#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/81/2018193.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018193_Fobs loop_ _publ_author_name 'Ahmed, Maqsood' 'Noureen, Sajida' 'Gros, Philippe C.' 'Guillot, Benoit' 'Jelsch, Christian' _publ_section_title ; 2,2'-(Ethane-1,2-diyl)bis[2-(5-bromothiophen-2-yl)-1,3-dioxolane] at 100K refined using a multipolar atom model ; _journal_coeditor_code KU3047 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o329 _journal_page_last o333 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.845 _cell_angle_gamma 90.000 _cell_length_a 19.2550 _cell_length_b 5.7804 _cell_length_c 16.9328 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.8334 _[local]_cod_data_source_file ku3047Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' written by MoPro.11' _shelx_refln_list_code 4 _shelx_f_calc_maximum 636.29 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -22 0 2 70.74 32.75 22.47 o -22 0 4 3947.72 3809.79 88.52 o -22 0 6 3882.46 3914.65 88.52 o -22 0 8 85.46 87.91 14.30 o -22 0 10 287.93 260.86 12.94 o -22 0 12 1715.20 1880.04 47.66 o -22 2 6 1114.22 941.04 26.56 o -22 2 7 97.35 76.26 11.58 o -22 2 8 370.84 357.55 12.94 o -22 2 9 126.53 129.10 8.85 o -21 1 1 410.58 403.93 12.94 o -21 1 2 112.37 110.04 6.40 o -21 1 3 1108.40 1125.57 23.15 o -21 1 4 10.62 28.46 7.49 o -21 1 5 55.24 51.68 7.49 o -21 1 6 277.53 253.10 10.89 o -21 1 7 1072.89 1114.68 25.19 o -21 1 8 673.33 702.04 15.66 o -21 1 9 891.65 881.80 17.70 o -21 1 10 3404.40 3282.07 52.43 o -21 1 11 23.14 42.35 6.74 o -21 1 12 1344.66 1297.17 26.56 o -21 1 13 1098.44 1026.16 21.11 o -21 1 14 1541.13 1566.81 29.96 o -20 0 2 764.33 730.63 21.79 o -20 0 4 6915.17 7217.83 142.99 o -20 0 6 3987.36 4144.12 88.52 o -20 0 8 1406.03 1443.57 36.77 o -20 0 10 7879.68 8252.84 156.61 o -20 0 12 13315.43 13012.52 224.71 o -20 0 14 1211.67 1294.44 32.68 o -20 0 16 5988.76 5320.77 122.57 o -20 2 1 556.50 470.66 17.02 o -20 2 2 42.64 68.84 10.89 o -20 2 3 751.60 757.19 21.11 o -20 2 4 1429.59 1414.97 37.45 o -20 2 5 1119.10 1040.46 32.00 o -20 2 6 1383.47 1340.06 28.60 o -20 2 7 142.04 147.63 10.89 o -20 2 8 2627.51 2584.80 42.90 o -20 2 9 39.25 33.23 6.13 o -20 2 10 6209.60 6210.06 95.33 o -20 2 11 1245.53 1274.70 23.83 o -20 2 12 5282.54 4909.48 74.90 o -20 2 13 677.96 687.06 14.98 o -20 2 14 8395.87 8266.46 129.38 o -19 1 1 349.80 350.20 8.85 o -19 1 2 2913.13 3119.33 50.39 o -19 1 3 15.29 0.00 8.85 o -19 1 4 9639.92 10200.29 156.61 o -19 1 5 208.19 215.51 8.85 o -19 1 6 7573.04 7885.14 129.38 o -19 1 7 79.52 55.50 6.67 o -19 1 8 5027.88 5262.21 74.90 o -19 1 9 120.04 112.08 6.33 o -19 1 10 15723.98 15552.38 224.71 o -19 1 11 361.43 409.31 10.21 o -19 1 12 5413.18 5651.01 88.52 o -19 1 13 52.56 43.31 6.67 o -19 1 14 821.63 807.58 17.02 o -19 1 15 1915.06 1935.20 40.17 o -19 1 16 313.41 423.33 16.34 o -19 3 1 25.84 24.99 11.58 o -19 3 2 5787.86 5318.72 95.33 o -19 3 3 71.81 67.34 8.17 o -19 3 4 906.85 832.09 21.79 o -19 3 5 562.41 566.67 18.39 o -19 3 6 3506.50 3337.22 61.96 o -19 3 7 235.11 235.40 11.58 o -19 3 8 5837.64 5320.08 88.52 o -19 3 9 764.62 742.89 18.39 o -19 3 10 2628.22 2618.17 51.07 o -19 3 11 1254.23 1231.80 25.19 o -19 3 12 3336.96 3055.32 58.56 o -19 3 13 135.65 120.32 13.62 o -18 0 2 767.98 817.11 22.47 o -18 0 4 5714.08 5835.55 108.95 o -18 0 6 23494.33 22858.73 367.70 o -18 0 8 1393.64 1324.40 26.56 o -18 0 10 41.61 52.02 8.17 o -18 0 12 7087.08 7612.77 142.99 o -18 0 14 3177.11 3409.40 81.71 o -18 0 16 3312.46 3096.18 74.90 o -18 2 1 699.26 657.16 16.34 o -18 2 2 5056.35 5225.44 88.52 o -18 2 3 1768.11 1790.16 36.77 o -18 2 4 6982.74 6665.60 129.38 o -18 2 5 4132.83 4135.95 74.90 o -18 2 6 4964.93 4803.26 74.90 o -18 2 7 355.48 364.84 9.53 o -18 2 8 4289.51 4302.78 68.09 o -18 2 9 56.31 72.72 6.47 o -18 2 10 174.43 197.81 7.49 o -18 2 11 450.06 464.94 11.58 o -18 2 12 5.20 13.01 5.86 o -18 2 13 505.94 489.18 11.58 o -18 2 14 75.24 109.90 5.92 o -18 2 15 524.35 511.04 12.26 o -18 2 16 1208.39 1079.27 25.88 o -18 4 2 2759.03 2865.34 64.01 o -18 4 3 135.32 157.70 17.02 o -18 4 4 4018.24 3850.64 74.90 o -18 4 6 364.26 312.07 11.58 o -18 4 7 431.76 422.58 12.94 o -18 4 8 3943.11 3636.83 64.01 o -18 4 9 440.04 455.00 12.94 o -17 1 1 1847.32 1937.92 29.28 o -17 1 2 2002.25 1974.69 34.05 o -17 1 3 1453.90 1470.12 25.19 o -17 1 4 682.06 672.55 12.94 o -17 1 5 416.42 391.06 8.17 o -17 1 6 1719.83 1794.92 26.56 o -17 1 7 3183.49 3334.50 46.30 o -17 1 8 259.71 270.87 6.81 o -17 1 9 1951.25 2100.66 31.32 o -17 1 10 2971.43 3215.34 46.98 o -17 1 11 45.52 37.66 5.72 o -17 1 12 1919.36 1888.21 30.64 o -17 1 13 1154.87 1111.27 21.11 o -17 1 14 1413.48 1289.00 23.15 o -17 1 15 244.45 223.41 8.85 o -17 1 16 11169.52 10642.89 170.23 o -17 1 17 485.10 481.48 12.94 o -17 1 18 3494.43 3011.06 53.79 o -17 3 1 1332.76 1321.68 29.28 o -17 3 2 5026.50 4971.45 88.52 o -17 3 3 185.56 196.86 9.53 o -17 3 4 3885.75 3945.97 68.09 o -17 3 5 365.68 420.00 12.94 o -17 3 6 126.24 114.67 9.53 o -17 3 7 464.73 466.71 14.98 o -17 3 8 91.43 75.38 8.85 o -17 3 9 358.46 356.40 11.58 o -17 3 10 166.45 164.78 6.60 o -17 3 11 437.61 412.10 10.21 o -17 3 12 2914.93 2814.95 51.75 o -17 3 13 29.22 70.20 10.89 o -17 3 14 5661.01 5492.36 88.52 o -17 3 15 562.46 558.22 13.62 o -16 0 2 842.31 881.80 22.47 o -16 0 4 3962.15 4349.08 81.71 o -16 0 6 1365.01 1602.90 28.60 o -16 0 8 5701.18 6494.00 108.95 o -16 0 10 10602.13 11391.91 177.04 o -16 0 12 9771.08 9880.25 197.47 o -16 0 14 4001.36 3947.33 74.90 o -16 0 16 9879.58 10070.91 197.47 o -16 0 18 11520.36 11643.86 231.52 o -16 2 1 42.71 53.32 6.20 o -16 2 2 556.96 460.99 12.94 o -16 2 3 74.23 63.39 8.17 o -16 2 4 464.24 466.98 10.21 o -16 2 5 2509.60 2537.82 38.13 o -16 2 6 957.91 1058.84 17.02 o -16 2 7 1040.82 1020.71 16.34 o -16 2 8 3423.58 3670.20 51.75 o -16 2 9 1650.99 1745.22 26.56 o -16 2 10 8253.99 8171.13 108.95 o -16 2 11 1685.22 1760.88 28.60 o -16 2 12 6009.76 6083.40 95.33 o -16 2 13 782.44 788.51 16.34 o -16 2 14 9429.29 9308.27 142.99 o -16 2 15 23.99 41.33 8.85 o -16 2 16 12048.93 11739.18 183.85 o -16 2 17 1033.59 1000.96 21.79 o -16 4 1 172.97 162.54 16.34 o -16 4 2 42.08 37.31 12.26 o -16 4 3 255.58 269.17 11.58 o -16 4 4 413.33 436.81 14.30 o -16 4 6 3767.47 3684.50 64.69 o -16 4 7 65.68 72.93 8.85 o -16 4 8 5432.53 5259.48 88.52 o -16 4 9 1254.36 1175.96 23.83 o -16 4 10 825.65 840.26 17.02 o -16 4 11 7.16 37.66 10.89 o -16 4 12 4225.75 4255.79 74.90 o -16 4 13 393.46 393.92 14.98 o -15 1 1 2091.01 1993.75 29.28 o -15 1 2 1177.48 1259.03 21.11 o -15 1 3 1652.25 1702.32 26.56 o -15 1 4 17611.73 17922.00 238.32 o -15 1 5 20.22 23.70 3.61 o -15 1 6 17705.17 19406.43 251.94 o -15 1 7 222.26 201.89 6.47 o -15 1 8 2146.69 2219.82 32.00 o -15 1 9 9.14 19.68 5.11 o -15 1 10 32340.87 35047.32 456.22 o -15 1 11 865.13 904.27 14.98 o -15 1 12 13866.57 14456.08 197.47 o -15 1 14 5683.38 5554.32 88.52 o -15 1 15 818.45 793.28 15.66 o -15 1 16 2328.12 2406.40 39.49 o -15 1 17 4.74 13.28 6.33 o -15 1 18 1864.93 1779.26 31.32 o -15 3 1 7.66 18.86 5.52 o -15 3 2 7861.66 7095.26 108.95 o -15 3 3 38.06 64.01 8.17 o -15 3 4 3028.51 2659.70 44.94 o -15 3 5 1927.46 1886.85 33.37 o -15 3 6 4773.57 4798.49 74.90 o -15 3 7 40.24 36.43 6.81 o -15 3 8 14136.48 14578.65 211.09 o -15 3 9 1714.34 1691.42 26.56 o -15 3 10 1739.95 1813.99 28.60 o -15 3 11 2170.63 2090.45 37.45 o -15 3 12 9339.83 9308.27 136.19 o -15 3 13 53.47 49.71 6.74 o -15 3 14 6336.97 6235.93 102.14 o -15 3 15 1004.04 954.66 21.11 o -15 3 16 901.78 877.03 23.15 o -15 5 1 340.02 310.23 16.34 o -15 5 2 2368.38 2101.34 42.90 o -15 5 4 1281.86 1269.25 28.60 o -15 5 5 266.69 231.99 13.62 o -15 5 6 1535.09 1581.79 32.68 o -15 5 7 45.51 35.48 10.21 o -15 5 8 8255.25 8709.06 142.99 o -15 5 9 609.08 601.53 18.39 o -14 0 2 8988.15 9308.27 163.42 o -14 0 4 9519.61 9655.55 163.42 o -14 0 6 33459.25 35748.68 537.93 o -14 0 8 16692.34 17962.86 285.99 o -14 0 10 3043.59 3142.48 55.84 o -14 0 12 21201.48 21176.84 340.46 o -14 0 14 1613.76 1658.06 33.37 o -14 0 16 441.40 461.26 15.66 o -14 0 18 399.66 529.28 21.11 o -14 2 1 2302.41 2168.07 32.00 o -14 2 2 14898.98 14067.96 190.66 o -14 2 3 2849.71 2727.11 39.49 o -14 2 4 14251.37 15205.10 204.28 o -14 2 5 3506.13 3568.74 49.71 o -14 2 6 9691.94 9832.59 129.38 o -14 2 7 178.73 193.79 5.92 o -14 2 8 13462.17 13502.79 170.23 o -14 2 9 1608.28 1666.23 23.83 o -14 2 10 5619.68 5492.36 74.90 o -14 2 11 2889.62 2870.79 40.86 o -14 2 12 779.08 802.13 14.30 o -14 2 13 11.35 22.06 6.26 o -14 2 14 81.47 105.14 7.49 o -14 2 15 573.48 565.92 12.94 o -14 2 16 198.34 233.76 10.21 o -14 2 17 249.56 234.44 8.85 o -14 2 18 780.92 656.28 17.02 o -14 4 1 28.41 24.31 9.53 o -14 4 2 6174.54 5973.77 102.14 o -14 4 3 725.29 779.66 19.07 o -14 4 4 4849.58 5055.88 81.71 o -14 4 5 490.77 483.05 12.26 o -14 4 6 1992.14 1905.23 34.05 o -14 4 7 659.83 665.27 13.62 o -14 4 8 5320.44 5300.34 74.90 o -14 4 9 145.99 164.51 6.81 o -14 4 10 9054.14 8988.24 136.19 o -14 4 11 38.16 27.17 9.53 o -14 4 12 244.42 249.90 11.58 o -14 4 13 46.76 42.90 10.89 o -14 4 14 784.96 721.78 17.02 o -13 1 1 2077.81 1996.48 29.28 o -13 1 2 1481.74 1599.50 25.19 o -13 1 3 1714.91 1707.77 26.56 o -13 1 4 12421.77 13060.18 177.04 o -13 1 5 297.06 320.78 6.81 o -13 1 6 9125.60 9369.56 129.38 o -13 1 7 1869.89 2042.10 29.28 o -13 1 8 603.30 668.26 11.58 o -13 1 9 555.09 554.55 10.21 o -13 1 10 2997.08 2893.26 41.54 o -13 1 11 249.14 270.12 6.60 o -13 1 12 16.65 46.30 4.56 o -13 1 13 4224.83 4136.63 58.56 o -13 1 14 3387.64 3404.64 50.39 o -13 1 15 523.52 530.44 10.21 o -13 1 16 9635.68 9308.27 136.19 o -13 1 17 220.21 223.07 7.49 o -13 1 18 2472.49 2428.19 48.35 o -13 1 19 550.12 556.59 17.02 o -13 3 1 461.54 496.12 9.53 o -13 3 2 14924.98 15089.35 211.09 o -13 3 3 644.12 661.04 12.94 o -13 3 4 6779.77 6727.56 95.33 o -13 3 5 3449.91 3404.64 48.35 o -13 3 6 4059.86 4049.47 55.84 o -13 3 7 130.31 123.72 5.79 o -13 3 8 789.41 751.74 12.94 o -13 3 9 169.21 176.22 5.24 o -13 3 10 459.54 444.37 11.58 o -13 3 11 94.29 93.56 6.06 o -13 3 12 3041.95 2951.14 43.58 o -13 3 13 666.67 660.50 14.30 o -13 3 14 3233.21 3055.32 51.07 o -13 3 15 1895.56 1875.27 33.37 o -13 3 16 924.94 920.61 21.11 o -13 3 17 86.56 87.02 8.17 o -13 5 1 163.90 166.76 12.94 o -13 5 2 5443.75 5532.53 102.14 o -13 5 3 657.99 677.59 19.07 o -13 5 4 1926.25 1900.47 37.45 o -13 5 5 120.20 104.93 11.58 o -13 5 6 173.66 183.78 11.58 o -13 5 7 316.60 334.61 12.26 o -13 5 8 1369.41 1432.67 27.24 o -13 5 9 271.53 248.33 11.58 o -13 5 10 549.79 532.42 15.66 o -13 5 11 26.14 28.33 9.53 o -13 5 12 1375.65 1473.53 32.00 o -12 0 2 5554.37 5787.88 102.14 o -12 0 4 7732.72 7789.81 122.57 o -12 0 6 985.48 1182.77 21.11 o -12 0 8 12820.37 13523.21 231.52 o -12 0 10 8340.47 9022.29 142.99 o -12 0 12 17997.22 18997.87 299.61 o -12 0 14 592.37 578.65 13.62 o -12 0 16 17527.50 17527.07 306.42 o -12 0 18 8555.19 8831.63 197.47 o -12 0 20 1459.19 1564.77 56.52 o -12 2 1 3595.77 3674.28 51.07 o -12 2 2 4075.23 4383.81 61.28 o -12 2 3 1496.41 1499.40 23.15 o -12 2 4 3.03 28.60 4.43 o -12 2 5 509.21 505.79 9.53 o -12 2 6 8.49 19.41 4.22 o -12 2 7 1472.18 1574.30 21.79 o -12 2 8 1810.93 1977.41 26.56 o -12 2 9 1433.96 1533.45 21.79 o -12 2 10 9161.32 9355.94 122.57 o -12 2 11 3183.44 3128.18 42.90 o -12 2 12 7506.60 7136.12 95.33 o -12 2 13 1005.95 979.17 16.34 o -12 2 14 6917.40 6611.80 95.33 o -12 2 15 168.51 149.60 6.67 o -12 2 16 13007.33 12712.91 183.85 o -12 2 17 1583.42 1531.41 29.28 o -12 2 18 7411.18 7068.02 108.95 o -12 2 19 231.97 216.33 15.66 o -12 4 1 1814.74 1783.35 30.64 o -12 4 2 370.10 440.63 12.26 o -12 4 3 340.90 280.61 10.89 o -12 4 4 5729.09 5625.14 88.52 o -12 4 5 0.25 10.15 4.90 o -12 4 6 3637.96 3875.84 55.84 o -12 4 7 598.33 623.25 12.26 o -12 4 8 2701.40 2699.20 40.17 o -12 4 9 504.28 493.26 12.94 o -12 4 10 1717.71 1663.51 30.64 o -12 4 11 553.69 540.66 14.98 o -12 4 12 2862.36 2955.91 48.35 o -12 4 13 53.42 63.39 6.40 o -12 4 14 11585.93 11371.48 177.04 o -12 4 15 347.85 335.22 13.62 o -11 1 1 5603.37 5965.60 81.71 o -11 1 2 2270.87 2360.09 32.68 o -11 1 3 1848.16 1843.95 25.88 o -11 1 4 17432.67 17683.68 231.52 o -11 1 5 1912.58 2070.70 30.64 o -11 1 6 19414.25 21742.01 285.99 o -11 1 7 617.85 616.78 10.21 o -11 1 8 5046.91 5237.69 68.09 o -11 1 9 1840.63 1864.38 27.24 o -11 1 10 30764.49 31506.50 408.56 o -11 1 11 1032.69 1025.48 15.66 o -11 1 12 17745.31 17724.54 238.32 o -11 1 13 2.90 0.07 4.36 o -11 1 14 11180.37 11187.63 149.80 o -11 1 15 240.80 222.53 5.99 o -11 1 16 8918.61 8606.92 122.57 o -11 1 17 159.68 138.09 8.17 o -11 1 18 5830.71 6018.03 108.95 o -11 1 19 627.86 650.69 21.11 o -11 3 1 386.28 411.28 8.85 o -11 3 2 7996.57 8675.01 115.76 o -11 3 3 59.74 38.88 5.86 o -11 3 4 566.54 601.33 10.89 o -11 3 5 4251.88 4382.45 59.92 o -11 3 6 10144.82 10452.23 136.19 o -11 3 8 19793.10 19501.76 251.94 o -11 3 9 7.00 13.89 6.33 o -11 3 10 2826.02 2855.81 41.54 o -11 3 11 380.41 369.47 9.53 o -11 3 12 9089.15 9117.62 129.38 o -11 3 13 352.43 332.50 8.85 o -11 3 14 13036.76 12147.74 183.85 o -11 3 15 1074.63 1073.82 23.15 o -11 3 16 4324.61 4292.56 74.90 o -11 3 17 1022.31 1005.05 23.15 o -11 3 18 636.18 623.93 19.75 o -11 5 1 799.08 943.77 21.11 o -11 5 2 2494.81 2597.74 49.71 o -11 5 3 56.29 58.22 7.49 o -11 5 4 577.04 604.46 14.30 o -11 5 5 164.84 169.35 8.85 o -11 5 6 3421.94 3713.78 62.65 o -11 5 7 407.94 398.96 11.58 o -11 5 8 10717.47 11024.21 170.23 o -11 5 9 418.33 425.85 13.62 o -11 5 10 2509.90 2648.13 50.39 o -11 5 11 79.83 71.09 12.94 o -11 5 12 2878.64 2788.40 50.39 o -11 5 13 92.39 112.22 12.94 o -10 0 2 30239.80 29388.82 456.22 o -10 0 4 16624.36 17268.31 265.56 o -10 0 6 64623.06 62665.73 1157.58 o -10 0 8 5763.90 6052.08 88.52 o -10 0 10 36925.91 37369.29 565.17 o -10 0 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51.00 5.79 o -10 4 12 2212.43 2189.18 35.41 o -10 4 13 543.31 503.34 12.26 o -10 4 14 1408.07 1461.27 27.92 o -10 4 16 615.88 560.74 17.02 o -10 6 1 255.40 252.42 14.30 o -10 6 2 3004.54 3036.25 59.24 o -10 6 3 817.48 857.29 22.47 o -10 6 4 1849.65 1937.92 36.77 o -10 6 5 971.74 1026.16 23.15 o -10 6 6 1210.27 1360.49 27.92 o -10 6 7 281.62 275.09 11.58 o -10 6 8 2451.49 2426.14 47.66 o -9 1 1 427.37 492.24 8.17 o -9 1 2 9675.83 9893.87 129.38 o -9 1 3 234.99 223.62 4.77 o -9 1 4 18368.69 19413.23 251.94 o -9 1 5 1894.50 2014.18 27.92 o -9 1 6 33153.92 33065.82 422.17 o -9 1 7 727.80 792.60 12.26 o -9 1 8 13676.03 14006.67 183.85 o -9 1 9 588.64 588.87 9.53 o -9 1 10 615.42 693.86 10.89 o -9 1 11 0.79 3.54 4.15 o -9 1 12 2711.29 2731.88 37.45 o -9 1 13 875.70 932.19 14.30 o -9 1 14 2489.03 2417.29 34.05 o -9 1 15 386.84 381.66 8.17 o -9 1 16 6587.89 6553.92 102.14 o -9 1 17 928.17 996.20 19.75 o -9 1 18 1918.37 2010.78 39.49 o -9 1 19 1367.32 1482.38 35.41 o -9 1 20 3131.77 3036.94 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12 3093.76 3339.27 88.52 o 10 2 0 7250.38 7027.17 95.33 o 10 2 1 5875.17 5713.66 81.71 o 10 2 2 2542.53 2507.85 36.77 o 10 2 3 1471.54 1491.23 22.47 o 10 2 4 198.61 188.89 6.33 o 10 2 5 215.52 216.47 6.81 o 10 2 6 333.09 340.26 7.49 o 10 2 7 1546.98 1583.16 25.19 o 10 2 8 900.87 977.81 16.34 o 10 2 9 33.63 37.18 7.49 o 10 2 10 1185.93 1244.05 23.15 o 10 2 11 31.80 17.02 7.49 o 10 2 12 3842.48 3870.39 63.33 o 10 4 0 7834.22 7231.45 102.14 o 10 4 1 126.58 126.45 6.74 o 10 4 2 381.15 415.16 10.89 o 10 4 3 475.57 463.23 12.94 o 10 4 4 2932.24 2799.29 49.71 o 10 4 5 382.26 386.43 12.26 o 10 4 6 364.34 335.08 12.94 o 10 4 7 68.17 88.25 10.21 o 10 4 8 2053.70 2079.55 38.13 o 10 4 9 16.25 35.27 12.26 o 10 6 0 906.86 945.13 23.15 o 10 6 1 795.77 788.51 22.47 o 11 1 0 0.66 17.02 4.15 o 11 1 1 115.26 131.28 4.77 o 11 1 2 153.50 173.09 5.04 o 11 1 3 1667.19 1709.13 23.83 o 11 1 4 2932.53 2855.81 38.81 o 11 1 5 5769.54 5713.66 74.90 o 11 1 6 8125.59 7919.18 108.95 o 11 1 7 1176.66 1261.08 21.11 o 11 1 8 386.01 332.84 10.89 o 11 1 9 231.92 222.12 11.58 o 11 1 10 6074.81 6262.49 108.95 o 11 1 11 525.71 546.10 20.43 o 11 1 12 3902.84 3931.67 74.90 o 11 3 0 93.04 95.74 6.47 o 11 3 1 122.64 133.19 5.86 o 11 3 2 445.38 500.35 10.21 o 11 3 3 903.79 854.56 14.30 o 11 3 4 1553.47 1464.67 23.83 o 11 3 5 1884.62 1796.29 31.32 o 11 3 6 451.00 423.20 12.94 o 11 3 7 10.50 0.68 5.65 o 11 3 8 8894.11 9049.52 129.38 o 11 3 9 1.66 6.60 8.17 o 11 3 10 3001.34 2795.89 47.66 o 11 5 0 105.40 114.26 11.58 o 11 5 1 56.90 49.16 11.58 o 11 5 2 1427.25 1481.02 30.64 o 11 5 3 134.16 159.27 12.94 o 11 5 4 96.81 98.19 13.62 o 11 5 5 88.26 64.96 14.30 o 12 0 0 12704.00 12672.05 217.90 o 12 0 2 4737.92 4523.40 74.90 o 12 0 4 5044.01 5022.52 88.52 o 12 0 6 16754.80 16246.92 272.37 o 12 0 8 8509.91 8804.39 177.04 o 12 0 10 109.50 150.08 21.11 o 12 2 0 3454.67 3327.69 46.98 o 12 2 1 1714.76 1670.31 24.51 o 12 2 2 3303.12 3187.42 44.94 o 12 2 3 705.65 732.00 12.26 o 12 2 4 4455.69 4197.24 59.24 o 12 2 5 561.81 582.94 11.58 o 12 2 6 9320.22 9791.73 136.19 o 12 2 7 3001.67 3023.32 46.30 o 12 2 8 3796.88 3979.34 62.65 o 12 2 9 2970.35 2997.44 47.66 o 12 2 10 3075.74 3146.56 55.16 o 12 4 0 703.77 647.02 13.62 o 12 4 1 199.40 173.09 8.85 o 12 4 2 7217.96 6850.13 115.76 o 12 4 3 57.61 30.98 9.53 o 12 4 4 4206.77 4339.55 81.71 o 12 4 5 43.29 24.92 12.94 o 12 4 6 2157.06 2243.66 46.30 o 12 4 7 134.16 145.38 12.26 o 13 1 0 29180.65 30968.57 401.75 o 13 1 1 1060.48 1066.33 16.34 o 13 1 2 9338.66 9662.36 129.38 o 13 1 3 527.48 510.90 9.53 o 13 1 4 9717.12 8654.58 115.76 o 13 1 5 0.83 8.17 4.22 o 13 1 6 8236.37 8545.64 122.57 o 13 1 7 103.45 100.10 8.85 o 13 1 8 1946.98 1869.83 32.68 o 13 1 10 13.48 51.48 13.62 o 13 3 0 1088.01 1022.07 17.02 o 13 3 1 344.42 354.56 8.17 o 13 3 2 10481.60 10663.32 156.61 o 13 3 3 208.69 185.89 8.17 o 13 3 4 7933.16 7565.10 115.76 o 13 3 5 162.32 147.69 8.17 o 13 3 6 241.46 261.07 9.53 o 13 3 7 205.31 187.12 9.53 o 13 3 8 692.27 689.78 19.75 o 13 5 0 124.97 156.75 12.26 o 13 5 1 54.40 49.91 12.94 o 13 5 2 4152.91 4214.94 81.71 o 13 5 3 120.57 117.66 14.30 o 14 0 0 19004.28 19147.67 326.85 o 14 0 2 10486.28 10241.15 163.42 o 14 0 4 199.86 205.37 8.17 o 14 0 6 1097.32 1131.70 28.60 o 14 0 8 706.84 778.30 29.96 o 14 0 10 899.46 1047.95 36.77 o 14 2 0 12907.54 11759.61 163.42 o 14 2 1 9173.57 8532.02 115.76 o 14 2 2 5313.68 5241.78 81.71 o 14 2 3 4152.30 4248.30 63.33 o 14 2 4 764.16 729.27 13.62 o 14 2 5 27.43 15.05 5.79 o 14 2 6 4.82 11.10 6.06 o 14 2 7 1201.00 1264.48 24.51 o 14 2 8 1.11 3.75 9.53 o 14 2 9 92.76 112.49 11.58 o 14 4 0 3664.22 3540.82 61.28 o 14 4 1 153.70 94.17 12.26 o 14 4 2 585.55 606.37 17.70 o 14 4 3 60.66 59.85 10.89 o 14 4 4 1554.35 1579.75 34.73 o 14 4 5 158.54 187.46 12.94 o 15 1 0 43.27 43.17 5.38 o 15 1 1 40.50 31.66 4.70 o 15 1 2 1439.17 1428.59 23.15 o 15 1 3 775.43 791.24 14.98 o 15 1 4 2185.45 2177.61 34.73 o 15 1 5 1449.82 1404.07 24.51 o 15 1 6 1553.04 1656.70 30.64 o 15 1 7 176.07 147.08 10.21 o 15 1 8 199.30 227.63 14.30 o 15 3 0 1001.67 981.90 19.07 o 15 3 1 648.30 693.86 15.66 o 15 3 2 367.62 363.14 10.89 o 15 3 3 524.07 477.26 13.62 o 15 3 4 83.45 84.57 8.17 o 15 3 5 229.18 234.92 12.26 o 15 3 6 107.64 151.44 13.62 o 16 0 0 2158.44 2140.84 42.22 o 16 0 2 2141.29 2050.95 39.49 o 16 0 4 1639.11 1728.19 40.17 o 16 0 6 5467.94 5462.40 136.19 o 16 0 8 1536.52 1521.19 44.94 o 16 2 0 966.20 883.16 17.70 o 16 2 1 962.51 988.03 19.07 o 16 2 2 997.77 1045.22 19.75 o 16 2 3 895.91 821.20 19.75 o 16 2 4 1135.67 974.41 26.56 o 16 2 5 1968.52 1907.96 37.45 o 16 2 6 2297.35 2227.99 43.58 o 16 4 0 51.61 1.57 14.98 o 16 4 2 3220.84 3189.46 68.09 o 17 1 0 8605.59 8981.43 129.38 o 17 1 1 99.30 123.79 6.67 o 17 1 2 2621.90 2413.21 40.86 o 17 1 3 23.39 27.71 7.49 o 17 1 4 1971.69 2051.63 38.81 o 17 1 5 184.81 197.33 10.21 o 17 1 6 7754.95 8382.21 142.99 o 17 3 0 1079.73 1041.14 23.15 o 17 3 1 236.12 242.48 12.26 o 17 3 2 2686.28 2691.02 56.52 o 17 3 3 99.57 54.47 17.02 o 18 0 0 11737.88 10261.57 183.85 o 18 0 2 6617.90 6870.56 149.80 o 18 0 4 380.75 441.24 21.79 o 18 2 0 5546.35 5540.70 95.33 o 18 2 1 1369.45 1470.12 34.05 o 18 2 2 4583.32 4392.66 88.52 o 18 2 3 181.14 165.53 11.58 o 18 2 4 2501.87 2466.32 55.84 o 19 1 0 1198.92 1180.05 21.79 o 19 1 1 122.33 121.61 6.67 o 19 1 2 1315.98 1357.77 27.24 o 19 1 3 38.18 32.55 8.17 o 19 3 0 2027.30 1916.81 50.39 o 20 0 0 53.85 39.22 15.66 o 20 0 2 191.51 247.24 17.02 o 20 2 0 401.60 362.25 14.98 o 21 1 0 4010.01 4310.27 88.52 o