#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/81/2018199.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018199_Fobs loop_ _publ_author_name 'Parkin, Sean R.' 'Behrman, Edward J.' _publ_section_title ; Channel-forming solvate crystals and isostructural solvent-free powder of 5-hydroxy-6-methyl-2-pyridone ; _journal_coeditor_code MX3051 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o324 _journal_page_last o328 _journal_volume 67 _journal_year 2011 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 25.2734 _cell_length_b 25.2734 _cell_length_c 5.2602 _exptl_crystal_F_000 1188.00 _reflns_d_resolution_high 0.8307 _[local]_cod_data_source_file mx3051Ic2sup5.hkl _[local]_cod_data_source_block Ic2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k09075' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 3 0 12314.25 10182.08 86.25 o -2 4 0 3625.22 4786.75 40.15 o -4 5 0 4184.09 2977.41 28.30 o -1 5 0 18170.99 18804.21 154.46 o -3 6 0 2206.86 1781.74 17.03 o 0 6 0 1873.21 1791.82 17.99 o -5 7 0 1544.22 1823.47 18.25 o -2 7 0 24140.19 26122.37 207.83 o -7 8 0 3674.61 3529.81 33.08 o -4 8 0 5987.62 5661.96 52.13 o -1 8 0 1244.78 975.93 13.22 o -6 9 0 9562.60 11288.07 98.60 o -3 9 0 921.57 974.95 13.04 o 0 9 0 2028.51 1887.33 20.93 o -8 10 0 2344.74 2516.59 25.84 o -5 10 0 5019.65 5288.98 48.87 o -2 10 0 959.19 809.33 23.48 o -10 11 0 1268.19 1127.12 15.72 o -7 11 0 926.90 1031.95 15.03 o -4 11 0 908.64 834.38 13.79 o -1 11 0 17867.40 21238.73 194.13 o -9 12 0 81.96 101.31 8.51 o -6 12 0 3357.39 3695.39 36.80 o -3 12 0 4924.02 5079.95 57.64 o 0 12 0 2564.54 3065.84 37.47 o -11 13 0 96.02 102.23 8.67 o -8 13 0 101.55 135.74 9.67 o -5 13 0 729.51 594.11 12.82 o -2 13 0 1982.96 2102.59 30.05 o -13 14 0 81.02 52.92 8.94 o -10 14 0 486.61 426.39 12.06 o -7 14 0 9.05 46.91 8.27 o -4 14 0 2346.57 2479.55 33.12 o -1 14 0 3895.96 4405.89 56.04 o -12 15 0 1.10 -4.93 8.67 o -9 15 0 821.20 1093.14 23.53 o -6 15 0 4162.28 4376.89 58.03 o -3 15 0 2216.11 2556.72 38.38 o 0 15 0 1041.52 1215.20 24.00 o -14 16 0 4.19 3.57 11.51 o -11 16 0 227.37 257.07 12.64 o -8 16 0 2177.83 2381.88 33.94 o -5 16 0 389.57 460.03 15.76 o -2 16 0 953.79 1097.92 26.75 o -16 17 0 95.53 93.63 21.55 o -13 17 0 39.18 40.75 12.38 o -10 17 0 747.65 734.48 21.23 o -7 17 0 4648.25 5316.03 64.79 o -4 17 0 780.04 816.25 22.01 o -1 17 0 1169.20 1274.78 30.46 o -15 18 0 25.79 10.43 17.61 o -12 18 0 726.21 607.18 22.29 o -9 18 0 202.73 214.75 25.24 o -6 18 0 11.28 21.94 15.61 o -3 18 0 33.70 21.61 13.50 o 0 18 0 1.94 5.82 20.33 o -17 19 0 1783.66 1928.73 48.34 o -14 19 0 370.96 313.84 18.49 o -11 19 0 348.26 324.02 20.84 o -8 19 0 786.44 824.52 27.59 o -5 19 0 887.91 819.56 25.79 o -2 19 0 640.62 637.89 26.71 o -19 20 0 88.75 68.97 26.97 o -16 20 0 1239.70 1332.60 39.30 o -13 20 0 140.08 126.75 18.53 o -10 20 0 30.23 26.95 24.36 o -7 20 0 47.42 86.45 28.15 o -4 20 0 1128.95 1312.00 82.77 o -1 20 0 682.26 715.22 37.84 o -18 21 0 132.41 138.77 26.33 o -15 21 0 1121.48 1130.37 34.39 o -12 21 0 393.68 353.02 20.79 o -9 21 0 458.62 379.50 37.79 o -6 21 0 20.96 9.86 26.15 o -3 21 0 1654.47 2065.66 62.17 o 0 21 0 591.85 665.85 50.18 o -20 22 0 32.91 49.21 30.25 o -17 22 0 22.23 26.89 30.23 o -14 22 0 2.81 16.54 21.41 o -11 22 0 2127.13 2458.84 84.82 o -8 22 0 656.39 561.36 37.19 o -5 22 0 817.33 922.69 55.86 o -2 22 0 531.05 593.43 57.36 o -22 23 0 4.50 -31.48 40.22 o -19 23 0 143.02 177.10 34.13 o -16 23 0 322.29 267.21 31.03 o -13 23 0 227.52 184.78 25.64 o -10 23 0 348.50 327.13 35.20 o -7 23 0 1.56 -1.48 31.99 o -4 23 0 489.49 463.65 44.58 o -1 23 0 198.57 227.08 41.85 o -21 24 0 0.83 -24.21 39.97 o -18 24 0 485.00 523.12 66.77 o -15 24 0 235.57 198.82 52.57 o -12 24 0 283.38 253.49 37.24 o -9 24 0 220.17 207.64 35.15 o -6 24 0 85.98 -22.51 37.24 o -3 24 0 129.77 74.48 44.77 o 0 24 0 1.68 -37.44 49.28 o -23 25 0 9.17 -30.10 53.79 o -20 25 0 203.44 117.53 44.11 o -17 25 0 838.99 953.99 75.01 o -14 25 0 20.26 -5.98 39.91 o -11 25 0 30.61 73.64 35.36 o -8 25 0 379.67 321.39 41.74 o -5 25 0 7.87 -43.39 43.39 o -2 25 0 0.09 59.39 49.05 o -25 26 0 14.00 -40.25 63.52 o -22 26 0 4.62 60.09 48.43 o -19 26 0 683.00 701.66 57.23 o -16 26 0 219.42 201.95 41.70 o -13 26 0 380.31 301.00 41.45 o -10 26 0 191.89 175.12 47.25 o -7 26 0 0.04 54.49 42.35 o -4 26 0 0.18 27.94 53.62 o -1 26 0 51.51 81.59 57.09 o -24 27 0 108.59 73.51 66.22 o -21 27 0 235.68 262.33 48.55 o -18 27 0 1020.12 1183.04 71.33 o -15 27 0 55.54 48.65 57.34 o -12 27 0 22.53 -39.04 39.04 o -9 27 0 236.20 57.45 57.72 o -6 27 0 0.88 8.38 52.23 o -3 27 0 15.55 -45.65 56.47 o -23 28 0 113.19 173.82 71.61 o -20 28 0 528.36 667.30 67.88 o -17 28 0 14.94 19.44 47.62 o -14 28 0 21.98 -23.93 68.97 o -11 28 0 3.65 19.06 49.90 o -8 28 0 41.49 63.01 69.85 o -5 28 0 8.69 -37.89 68.38 o -22 29 0 54.15 -4.28 84.52 o -19 29 0 62.30 70.25 63.98 o -16 29 0 113.36 135.45 67.59 o -13 29 0 80.13 168.05 81.00 o -10 29 0 95.87 89.09 58.04 o -7 29 0 0.16 4.04 63.01 o -18 30 0 6.74 -70.65 70.65 o -15 30 0 29.63 -11.38 78.51 o -12 30 0 0.29 -69.67 79.29 o -1 1 1 3344.29 2466.25 23.77 o -3 2 1 327.76 397.15 5.46 o 0 2 1 4391.38 4350.02 33.47 o -5 3 1 8250.69 7482.29 61.02 o -2 3 1 11205.24 10786.86 88.74 o 1 3 1 36370.65 37775.30 319.85 o -7 4 1 17954.38 17848.03 149.53 o -4 4 1 5317.67 5442.19 44.74 o -1 4 1 26336.81 25563.53 197.53 o 2 4 1 21829.98 22234.45 195.83 o -9 5 1 12318.99 13425.40 140.57 o -6 5 1 7890.70 7380.44 62.64 o -3 5 1 19255.53 20914.05 171.32 o 0 5 1 65185.34 67000.54 528.91 o 3 5 1 4833.50 4684.73 49.11 o -11 6 1 6.85 26.52 9.82 o -8 6 1 8992.20 9437.90 78.12 o -5 6 1 263.09 203.67 9.52 o -2 6 1 38950.01 39480.00 297.56 o 1 6 1 13569.39 14764.65 120.61 o 4 6 1 16388.91 18153.29 163.44 o -13 7 1 144.24 136.45 9.68 o -10 7 1 180.21 179.84 10.08 o -7 7 1 349.88 355.81 9.10 o -4 7 1 3268.59 3111.98 26.27 o -1 7 1 31680.77 34302.34 263.74 o 2 7 1 1.52 -4.52 5.58 o 5 7 1 1633.57 1799.01 42.55 o -15 8 1 364.81 402.26 20.45 o -12 8 1 237.33 187.23 12.03 o -9 8 1 1048.96 1057.90 16.06 o -6 8 1 2426.40 2421.93 25.44 o -3 8 1 31084.82 33459.87 264.73 o 0 8 1 195.90 173.76 11.45 o 3 8 1 2096.80 2113.59 27.43 o 6 8 1 420.29 446.16 18.78 o -17 9 1 1385.48 1584.99 30.11 o -14 9 1 3335.72 3518.96 46.48 o -11 9 1 522.08 496.10 12.03 o -8 9 1 7435.36 8308.15 76.24 o -5 9 1 69.91 41.35 5.73 o -2 9 1 22.72 12.71 5.58 o 1 9 1 580.81 563.52 11.27 o 4 9 1 2.99 -4.89 8.73 o 7 9 1 1937.16 2314.63 41.97 o -19 10 1 18.46 15.04 15.39 o -16 10 1 72.49 52.77 13.85 o -13 10 1 90.40 92.98 8.52 o -10 10 1 11017.27 12497.97 114.52 o -7 10 1 1985.89 2295.59 25.57 o -4 10 1 1.64 2.94 5.69 o -1 10 1 151.64 73.02 10.86 o 2 10 1 749.73 610.66 17.61 o 5 10 1 563.96 421.46 14.60 o 8 10 1 299.18 246.08 16.20 o -21 11 1 26.03 14.42 19.55 o -18 11 1 1.16 18.58 14.06 o -15 11 1 489.63 475.32 18.62 o -12 11 1 2810.13 3313.54 38.55 o -9 11 1 136.04 96.19 8.20 o -6 11 1 12156.85 13672.53 134.98 o -3 11 1 10145.48 11962.08 99.87 o 0 11 1 181.56 158.96 8.67 o 3 11 1 119.91 72.09 9.37 o 6 11 1 1500.25 1521.77 49.89 o 9 11 1 606.38 578.56 23.59 o -23 12 1 0.34 17.65 26.17 o -20 12 1 8.88 1.94 15.10 o -17 12 1 30.25 28.90 11.93 o -14 12 1 1390.27 1541.34 24.54 o -11 12 1 167.63 174.92 10.18 o -8 12 1 694.42 664.15 21.72 o -5 12 1 7862.10 8882.77 76.06 o -2 12 1 7766.02 8904.23 85.71 o 1 12 1 10.46 26.03 8.83 o 4 12 1 203.37 164.32 20.68 o 7 12 1 1.04 4.81 17.19 o 10 12 1 688.25 603.65 37.43 o -25 13 1 126.75 128.11 43.73 o -22 13 1 94.07 90.85 20.42 o -19 13 1 51.72 37.23 13.77 o -16 13 1 2.80 23.60 18.20 o -13 13 1 569.82 500.23 15.87 o -10 13 1 1733.45 1871.97 25.86 o -7 13 1 4697.82 5708.98 57.52 o -4 13 1 1.16 -1.97 7.54 o -1 13 1 1993.57 2301.25 30.05 o 2 13 1 267.90 211.59 12.03 o 5 13 1 23.14 -4.89 13.64 o 8 13 1 156.23 137.11 24.36 o 11 13 1 26.74 13.86 31.07 o -27 14 1 49.91 23.43 65.47 o -24 14 1 342.97 321.19 35.95 o -21 14 1 99.04 85.79 15.81 o -18 14 1 172.36 215.23 18.97 o -15 14 1 65.80 49.02 12.78 o -12 14 1 730.69 602.59 21.72 o -9 14 1 4076.38 4573.00 50.32 o -6 14 1 2516.22 2810.50 31.68 o -3 14 1 108.03 117.43 11.05 o 0 14 1 922.42 828.02 16.55 o 3 14 1 0.07 -4.10 13.28 o 6 14 1 105.48 123.18 26.41 o 9 14 1 4.52 -10.43 24.47 o 12 14 1 81.10 92.32 49.17 o -29 15 1 3.35 -44.95 82.47 o -26 15 1 182.47 194.33 46.02 o -23 15 1 191.42 168.03 30.82 o -20 15 1 39.99 37.38 22.39 o -17 15 1 22.75 20.64 15.64 o -14 15 1 107.45 93.38 14.80 o -11 15 1 6200.92 6811.18 83.35 o -8 15 1 3052.89 3139.14 38.54 o -5 15 1 747.18 659.15 16.67 o -2 15 1 189.18 155.94 17.02 o 1 15 1 930.28 980.33 32.28 o 4 15 1 6780.66 8460.26 127.99 o 7 15 1 65.47 103.24 44.61 o 10 15 1 69.32 58.72 42.67 o 13 15 1 42.71 -72.15 74.65 o -28 16 1 6.60 -51.24 51.24 o -25 16 1 1153.58 1384.59 92.15 o -22 16 1 463.15 444.49 34.30 o -19 16 1 372.96 298.78 28.20 o -16 16 1 1.10 0.29 16.73 o -13 16 1 184.36 143.09 14.17 o -10 16 1 2380.66 2906.73 38.71 o -7 16 1 3804.21 4393.93 54.32 o -4 16 1 7.40 15.14 12.45 o -1 16 1 2502.81 2867.52 47.30 o 2 16 1 566.80 592.61 19.96 o 5 16 1 181.69 153.24 26.25 o 8 16 1 212.89 184.38 37.21 o 11 16 1 14.36 -38.33 53.21 o 14 16 1 37.69 -74.81 137.81 o -27 17 1 308.14 333.28 56.67 o -24 17 1 2.39 29.11 37.56 o -21 17 1 79.86 93.20 28.47 o -18 17 1 65.23 48.34 14.97 o -15 17 1 782.08 815.81 36.39 o -12 17 1 633.41 682.68 30.52 o -9 17 1 56.70 49.73 16.14 o -6 17 1 135.68 102.48 13.67 o -3 17 1 1157.95 1174.08 36.68 o 0 17 1 595.49 589.87 23.15 o 3 17 1 7438.59 9555.07 149.36 o 6 17 1 200.79 120.04 30.19 o 9 17 1 154.32 63.47 48.48 o 12 17 1 166.47 261.96 72.36 o -29 18 1 88.01 172.07 64.83 o -26 18 1 131.85 95.17 40.07 o -23 18 1 0.60 36.03 32.56 o -20 18 1 0.01 57.85 35.56 o -17 18 1 137.48 137.30 18.21 o -14 18 1 2429.44 2898.17 67.79 o -11 18 1 368.48 362.24 16.34 o -8 18 1 0.07 24.78 12.02 o -5 18 1 20.88 9.99 14.75 o -2 18 1 35.06 41.58 19.66 o 1 18 1 81.01 41.80 39.10 o 4 18 1 208.55 177.28 31.99 o 7 18 1 9.04 -36.87 36.87 o 10 18 1 0.03 -53.21 54.70 o -28 19 1 4.42 23.65 71.38 o -25 19 1 808.04 868.36 47.97 o -22 19 1 1.55 10.77 33.02 o -19 19 1 129.26 141.96 21.29 o -16 19 1 292.85 287.91 27.29 o -13 19 1 18.94 42.51 16.14 o -10 19 1 0.77 -6.57 14.26 o -7 19 1 641.78 524.66 35.51 o -4 19 1 65.19 67.79 20.76 o -1 19 1 0.00 31.25 23.54 o 2 19 1 2818.16 3429.85 77.51 o 5 19 1 645.32 656.81 43.66 o 8 19 1 419.13 528.85 59.39 o -27 20 1 582.77 780.72 89.22 o -24 20 1 1.07 -37.87 41.97 o -21 20 1 11.22 -29.90 29.90 o -18 20 1 325.14 368.27 26.51 o -15 20 1 594.08 595.32 24.67 o -12 20 1 0.45 -14.61 14.84 o -9 20 1 3.61 8.70 15.85 o -6 20 1 2370.73 2859.01 75.35 o -3 20 1 219.52 196.43 30.88 o 0 20 1 220.08 220.48 32.87 o 3 20 1 1264.14 1563.32 54.69 o 6 20 1 255.86 221.24 44.67 o 9 20 1 2.90 -25.98 60.06 o -29 21 1 4.49 -72.81 72.81 o -26 21 1 105.26 72.26 53.79 o -23 21 1 63.23 32.32 36.04 o -20 21 1 53.38 44.96 26.94 o -17 21 1 1917.24 2205.47 50.00 o -14 21 1 143.43 119.85 19.60 o -11 21 1 0.28 5.47 17.90 o -8 21 1 453.88 481.34 27.81 o -5 21 1 341.01 271.46 32.71 o -2 21 1 54.75 70.97 30.23 o 1 21 1 503.94 505.18 39.29 o 4 21 1 120.88 50.81 50.73 o 7 21 1 289.16 262.50 68.28 o -28 22 1 12.77 98.95 62.57 o -25 22 1 408.06 454.02 54.88 o -22 22 1 191.72 153.40 36.20 o -19 22 1 22.23 18.40 26.98 o -16 22 1 65.97 43.44 22.63 o -13 22 1 100.30 59.24 19.79 o -10 22 1 4.27 34.34 19.38 o -7 22 1 203.65 212.06 31.86 o -4 22 1 220.38 225.68 33.16 o -1 22 1 95.65 88.42 33.28 o 2 22 1 22.37 2.64 43.44 o 5 22 1 2.81 30.42 52.41 o -27 23 1 2.95 3.40 63.37 o -24 23 1 537.84 623.71 61.46 o -21 23 1 266.01 212.90 36.74 o -18 23 1 149.01 93.22 36.88 o -15 23 1 258.74 146.12 28.68 o -12 23 1 174.99 120.01 22.97 o -9 23 1 306.41 297.87 31.32 o -6 23 1 27.28 20.36 32.68 o -3 23 1 80.97 84.02 38.47 o 0 23 1 32.34 56.32 44.98 o 3 23 1 88.64 52.31 49.51 o -26 24 1 130.30 182.77 56.74 o -23 24 1 752.60 957.39 78.02 o -20 24 1 147.98 156.71 37.40 o -17 24 1 276.87 257.15 33.23 o -14 24 1 21.84 22.77 30.38 o -11 24 1 7.84 -32.13 32.13 o -8 24 1 18.14 46.26 33.30 o -5 24 1 313.27 294.34 46.23 o -2 24 1 1.47 50.06 50.34 o 1 24 1 0.15 -24.89 51.57 o -25 25 1 326.18 406.44 60.78 o -22 25 1 190.72 201.84 46.71 o -19 25 1 50.13 52.59 45.49 o -16 25 1 0.06 -16.15 49.06 o -13 25 1 278.20 117.97 42.85 o -10 25 1 367.20 351.60 50.89 o -7 25 1 53.04 59.08 46.07 o -4 25 1 22.52 -54.00 54.00 o -1 25 1 20.39 30.62 55.01 o -24 26 1 343.28 382.02 71.30 o -21 26 1 36.58 94.89 52.69 o -18 26 1 21.41 10.07 53.57 o -15 26 1 73.17 134.24 52.60 o -12 26 1 35.03 29.84 41.16 o -9 26 1 578.61 598.48 54.18 o -6 26 1 65.82 169.28 48.26 o -3 26 1 22.95 52.59 62.84 o 0 26 1 29.82 158.11 169.31 o -23 27 1 14.54 64.47 56.88 o -20 27 1 26.37 9.37 61.99 o -17 27 1 128.27 60.08 56.83 o -14 27 1 253.29 234.92 53.30 o -11 27 1 5.53 10.09 46.04 o -8 27 1 173.23 223.16 53.74 o -5 27 1 0.09 38.62 56.31 o -22 28 1 1.15 -25.58 101.39 o -19 28 1 18.74 47.02 57.28 o -16 28 1 2.48 44.10 66.32 o -13 28 1 16.81 104.22 66.62 o -10 28 1 42.19 15.97 58.80 o -7 28 1 2.98 -52.23 52.23 o -21 29 1 92.83 -38.92 79.50 o -18 29 1 207.20 190.29 62.83 o -15 29 1 90.95 115.42 62.57 o -12 29 1 134.83 238.56 71.15 o -9 29 1 21.27 35.46 60.87 o -14 30 1 74.92 -106.31 232.30 o 0 1 2 10665.04 10918.46 93.28 o -2 2 2 4283.59 3802.66 34.62 o 1 2 2 4741.65 4980.79 40.45 o -4 3 2 569.35 556.74 10.15 o -1 3 2 17897.70 18336.56 153.89 o 2 3 2 4020.32 4155.70 37.19 o -6 4 2 24.84 16.61 6.75 o -3 4 2 66.14 66.58 6.80 o 0 4 2 13211.07 13735.70 108.58 o 3 4 2 1258.48 1453.99 20.84 o -8 5 2 2196.20 2733.10 27.35 o -5 5 2 37.16 34.05 6.49 o -2 5 2 4629.53 4938.72 52.24 o 1 5 2 792.78 640.76 13.64 o 4 5 2 2827.48 3422.10 34.40 o -10 6 2 59.62 78.35 7.74 o -7 6 2 573.49 745.71 11.66 o -4 6 2 36.44 7.45 9.62 o -1 6 2 2160.91 2265.74 23.77 o 2 6 2 1070.64 1377.49 18.62 o 5 6 2 0.93 -7.93 8.23 o -12 7 2 563.80 580.92 22.89 o -9 7 2 421.96 433.84 16.32 o -6 7 2 71.23 99.76 7.32 o -3 7 2 53.59 35.01 7.57 o 0 7 2 11.06 11.20 6.75 o 3 7 2 4985.99 5938.57 56.13 o 6 7 2 32.61 18.07 9.79 o -14 8 2 860.34 928.00 20.80 o -11 8 2 744.80 849.70 17.14 o -8 8 2 794.17 720.10 13.46 o -5 8 2 58.01 16.30 9.39 o -2 8 2 14.02 -3.42 7.04 o 1 8 2 1831.77 2017.93 24.47 o 4 8 2 96.62 70.50 9.72 o 7 8 2 212.76 155.63 11.09 o -16 9 2 2121.42 2159.75 44.31 o -13 9 2 959.32 897.05 19.94 o -10 9 2 344.57 326.17 10.66 o -7 9 2 2367.09 2570.18 30.52 o -4 9 2 3488.86 4374.16 43.17 o -1 9 2 10636.31 11507.52 94.52 o 2 9 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