#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/81/2018198.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018198_Fobs loop_ _publ_author_name 'Parkin, Sean R.' 'Behrman, Edward J.' _publ_section_title ; Channel-forming solvate crystals and isostructural solvent-free powder of 5-hydroxy-6-methyl-2-pyridone ; _journal_coeditor_code MX3051 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o324 _journal_page_last o328 _journal_volume 67 _journal_year 2011 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 24.9131 _cell_length_b 24.9131 _cell_length_c 5.2462 _exptl_crystal_F_000 1188.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file mx3051Ic1sup4.hkl _[local]_cod_data_source_block Ic1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k09075' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 3 0 13626.91 9882.44 120.26 o -2 4 0 3350.53 5071.24 65.85 o -4 5 0 4391.69 2830.07 34.22 o -1 5 0 16570.62 17848.12 223.21 o -3 6 0 1649.43 1097.11 15.81 o 0 6 0 1767.58 1588.59 20.83 o -5 7 0 1533.02 2037.82 25.86 o -2 7 0 26961.01 29619.06 414.33 o -7 8 0 3568.93 3048.41 39.02 o -4 8 0 6689.15 5901.19 77.35 o -1 8 0 1324.38 885.59 14.13 o -6 9 0 11084.99 13074.66 158.06 o -3 9 0 1233.73 1055.97 18.73 o 0 9 0 3821.35 3545.56 43.34 o -8 10 0 2609.24 2452.61 31.74 o -5 10 0 6057.83 6275.92 82.74 o -2 10 0 1388.77 1110.50 18.15 o -10 11 0 1052.09 937.38 22.45 o -7 11 0 679.60 702.13 16.54 o -4 11 0 1163.60 1154.74 21.42 o -1 11 0 24398.40 27026.29 337.73 o -9 12 0 245.25 238.66 8.35 o -6 12 0 3801.30 3912.19 58.87 o -3 12 0 4932.36 4760.19 63.81 o 0 12 0 5054.56 5692.78 94.51 o -11 13 0 280.08 255.75 9.08 o -8 13 0 71.91 122.92 11.81 o -5 13 0 525.26 551.25 23.63 o -2 13 0 1758.32 1773.47 29.20 o -13 14 0 240.03 241.36 10.76 o -10 14 0 772.94 660.93 31.90 o -7 14 0 24.85 88.28 16.54 o -4 14 0 4667.32 4658.43 71.48 o -1 14 0 5824.34 5876.51 165.39 o -12 15 0 2.22 -1.18 6.68 o -9 15 0 1380.55 1669.62 33.49 o -6 15 0 4952.28 5250.93 84.42 o -3 15 0 2763.29 3013.76 86.24 o 0 15 0 2444.37 2596.90 47.59 o -14 16 0 0.47 -3.54 8.35 o -11 16 0 286.99 343.51 18.90 o -8 16 0 2163.65 2362.34 66.16 o -5 16 0 888.57 890.79 26.11 o -2 16 0 1109.09 1256.75 29.69 o -16 17 0 126.92 145.16 12.45 o -13 17 0 7.28 -5.80 9.08 o -10 17 0 1588.33 1559.17 40.91 o -7 17 0 9055.20 9924.27 281.17 o -4 17 0 751.90 797.71 27.52 o -1 17 0 2037.57 1980.08 55.53 o -15 18 0 10.65 8.27 13.00 o -12 18 0 1155.23 1078.99 28.35 o -9 18 0 128.50 123.63 17.42 o -6 18 0 5.34 9.03 12.45 o -3 18 0 27.27 11.44 15.29 o 0 18 0 5.17 -1.82 10.76 o -17 19 0 3678.15 3534.52 74.00 o -14 19 0 813.70 769.94 24.40 o -11 19 0 1210.20 1195.53 39.99 o -8 19 0 929.46 1005.35 35.78 o -5 19 0 2000.13 1842.37 54.34 o -2 19 0 2393.84 2372.47 73.25 o -19 20 0 409.66 332.79 22.51 o -16 20 0 2430.59 2722.21 53.39 o -13 20 0 328.47 307.29 34.26 o -10 20 0 7.32 -16.54 17.10 o -7 20 0 3.51 20.77 15.29 o -4 20 0 3308.36 3627.53 105.59 o -1 20 0 2114.07 2278.74 77.97 o -18 21 0 731.79 759.20 96.87 o -15 21 0 2695.97 2995.27 76.91 o -12 21 0 867.70 892.89 75.61 o -9 21 0 1061.45 1038.05 40.70 o -6 21 0 62.26 71.06 19.66 o -3 21 0 4770.98 5116.71 131.48 o 0 21 0 1746.33 1997.30 60.55 o -20 22 0 41.04 34.80 21.67 o -17 22 0 129.74 80.61 20.44 o -14 22 0 8.67 3.70 19.16 o -11 22 0 5356.21 5843.84 189.02 o -8 22 0 1205.12 1123.73 45.74 o -5 22 0 2265.91 2410.12 71.61 o -2 22 0 1568.70 1655.58 55.80 o -22 23 0 95.48 235.67 56.71 o -19 23 0 546.55 426.30 36.64 o -16 23 0 482.02 494.05 36.62 o -13 23 0 188.30 139.03 36.62 o -10 23 0 624.58 711.35 37.99 o -7 23 0 5.53 -11.81 25.06 o -4 23 0 1193.40 1282.87 75.61 o -1 23 0 353.19 314.23 42.58 o -21 24 0 17.99 46.40 41.67 o -18 24 0 1089.71 1168.05 67.34 o -15 24 0 831.65 931.21 59.07 o -12 24 0 813.91 725.05 56.71 o -9 24 0 955.57 1026.10 48.25 o -6 24 0 230.07 200.26 30.60 o -3 24 0 328.34 255.69 64.98 o 0 24 0 17.84 39.44 76.79 o -23 25 0 53.57 33.08 45.86 o -20 25 0 233.86 174.46 60.96 o -17 25 0 2180.05 2276.17 94.17 o -14 25 0 34.35 40.66 24.18 o -11 25 0 156.27 115.08 28.84 o -8 25 0 1250.71 1239.21 52.75 o -5 25 0 17.63 -26.12 26.12 o -2 25 0 10.55 -19.76 54.45 o -25 26 0 14.00 -41.87 68.52 o -22 26 0 0.56 7.20 35.20 o -19 26 0 1338.92 1399.47 80.14 o -16 26 0 1063.85 1264.08 67.48 o -13 26 0 1005.94 916.62 49.96 o -10 26 0 681.83 657.67 42.58 o -7 26 0 10.37 35.60 48.44 o -4 26 0 23.60 -16.88 34.97 o -1 26 0 127.08 118.49 103.96 o -24 27 0 739.79 752.15 79.03 o -21 27 0 477.56 562.30 81.02 o -18 27 0 4210.39 4725.76 172.65 o -15 27 0 138.06 165.28 38.32 o -12 27 0 49.54 15.81 32.29 o -9 27 0 657.85 619.12 43.64 o -6 27 0 14.41 47.68 72.06 o -3 27 0 50.68 -27.80 60.14 o 0 27 0 7.09 58.59 60.45 o -26 28 0 885.36 1116.06 105.02 o -23 28 0 307.89 286.83 183.11 o -20 28 0 1268.70 1363.93 93.64 o -17 28 0 6.42 25.14 29.93 o -14 28 0 1.24 7.92 50.80 o -11 28 0 40.33 11.81 32.30 o -8 28 0 442.63 433.72 55.80 o -5 28 0 127.91 72.49 52.57 o -2 28 0 5.32 65.52 86.24 o -25 29 0 13.61 50.84 86.83 o -22 29 0 18.37 -62.88 62.88 o -19 29 0 728.92 771.57 79.55 o -16 29 0 608.04 582.03 53.93 o -13 29 0 370.70 325.21 45.42 o -10 29 0 316.99 418.61 59.87 o -7 29 0 0.08 35.90 41.92 o -4 29 0 248.37 211.51 99.24 o -24 30 0 44.11 28.73 83.35 o -21 30 0 814.31 938.86 98.78 o -18 30 0 240.49 186.14 53.15 o -15 30 0 224.22 163.89 47.08 o -12 30 0 0.20 59.46 46.70 o -9 30 0 206.04 213.69 53.26 o -6 30 0 0.15 -18.90 77.97 o -23 31 0 251.93 282.10 103.96 o -20 31 0 890.56 1034.56 95.69 o -17 31 0 19.10 -15.07 47.08 o -14 31 0 75.31 82.03 59.15 o -11 31 0 66.28 88.38 61.75 o -8 31 0 11.24 -42.24 71.68 o -19 32 0 1143.94 1162.25 82.88 o -16 32 0 6.13 -49.70 66.53 o -13 32 0 17.43 -64.18 64.18 o -1 1 1 2883.41 2040.30 33.41 o -3 2 1 91.03 167.89 5.01 o 0 2 1 4302.58 4608.15 73.25 o -5 3 1 7514.05 6685.12 90.77 o -2 3 1 12721.71 11550.83 170.12 o 1 3 1 35278.73 35962.09 470.13 o -7 4 1 19503.12 18642.82 313.07 o -4 4 1 6038.19 6082.32 70.11 o -1 4 1 24065.12 22917.16 297.05 o 2 4 1 23370.77 23577.12 311.62 o -9 5 1 15620.72 16560.57 245.04 o -6 5 1 10046.99 9223.13 140.58 o -3 5 1 17794.46 19257.07 381.59 o 0 5 1 72895.95 71494.55 1430.65 o 3 5 1 3844.17 3770.53 48.94 o -11 6 1 10.97 24.15 7.38 o -8 6 1 11712.65 11938.94 147.85 o -5 6 1 145.88 126.42 5.01 o -2 6 1 39776.17 40111.88 634.40 o 1 6 1 16845.28 17699.62 226.82 o 4 6 1 18615.62 19871.28 248.65 o -13 7 1 170.42 160.51 15.36 o -10 7 1 320.40 349.18 15.36 o -7 7 1 535.86 606.93 11.34 o -4 7 1 2478.65 2247.91 29.93 o -1 7 1 41832.20 44032.49 791.53 o 2 7 1 9.28 -9.45 9.45 o 5 7 1 2497.78 2769.15 57.89 o -15 8 1 211.12 248.63 11.80 o -12 8 1 522.76 420.94 14.13 o -9 8 1 2030.26 1955.68 57.89 o -6 8 1 2642.88 2645.84 43.71 o -3 8 1 37783.38 39236.19 535.17 o 0 8 1 130.89 137.69 14.18 o 3 8 1 1626.43 1715.27 27.23 o 6 8 1 568.72 619.57 27.17 o -17 9 1 2444.63 2721.36 86.24 o -14 9 1 4466.20 4758.13 191.38 o -11 9 1 811.65 865.25 17.48 o -8 9 1 9852.40 10438.97 167.76 o -5 9 1 11.08 28.35 5.91 o -2 9 1 364.15 430.38 10.76 o 1 9 1 845.01 974.76 17.48 o 4 9 1 5.31 -3.31 7.86 o 7 9 1 3657.00 4181.69 126.41 o -19 10 1 76.85 104.32 14.13 o -16 10 1 80.00 105.86 24.81 o -13 10 1 95.62 124.19 11.81 o -10 10 1 13716.38 14199.84 156.05 o -7 10 1 3580.96 4121.64 68.52 o -4 10 1 229.00 246.59 20.08 o -1 10 1 62.48 18.87 5.91 o 2 10 1 1227.77 995.21 42.53 o 5 10 1 587.32 457.53 18.15 o 8 10 1 311.85 264.95 17.89 o -21 11 1 92.26 94.19 38.99 o -18 11 1 0.04 -7.86 7.86 o -15 11 1 1029.04 1075.59 25.53 o -12 11 1 3234.97 3685.07 66.16 o -9 11 1 190.15 149.19 8.35 o -6 11 1 17716.70 18663.05 539.89 o -3 11 1 13630.78 15834.84 197.29 o 0 11 1 300.26 229.77 13.00 o 3 11 1 253.88 174.11 36.62 o 6 11 1 2444.07 2390.83 53.16 o 9 11 1 1709.93 1703.99 44.89 o -23 12 1 7.59 10.04 21.26 o -20 12 1 19.58 20.08 15.04 o -17 12 1 53.15 40.84 13.00 o -14 12 1 1410.61 1474.42 44.89 o -11 12 1 133.76 162.97 10.63 o -8 12 1 527.23 599.10 14.13 o -5 12 1 9841.19 10804.70 129.28 o -2 12 1 10797.67 12044.36 284.71 o 1 12 1 23.78 36.03 9.61 o 4 12 1 528.16 466.56 22.51 o 7 12 1 7.54 -8.51 12.45 o 10 12 1 1730.75 1687.37 62.61 o -25 13 1 724.49 722.25 39.68 o -22 13 1 95.64 57.89 17.48 o -19 13 1 47.09 28.94 15.36 o -16 13 1 34.40 42.91 9.61 o -13 13 1 1347.90 1231.75 24.90 o -10 13 1 2768.59 3110.45 99.24 o -7 13 1 4960.77 5445.16 81.52 o -4 13 1 0.01 -3.04 5.67 o -1 13 1 2646.65 2970.03 50.12 o 2 13 1 278.76 257.48 14.76 o 5 13 1 28.84 13.39 12.45 o 8 13 1 429.96 357.10 31.90 o 11 13 1 154.91 150.48 25.99 o -27 14 1 238.24 314.33 112.23 o -24 14 1 1391.14 1550.99 55.06 o -21 14 1 247.22 186.09 23.39 o -18 14 1 428.33 391.09 21.26 o -15 14 1 85.89 78.85 10.57 o -12 14 1 857.27 774.41 19.84 o -9 14 1 4565.46 5326.62 72.55 o -6 14 1 4020.45 4167.65 59.07 o -3 14 1 382.78 320.16 13.37 o 0 14 1 2519.24 2416.36 45.92 o 3 14 1 134.77 82.70 13.55 o 6 14 1 172.17 175.66 31.90 o 9 14 1 95.42 62.41 24.18 o 12 14 1 248.49 300.07 29.93 o -29 15 1 36.00 14.18 51.79 o -26 15 1 822.28 898.92 47.59 o -23 15 1 241.65 264.21 36.62 o -20 15 1 310.61 238.27 48.44 o -17 15 1 3.82 12.36 10.02 o -14 15 1 89.95 78.85 8.21 o -11 15 1 8958.00 9786.35 277.63 o -8 15 1 5060.94 5319.46 120.50 o -5 15 1 1169.38 1111.15 46.07 o -2 15 1 228.23 159.57 11.70 o 1 15 1 2164.99 2175.59 45.92 o 4 15 1 16783.00 19220.40 364.37 o 7 15 1 64.76 48.44 23.39 o 10 15 1 233.44 213.11 31.78 o 13 15 1 72.37 36.79 48.94 o -31 16 1 883.21 897.30 84.01 o -28 16 1 10.12 84.10 69.70 o -25 16 1 4032.82 4495.35 131.86 o -22 16 1 1469.15 1538.09 53.46 o -19 16 1 754.20 803.15 27.25 o -16 16 1 2.86 -3.71 21.26 o -13 16 1 113.61 106.04 14.18 o -10 16 1 4418.87 5221.61 76.64 o -7 16 1 5545.16 5951.17 125.46 o -4 16 1 60.33 43.44 11.81 o -1 16 1 4499.16 4710.12 144.13 o 2 16 1 2350.02 2426.26 88.60 o 5 16 1 312.66 271.06 28.46 o 8 16 1 539.30 464.09 40.91 o 11 16 1 201.31 238.35 42.58 o 14 16 1 67.66 36.65 57.27 o -30 17 1 673.49 765.46 76.05 o -27 17 1 1178.16 1298.20 68.26 o -24 17 1 0.21 11.54 28.92 o -21 17 1 77.26 86.09 19.84 o -18 17 1 247.80 179.34 17.89 o -15 17 1 1177.19 1061.87 49.62 o -12 17 1 1869.24 1971.72 44.25 o -9 17 1 67.83 48.30 12.16 o -6 17 1 269.84 219.57 17.48 o -3 17 1 1812.66 1768.48 40.91 o 0 17 1 748.56 694.49 47.26 o 3 17 1 15721.06 17821.95 382.88 o 6 17 1 790.22 775.52 47.26 o 9 17 1 607.83 610.70 45.11 o 12 17 1 1032.40 1188.67 68.12 o -29 18 1 382.06 385.71 58.13 o -26 18 1 1062.84 1262.89 93.33 o -23 18 1 20.56 3.12 23.21 o -20 18 1 0.14 3.08 17.89 o -17 18 1 81.74 73.14 21.26 o -14 18 1 4925.16 5462.46 100.08 o -11 18 1 571.67 633.67 19.16 o -8 18 1 47.50 9.79 14.18 o -5 18 1 11.17 6.12 14.13 o -2 18 1 2.87 22.84 13.00 o 1 18 1 237.43 209.59 22.14 o 4 18 1 972.87 973.39 37.97 o 7 18 1 40.56 48.75 35.44 o 10 18 1 5.44 -3.80 62.61 o 13 18 1 718.58 884.17 215.01 o -31 19 1 119.62 83.68 63.35 o -28 19 1 88.79 67.45 82.70 o -25 19 1 3494.46 3929.50 144.13 o -22 19 1 17.39 21.71 41.35 o -19 19 1 179.10 201.93 27.53 o -16 19 1 158.33 186.19 21.13 o -13 19 1 8.90 6.62 11.80 o -10 19 1 0.01 -7.74 13.95 o -7 19 1 913.97 916.64 33.22 o -4 19 1 352.50 375.41 25.86 o -1 19 1 5.61 1.87 15.36 o 2 19 1 4773.11 5175.78 120.09 o 5 19 1 2140.04 2346.57 80.19 o 8 19 1 1619.69 1818.54 119.98 o 11 19 1 8.73 -55.80 55.80 o -30 20 1 229.62 62.70 66.33 o -27 20 1 2271.97 2336.26 96.51 o -24 20 1 46.64 57.89 31.74 o -21 20 1 88.35 92.04 41.35 o -18 20 1 540.87 575.56 40.17 o -15 20 1 2437.38 2468.66 60.96 o -12 20 1 9.28 11.26 12.45 o -9 20 1 36.92 25.86 13.95 o -6 20 1 4788.62 5134.03 107.83 o -3 20 1 720.32 760.96 72.06 o 0 20 1 378.81 309.68 27.53 o 3 20 1 3245.19 3651.18 137.59 o 6 20 1 579.03 537.09 70.95 o 9 20 1 0.10 -34.39 78.47 o -29 21 1 1.31 28.81 54.47 o -26 21 1 156.40 163.89 42.38 o -23 21 1 403.31 323.78 51.98 o -20 21 1 192.54 113.89 37.80 o -17 21 1 5227.59 5576.35 144.63 o -14 21 1 327.32 298.32 34.26 o -11 21 1 23.33 36.16 30.72 o -8 21 1 828.10 828.30 63.79 o -5 21 1 961.92 930.92 118.14 o -2 21 1 104.18 116.45 36.62 o 1 21 1 614.35 570.01 38.32 o 4 21 1 533.21 606.39 85.06 o 7 21 1 1198.83 1380.32 122.72 o 10 21 1 117.14 169.23 129.95 o -31 22 1 3.46 66.16 82.70 o -28 22 1 42.44 47.26 66.16 o -25 22 1 1021.35 1081.48 109.87 o -22 22 1 449.43 418.34 50.51 o -19 22 1 2.34 20.78 24.18 o -16 22 1 130.93 82.27 23.21 o -13 22 1 338.53 232.89 30.70 o -10 22 1 68.64 60.38 21.42 o -7 22 1 1029.02 1165.21 54.34 o -4 22 1 539.71 475.64 34.61 o -1 22 1 90.89 35.87 27.53 o 2 22 1 347.85 328.98 62.61 o 5 22 1 6.23 99.40 73.46 o 8 22 1 40.44 45.18 76.47 o -30 23 1 0.02 -82.70 82.70 o -27 23 1 0.07 -48.25 48.25 o -24 23 1 1552.86 1800.26 131.13 o -21 23 1 968.02 999.59 118.14 o -18 23 1 324.53 272.67 32.92 o -15 23 1 744.83 639.42 42.83 o -12 23 1 564.89 381.55 32.29 o -9 23 1 662.35 590.37 37.56 o -6 23 1 6.09 11.11 22.51 o -3 23 1 382.25 383.75 35.89 o 0 23 1 137.49 206.76 98.05 o 3 23 1 585.89 583.26 84.06 o 6 23 1 616.19 534.36 103.22 o -29 24 1 459.98 673.39 118.14 o -26 24 1 453.06 563.63 74.43 o -23 24 1 3033.53 3694.87 141.95 o -20 24 1 435.67 430.99 67.34 o -17 24 1 746.79 579.23 44.89 o -14 24 1 6.93 -4.26 24.40 o -11 24 1 194.23 220.68 30.07 o -8 24 1 251.32 248.09 29.93 o -5 24 1 541.50 513.45 39.02 o -2 24 1 5.63 -18.31 26.58 o 1 24 1 1.80 64.11 53.28 o 4 24 1 50.49 63.77 67.53 o -28 25 1 257.82 229.25 64.60 o -25 25 1 1437.01 1520.86 99.84 o -22 25 1 639.44 713.87 65.55 o -19 25 1 83.94 49.76 27.82 o -16 25 1 11.84 51.93 34.02 o -13 25 1 984.16 859.00 49.37 o -10 25 1 957.53 846.72 48.11 o -7 25 1 50.12 33.08 35.44 o -4 25 1 54.46 21.03 33.98 o -1 25 1 17.86 24.02 54.47 o 2 25 1 70.55 -32.40 88.60 o -27 26 1 280.31 214.88 76.07 o -24 26 1 1601.57 1780.73 180.75 o -21 26 1 78.30 149.92 44.25 o -18 26 1 103.17 107.21 42.05 o -15 26 1 311.36 292.32 43.13 o -12 26 1 186.28 225.72 36.64 o -9 26 1 1834.03 2027.22 77.20 o -6 26 1 451.73 390.70 39.02 o -3 26 1 156.03 188.22 96.87 o 0 26 1 153.85 211.85 83.88 o 3 26 1 67.72 143.86 102.94 o -26 27 1 344.91 309.52 80.33 o -23 27 1 33.82 108.58 51.36 o -20 27 1 204.11 150.04 53.48 o -17 27 1 508.44 534.17 52.45 o -14 27 1 1238.40 1308.98 86.24 o -11 27 1 0.06 32.17 31.03 o -8 27 1 562.30 512.23 50.04 o -5 27 1 1.96 -5.06 34.02 o -2 27 1 83.61 204.38 63.49 o 1 27 1 17.14 24.12 96.73 o -25 28 1 38.77 105.38 61.43 o -22 28 1 26.32 80.14 61.21 o -19 28 1 177.89 270.49 194.93 o -16 28 1 31.71 66.16 45.38 o -13 28 1 22.02 34.00 37.99 o -10 28 1 146.21 72.19 39.24 o -7 28 1 8.64 32.34 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