#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017823.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017823_Fobs loop_ _publ_author_name 'Kruszynski, Rafal' 'Trzesowska-Kruszynska, Agata' _publ_section_title ; Halogen, hydrogen and electrostatic interactions in 2-amino-5-chloro-1,3-benzoxazol-3-ium nitrate and 2-amino-5-chloro-1,3-benzoxazol-3-ium perchlorate ; _journal_coeditor_code GD3352 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o449 _journal_page_last o454 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.138 _cell_angle_gamma 90.000 _cell_length_a 6.8900 _cell_length_b 20.3139 _cell_length_c 7.2562 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file gd3352Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fe114 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 6923.06 7221.31 78.28 o 4 0 0 139.95 152.51 1.55 o 5 0 0 93.20 97.93 1.14 o 6 0 0 356.34 350.64 3.96 o 7 0 0 64.48 57.64 0.99 o 1 1 0 190.19 147.01 1.04 o 2 1 0 1895.33 1933.31 14.21 o 3 1 0 247.18 219.26 1.47 o 4 1 0 512.51 519.34 3.37 o 5 1 0 106.75 103.12 0.84 o 6 1 0 2.58 3.94 0.30 o 7 1 0 22.96 26.25 0.45 o 0 2 0 94.36 68.65 0.85 o 1 2 0 362.24 362.48 2.58 o 2 2 0 29.11 24.51 0.27 o 3 2 0 321.80 391.46 3.46 o 4 2 0 661.52 700.55 4.50 o 5 2 0 160.08 157.46 1.18 o 6 2 0 0.27 0.13 0.19 o 7 2 0 1.64 1.90 0.24 o 2 3 0 987.79 1039.12 7.93 o 3 3 0 516.59 526.64 3.39 o 4 3 0 534.71 543.96 3.53 o 5 3 0 5.33 6.11 0.26 o 6 3 0 95.00 95.83 0.83 o 7 3 0 163.20 164.46 1.51 o 0 4 0 767.36 821.35 8.38 o 1 4 0 635.62 677.62 4.76 o 2 4 0 693.73 723.59 4.59 o 3 4 0 2017.31 2121.88 13.46 o 4 4 0 96.89 91.44 0.76 o 5 4 0 35.28 36.16 0.46 o 6 4 0 101.62 108.57 0.92 o 7 4 0 15.32 17.49 0.47 o 1 5 0 11.37 12.23 0.27 o 2 5 0 2515.58 2526.55 16.05 o 3 5 0 33.24 42.05 0.39 o 4 5 0 180.55 153.61 1.11 o 5 5 0 387.48 382.56 2.57 o 6 5 0 57.08 57.22 0.61 o 7 5 0 62.75 60.64 0.76 o 0 6 0 1618.20 1691.47 15.24 o 1 6 0 633.82 609.13 4.67 o 2 6 0 307.40 285.78 1.87 o 3 6 0 843.05 898.33 5.70 o 4 6 0 64.27 55.09 0.55 o 5 6 0 11.13 11.12 0.30 o 6 6 0 409.54 398.31 2.87 o 7 6 0 5.88 10.32 0.39 o 1 7 0 1969.62 2066.43 13.13 o 2 7 0 1623.76 1664.78 10.54 o 3 7 0 204.98 233.89 1.58 o 4 7 0 920.31 968.23 6.17 o 5 7 0 353.03 341.48 2.32 o 6 7 0 4.74 6.70 0.39 o 7 7 0 174.21 179.13 1.83 o 0 8 0 2412.91 2395.77 21.51 o 1 8 0 274.67 292.58 1.91 o 2 8 0 0.31 0.65 0.12 o 3 8 0 342.26 326.41 2.16 o 4 8 0 8.86 7.78 0.28 o 5 8 0 3.49 4.16 0.24 o 6 8 0 136.04 129.07 1.20 o 7 8 0 0.19 0.96 0.29 o 1 9 0 521.00 487.86 3.31 o 2 9 0 776.28 758.97 5.09 o 3 9 0 158.58 171.30 1.20 o 4 9 0 63.97 58.08 0.53 o 5 9 0 197.09 205.53 1.69 o 6 9 0 30.69 27.64 0.51 o 0 10 0 370.26 333.85 3.07 o 1 10 0 493.77 554.13 3.75 o 2 10 0 81.08 87.93 0.71 o 3 10 0 854.41 896.53 6.02 o 4 10 0 5.45 3.56 0.19 o 5 10 0 0.01 1.65 0.30 o 6 10 0 126.53 123.61 1.18 o 1 11 0 731.82 781.14 5.59 o 2 11 0 144.02 172.39 1.27 o 3 11 0 257.92 240.51 1.74 o 4 11 0 0.68 1.93 0.19 o 5 11 0 160.91 152.17 1.33 o 6 11 0 70.81 66.82 0.79 o 0 12 0 18.42 12.88 0.31 o 1 12 0 600.66 562.70 3.82 o 2 12 0 409.58 394.86 2.73 o 3 12 0 677.26 655.37 4.76 o 4 12 0 81.89 84.80 0.84 o 5 12 0 142.20 146.32 1.30 o 6 12 0 10.06 10.46 0.39 o 1 13 0 154.92 154.05 1.15 o 2 13 0 121.92 122.78 0.97 o 3 13 0 1.27 1.99 0.19 o 4 13 0 7.28 12.82 0.38 o 5 13 0 11.92 15.12 0.42 o 6 13 0 13.38 13.14 0.43 o 0 14 0 886.98 893.06 8.04 o 1 14 0 77.34 79.66 0.68 o 2 14 0 27.71 26.82 0.37 o 3 14 0 215.58 205.98 1.55 o 4 14 0 389.83 362.64 2.78 o 5 14 0 55.01 42.45 0.61 o 6 14 0 7.79 6.51 0.35 o 1 15 0 214.11 211.52 1.47 o 2 15 0 89.65 90.05 0.78 o 3 15 0 247.15 245.85 2.10 o 4 15 0 903.69 899.25 6.52 o 5 15 0 45.24 44.44 0.62 o 0 16 0 836.83 846.48 7.66 o 1 16 0 65.00 71.02 0.61 o 2 16 0 61.96 57.72 0.62 o 3 16 0 2.22 2.51 0.23 o 4 16 0 0.01 1.10 0.27 o 5 16 0 22.52 17.57 0.48 o 1 17 0 210.34 205.15 1.54 o 2 17 0 73.03 77.02 0.78 o 3 17 0 2.41 2.23 0.26 o 4 17 0 13.01 15.44 0.45 o 5 17 0 5.09 6.42 0.37 o 0 18 0 24.16 22.04 0.49 o 1 18 0 49.15 46.72 0.53 o 2 18 0 342.40 317.04 2.82 o 3 18 0 119.70 122.60 1.22 o 4 18 0 47.73 44.51 0.68 o 5 18 0 49.35 51.80 0.77 o 1 19 0 24.55 28.06 0.47 o 2 19 0 2.23 3.20 0.28 o 3 19 0 58.13 58.02 0.83 o 4 19 0 17.22 21.07 0.51 o 0 20 0 192.52 193.44 2.64 o 1 20 0 109.94 110.79 1.03 o 2 20 0 182.18 175.49 1.62 o 3 20 0 59.74 61.76 0.80 o 4 20 0 17.65 23.72 0.57 o 1 21 0 5.26 4.25 0.29 o 2 21 0 61.89 66.67 0.82 o 3 21 0 8.25 9.24 0.39 o 0 22 0 37.08 34.12 1.36 o 1 22 0 1.06 2.60 0.32 o 2 22 0 44.61 47.49 0.77 o 3 22 0 1.44 1.85 0.31 o 1 23 0 98.78 104.03 1.91 o 2 23 0 46.35 44.68 0.76 o 0 24 0 83.08 92.25 1.58 o -7 1 1 3.31 5.84 0.27 o -6 1 1 1088.51 1081.90 6.98 o -5 1 1 240.38 253.12 1.75 o -4 1 1 147.09 153.93 1.09 o -3 1 1 105.57 113.34 0.81 o -2 1 1 17.81 18.57 0.25 o -1 1 1 4.49 3.99 0.11 o 0 1 1 2.25 8.01 0.27 o 1 1 1 342.05 327.68 2.11 o 2 1 1 207.41 198.03 1.32 o 3 1 1 139.24 141.20 1.01 o 4 1 1 7.42 9.73 0.27 o 5 1 1 1137.18 1154.69 7.39 o 6 1 1 135.06 128.47 1.06 o 7 1 1 44.38 44.95 0.62 o -7 2 1 0.43 0.00 0.21 o -6 2 1 77.38 74.00 0.79 o -5 2 1 837.72 858.92 5.51 o -4 2 1 412.32 464.04 3.02 o -3 2 1 0.09 1.40 0.11 o -2 2 1 268.40 265.84 1.73 o -1 2 1 4286.99 4120.60 35.43 o 0 2 1 345.30 309.81 2.81 o 1 2 1 99.67 95.26 0.66 o 2 2 1 54.61 56.45 0.46 o 3 2 1 247.28 245.35 1.65 o 4 2 1 47.29 46.46 0.47 o 5 2 1 140.54 136.83 1.08 o 6 2 1 192.19 192.97 1.46 o 7 2 1 6.31 6.67 0.42 o -7 3 1 125.18 120.76 1.02 o -6 3 1 71.79 64.53 0.63 o -5 3 1 78.24 77.00 0.70 o -4 3 1 204.91 245.44 1.67 o -3 3 1 568.74 680.61 4.33 o -2 3 1 178.57 195.42 1.30 o -1 3 1 1218.97 1201.94 9.65 o 0 3 1 75.60 64.36 0.50 o 1 3 1 348.09 330.37 2.95 o 2 3 1 2.97 3.32 0.13 o 3 3 1 295.70 323.94 2.14 o 4 3 1 28.39 33.20 0.45 o 5 3 1 199.76 201.57 1.47 o 6 3 1 48.85 47.18 0.60 o 7 3 1 0.56 1.62 0.30 o -7 4 1 73.06 72.90 0.72 o -6 4 1 63.77 56.96 0.58 o -5 4 1 1529.99 1512.07 9.57 o -4 4 1 328.09 342.50 2.27 o -3 4 1 605.01 620.45 4.19 o -2 4 1 1625.86 1791.25 11.40 o -1 4 1 2042.34 1904.11 12.87 o 0 4 1 747.58 691.98 4.67 o 1 4 1 4657.23 4574.88 38.91 o 2 4 1 157.58 170.62 1.34 o 3 4 1 468.87 471.63 3.06 o 4 4 1 756.40 737.75 4.75 o 5 4 1 194.13 189.01 1.39 o 6 4 1 8.83 9.56 0.34 o 7 4 1 131.20 129.22 1.44 o -7 5 1 25.73 25.14 0.44 o -6 5 1 1.50 2.23 0.20 o -5 5 1 323.76 321.62 2.18 o -4 5 1 201.97 181.79 1.27 o -3 5 1 536.23 590.04 3.78 o -2 5 1 19.01 23.09 0.23 o -1 5 1 4522.56 4320.59 30.78 o 0 5 1 129.98 138.15 2.46 o 1 5 1 42.27 39.26 0.38 o 2 5 1 3128.29 3328.22 30.00 o 3 5 1 389.25 439.95 2.99 o 4 5 1 103.61 96.51 0.78 o 5 5 1 179.94 185.71 1.43 o 6 5 1 45.84 45.49 0.64 o -7 6 1 230.09 205.31 2.20 o -6 6 1 34.43 29.30 0.43 o -5 6 1 2.27 2.88 0.21 o -4 6 1 50.22 56.74 0.51 o -3 6 1 440.02 512.10 3.29 o -2 6 1 622.79 779.26 4.95 o -1 6 1 145.11 160.27 1.13 o 0 6 1 805.07 820.02 5.21 o 1 6 1 465.66 419.78 3.97 o 2 6 1 696.73 739.97 5.28 o 3 6 1 251.23 265.10 1.78 o 4 6 1 120.67 122.48 0.94 o 5 6 1 40.77 40.07 0.51 o 6 6 1 0.80 0.68 0.26 o -7 7 1 14.81 19.26 0.50 o -6 7 1 214.71 211.88 1.55 o -5 7 1 24.00 22.50 0.35 o -4 7 1 357.63 347.95 2.31 o -3 7 1 1165.37 1265.87 8.00 o -2 7 1 2434.87 2602.95 16.50 o -1 7 1 97.41 121.83 0.89 o 0 7 1 1222.61 1167.45 7.81 o 1 7 1 2777.16 2709.12 19.23 o 2 7 1 457.99 473.03 3.43 o 3 7 1 8.37 15.80 0.31 o 4 7 1 355.58 353.53 2.37 o 5 7 1 0.11 0.31 0.27 o 6 7 1 0.32 0.37 0.26 o -7 8 1 0.01 0.80 0.29 o -6 8 1 2.52 2.72 0.23 o -5 8 1 110.07 103.95 0.84 o -4 8 1 355.67 324.96 2.17 o -3 8 1 364.75 434.06 2.82 o -2 8 1 513.60 492.11 3.16 o -1 8 1 335.02 346.89 2.38 o 0 8 1 147.90 123.52 0.90 o 1 8 1 212.77 209.40 1.58 o 2 8 1 32.59 47.30 0.50 o 3 8 1 231.70 223.96 1.88 o 4 8 1 58.29 55.60 0.63 o 5 8 1 56.06 51.77 0.66 o 6 8 1 152.26 151.37 1.38 o -7 9 1 16.20 19.81 0.52 o -6 9 1 35.49 34.82 0.50 o -5 9 1 0.20 1.09 0.17 o -4 9 1 179.88 195.63 1.38 o -3 9 1 597.16 613.81 3.94 o -2 9 1 2.33 0.62 0.10 o -1 9 1 1801.84 1897.35 13.47 o 0 9 1 317.36 324.28 2.23 o 1 9 1 943.93 988.24 6.59 o 2 9 1 1025.10 1052.32 7.48 o 3 9 1 606.82 621.61 4.52 o 4 9 1 160.57 150.17 1.29 o 5 9 1 558.55 547.77 4.09 o 6 9 1 12.73 15.10 0.46 o -7 10 1 93.74 92.02 1.05 o -6 10 1 317.24 319.73 2.52 o -5 10 1 961.95 949.63 6.43 o -4 10 1 37.25 32.47 0.38 o -3 10 1 1673.00 1726.10 10.90 o -2 10 1 1447.51 1544.28 10.30 o -1 10 1 743.68 870.51 5.83 o 0 10 1 405.64 349.63 2.27 o 1 10 1 1480.48 1571.30 11.12 o 2 10 1 53.00 56.23 0.57 o 3 10 1 239.82 233.29 1.83 o 4 10 1 317.84 300.61 2.34 o 5 10 1 0.03 0.75 0.33 o 6 10 1 83.15 80.88 0.99 o -7 11 1 79.83 79.49 0.97 o -6 11 1 19.01 19.33 0.46 o -5 11 1 113.66 105.88 0.93 o -4 11 1 256.48 260.62 1.79 o -3 11 1 397.58 372.63 2.46 o -2 11 1 115.99 126.14 0.97 o -1 11 1 445.06 434.10 3.85 o 0 11 1 1311.85 1330.10 8.40 o 1 11 1 63.06 71.15 0.65 o 2 11 1 557.49 524.99 3.83 o 3 11 1 729.31 733.69 5.31 o 4 11 1 113.51 109.41 1.03 o 5 11 1 184.35 188.31 1.61 o 6 11 1 44.20 47.68 0.69 o -6 12 1 8.18 8.88 0.34 o -5 12 1 23.10 21.14 0.39 o -4 12 1 27.22 24.89 0.40 o -3 12 1 1.40 3.60 0.22 o -2 12 1 176.63 194.91 1.52 o -1 12 1 114.54 128.71 0.98 o 0 12 1 440.78 507.09 3.46 o 1 12 1 262.59 280.35 2.11 o 2 12 1 309.62 325.46 2.45 o 3 12 1 15.01 17.50 0.40 o 4 12 1 176.10 168.81 1.44 o 5 12 1 20.75 22.65 0.49 o 6 12 1 45.16 46.08 0.68 o -6 13 1 111.03 110.71 1.18 o -5 13 1 68.57 74.16 0.79 o -4 13 1 901.79 907.23 6.14 o -3 13 1 0.43 0.86 0.14 o -2 13 1 394.20 427.76 3.16 o -1 13 1 587.49 556.18 3.80 o 0 13 1 53.90 61.39 0.55 o 1 13 1 90.27 90.28 0.80 o 2 13 1 1186.32 1178.43 8.39 o 3 13 1 1.07 1.38 0.21 o 4 13 1 2.42 2.65 0.25 o 5 13 1 151.01 152.95 1.39 o -6 14 1 34.18 33.86 0.61 o -5 14 1 78.16 78.79 0.90 o -4 14 1 3.37 5.83 0.33 o -3 14 1 1.27 1.61 0.17 o -2 14 1 660.52 676.18 4.61 o -1 14 1 26.85 22.31 0.29 o 0 14 1 157.11 158.13 1.12 o 1 14 1 414.32 406.24 3.23 o 2 14 1 145.34 140.54 1.20 o 3 14 1 1.19 1.09 0.21 o 4 14 1 163.72 172.77 1.49 o 5 14 1 4.35 6.17 0.33 o -6 15 1 0.02 0.78 0.28 o -5 15 1 47.73 47.56 0.69 o -4 15 1 4.26 4.41 0.26 o -3 15 1 39.79 38.03 0.50 o -2 15 1 255.25 240.31 1.76 o -1 15 1 39.00 35.59 0.40 o 0 15 1 100.92 105.87 0.81 o 1 15 1 26.69 35.29 0.46 o 2 15 1 201.93 201.77 1.63 o 3 15 1 42.50 41.74 0.56 o 4 15 1 30.56 32.78 0.70 o 5 15 1 5.67 6.06 0.34 o -5 16 1 241.46 244.62 2.21 o -4 16 1 1.18 0.63 0.23 o -3 16 1 1.61 1.51 0.20 o -2 16 1 1636.19 1660.55 11.10 o -1 16 1 12.78 8.06 0.27 o 0 16 1 392.32 389.43 2.58 o 1 16 1 948.66 895.36 6.43 o 2 16 1 19.18 15.10 0.36 o 3 16 1 100.12 91.06 0.90 o 4 16 1 137.73 137.33 1.37 o 5 16 1 17.28 20.86 0.49 o -5 17 1 81.30 82.38 1.07 o -4 17 1 8.03 9.35 0.38 o -3 17 1 112.05 106.43 1.08 o -2 17 1 4.21 6.48 0.30 o -1 17 1 571.09 560.68 3.88 o 0 17 1 105.71 113.16 0.94 o 1 17 1 443.39 425.32 3.35 o 2 17 1 128.11 132.82 1.17 o 3 17 1 7.91 7.36 0.35 o 4 17 1 19.08 19.23 0.46 o -5 18 1 1.20 2.30 0.35 o -4 18 1 8.19 8.43 0.40 o -3 18 1 8.57 8.75 0.33 o -2 18 1 3.30 5.07 0.26 o -1 18 1 0.39 1.50 0.27 o 0 18 1 29.86 28.44 0.55 o 1 18 1 25.95 32.83 0.48 o 2 18 1 52.05 60.28 0.74 o 3 18 1 9.58 9.33 0.35 o 4 18 1 21.88 21.33 0.52 o -4 19 1 161.54 166.02 1.74 o -3 19 1 96.96 92.83 1.00 o -2 19 1 106.10 99.19 0.96 o -1 19 1 1057.72 1035.91 7.02 o 0 19 1 163.11 160.95 1.43 o 1 19 1 111.49 111.76 1.12 o 2 19 1 196.01 179.75 1.60 o 3 19 1 34.50 37.23 0.61 o 4 19 1 5.34 7.04 0.39 o -4 20 1 0.09 0.00 0.31 o -3 20 1 17.22 19.79 0.53 o -2 20 1 219.77 200.49 1.80 o -1 20 1 4.36 9.21 0.98 o 0 20 1 59.49 61.15 0.69 o 1 20 1 370.11 384.68 3.37 o 2 20 1 16.68 15.03 0.54 o 3 20 1 109.76 106.13 1.14 o -4 21 1 28.36 35.28 0.71 o -3 21 1 36.02 35.70 0.67 o -2 21 1 2.98 3.21 0.28 o -1 21 1 0.71 2.09 0.28 o 0 21 1 1.34 2.07 0.26 o 1 21 1 35.60 33.40 0.67 o 2 21 1 45.10 38.17 0.70 o 3 21 1 13.58 13.49 0.51 o -3 22 1 45.42 44.32 0.75 o -2 22 1 45.86 46.85 0.74 o -1 22 1 3.21 3.69 0.31 o 0 22 1 41.16 43.26 0.84 o 1 22 1 48.90 49.67 0.79 o 2 22 1 6.76 8.95 0.44 o -2 23 1 4.93 4.23 0.39 o -1 23 1 26.61 30.98 0.69 o 0 23 1 30.19 33.79 0.83 o 1 23 1 6.20 9.81 0.50 o -8 0 2 39.10 35.05 0.81 o -7 0 2 179.42 190.12 2.25 o -6 0 2 2.28 2.90 0.36 o -5 0 2 724.87 739.75 6.74 o -4 0 2 442.34 443.41 4.08 o -3 0 2 201.66 259.94 2.67 o -2 0 2 2063.42 2046.56 20.16 o 0 0 2 1109.46 1302.38 12.76 o 1 0 2 811.75 748.06 6.70 o 2 0 2 1496.09 1369.88 12.22 o 3 0 2 179.91 171.20 1.72 o 4 0 2 1149.90 1137.75 10.26 o 5 0 2 1.23 1.76 0.31 o 6 0 2 28.12 32.05 0.80 o -8 1 2 18.83 14.39 0.43 o -7 1 2 167.29 164.80 1.42 o -6 1 2 39.44 31.41 0.73 o -5 1 2 75.29 77.30 0.65 o -4 1 2 147.79 164.42 1.15 o -3 1 2 4916.44 5120.84 35.56 o -2 1 2 2161.65 2066.87 14.39 o -1 1 2 289.55 290.32 1.87 o 1 1 2 978.11 997.87 6.30 o 2 1 2 583.24 580.63 3.81 o 3 1 2 631.87 617.54 3.99 o 4 1 2 67.24 78.34 0.69 o 5 1 2 1.48 1.81 0.22 o 6 1 2 88.54 86.10 0.87 o -8 2 2 0.05 0.00 0.24 o -7 2 2 30.08 28.94 0.49 o -6 2 2 51.64 55.95 0.58 o -5 2 2 2.40 2.64 0.16 o -4 2 2 237.02 224.07 1.52 o -3 2 2 111.59 111.22 0.83 o -2 2 2 1802.93 1793.63 11.88 o -1 2 2 9331.71 9473.67 110.13 o 1 2 2 211.41 201.74 1.34 o 2 2 2 284.30 291.27 2.03 o 3 2 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1.49 o -2 5 2 870.42 835.48 5.61 o -1 5 2 17.21 14.47 0.21 o 0 5 2 756.19 747.63 5.59 o 1 5 2 27.27 25.33 0.38 o 2 5 2 215.61 204.69 1.48 o 3 5 2 82.98 92.62 0.79 o 4 5 2 67.52 76.87 0.73 o 5 5 2 3.41 3.44 0.33 o 6 5 2 90.78 85.73 1.29 o -7 6 2 400.22 384.34 2.92 o -6 6 2 36.08 32.44 0.43 o -5 6 2 1125.74 1151.33 7.33 o -4 6 2 982.42 1017.25 6.46 o -3 6 2 860.42 894.05 5.67 o -2 6 2 2078.77 2071.41 13.89 o -1 6 2 955.99 980.24 6.98 o 0 6 2 108.65 109.06 0.81 o 1 6 2 693.32 656.50 5.58 o 2 6 2 1895.26 1864.94 12.40 o 3 6 2 217.35 210.26 1.75 o 4 6 2 322.63 307.34 2.52 o 5 6 2 252.84 252.38 2.17 o 6 6 2 71.12 68.45 0.83 o -7 7 2 2.44 4.15 0.29 o -6 7 2 84.74 84.61 0.75 o -5 7 2 27.64 25.08 0.60 o -4 7 2 22.93 22.46 0.30 o -3 7 2 426.09 448.41 2.90 o -2 7 2 413.93 401.38 2.75 o -1 7 2 983.51 998.06 7.11 o 0 7 2 70.56 64.48 0.55 o 1 7 2 240.15 236.47 1.78 o 2 7 2 1.16 2.35 0.25 o 3 7 2 232.87 239.01 2.01 o 4 7 2 49.55 47.80 0.60 o 5 7 2 6.38 11.44 0.41 o 6 7 2 52.15 54.54 0.75 o -7 8 2 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