29.25 o 10 22 2 1407.65 1390.13 26.71 o 11 22 2 32.97 15.01 20.35 o 12 22 2 19.84 31.08 28.86 o 13 22 2 60.49 93.61 17.01 o 14 22 2 271.86 285.07 52.86 o 15 22 2 283.40 337.96 39.50 o 16 22 2 119.64 140.31 25.96 o -16 23 2 269.34 321.54 85.98 o -15 23 2 33.30 44.19 64.40 o -14 23 2 137.66 82.09 21.57 o -13 23 2 47.07 34.07 19.44 o -12 23 2 40.88 44.86 40.10 o -11 23 2 0.33 0.00 13.36 o -10 23 2 1.43 -0.76 13.67 o -9 23 2 215.54 238.14 32.81 o -8 23 2 3.06 1.34 11.61 o -7 23 2 785.50 763.24 22.53 o -6 23 2 1919.59 1913.95 198.98 o -5 23 2 33.11 38.07 12.45 o -4 23 2 10.21 31.05 10.52 o -3 23 2 260.35 285.42 14.68 o -2 23 2 23.51 49.14 15.80 o -1 23 2 74.63 97.11 21.26 o 0 23 2 414.97 444.75 19.45 o 1 23 2 12.74 37.14 11.85 o 2 23 2 270.15 272.83 14.84 o 3 23 2 748.95 754.87 16.93 o 4 23 2 319.57 327.33 11.40 o 5 23 2 1.02 10.62 8.36 o 6 23 2 541.35 546.58 15.40 o 7 23 2 853.23 844.42 19.02 o 8 23 2 1192.04 1196.01 24.80 o 9 23 2 6.49 1.03 10.75 o 10 23 2 636.61 599.10 23.40 o 11 23 2 869.67 821.94 33.13 o 12 23 2 19.07 45.59 69.56 o 13 23 2 0.96 -13.25 17.59 o 14 23 2 212.78 214.91 44.96 o 15 23 2 6.74 44.82 42.22 o 16 23 2 4.03 -49.83 49.83 o -15 24 2 92.00 122.03 28.58 o -14 24 2 1072.02 1095.11 48.23 o -13 24 2 909.76 931.74 46.19 o -12 24 2 5.41 3.87 25.21 o -11 24 2 913.20 930.09 135.87 o -10 24 2 76.18 82.98 34.33 o -9 24 2 15.28 34.02 17.05 o -8 24 2 388.49 349.59 32.51 o -7 24 2 542.73 516.00 20.97 o -6 24 2 1940.34 1965.66 72.71 o -5 24 2 0.01 28.55 12.15 o -4 24 2 0.58 5.89 12.11 o -3 24 2 664.27 645.39 39.81 o -2 24 2 24.79 14.51 19.74 o -1 24 2 1632.25 1662.28 31.33 o 0 24 2 78.86 79.45 10.34 o 1 24 2 1602.95 1585.58 34.03 o 2 24 2 589.32 601.82 18.55 o 3 24 2 84.86 82.74 26.12 o 4 24 2 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o 7 25 2 61.09 70.45 30.98 o 8 25 2 858.87 813.57 19.47 o 9 25 2 142.22 121.85 11.68 o 10 25 2 314.72 309.58 45.88 o 11 25 2 527.19 483.92 22.02 o 12 25 2 13.12 4.86 16.06 o 13 25 2 125.66 107.44 21.03 o 14 25 2 27.18 0.32 21.61 o 15 25 2 46.18 70.31 28.59 o -15 26 2 107.90 111.18 42.54 o -14 26 2 165.76 201.07 53.16 o -13 26 2 2.76 67.22 57.41 o -12 26 2 170.96 196.91 34.02 o -11 26 2 196.68 178.56 98.73 o -10 26 2 1409.27 1452.69 214.37 o -9 26 2 478.27 484.06 20.22 o -8 26 2 61.61 53.04 15.53 o -7 26 2 87.14 69.11 33.72 o -6 26 2 1341.59 1359.95 38.31 o -5 26 2 1955.20 1978.73 47.49 o -4 26 2 130.09 83.72 24.91 o -3 26 2 1875.48 1972.18 158.81 o -2 26 2 31.55 69.21 10.53 o -1 26 2 34.88 78.24 20.35 o 0 26 2 36.56 30.73 15.80 o 1 26 2 225.48 250.15 13.80 o 2 26 2 76.93 113.16 11.99 o 3 26 2 1002.98 1023.94 25.73 o 4 26 2 602.66 587.53 46.50 o 5 26 2 209.87 193.99 14.22 o 6 26 2 1665.77 1722.83 33.30 o 7 26 2 1036.52 1099.60 93.02 o 8 26 2 2199.42 2212.98 37.74 o 9 26 2 33.35 63.09 55.89 o 10 26 2 0.07 20.15 66.22 o 11 26 2 62.45 70.92 113.30 o 12 26 2 100.27 76.39 17.66 o 13 26 2 201.75 205.05 26.73 o 14 26 2 7.86 -27.03 27.03 o -14 27 2 27.91 78.16 32.08 o -13 27 2 253.62 244.52 35.38 o -12 27 2 89.50 93.41 24.91 o -11 27 2 78.92 36.59 18.98 o -10 27 2 53.60 79.73 29.77 o -9 27 2 444.65 506.77 24.92 o -8 27 2 91.92 93.00 17.67 o -7 27 2 169.48 170.75 24.91 o -6 27 2 1.20 10.80 21.57 o -5 27 2 153.29 178.62 27.95 o -4 27 2 39.60 13.06 30.98 o -3 27 2 593.06 590.42 17.98 o -2 27 2 1275.35 1245.48 29.12 o -1 27 2 497.28 540.01 52.57 o 0 27 2 30.80 95.08 25.82 o 1 27 2 823.57 799.42 28.08 o 2 27 2 555.99 586.56 28.57 o 3 27 2 1108.29 1123.51 27.54 o 4 27 2 1596.22 1586.13 63.26 o 5 27 2 2.40 14.15 11.92 o 6 27 2 83.60 66.72 18.23 o 7 27 2 210.69 190.20 14.30 o 8 27 2 127.36 132.23 14.11 o 9 27 2 17.55 9.53 22.78 o 10 27 2 433.68 407.25 46.18 o 11 27 2 6.85 42.20 58.93 o 12 27 2 107.69 91.35 19.35 o 13 27 2 101.68 108.15 40.10 o 14 27 2 287.25 197.78 52.56 o -14 28 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