#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/78/2017892.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2017892_Fobs
loop_
_publ_author_name
'Smith, Graham'
'Wermuth, Urs D.'
_publ_section_title
;
Three-dimensional hydrogen-bonded structures in the guanidinium salts
of the monocyclic dicarboxylic acids
rac-trans-cyclohexane-1,2-dicarboxylic acid (2:1,
anhydrous), isophthalic acid (1:1, monohydrate) and terephthalic acid
(2:1, trihydrate)
;
_journal_coeditor_code GD3361
_journal_issue 12
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first o575
_journal_page_last o580
_journal_volume 66
_journal_year 2010
_space_group_IT_number 15
_symmetry_space_group_name_Hall '-C 2yc'
_symmetry_space_group_name_H-M 'C 1 2/c 1'
_cell_angle_alpha 90.000
_cell_angle_beta 110.297
_cell_angle_gamma 90.000
_cell_length_a 18.0402
_cell_length_b 5.1420
_cell_length_c 18.1496
_exptl_crystal_F_000 720.00
_reflns_d_resolution_high 0.8111
_[local]_cod_data_source_file gd3361IIIsup4.hkl
_[local]_cod_data_source_block III
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' gs08gs27_TPAGUr(III)'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 239.26
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
4 0 0 239.55 201.54 5.13 o
6 0 0 24922.97 24026.66 326.34 o
8 0 0 3178.59 3479.72 32.88 o
10 0 0 2487.96 2782.89 32.89 o
12 0 0 1029.33 1056.14 18.75 o
14 0 0 773.83 695.88 17.04 o
16 0 0 5.50 8.23 9.23 o
18 0 0 165.59 132.60 22.73 o
20 0 0 112.44 125.32 15.90 o
1 1 0 3377.49 3647.65 17.83 o
3 1 0 3914.54 3722.31 24.85 o
5 1 0 4496.38 4575.27 39.17 o
7 1 0 10.41 24.42 3.98 o
9 1 0 566.14 595.11 10.81 o
11 1 0 249.93 245.44 5.86 o
13 1 0 187.32 166.83 7.67 o
15 1 0 0.13 7.46 9.42 o
17 1 0 430.00 420.01 17.28 o
19 1 0 23.97 29.00 14.41 o
0 2 0 4266.57 4056.21 19.39 o
2 2 0 3621.70 3226.77 14.02 o
4 2 0 96.74 75.67 3.90 o
6 2 0 98.05 80.20 4.75 o
8 2 0 34.48 42.67 5.80 o
10 2 0 296.70 294.01 7.22 o
12 2 0 40.87 40.86 7.93 o
14 2 0 228.98 209.70 10.91 o
16 2 0 767.58 737.93 18.57 o
18 2 0 0.28 2.78 9.69 o
1 3 0 1162.23 1278.17 13.89 o
3 3 0 8.27 21.17 3.58 o
5 3 0 770.05 780.81 28.64 o
7 3 0 730.19 685.39 19.22 o
9 3 0 75.16 82.37 7.42 o
11 3 0 0.93 3.77 6.46 o
13 3 0 0.28 8.81 8.24 o
15 3 0 107.59 119.34 11.03 o
17 3 0 0.60 6.96 10.94 o
0 4 0 27.79 28.26 12.50 o
2 4 0 0.10 3.49 5.13 o
4 4 0 121.87 128.98 15.41 o
6 4 0 595.38 626.06 16.00 o
8 4 0 148.88 136.88 8.50 o
10 4 0 0.10 1.39 9.88 o
12 4 0 37.74 27.84 10.06 o
14 4 0 2.71 12.29 9.89 o
16 4 0 62.80 59.01 12.51 o
1 5 0 180.34 184.67 11.58 o
3 5 0 28.12 26.75 9.26 o
5 5 0 10.16 12.28 7.34 o
7 5 0 14.61 13.49 8.06 o
9 5 0 0.18 8.16 11.15 o
11 5 0 8.17 5.75 12.42 o
0 6 0 247.22 264.22 22.28 o
2 6 0 133.45 103.31 11.00 o
4 6 0 147.84 201.42 22.57 o
6 6 0 266.53 326.46 28.97 o
-19 1 1 91.04 97.25 10.77 o
-17 1 1 90.68 84.96 9.54 o
-15 1 1 23.00 23.95 8.05 o
-13 1 1 60.17 58.89 3.55 o
-11 1 1 1495.94 1449.00 10.23 o
-9 1 1 600.32 606.05 8.13 o
-7 1 1 83.63 133.47 3.48 o
-5 1 1 2366.51 2108.07 19.13 o
-3 1 1 6214.04 5602.09 31.99 o
-1 1 1 366.52 440.49 5.69 o
1 1 1 739.63 563.86 6.83 o
3 1 1 1825.93 1741.68 29.50 o
5 1 1 354.15 483.22 13.73 o
7 1 1 28.14 10.49 4.21 o
9 1 1 1468.16 1528.37 15.98 o
11 1 1 2053.55 2171.92 23.73 o
13 1 1 89.58 83.13 6.80 o
15 1 1 1.12 7.64 9.51 o
17 1 1 711.89 665.63 20.81 o
19 1 1 182.66 185.44 26.28 o
-20 2 1 17.05 25.44 14.28 o
-18 2 1 96.53 93.00 11.50 o
-16 2 1 143.12 147.70 11.22 o
-14 2 1 88.23 80.85 9.43 o
-12 2 1 552.92 545.63 14.16 o
-10 2 1 2.25 2.07 2.55 o
-8 2 1 1052.39 1009.90 12.36 o
-6 2 1 0.75 3.22 3.64 o
-4 2 1 608.86 512.30 6.44 o
-2 2 1 111.94 114.40 4.71 o
0 2 1 372.15 340.26 5.03 o
2 2 1 9921.58 10268.03 46.09 o
4 2 1 2165.13 2517.03 25.23 o
6 2 1 212.49 201.80 11.84 o
8 2 1 842.29 949.74 14.59 o
10 2 1 389.94 362.12 8.38 o
12 2 1 1200.39 1169.25 14.55 o
14 2 1 1224.90 1194.44 26.26 o
16 2 1 285.05 267.02 16.64 o
18 2 1 0.87 0.59 9.37 o
-17 3 1 34.27 48.39 11.55 o
-15 3 1 9.58 9.81 8.68 o
-13 3 1 2228.24 2310.26 29.00 o
-11 3 1 2339.82 2368.06 28.04 o
-9 3 1 648.22 631.44 13.05 o
-7 3 1 544.26 548.63 13.20 o
-5 3 1 3978.45 4216.33 46.25 o
-3 3 1 3636.81 3739.30 23.73 o
-1 3 1 13.61 14.71 3.55 o
1 3 1 326.41 338.79 9.39 o
3 3 1 3.08 3.80 3.63 o
5 3 1 4.69 6.27 3.78 o
7 3 1 98.73 92.46 7.04 o
9 3 1 68.42 68.04 7.55 o
11 3 1 798.30 758.84 14.46 o
13 3 1 316.44 299.86 11.41 o
15 3 1 2.88 13.32 10.45 o
17 3 1 95.75 94.72 11.55 o
-16 4 1 38.23 43.82 11.57 o
-14 4 1 2.85 11.94 9.68 o
-12 4 1 198.70 174.75 13.60 o
-10 4 1 287.45 282.62 30.88 o
-8 4 1 14.63 12.92 9.21 o
-6 4 1 139.12 148.72 7.10 o
-4 4 1 341.02 379.89 9.90 o
-2 4 1 40.00 41.04 6.89 o
0 4 1 23.15 15.29 4.79 o
2 4 1 358.83 365.36 11.58 o
4 4 1 92.73 101.02 10.23 o
6 4 1 23.34 31.08 5.62 o
8 4 1 9.02 12.49 6.60 o
10 4 1 527.93 482.27 13.96 o
12 4 1 1.26 0.80 9.51 o
14 4 1 90.05 93.45 12.08 o
-13 5 1 38.38 34.43 11.44 o
-11 5 1 0.44 8.95 11.70 o
-9 5 1 143.33 145.29 13.94 o
-7 5 1 20.78 29.10 10.98 o
-5 5 1 78.13 81.39 8.76 o
-3 5 1 48.51 57.21 10.46 o
-1 5 1 206.78 211.54 9.68 o
1 5 1 301.99 303.92 15.26 o
3 5 1 46.43 46.75 10.63 o
5 5 1 219.66 198.91 10.84 o
7 5 1 0.24 -0.28 7.94 o
9 5 1 44.81 42.62 12.26 o
11 5 1 17.66 20.43 11.37 o
-6 6 1 4.34 2.84 18.20 o
-4 6 1 12.27 16.82 12.79 o
-2 6 1 16.99 11.26 11.05 o
0 6 1 303.23 293.27 14.11 o
2 6 1 21.16 16.77 9.30 o
4 6 1 192.95 205.13 15.80 o
6 6 1 48.79 68.23 19.46 o
-20 0 2 135.36 156.58 16.72 o
-18 0 2 659.91 582.61 23.86 o
-16 0 2 1250.44 1061.67 34.26 o
-14 0 2 3.96 5.55 6.75 o
-12 0 2 1929.11 1938.91 28.40 o
-10 0 2 6019.88 6603.54 45.43 o
-8 0 2 8624.00 9698.20 34.54 o
-6 0 2 441.95 468.42 14.13 o
-4 0 2 8990.17 9424.10 116.30 o
2 0 2 435.29 323.41 7.14 o
4 0 2 681.88 763.23 15.60 o
6 0 2 1567.13 1675.05 24.48 o
8 0 2 1184.83 1293.91 23.95 o
10 0 2 43.91 24.82 8.91 o
12 0 2 1096.19 1188.70 21.41 o
14 0 2 1106.76 1074.04 42.28 o
16 0 2 191.02 176.82 12.87 o
18 0 2 41.16 40.71 19.17 o
20 0 2 6.23 14.15 19.44 o
-21 1 2 32.95 30.69 11.90 o
-19 1 2 4.66 11.62 9.40 o
-17 1 2 148.17 171.89 8.99 o
-15 1 2 146.16 144.44 12.47 o
-13 1 2 180.44 192.79 4.89 o
-11 1 2 156.81 163.51 4.28 o
-9 1 2 2809.15 2972.42 16.01 o
-7 1 2 529.08 541.03 7.40 o
-5 1 2 347.08 373.46 4.87 o
-3 1 2 1059.20 1097.07 4.67 o
-1 1 2 781.52 778.55 7.55 o
1 1 2 2932.65 3338.04 20.53 o
3 1 2 362.99 315.42 5.37 o
7 1 2 663.95 716.87 11.40 o
9 1 2 1712.53 1852.74 18.01 o
11 1 2 1038.23 1048.24 13.89 o
13 1 2 282.83 299.87 9.47 o
15 1 2 38.62 28.77 8.80 o
17 1 2 3.98 16.20 11.10 o
19 1 2 6.93 26.96 18.00 o
-20 2 2 2.95 5.68 13.79 o
-18 2 2 527.24 531.71 16.87 o
-16 2 2 9.16 20.24 6.96 o
-14 2 2 272.44 257.84 11.80 o
-12 2 2 1533.08 1485.41 20.75 o
-10 2 2 513.55 492.65 14.90 o
-8 2 2 1087.12 961.05 14.62 o
-6 2 2 2222.44 2254.66 12.55 o
-4 2 2 6058.05 5814.06 33.26 o
-2 2 2 145.57 135.00 4.48 o
0 2 2 231.23 153.62 4.75 o
2 2 2 9139.34 9002.07 61.11 o
4 2 2 1292.80 1570.41 18.55 o
6 2 2 3704.96 3581.14 63.23 o
8 2 2 1327.60 1329.86 17.84 o
10 2 2 322.88 291.44 8.36 o
12 2 2 3025.56 2978.81 23.57 o
14 2 2 34.14 32.68 11.75 o
16 2 2 7.13 19.01 11.75 o
18 2 2 32.43 44.92 14.35 o
-17 3 2 0.19 9.28 10.16 o
-15 3 2 655.31 641.16 17.71 o
-13 3 2 482.79 496.38 14.70 o
-11 3 2 225.49 232.98 10.59 o
-9 3 2 262.43 243.36 8.73 o
-7 3 2 39.92 37.43 6.57 o
-5 3 2 1035.28 1106.46 13.67 o
-3 3 2 94.25 72.56 5.50 o
-1 3 2 2000.17 1926.65 21.97 o
1 3 2 164.81 160.51 7.19 o
3 3 2 2.82 1.47 4.73 o
5 3 2 88.33 76.28 7.51 o
7 3 2 41.51 49.83 6.59 o
9 3 2 96.93 97.85 10.31 o
11 3 2 20.74 31.03 7.05 o
13 3 2 490.43 492.02 13.09 o
15 3 2 64.05 70.34 11.05 o
17 3 2 79.57 102.40 12.82 o
-16 4 2 70.95 72.56 11.62 o
-14 4 2 189.28 210.37 13.49 o
-12 4 2 85.20 61.84 10.06 o
-10 4 2 5.59 4.09 10.50 o
-8 4 2 41.73 57.45 9.85 o
-6 4 2 2.91 -0.23 6.67 o
-4 4 2 297.74 297.47 7.47 o
-2 4 2 832.23 876.68 21.12 o
0 4 2 530.61 538.63 13.52 o
2 4 2 35.18 33.14 6.46 o
4 4 2 11.13 13.84 9.23 o
6 4 2 1189.79 1223.88 16.11 o
8 4 2 14.83 6.83 7.06 o
10 4 2 4.23 6.44 7.38 o
12 4 2 842.36 840.76 20.44 o
14 4 2 364.24 380.87 16.84 o
-13 5 2 5.72 2.84 11.18 o
-11 5 2 149.45 170.36 15.76 o
-9 5 2 110.54 120.78 13.14 o
-7 5 2 3.56 3.30 9.75 o
-5 5 2 427.60 449.59 13.69 o
-3 5 2 379.99 389.28 9.71 o
-1 5 2 35.59 48.49 8.35 o
1 5 2 1283.48 1361.66 27.51 o
3 5 2 5.87 11.15 9.39 o
5 5 2 10.75 12.33 7.74 o
7 5 2 95.79 79.30 11.67 o
9 5 2 2.44 8.34 10.71 o
11 5 2 27.60 47.19 14.06 o
-6 6 2 4.19 10.76 17.03 o
-4 6 2 90.31 108.93 21.43 o
-2 6 2 190.64 152.43 15.06 o
0 6 2 186.98 207.72 12.59 o
2 6 2 8.79 13.61 11.75 o
4 6 2 56.28 56.04 13.53 o
-21 1 3 32.12 28.05 10.88 o
-19 1 3 11.19 4.44 9.68 o
-17 1 3 15.76 14.88 6.89 o
-15 1 3 82.10 86.09 7.29 o
-13 1 3 178.76 165.57 4.21 o
-11 1 3 409.55 366.71 4.94 o
-9 1 3 1941.43 1895.27 13.16 o
-7 1 3 3426.71 3816.38 14.22 o
-5 1 3 784.32 643.47 4.50 o
-3 1 3 1410.09 1365.56 14.68 o
-1 1 3 13691.72 13937.20 163.96 o
1 1 3 57244.33 55600.04 365.88 o
3 1 3 2008.82 2243.03 41.80 o
5 1 3 616.52 502.34 7.50 o
7 1 3 1749.29 1922.31 22.26 o
9 1 3 956.40 970.75 7.49 o
11 1 3 160.48 164.27 6.76 o
13 1 3 34.55 39.23 6.99 o
15 1 3 18.37 28.41 9.10 o
17 1 3 13.13 18.57 9.70 o
19 1 3 0.00 -10.09 24.35 o
-20 2 3 37.12 53.60 14.45 o
-18 2 3 42.88 39.76 9.46 o
-16 2 3 150.75 129.35 10.85 o
-14 2 3 13.95 15.17 5.74 o
-12 2 3 1579.95 1535.30 16.22 o
-10 2 3 32.71 38.72 3.64 o
-8 2 3 687.05 716.96 6.74 o
-6 2 3 6.70 7.97 4.03 o
-4 2 3 3089.38 3302.71 19.24 o
-2 2 3 10.21 17.47 4.37 o
0 2 3 248.74 207.54 10.56 o
4 2 3 147.03 133.03 11.56 o
6 2 3 490.35 558.78 7.56 o
8 2 3 173.54 176.38 8.74 o
10 2 3 198.17 205.15 7.95 o
12 2 3 163.29 175.99 8.54 o
14 2 3 4.40 7.72 10.41 o
16 2 3 23.99 34.22 12.31 o
18 2 3 4.65 -0.11 13.99 o
-19 3 3 7.97 8.91 11.88 o
-17 3 3 174.23 172.03 12.81 o
-15 3 3 2134.97 2152.77 29.18 o
-13 3 3 2.42 7.68 8.90 o
-11 3 3 44.52 40.12 7.93 o
-9 3 3 906.71 892.41 16.12 o
-7 3 3 21.57 25.25 4.27 o
-5 3 3 854.43 898.97 9.37 o
-3 3 3 1354.01 1300.72 26.74 o
-1 3 3 464.08 489.92 12.39 o
1 3 3 32.51 28.80 5.77 o
3 3 3 1998.73 2047.71 31.24 o
5 3 3 288.17 313.33 9.56 o
7 3 3 184.01 187.80 6.72 o
9 3 3 993.78 999.08 40.87 o
11 3 3 9.13 4.16 8.47 o
13 3 3 1.09 10.06 8.84 o
15 3 3 6.92 17.46 10.46 o
17 3 3 47.04 43.17 11.64 o
-16 4 3 67.56 76.97 11.36 o
-14 4 3 399.77 413.88 16.15 o
-12 4 3 95.84 90.13 9.98 o
-10 4 3 0.19 0.69 10.23 o
-8 4 3 1.35 5.71 6.55 o
-6 4 3 252.06 247.64 13.90 o
-4 4 3 159.71 153.20 8.27 o
-2 4 3 1415.26 1420.25 23.95 o
0 4 3 469.22 476.57 10.55 o
2 4 3 1.82 5.37 7.82 o
4 4 3 4.19 6.46 6.50 o
6 4 3 0.68 5.62 5.83 o
8 4 3 514.44 560.59 15.84 o
10 4 3 27.60 23.62 8.69 o
12 4 3 127.52 111.38 9.79 o
14 4 3 68.21 82.95 11.97 o
-13 5 3 0.30 10.94 13.40 o
-11 5 3 174.54 180.16 16.13 o
-9 5 3 60.39 61.09 11.46 o
-7 5 3 102.05 98.91 11.58 o
-5 5 3 86.17 98.80 8.93 o
-3 5 3 840.25 873.82 17.52 o
-1 5 3 601.89 550.62 18.89 o
1 5 3 9.41 17.10 10.05 o
3 5 3 18.39 16.88 9.27 o
5 5 3 54.80 57.17 11.19 o
7 5 3 121.87 134.05 13.41 o
9 5 3 24.99 20.18 12.12 o
11 5 3 3.18 3.33 12.64 o
-6 6 3 11.43 5.73 17.91 o
-4 6 3 28.33 49.37 20.09 o
-2 6 3 10.68 15.95 12.19 o
0 6 3 21.89 29.02 9.17 o
2 6 3 50.14 34.89 13.11 o
4 6 3 0.84 0.18 12.06 o
-20 0 4 532.94 449.70 27.61 o
-18 0 4 416.80 453.22 25.61 o
-16 0 4 1996.26 1913.46 31.12 o
-14 0 4 34.17 49.43 5.09 o
-12 0 4 821.02 840.28 10.66 o
-10 0 4 1988.17 2202.39 14.94 o
-8 0 4 324.46 348.00 5.53 o
-6 0 4 5497.42 5861.52 36.88 o
-4 0 4 20747.93 19691.76 592.44 o
-2 0 4 6507.62 6280.85 48.07 o
0 0 4 698.61 762.51 15.07 o
2 0 4 16875.08 15423.11 254.67 o
6 0 4 1556.71 1890.29 29.86 o
8 0 4 3003.69 3182.55 41.42 o
10 0 4 244.54 326.90 13.01 o
12 0 4 484.96 434.38 15.47 o
14 0 4 12.04 8.96 10.21 o
16 0 4 31.54 35.62 11.75 o
18 0 4 621.74 567.46 35.57 o
-21 1 4 121.71 124.09 12.36 o
-19 1 4 71.52 59.00 10.33 o
-17 1 4 170.13 158.18 8.76 o
-15 1 4 79.31 82.80 6.80 o
-13 1 4 19.85 21.23 4.14 o
-11 1 4 1445.75 1428.14 18.31 o
-9 1 4 94.56 126.12 4.78 o
-7 1 4 680.57 631.92 6.56 o
-5 1 4 4340.48 4074.63 12.68 o
-3 1 4 8010.78 8056.05 44.49 o
-1 1 4 24353.45 23742.62 198.36 o
1 1 4 4924.51 4512.27 16.01 o
3 1 4 4706.15 4395.52 18.66 o
5 1 4 155.90 146.82 5.51 o
7 1 4 250.80 271.34 5.87 o
9 1 4 65.10 64.66 5.33 o
11 1 4 2.74 11.37 5.78 o
13 1 4 2198.06 2091.83 28.49 o
15 1 4 248.93 252.66 13.10 o
17 1 4 30.35 37.89 10.54 o
-20 2 4 36.54 40.31 14.01 o
-18 2 4 17.61 29.83 9.48 o
-16 2 4 42.86 33.26 9.03 o
-14 2 4 5.13 9.09 5.92 o
-12 2 4 2103.99 2073.08 21.72 o
-10 2 4 1441.80 1461.11 12.88 o
-8 2 4 109.71 85.94 3.59 o
-6 2 4 4179.92 4236.33 20.12 o
-4 2 4 3001.41 3603.49 18.89 o
-2 2 4 28.92 12.13 6.32 o
0 2 4 102.78 76.87 4.95 o
4 2 4 350.98 315.69 8.23 o
6 2 4 141.73 155.73 5.25 o
8 2 4 525.79 487.57 13.00 o
10 2 4 427.49 381.97 10.36 o
12 2 4 33.24 38.16 6.67 o
14 2 4 9.45 18.82 9.30 o
16 2 4 269.12 264.85 17.48 o
18 2 4 184.96 158.37 17.96 o
-19 3 4 2.88 16.29 10.56 o
-17 3 4 18.87 23.49 10.61 o
-15 3 4 123.61 134.24 10.82 o
-13 3 4 346.05 333.00 12.77 o
-11 3 4 223.87 210.18 10.40 o
-9 3 4 247.13 241.80 9.52 o
-7 3 4 856.51 928.81 13.37 o
-5 3 4 1.37 1.72 4.27 o
-3 3 4 649.80 583.73 13.92 o
-1 3 4 55.37 44.77 5.11 o
1 3 4 924.25 862.20 25.56 o
3 3 4 1041.40 1121.08 20.67 o
5 3 4 719.69 657.23 16.57 o
7 3 4 15.93 13.44 8.06 o
9 3 4 297.03 273.28 14.31 o
11 3 4 330.73 344.76 13.55 o
13 3 4 76.86 81.88 10.99 o
15 3 4 2.18 11.94 10.75 o
-16 4 4 40.48 45.84 14.67 o
-14 4 4 30.46 27.98 10.79 o
-12 4 4 679.92 678.50 17.31 o
-10 4 4 22.41 33.63 8.08 o
-8 4 4 1.05 12.22 9.41 o
-6 4 4 94.49 92.20 7.72 o
-4 4 4 282.23 315.68 11.89 o
-2 4 4 319.80 308.90 13.11 o
0 4 4 71.05 78.02 8.07 o
2 4 4 137.04 140.31 11.39 o
4 4 4 13.22 13.87 6.74 o
6 4 4 387.46 393.23 12.75 o
8 4 4 100.52 121.93 9.54 o
10 4 4 11.05 4.93 8.28 o
12 4 4 86.85 89.56 9.83 o
14 4 4 36.71 55.01 11.85 o
-13 5 4 27.04 38.01 15.07 o
-11 5 4 206.31 193.64 16.32 o
-9 5 4 167.02 150.02 14.00 o
-7 5 4 15.83 16.82 10.97 o
-5 5 4 68.67 74.21 8.77 o
-3 5 4 227.50 212.82 10.68 o
-1 5 4 13.83 26.18 10.01 o
1 5 4 7.93 13.05 9.47 o
3 5 4 308.64 317.54 16.46 o
5 5 4 2.53 1.26 9.93 o
7 5 4 1.78 -0.97 10.83 o
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1 3 10 638.92 663.66 17.72 o
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1 5 10 65.89 61.18 14.01 o
3 5 10 25.39 18.54 12.35 o
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1 1 11 16.99 19.96 5.20 o
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0 2 11 1229.09 1182.30 16.51 o
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1 3 11 149.65 137.13 14.87 o
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5 3 11 0.00 8.71 10.42 o
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1 5 11 93.90 95.13 14.47 o
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0 0 12 2629.10 2527.14 28.38 o
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-1 1 12 292.23 296.33 8.79 o
1 1 12 214.42 218.31 7.08 o
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5 1 12 9.07 7.86 5.09 o
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11 1 12 77.83 76.13 8.91 o
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-20 2 12 44.63 34.97 13.26 o
-18 2 12 70.18 73.32 15.09 o
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-8 2 12 103.53 101.56 9.51 o
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-2 2 12 572.67 539.10 11.80 o
0 2 12 95.27 99.88 11.07 o
2 2 12 1322.99 1248.67 16.73 o
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6 2 12 64.70 64.83 10.03 o
8 2 12 355.22 325.50 12.67 o
10 2 12 31.03 25.31 9.81 o
12 2 12 94.13 102.15 11.17 o
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-3 3 12 2.59 9.92 8.00 o
-1 3 12 417.35 388.83 13.00 o
1 3 12 134.07 163.19 12.64 o
3 3 12 282.89 274.40 11.98 o
5 3 12 178.19 168.49 14.26 o
7 3 12 13.40 17.71 12.13 o
9 3 12 10.75 32.97 11.93 o
-14 4 12 192.48 253.50 18.46 o
-12 4 12 18.82 1.46 14.78 o
-10 4 12 48.59 55.05 18.48 o
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-6 4 12 8.98 17.41 8.04 o
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-2 4 12 304.13 339.06 17.18 o
0 4 12 196.83 191.15 11.88 o
2 4 12 37.91 39.77 17.45 o
4 4 12 62.14 69.89 14.10 o
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-9 5 12 23.34 15.96 20.10 o
-7 5 12 13.89 15.43 13.65 o
-5 5 12 1.65 11.18 13.38 o
-3 5 12 0.86 5.57 10.16 o
-1 5 12 83.04 77.94 14.37 o
1 5 12 67.24 84.39 19.76 o
-21 1 13 14.47 29.09 14.26 o
-19 1 13 17.32 22.17 12.11 o
-17 1 13 19.39 32.66 9.20 o
-15 1 13 23.31 31.20 7.10 o
-13 1 13 17.69 26.19 7.67 o
-11 1 13 958.87 931.43 22.17 o
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-7 1 13 142.32 151.30 9.26 o
-5 1 13 1142.08 1251.23 15.19 o
-3 1 13 879.57 767.39 11.24 o
-1 1 13 14.89 16.85 5.68 o
1 1 13 422.23 373.33 9.22 o
3 1 13 275.27 316.80 10.65 o
5 1 13 1017.73 1032.69 14.04 o
7 1 13 253.16 256.20 9.06 o
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11 1 13 5.19 11.09 8.95 o
-20 2 13 0.00 -1.90 13.71 o
-18 2 13 0.21 3.53 12.58 o
-16 2 13 3.22 6.96 8.95 o
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-12 2 13 104.89 89.51 11.73 o
-10 2 13 75.20 79.76 7.50 o
-8 2 13 0.81 3.13 9.48 o
-6 2 13 0.19 7.24 4.66 o
-4 2 13 227.10 223.76 7.83 o
-2 2 13 1095.14 1161.74 17.09 o
0 2 13 683.98 718.29 27.36 o
2 2 13 99.95 97.76 7.55 o
4 2 13 57.27 57.52 7.17 o
6 2 13 9.61 7.83 7.40 o
8 2 13 0.82 10.61 8.69 o
10 2 13 15.43 18.78 9.59 o
-17 3 13 8.10 7.35 10.24 o
-15 3 13 46.54 41.63 10.89 o
-13 3 13 233.92 187.47 14.83 o
-11 3 13 7.70 14.47 10.01 o
-9 3 13 71.22 78.21 12.69 o
-7 3 13 261.05 253.75 10.97 o
-5 3 13 1314.52 1221.81 24.70 o
-3 3 13 255.15 240.56 11.95 o
-1 3 13 1.69 3.65 9.72 o
1 3 13 659.12 624.16 19.42 o
3 3 13 187.55 172.95 17.17 o
5 3 13 34.44 26.42 10.94 o
7 3 13 134.32 130.72 14.74 o
9 3 13 1.10 0.07 9.74 o
-14 4 13 31.05 21.80 12.89 o
-12 4 13 114.43 102.76 14.41 o
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-6 4 13 205.07 223.57 15.21 o
-4 4 13 11.75 9.52 8.77 o
-2 4 13 13.13 21.07 9.80 o
0 4 13 21.36 24.30 10.22 o
2 4 13 8.86 9.89 10.71 o
4 4 13 358.92 310.04 19.14 o
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-3 5 13 12.51 11.86 10.64 o
-1 5 13 327.68 377.12 21.14 o
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-18 0 14 1747.79 1682.06 46.09 o
-16 0 14 153.33 157.51 20.40 o
-14 0 14 1.84 12.59 15.94 o
-12 0 14 28.83 32.47 14.39 o
-10 0 14 2.03 3.65 12.24 o
-8 0 14 2271.98 2309.96 46.66 o
-6 0 14 472.67 444.08 21.74 o
-4 0 14 18.21 20.11 14.37 o
-2 0 14 194.93 188.57 17.38 o
0 0 14 837.65 808.95 20.87 o
2 0 14 713.93 613.21 14.84 o
4 0 14 243.55 202.51 11.19 o
6 0 14 83.49 71.50 9.40 o
8 0 14 2.08 9.52 10.07 o
10 0 14 37.96 37.77 11.62 o
-19 1 14 91.82 85.61 14.94 o
-17 1 14 447.90 485.43 16.02 o
-15 1 14 145.87 165.41 15.08 o
-13 1 14 517.13 517.27 13.88 o
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-7 1 14 5.24 11.30 7.81 o
-5 1 14 85.22 110.21 11.21 o
-3 1 14 25.15 30.63 5.15 o
-1 1 14 208.68 201.76 7.62 o
1 1 14 7.95 15.94 6.17 o
3 1 14 10.01 10.88 6.22 o
5 1 14 108.12 91.29 7.03 o
7 1 14 4.19 7.66 6.72 o
9 1 14 197.22 202.76 9.99 o
11 1 14 2.74 1.29 9.23 o
-18 2 14 55.77 62.05 13.72 o
-16 2 14 224.11 212.49 13.13 o
-14 2 14 49.37 42.96 11.04 o
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-2 2 14 140.18 147.10 12.67 o
0 2 14 783.97 735.46 15.49 o
2 2 14 14.38 16.74 6.80 o
4 2 14 34.07 32.65 9.15 o
6 2 14 17.00 12.06 9.80 o
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10 2 14 28.44 56.17 11.12 o
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-15 3 14 27.98 26.39 11.78 o
-13 3 14 69.67 81.89 13.79 o
-11 3 14 5.07 14.45 11.65 o
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-5 3 14 122.20 101.20 9.76 o
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-1 3 14 60.61 68.50 16.17 o
1 3 14 381.35 415.29 27.68 o
3 3 14 20.77 26.60 13.47 o
5 3 14 0.84 7.10 12.58 o
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0 4 14 71.24 84.51 19.70 o
2 4 14 168.14 189.99 17.29 o
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-17 1 15 323.82 331.65 19.47 o
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-7 1 15 332.56 306.09 14.80 o
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-3 1 15 49.74 81.32 8.58 o
-1 1 15 2.40 13.73 7.69 o
1 1 15 22.10 18.11 8.28 o
3 1 15 110.57 95.19 7.61 o
5 1 15 2.89 5.35 6.28 o
7 1 15 109.00 101.91 8.08 o
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-18 2 15 0.51 3.33 18.70 o
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-14 2 15 405.57 396.99 17.85 o
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-2 2 15 23.63 17.82 10.09 o
0 2 15 122.32 126.61 9.34 o
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4 2 15 53.55 59.02 10.24 o
6 2 15 180.55 180.77 11.40 o
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-11 3 15 13.76 16.08 12.71 o
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-1 3 15 4.04 14.48 11.41 o
1 3 15 343.42 326.04 19.53 o
3 3 15 2.92 1.88 11.21 o
5 3 15 5.19 9.45 13.73 o
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-10 4 15 55.83 47.22 14.99 o
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0 4 15 20.95 12.21 18.63 o
2 4 15 8.24 13.12 12.46 o
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-14 0 16 386.15 436.46 27.69 o
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-10 0 16 748.79 790.03 32.99 o
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0 0 16 64.29 77.89 8.68 o
2 0 16 70.53 76.40 8.77 o
4 0 16 58.59 60.29 10.26 o
6 0 16 399.18 422.30 16.08 o
8 0 16 14.56 20.59 11.03 o
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-1 1 16 304.06 315.06 10.96 o
1 1 16 75.89 78.60 9.61 o
3 1 16 402.96 381.26 11.28 o
5 1 16 110.16 112.32 8.89 o
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0 2 16 291.60 260.33 10.70 o
2 2 16 288.61 266.79 10.94 o
4 2 16 87.82 90.69 9.63 o
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-1 3 16 58.05 83.55 12.82 o
1 3 16 231.02 229.40 16.82 o
3 3 16 19.40 21.55 13.28 o
5 3 16 98.50 89.72 16.69 o
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-1 1 17 138.87 151.81 9.28 o
1 1 17 189.29 173.15 10.04 o
3 1 17 123.51 113.61 8.89 o
5 1 17 0.01 5.24 7.65 o
7 1 17 0.65 4.50 9.29 o
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0 2 17 13.59 20.20 9.90 o
2 2 17 68.94 69.42 8.70 o
4 2 17 57.61 60.63 9.68 o
6 2 17 4.56 7.88 11.88 o
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-7 3 17 31.40 26.92 9.83 o
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-1 3 17 23.99 22.17 12.85 o
1 3 17 228.74 227.51 18.83 o
3 3 17 0.25 3.38 14.62 o
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0 0 18 34.69 45.40 12.47 o
2 0 18 64.03 70.16 13.81 o
4 0 18 23.03 12.54 12.00 o
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-7 1 18 49.31 50.39 11.97 o
-5 1 18 282.60 274.42 12.47 o
-3 1 18 27.25 20.51 8.95 o
-1 1 18 0.12 6.25 7.49 o
1 1 18 20.72 18.26 7.75 o
3 1 18 9.01 9.67 7.93 o
5 1 18 162.17 166.57 10.76 o
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-14 2 18 79.23 89.41 23.94 o
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-10 2 18 0.43 12.60 10.92 o
-8 2 18 3.44 7.06 11.77 o
-6 2 18 17.52 14.08 11.27 o
-4 2 18 102.58 97.37 14.36 o
-2 2 18 34.19 28.25 12.08 o
0 2 18 30.16 46.33 9.79 o
2 2 18 120.38 126.05 15.87 o
4 2 18 14.57 18.78 11.85 o
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-11 3 18 2.55 11.66 12.81 o
-9 3 18 0.06 9.31 12.76 o
-7 3 18 91.48 94.80 22.71 o
-5 3 18 2.11 4.13 11.41 o
-3 3 18 78.20 76.64 14.80 o
-1 3 18 0.58 1.15 12.66 o
1 3 18 0.00 -0.77 13.27 o
-17 1 19 46.37 44.84 15.41 o
-15 1 19 519.63 500.18 37.61 o
-13 1 19 92.16 108.45 15.40 o
-11 1 19 41.19 41.48 12.66 o
-9 1 19 560.62 536.23 20.32 o
-7 1 19 88.05 104.63 14.28 o
-5 1 19 133.34 136.28 10.87 o
-3 1 19 616.98 557.20 14.87 o
-1 1 19 1.32 6.06 9.80 o
1 1 19 49.92 46.13 9.97 o
3 1 19 19.46 13.48 8.97 o
-14 2 19 11.28 21.86 19.11 o
-12 2 19 233.17 226.62 17.25 o
-10 2 19 19.23 36.21 20.84 o
-8 2 19 4.35 5.90 12.02 o
-6 2 19 1.35 4.29 12.48 o
-4 2 19 28.04 30.68 12.97 o
-2 2 19 316.31 316.84 25.30 o
0 2 19 56.96 50.55 11.60 o
2 2 19 285.80 309.37 16.90 o
-11 3 19 0.06 -6.55 13.77 o
-9 3 19 9.36 4.12 21.79 o
-7 3 19 26.72 28.26 20.66 o
-5 3 19 1.84 -0.48 12.59 o
-3 3 19 2.87 3.42 13.29 o
-16 0 20 50.31 50.85 19.65 o
-14 0 20 140.19 143.74 24.30 o
-12 0 20 0.15 21.41 16.81 o
-10 0 20 0.01 2.32 18.14 o
-8 0 20 18.94 9.52 14.90 o
-4 0 20 773.70 751.09 26.33 o
-2 0 20 34.95 33.16 12.79 o
0 0 20 363.60 369.84 30.39 o
2 0 20 158.89 150.79 17.93 o
-15 1 20 15.74 26.84 14.46 o
-13 1 20 25.75 13.03 18.82 o
-11 1 20 8.38 8.33 17.78 o
-9 1 20 44.63 44.59 13.58 o
-7 1 20 555.42 545.84 22.26 o
-5 1 20 216.97 224.29 20.83 o
-3 1 20 3.41 12.37 8.51 o
-1 1 20 398.29 380.55 16.44 o
1 1 20 11.95 9.15 9.18 o
-12 2 20 134.12 154.73 23.86 o
-10 2 20 7.59 24.19 20.67 o
-8 2 20 0.93 1.84 12.00 o
-6 2 20 50.48 56.33 14.30 o
-4 2 20 0.43 2.94 13.63 o
-2 2 20 0.84 8.79 11.57 o
-13 1 21 219.02 240.75 27.00 o
-11 1 21 123.06 136.77 23.06 o
-9 1 21 47.17 38.62 14.80 o
-7 1 21 0.88 -5.70 13.08 o
-5 1 21 13.07 10.15 13.84 o
-3 1 21 63.03 71.37 23.84 o
-1 1 21 19.29 20.61 11.39 o
-10 2 21 127.86 141.20 25.64 o
-8 2 21 24.59 26.18 14.76 o
-6 2 21 0.83 2.76 14.07 o
-10 0 22 661.08 645.10 36.42 o
-8 0 22 365.47 312.92 27.13 o
-6 0 22 295.04 309.27 19.56 o
-4 0 22 7.62 11.48 13.52 o
-9 1 22 0.05 1.44 13.84 o
-7 1 22 7.74 18.43 13.74 o