#------------------------------------------------------------------------------ #$Date: 2011-05-17 10:53:27 +0300 (Tue, 17 May 2011) $ #$Revision: 19531 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2018027.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018027_Fobs loop_ _publ_author_name 'Th\'ebault, Fr\'ed\'eric' '\"Ohrstr\"om, Lars' 'Haukka, Matti' _publ_section_title ; 2,3,6,7,10,11-Hexahydroxytriphenylene tetrahydrate: a new form of an important starting material for supramolecular chemistry and covalent organic frameworks ; _journal_coeditor_code EG3069 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o143 _journal_page_last o145 _journal_volume 67 _journal_year 2011 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.2694 _cell_length_b 16.5639 _cell_length_c 7.2237 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file eg3069Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LH6NaBH4_MSa in Pbcn (colourless block)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 197.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' 'x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 674.26 601.98 13.52 o 4 0 0 2632.49 2464.30 26.68 o 6 0 0 13889.08 14298.54 109.66 o 8 0 0 10732.82 11100.13 88.14 o 10 0 0 271.62 286.96 21.43 o 12 0 0 272.43 329.21 37.22 o 14 0 0 410.71 364.73 32.83 o 16 0 0 331.55 410.78 57.82 o 1 1 0 5886.29 5673.13 43.73 o 3 1 0 2.04 1.15 6.13 o 5 1 0 599.15 631.72 11.90 o 7 1 0 1199.45 1444.40 19.34 o 9 1 0 24.32 14.66 9.11 o 11 1 0 142.18 140.85 13.18 o 13 1 0 3.78 15.18 16.14 o 15 1 0 1270.43 1110.79 64.00 o 17 1 0 21.68 -17.25 39.48 o 0 2 0 2544.34 2337.11 26.97 o 2 2 0 147.63 166.85 6.31 o 4 2 0 146.57 133.61 8.56 o 6 2 0 1591.83 1566.25 19.18 o 8 2 0 2887.55 2914.94 27.97 o 10 2 0 315.08 330.91 14.25 o 12 2 0 38.39 51.27 13.36 o 14 2 0 140.43 173.78 20.14 o 16 2 0 56.51 73.21 29.61 o 1 3 0 630.32 603.66 10.14 o 3 3 0 500.67 439.43 15.11 o 5 3 0 1832.00 1711.06 22.48 o 7 3 0 818.74 850.55 16.12 o 9 3 0 24.51 19.07 10.20 o 11 3 0 7.83 15.56 14.87 o 13 3 0 0.23 6.37 16.00 o 15 3 0 36.79 26.67 27.21 o 0 4 0 16.33 -8.77 8.77 o 2 4 0 258.01 260.75 8.86 o 4 4 0 2159.61 2147.84 21.43 o 6 4 0 0.31 7.77 9.02 o 8 4 0 11.86 10.90 8.72 o 10 4 0 197.10 226.20 13.60 o 12 4 0 19.33 10.64 16.05 o 14 4 0 0.18 -8.49 17.44 o 16 4 0 0.02 38.62 36.19 o 1 5 0 1049.25 1025.41 13.77 o 3 5 0 843.33 961.95 13.93 o 5 5 0 2461.28 2306.36 24.67 o 7 5 0 603.78 621.17 15.25 o 9 5 0 261.35 249.73 13.02 o 11 5 0 54.33 57.56 14.99 o 13 5 0 50.54 34.84 27.69 o 15 5 0 37.82 -16.01 31.77 o 0 6 0 1556.70 1617.78 24.93 o 2 6 0 376.27 379.06 12.82 o 4 6 0 14247.88 15166.13 84.67 o 6 6 0 745.78 814.46 18.72 o 8 6 0 960.79 1017.93 20.05 o 10 6 0 1303.71 1353.02 26.68 o 12 6 0 3591.77 3613.78 77.55 o 14 6 0 47.55 39.94 26.07 o 16 6 0 52.76 49.71 65.12 o 1 7 0 3267.31 2873.68 23.57 o 3 7 0 5066.54 5718.48 39.17 o 5 7 0 1759.00 1799.64 25.58 o 7 7 0 306.22 297.07 12.28 o 9 7 0 325.52 393.20 16.55 o 11 7 0 9806.85 9966.26 91.85 o 13 7 0 11.57 -19.94 19.94 o 15 7 0 79.57 99.27 54.19 o 0 8 0 15565.27 14826.52 134.05 o 2 8 0 187.86 210.67 9.72 o 4 8 0 491.92 663.97 14.27 o 6 8 0 3291.58 3526.99 30.92 o 8 8 0 12.96 31.52 11.07 o 10 8 0 105.81 147.09 18.50 o 12 8 0 47.39 49.26 21.67 o 14 8 0 734.11 681.13 52.78 o 1 9 0 5397.92 5119.98 37.95 o 3 9 0 2278.43 2189.00 23.21 o 5 9 0 0.44 -7.18 7.18 o 7 9 0 239.89 248.40 19.39 o 9 9 0 170.40 262.51 21.39 o 11 9 0 498.47 519.70 35.97 o 13 9 0 162.70 154.61 25.65 o 15 9 0 5.86 91.58 45.04 o 0 10 0 609.01 542.15 21.32 o 2 10 0 385.78 354.43 10.80 o 4 10 0 40.14 27.41 8.85 o 6 10 0 151.35 152.12 13.64 o 8 10 0 446.30 545.51 33.77 o 10 10 0 2.08 29.85 23.99 o 12 10 0 241.40 189.49 26.87 o 14 10 0 10.07 -30.24 30.24 o 1 11 0 542.62 570.08 14.67 o 3 11 0 304.83 284.59 12.52 o 5 11 0 147.63 154.89 14.59 o 7 11 0 10.45 7.36 16.39 o 9 11 0 66.29 109.39 22.91 o 11 11 0 0.02 -4.06 26.82 o 13 11 0 6.90 -21.25 21.25 o 0 12 0 214.69 255.93 17.08 o 2 12 0 1072.01 1164.91 19.36 o 4 12 0 640.07 667.16 16.85 o 6 12 0 154.88 146.98 15.60 o 8 12 0 117.92 86.83 20.59 o 10 12 0 30.96 16.73 34.27 o 12 12 0 62.42 109.83 32.73 o 1 13 0 1511.69 1340.52 30.25 o 3 13 0 238.01 238.57 13.20 o 5 13 0 620.52 580.21 27.10 o 7 13 0 138.37 102.27 33.42 o 9 13 0 361.38 349.15 39.07 o 11 13 0 53.42 13.42 59.60 o 13 13 0 6.96 -18.55 53.68 o 0 14 0 548.74 525.22 58.08 o 2 14 0 1347.26 1229.09 42.50 o 4 14 0 378.40 351.28 19.20 o 6 14 0 106.50 87.24 29.84 o 8 14 0 168.26 162.81 32.89 o 10 14 0 160.24 124.11 33.70 o 1 15 0 83.56 97.21 27.94 o 3 15 0 725.06 702.19 39.51 o 5 15 0 174.36 85.92 67.82 o 7 15 0 39.82 75.92 43.94 o 9 15 0 432.27 406.09 40.82 o 11 15 0 56.12 153.14 63.94 o 0 16 0 4020.48 4187.24 298.16 o 2 16 0 82.73 62.11 32.13 o 4 16 0 9.09 -31.43 43.14 o 6 16 0 143.85 201.58 37.41 o 8 16 0 543.53 395.39 70.45 o 10 16 0 142.31 66.57 45.73 o 3 17 0 282.32 289.11 41.52 o 5 17 0 2.10 30.49 33.09 o 7 17 0 3.24 8.40 37.24 o 9 17 0 33.12 67.53 46.80 o 0 18 0 14.37 -42.23 57.62 o 2 18 0 2.81 -27.67 71.16 o 4 18 0 3.00 -32.23 32.81 o 6 18 0 4.51 -38.87 55.31 o 1 19 0 34.61 46.57 47.17 o 3 19 0 0.46 13.14 92.36 o 5 19 0 0.01 -50.13 50.13 o 1 1 1 2439.27 2258.83 12.94 o 2 1 1 172.17 172.28 4.56 o 3 1 1 7533.82 7177.26 27.69 o 4 1 1 1619.90 1708.62 11.59 o 5 1 1 1598.49 1576.26 11.68 o 6 1 1 277.32 209.91 6.74 o 7 1 1 1253.41 1349.61 13.28 o 8 1 1 245.73 242.08 7.68 o 9 1 1 657.01 715.49 15.52 o 10 1 1 649.89 661.26 13.05 o 11 1 1 68.26 53.05 8.59 o 12 1 1 234.94 241.06 12.01 o 13 1 1 10.99 2.21 11.48 o 14 1 1 87.10 81.60 15.02 o 15 1 1 0.11 -8.30 14.62 o 16 1 1 198.85 163.21 23.04 o 17 1 1 156.56 68.60 35.00 o 0 2 1 278.87 241.66 9.09 o 1 2 1 8343.06 7793.62 32.20 o 2 2 1 59.59 81.12 4.69 o 3 2 1 9197.12 8666.71 32.61 o 4 2 1 253.09 248.26 6.33 o 5 2 1 0.97 -0.15 5.04 o 6 2 1 1424.95 1357.62 13.03 o 7 2 1 68.52 85.27 6.94 o 8 2 1 262.52 273.08 8.51 o 9 2 1 315.13 361.41 10.06 o 10 2 1 197.72 233.31 9.06 o 11 2 1 98.66 130.65 8.95 o 12 2 1 339.95 298.00 12.64 o 13 2 1 46.39 21.50 13.42 o 14 2 1 0.31 21.21 14.95 o 15 2 1 14.93 -11.28 15.29 o 16 2 1 9.03 3.69 19.49 o 1 3 1 1858.97 1817.00 12.39 o 2 3 1 530.67 494.21 9.67 o 3 3 1 5.62 5.41 4.46 o 4 3 1 7821.15 7360.90 30.99 o 5 3 1 7.72 7.38 5.57 o 6 3 1 91.80 99.40 6.72 o 7 3 1 149.19 173.41 7.48 o 8 3 1 13.08 19.71 5.22 o 9 3 1 113.62 105.94 7.73 o 10 3 1 38.79 33.24 7.53 o 11 3 1 9.64 7.68 7.61 o 12 3 1 166.08 162.92 11.52 o 13 3 1 73.83 80.52 14.78 o 14 3 1 65.02 51.55 16.97 o 15 3 1 11.50 16.33 16.10 o 16 3 1 2.82 31.30 22.04 o 0 4 1 150.51 138.17 9.63 o 1 4 1 1.04 -2.97 4.26 o 2 4 1 664.69 683.44 8.05 o 3 4 1 2443.96 2313.74 15.75 o 4 4 1 580.53 539.22 7.61 o 5 4 1 3017.91 2983.92 18.76 o 6 4 1 189.51 235.22 7.64 o 7 4 1 843.73 880.65 12.01 o 8 4 1 236.77 238.27 8.99 o 9 4 1 0.35 -5.58 6.90 o 10 4 1 294.95 328.95 11.78 o 11 4 1 550.40 518.38 13.57 o 12 4 1 266.33 248.45 14.17 o 13 4 1 70.03 63.09 14.69 o 14 4 1 0.20 -6.19 16.83 o 15 4 1 12.66 5.47 19.06 o 16 4 1 0.63 -17.96 23.95 o 1 5 1 2350.14 2251.15 15.09 o 2 5 1 345.58 333.04 6.47 o 3 5 1 555.58 534.48 9.41 o 4 5 1 6071.26 6020.86 32.76 o 5 5 1 415.25 400.47 9.38 o 6 5 1 5.95 4.47 5.71 o 7 5 1 241.74 296.40 8.24 o 8 5 1 563.90 534.72 11.02 o 9 5 1 12.51 19.65 7.50 o 10 5 1 227.84 250.27 11.17 o 11 5 1 26.25 25.21 9.95 o 12 5 1 1233.42 1185.90 23.94 o 13 5 1 122.51 98.59 15.62 o 14 5 1 250.33 258.67 21.34 o 15 5 1 57.16 69.18 21.67 o 16 5 1 9.89 28.58 33.44 o 0 6 1 192.49 204.17 10.91 o 1 6 1 1393.06 1301.49 12.51 o 2 6 1 359.29 384.30 7.51 o 3 6 1 5482.85 5589.98 27.95 o 4 6 1 1022.19 1159.65 16.02 o 5 6 1 933.07 1041.98 13.61 o 6 6 1 1138.93 1131.75 13.61 o 7 6 1 375.39 419.17 9.86 o 8 6 1 1.31 -6.22 6.22 o 9 6 1 284.43 258.84 10.07 o 10 6 1 449.70 400.70 13.01 o 11 6 1 4.51 -0.80 11.86 o 12 6 1 45.02 47.83 17.17 o 13 6 1 163.63 155.29 18.39 o 14 6 1 179.65 212.55 22.49 o 15 6 1 63.85 31.21 21.46 o 16 6 1 0.31 84.21 33.07 o 1 7 1 9.76 5.63 6.70 o 2 7 1 499.88 563.36 9.98 o 3 7 1 495.38 675.45 10.81 o 4 7 1 228.59 225.02 9.86 o 5 7 1 2071.71 2200.64 18.87 o 6 7 1 189.52 205.12 8.63 o 7 7 1 849.93 865.11 14.58 o 8 7 1 78.80 86.41 7.34 o 9 7 1 315.04 322.48 10.07 o 10 7 1 1008.22 1049.89 24.23 o 11 7 1 3685.67 3646.92 38.32 o 12 7 1 708.12 719.37 32.72 o 13 7 1 680.67 619.63 27.28 o 14 7 1 10.79 16.65 18.58 o 15 7 1 0.11 -22.45 22.45 o 0 8 1 458.52 425.42 14.92 o 1 8 1 1687.59 1709.96 15.20 o 2 8 1 980.99 1058.84 14.26 o 3 8 1 14.77 9.23 5.70 o 4 8 1 1301.54 1420.97 14.84 o 5 8 1 47.94 35.71 6.50 o 6 8 1 175.73 235.18 9.58 o 7 8 1 285.48 295.66 10.49 o 8 8 1 396.35 382.18 11.41 o 9 8 1 87.16 78.64 12.17 o 10 8 1 549.34 587.15 19.11 o 11 8 1 1.82 -15.10 16.60 o 12 8 1 448.64 530.11 25.12 o 13 8 1 22.13 9.11 19.44 o 14 8 1 104.82 125.07 21.82 o 15 8 1 53.69 153.60 27.92 o 1 9 1 399.10 432.56 8.62 o 2 9 1 150.62 182.95 7.45 o 3 9 1 8.12 -3.92 5.48 o 4 9 1 15.51 4.17 6.10 o 5 9 1 608.92 602.36 13.16 o 6 9 1 7.58 9.71 7.76 o 7 9 1 105.05 118.17 10.24 o 8 9 1 26.45 35.92 9.83 o 9 9 1 25.53 30.24 10.53 o 10 9 1 485.43 458.11 25.80 o 11 9 1 390.91 465.13 21.19 o 12 9 1 319.02 314.87 22.65 o 13 9 1 10.44 13.26 21.84 o 14 9 1 94.30 105.25 22.69 o 15 9 1 0.10 -32.49 32.49 o 0 10 1 90.11 89.64 11.97 o 1 10 1 106.86 115.83 8.17 o 2 10 1 467.22 505.63 10.63 o 3 10 1 403.50 409.48 9.18 o 4 10 1 418.20 446.98 11.09 o 5 10 1 29.76 25.44 7.62 o 6 10 1 181.10 189.76 11.08 o 7 10 1 141.40 147.88 11.70 o 8 10 1 210.99 207.98 12.38 o 9 10 1 85.05 91.06 15.95 o 10 10 1 100.02 65.85 16.69 o 11 10 1 26.69 35.71 16.50 o 12 10 1 0.56 -17.10 17.10 o 13 10 1 5.37 39.59 30.77 o 14 10 1 3.80 1.28 26.45 o 1 11 1 221.27 219.20 9.52 o 2 11 1 84.22 73.64 7.03 o 3 11 1 174.97 201.76 8.05 o 4 11 1 825.82 882.39 16.36 o 5 11 1 13.94 17.86 8.41 o 6 11 1 205.56 207.42 12.73 o 7 11 1 7.28 1.24 9.91 o 8 11 1 29.64 38.23 11.94 o 9 11 1 14.69 21.60 17.47 o 10 11 1 59.73 153.85 19.72 o 11 11 1 18.94 34.10 17.44 o 12 11 1 15.98 6.59 17.73 o 13 11 1 26.08 27.67 22.57 o 14 11 1 10.27 41.96 34.61 o 0 12 1 533.86 484.75 18.87 o 1 12 1 891.96 879.39 15.79 o 2 12 1 4.23 3.40 7.21 o 3 12 1 702.57 694.36 13.70 o 4 12 1 71.49 58.09 9.20 o 5 12 1 510.99 567.64 14.79 o 6 12 1 36.78 43.16 12.23 o 7 12 1 541.30 442.96 17.40 o 8 12 1 8.28 26.68 23.98 o 9 12 1 179.73 129.15 20.64 o 10 12 1 2.51 6.88 18.29 o 11 12 1 204.49 181.08 24.68 o 12 12 1 11.59 -19.48 19.48 o 13 12 1 31.64 -36.51 36.51 o 1 13 1 2775.73 2752.50 28.59 o 2 13 1 1500.34 1491.42 20.41 o 3 13 1 42.59 42.96 9.26 o 4 13 1 270.92 297.16 13.23 o 5 13 1 0.05 -10.94 10.94 o 6 13 1 499.42 408.05 23.93 o 7 13 1 1583.39 1284.03 45.74 o 8 13 1 463.44 376.23 24.13 o 9 13 1 134.45 155.36 25.05 o 10 13 1 19.41 50.37 23.98 o 11 13 1 51.14 27.49 23.95 o 12 13 1 50.07 21.52 27.14 o 0 14 1 9789.25 9644.60 98.27 o 1 14 1 2913.54 2893.98 32.95 o 2 14 1 1042.51 1020.48 33.98 o 3 14 1 70.43 78.26 12.04 o 4 14 1 162.66 177.65 14.54 o 5 14 1 106.58 67.77 17.87 o 6 14 1 1334.32 1208.80 51.56 o 7 14 1 0.19 -0.92 15.51 o 8 14 1 565.99 525.57 28.05 o 9 14 1 169.04 123.98 28.61 o 10 14 1 0.74 6.64 30.33 o 11 14 1 1.89 10.89 27.52 o 12 14 1 18.02 7.62 44.60 o 1 15 1 105.53 168.44 25.51 o 2 15 1 225.46 253.54 29.56 o 3 15 1 22.58 37.61 20.74 o 4 15 1 0.13 13.28 27.89 o 5 15 1 30.20 5.74 21.48 o 6 15 1 33.31 38.48 21.00 o 7 15 1 11.87 23.65 21.16 o 8 15 1 0.00 7.96 21.50 o 9 15 1 19.61 22.29 28.08 o 10 15 1 12.43 18.65 32.68 o 11 15 1 16.56 76.17 58.81 o 0 16 1 424.00 479.59 41.03 o 1 16 1 333.68 279.68 23.98 o 2 16 1 0.40 62.30 42.62 o 3 16 1 5.43 5.56 20.16 o 4 16 1 19.55 79.38 27.51 o 5 16 1 109.39 156.14 35.63 o 6 16 1 23.29 26.93 24.75 o 7 16 1 39.49 38.46 25.12 o 8 16 1 27.65 0.52 24.88 o 9 16 1 4.16 6.70 29.18 o 10 16 1 6.98 41.05 61.18 o 1 17 1 18.79 133.01 64.73 o 2 17 1 69.77 66.71 23.62 o 3 17 1 1.19 6.28 22.58 o 4 17 1 0.30 -2.24 27.33 o 5 17 1 53.63 53.13 26.20 o 6 17 1 5.06 0.19 26.50 o 7 17 1 0.00 -25.46 25.46 o 8 17 1 0.64 -19.16 26.19 o 0 18 1 17.81 -39.21 39.21 o 1 18 1 1.12 25.99 25.88 o 2 18 1 79.04 43.96 35.11 o 3 18 1 2.98 -9.00 21.53 o 4 18 1 0.38 30.02 23.52 o 5 18 1 1.89 -13.94 33.13 o 6 18 1 44.97 24.29 27.53 o 7 18 1 29.84 14.68 30.58 o 1 19 1 64.89 93.46 39.45 o 2 19 1 100.55 42.56 41.13 o 3 19 1 99.32 99.29 45.18 o 4 19 1 317.94 354.03 73.81 o 0 0 2 1561.62 1525.20 38.83 o 1 0 2 37093.23 35808.27 193.39 o 2 0 2 38947.22 38595.16 207.69 o 3 0 2 6963.71 7125.72 43.52 o 4 0 2 6710.80 6330.06 42.84 o 5 0 2 1879.61 1940.32 25.65 o 6 0 2 2550.69 2597.77 28.67 o 7 0 2 209.48 227.50 12.59 o 8 0 2 11.39 -6.02 10.90 o 9 0 2 539.51 568.77 21.14 o 10 0 2 390.15 474.63 21.51 o 11 0 2 104.13 111.85 18.67 o 12 0 2 36.77 7.54 19.26 o 13 0 2 512.30 453.38 32.99 o 14 0 2 109.66 24.76 26.42 o 15 0 2 25.51 39.11 25.01 o 16 0 2 423.03 391.71 34.66 o 1 1 2 9459.03 9130.70 43.90 o 2 1 2 17321.60 16515.32 64.30 o 3 1 2 2633.67 2467.71 15.95 o 4 1 2 0.18 1.97 4.52 o 5 1 2 397.50 470.22 10.36 o 6 1 2 3096.42 3475.60 23.22 o 7 1 2 994.83 1043.38 14.47 o 8 1 2 776.05 792.77 16.15 o 9 1 2 1199.90 1190.55 19.28 o 10 1 2 514.71 556.29 15.72 o 11 1 2 45.53 18.78 11.25 o 12 1 2 211.40 196.43 16.55 o 13 1 2 386.60 354.24 22.04 o 14 1 2 56.32 66.90 19.04 o 15 1 2 3.08 -12.77 16.25 o 16 1 2 155.93 100.44 21.77 o 0 2 2 11232.35 10293.25 76.91 o 1 2 2 2175.79 1940.57 16.07 o 2 2 2 8.02 8.95 6.23 o 3 2 2 899.14 840.18 11.06 o 4 2 2 906.34 905.94 11.24 o 5 2 2 535.06 521.99 9.48 o 6 2 2 69.94 77.94 6.93 o 7 2 2 392.60 403.13 8.99 o 8 2 2 1035.55 981.54 16.20 o 9 2 2 26.26 30.25 8.99 o 10 2 2 222.32 200.64 12.27 o 11 2 2 73.29 63.44 12.39 o 12 2 2 7.71 6.79 13.40 o 13 2 2 23.05 20.63 16.36 o 14 2 2 4.48 -8.37 17.01 o 15 2 2 93.68 100.43 19.95 o 16 2 2 13.20 -20.98 20.98 o 1 3 2 2744.62 2518.83 19.11 o 2 3 2 2743.71 2657.71 17.21 o 3 3 2 709.80 576.25 9.04 o 4 3 2 288.84 288.92 8.02 o 5 3 2 145.02 159.83 6.82 o 6 3 2 146.78 159.81 6.54 o 7 3 2 65.32 52.56 5.88 o 8 3 2 3.59 -2.29 5.38 o 9 3 2 9.53 15.49 6.03 o 10 3 2 238.78 245.59 9.35 o 11 3 2 26.82 34.53 8.58 o 12 3 2 0.56 -11.97 13.38 o 13 3 2 13.70 16.57 16.53 o 14 3 2 13.91 -17.23 17.23 o 15 3 2 12.42 23.18 19.55 o 16 3 2 56.20 62.20 24.47 o 0 4 2 1753.12 1638.68 24.24 o 1 4 2 0.60 0.15 5.79 o 2 4 2 182.45 175.08 6.94 o 3 4 2 677.72 744.90 10.56 o 4 4 2 185.30 189.33 7.42 o 5 4 2 245.44 251.19 8.00 o 6 4 2 95.31 91.28 6.43 o 7 4 2 23.00 31.68 5.85 o 8 4 2 38.80 42.83 6.41 o 9 4 2 30.89 33.51 6.76 o 10 4 2 14.73 14.56 7.21 o 11 4 2 0.04 -1.79 9.25 o 12 4 2 58.36 30.44 25.30 o 13 4 2 13.33 8.27 20.46 o 14 4 2 0.00 -7.62 19.90 o 15 4 2 0.22 -1.69 24.32 o 16 4 2 6.72 -15.55 24.63 o 1 5 2 3060.06 3002.12 20.02 o 2 5 2 693.52 557.15 10.24 o 3 5 2 540.13 483.77 9.22 o 4 5 2 825.75 741.54 11.01 o 5 5 2 82.13 75.32 6.40 o 6 5 2 27.49 17.86 6.21 o 7 5 2 364.41 341.87 9.45 o 8 5 2 57.54 61.64 7.45 o 9 5 2 5.16 -0.92 6.92 o 10 5 2 80.48 76.74 8.52 o 11 5 2 33.74 27.45 10.16 o 12 5 2 2.97 -2.64 13.97 o 13 5 2 10.53 -9.18 18.65 o 14 5 2 120.46 101.36 23.28 o 15 5 2 26.39 36.19 22.43 o 16 5 2 50.24 15.60 35.56 o 0 6 2 3244.38 2889.68 27.27 o 1 6 2 5981.46 6007.16 31.23 o 2 6 2 918.56 1050.56 12.94 o 3 6 2 3287.90 3254.15 19.69 o 4 6 2 2446.29 2493.30 17.37 o 5 6 2 636.56 693.66 10.32 o 6 6 2 986.40 994.27 13.77 o 7 6 2 747.77 768.35 12.70 o 8 6 2 16.67 10.39 7.27 o 9 6 2 2220.27 2258.13 21.80 o 10 6 2 1798.12 1783.91 21.99 o 11 6 2 104.02 95.77 11.90 o 12 6 2 585.36 599.96 31.34 o 13 6 2 814.46 925.07 42.37 o 14 6 2 409.94 426.23 28.99 o 15 6 2 201.72 253.05 30.84 o 1 7 2 1759.83 1863.39 16.53 o 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