#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:20:17 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180851 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018200.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018200_Fobs loop_ _publ_author_name 'Parkin, Sean R.' 'Behrman, Edward J.' _publ_section_title ; Channel-forming solvate crystals and isostructural solvent-free powder of 5-hydroxy-6-methyl-2-pyridone ; _journal_coeditor_code MX3051 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o324 _journal_page_last o328 _journal_volume 67 _journal_year 2011 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 24.9194 _cell_length_b 24.9194 _cell_length_c 5.2541 _exptl_crystal_F_000 1188.00 _reflns_d_resolution_high 0.7703 _cod_data_source_file mx3051Ic3sup6.hkl _cod_data_source_block Ic3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k09075' _shelx_refln_list_code 4 _shelx_f_calc_maximum 271.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 40906.91 11367.86 15102.06 o 0 3 0 13571.98 10317.57 89.48 o -2 4 0 3348.79 4720.82 39.01 o -4 5 0 4377.43 2932.91 26.37 o -1 5 0 16626.99 17350.39 148.16 o -3 6 0 1689.54 1176.07 24.92 o 0 6 0 1822.58 1681.22 14.58 o -5 7 0 1573.95 1878.28 16.55 o -2 7 0 27184.29 28479.31 233.35 o -7 8 0 3530.54 3210.86 27.93 o -4 8 0 6746.86 6200.46 55.17 o -1 8 0 1390.69 998.36 18.00 o -6 9 0 11268.55 12807.46 106.68 o -3 9 0 1256.56 1148.93 11.75 o 0 9 0 3793.11 3727.20 31.90 o -8 10 0 2719.55 2615.04 23.53 o -5 10 0 6235.58 6251.57 52.54 o -2 10 0 1406.56 1207.06 11.75 o -10 11 0 1078.56 903.96 11.75 o -7 11 0 713.27 756.33 9.69 o -4 11 0 1119.90 1107.40 11.75 o -1 11 0 25323.66 26988.37 233.94 o -9 12 0 276.61 295.21 16.61 o -6 12 0 3873.85 4031.38 34.59 o -3 12 0 5045.06 4886.56 43.07 o 0 12 0 5234.34 5765.92 119.04 o -11 13 0 316.97 294.61 12.46 o -8 13 0 66.25 111.61 4.61 o -5 13 0 532.44 515.18 11.07 o -2 13 0 1792.43 1864.97 20.49 o -13 14 0 223.33 228.72 9.69 o -10 14 0 728.90 751.19 11.07 o -7 14 0 29.00 74.46 5.54 o -4 14 0 4799.32 4887.90 109.35 o -1 14 0 6077.44 6161.22 91.36 o -12 15 0 1.24 1.11 4.61 o -9 15 0 1445.19 1660.76 20.96 o -6 15 0 5196.63 5294.31 62.41 o -3 15 0 2839.33 3099.73 65.06 o 0 15 0 2584.27 2770.03 39.01 o -14 16 0 1.29 -1.85 4.95 o -11 16 0 328.31 387.29 12.46 o -8 16 0 2242.90 2528.75 51.22 o -5 16 0 952.72 1020.65 15.30 o -2 16 0 1188.65 1344.22 22.45 o -16 17 0 141.73 159.73 9.21 o -13 17 0 10.90 19.38 8.31 o -10 17 0 1703.22 1713.95 23.25 o -7 17 0 9496.25 10106.99 121.61 o -4 17 0 807.16 893.63 16.61 o -1 17 0 2197.84 2138.46 33.22 o -15 18 0 11.00 0.79 8.31 o -12 18 0 1224.10 1103.79 37.37 o -9 18 0 143.51 174.81 8.65 o -6 18 0 4.25 15.23 6.92 o -3 18 0 26.44 23.53 9.69 o 0 18 0 10.61 10.28 8.31 o -17 19 0 3785.46 3809.90 70.60 o -14 19 0 857.53 840.94 16.35 o -11 19 0 1282.32 1265.67 33.22 o -8 19 0 1016.90 1114.37 21.94 o -5 19 0 2056.11 2057.21 33.88 o -2 19 0 2521.69 2507.65 40.55 o -19 20 0 464.74 407.64 17.62 o -16 20 0 2679.72 2984.96 85.82 o -13 20 0 342.21 349.08 11.26 o -10 20 0 13.85 11.07 7.83 o -7 20 0 6.28 24.30 8.65 o -4 20 0 3590.38 3851.42 57.13 o -1 20 0 2289.21 2369.25 39.87 o -18 21 0 800.08 825.52 21.94 o -15 21 0 2988.03 3146.80 48.47 o -12 21 0 1025.00 987.09 22.45 o -9 21 0 1143.82 1138.99 35.99 o -6 21 0 68.08 67.73 12.61 o -3 21 0 5184.52 5431.04 85.14 o 0 21 0 1964.80 2191.06 143.96 o -20 22 0 28.55 5.77 11.26 o -17 22 0 134.04 99.43 16.61 o -14 22 0 7.21 -5.84 9.69 o -11 22 0 5774.43 5943.68 88.03 o -8 22 0 1361.83 1349.04 31.14 o -5 22 0 2551.94 2578.93 48.94 o -2 22 0 1726.33 1802.70 38.76 o -22 23 0 119.07 137.93 29.07 o -19 23 0 595.69 613.64 21.94 o -16 23 0 528.79 590.99 27.68 o -13 23 0 203.83 132.12 11.74 o -10 23 0 694.12 801.34 35.99 o -7 23 0 4.55 -6.18 12.61 o -4 23 0 1324.77 1454.07 53.99 o -1 23 0 369.73 348.12 38.76 o -21 24 0 16.41 13.84 20.76 o -18 24 0 1172.54 1273.93 58.14 o -15 24 0 982.13 1025.90 38.76 o -12 24 0 872.18 863.02 23.95 o -9 24 0 1011.99 1151.50 33.88 o -6 24 0 262.89 192.73 17.29 o -3 24 0 375.85 325.30 21.53 o 0 24 0 22.26 6.51 15.88 o -23 25 0 56.28 45.68 18.00 o -20 25 0 245.63 195.22 21.53 o -17 25 0 2405.04 2576.21 177.18 o -14 25 0 51.57 31.84 23.53 o -11 25 0 168.13 126.16 14.58 o -8 25 0 1383.30 1361.63 37.04 o -5 25 0 14.40 -13.10 14.58 o -2 25 0 13.04 20.55 17.91 o -25 26 0 20.95 19.12 20.49 o -22 26 0 0.22 10.42 16.55 o -19 26 0 1454.30 1517.20 51.22 o -16 26 0 1186.49 1326.67 56.75 o -13 26 0 1094.28 1065.59 32.59 o -10 26 0 766.28 782.13 30.30 o -7 26 0 15.86 15.45 27.68 o -4 26 0 27.02 8.31 17.62 o -1 26 0 142.99 131.61 24.92 o -24 27 0 827.21 838.64 56.75 o -21 27 0 529.47 587.67 55.37 o -18 27 0 4808.23 5417.54 168.88 o -15 27 0 157.09 150.24 26.30 o -12 27 0 43.02 6.77 17.29 o -9 27 0 771.73 706.72 29.70 o -6 27 0 24.09 41.11 19.28 o -3 27 0 57.90 40.77 21.27 o 0 27 0 10.71 13.05 25.57 o -26 28 0 1030.41 1059.53 51.22 o -23 28 0 342.53 329.42 31.20 o -20 28 0 1479.43 1570.64 119.04 o -17 28 0 7.96 23.69 17.29 o -14 28 0 0.90 -7.29 19.38 o -11 28 0 39.77 19.87 16.55 o -8 28 0 479.04 418.87 28.59 o -5 28 0 152.96 127.77 25.09 o -2 28 0 11.92 19.58 25.09 o -25 29 0 16.37 9.20 25.57 o -22 29 0 14.26 8.86 28.59 o -19 29 0 834.55 875.00 37.84 o -16 29 0 704.23 682.11 52.60 o -13 29 0 440.05 465.69 27.93 o -10 29 0 381.77 334.07 30.45 o -7 29 0 0.28 -12.50 29.92 o -4 29 0 267.10 200.43 31.90 o -24 30 0 51.46 45.86 26.36 o -21 30 0 903.54 1126.70 74.75 o -18 30 0 272.60 257.15 29.18 o -15 30 0 247.59 288.49 41.53 o -12 30 0 0.30 -1.25 26.30 o -9 30 0 231.71 205.75 31.20 o -6 30 0 0.05 2.37 27.20 o -23 31 0 324.41 352.80 36.36 o -20 31 0 1123.71 1245.68 113.51 o -17 31 0 24.16 62.75 31.20 o -14 31 0 88.35 53.22 25.94 o -11 31 0 78.06 105.76 95.51 o -8 31 0 14.62 2.14 29.92 o -19 32 0 1338.82 1437.95 58.14 o -16 32 0 4.35 -24.61 25.94 o -13 32 0 25.77 30.02 37.04 o -1 1 1 2895.88 1939.94 34.61 o -3 2 1 75.36 163.34 3.92 o 0 2 1 4238.95 4437.53 48.45 o -5 3 1 7426.08 6577.46 123.20 o -2 3 1 12608.68 11339.02 164.72 o 1 3 1 35413.19 35228.65 707.35 o -7 4 1 19431.96 18561.88 286.54 o -4 4 1 6124.23 6057.09 135.66 o -1 4 1 24141.89 22521.46 513.55 o 2 4 1 23692.10 23044.48 578.61 o -9 5 1 15811.70 16642.07 235.32 o -6 5 1 10227.14 9209.94 175.80 o -3 5 1 17891.80 18762.39 496.94 o 0 5 1 73731.34 69932.30 2159.41 o 3 5 1 3814.66 3650.13 99.67 o -11 6 1 12.23 37.84 4.15 o -8 6 1 11764.90 11954.07 150.88 o -5 6 1 138.56 108.54 2.48 o -2 6 1 39886.37 38763.52 721.19 o 1 6 1 17024.35 17427.33 426.35 o 4 6 1 18888.45 19776.94 622.91 o -13 7 1 168.68 158.61 5.54 o -10 7 1 327.51 355.88 6.92 o -7 7 1 497.78 581.43 7.83 o -4 7 1 2429.63 2185.02 38.76 o -1 7 1 41759.77 42635.52 1263.81 o 2 7 1 13.38 5.54 2.48 o 5 7 1 2545.09 2831.08 52.60 o -15 8 1 234.12 289.37 7.83 o -12 8 1 545.57 422.23 7.83 o -9 8 1 2077.48 1928.61 26.30 o -6 8 1 2698.38 2592.61 69.21 o -3 8 1 38287.60 38326.01 660.28 o 0 8 1 140.39 147.57 11.07 o 3 8 1 1683.81 1716.95 31.84 o 6 8 1 573.09 693.49 10.63 o -17 9 1 2554.55 2745.54 98.28 o -14 9 1 4538.10 4890.16 46.86 o -11 9 1 871.60 907.99 13.84 o -8 9 1 10154.59 10697.30 217.33 o -5 9 1 9.97 29.66 4.15 o -2 9 1 354.36 405.59 5.87 o 1 9 1 848.45 964.09 33.22 o 4 9 1 2.49 9.69 3.92 o 7 9 1 3869.77 4308.01 65.06 o -19 10 1 87.07 109.79 7.83 o -16 10 1 75.89 104.26 6.64 o -13 10 1 83.23 122.93 4.61 o -10 10 1 13951.46 14586.76 260.24 o -7 10 1 3798.07 4139.35 81.67 o -4 10 1 218.27 248.12 4.61 o -1 10 1 87.18 22.49 2.77 o 2 10 1 1280.66 1075.89 30.45 o 5 10 1 589.54 488.74 11.07 o 8 10 1 356.27 323.67 9.21 o -21 11 1 94.56 99.74 9.79 o -18 11 1 0.21 -2.77 8.31 o -15 11 1 1084.78 1145.97 33.22 o -12 11 1 3347.23 3727.94 33.28 o -9 11 1 181.65 171.65 4.61 o -6 11 1 18202.98 18853.54 382.05 o -3 11 1 14145.24 15759.00 376.51 o 0 11 1 309.15 252.76 23.53 o 3 11 1 258.60 209.25 6.92 o 6 11 1 2511.54 2473.11 71.98 o 9 11 1 1790.22 1758.41 65.06 o -23 12 1 12.06 20.66 19.38 o -20 12 1 27.29 11.07 9.69 o -17 12 1 61.19 46.58 15.23 o -14 12 1 1405.94 1535.23 33.22 o -11 12 1 153.18 166.11 5.87 o -8 12 1 522.94 590.58 9.69 o -5 12 1 9954.79 10802.63 189.64 o -2 12 1 11078.56 12046.40 412.50 o 1 12 1 17.43 37.87 4.61 o 4 12 1 600.59 515.00 11.75 o 7 12 1 9.15 6.92 5.87 o 10 12 1 1870.14 1768.31 63.68 o -25 13 1 769.01 836.15 33.88 o -22 13 1 113.34 95.68 20.76 o -19 13 1 41.31 24.52 6.64 o -16 13 1 33.85 26.58 5.54 o -13 13 1 1382.35 1279.13 17.62 o -10 13 1 2829.12 3176.83 31.32 o -7 13 1 5145.44 5639.71 76.13 o -4 13 1 0.00 1.85 2.48 o -1 13 1 2812.60 2972.46 145.35 o 2 13 1 284.69 296.23 7.12 o 5 13 1 42.23 19.82 8.31 o 8 13 1 452.14 454.90 14.58 o 11 13 1 182.86 132.34 49.83 o -27 14 1 303.87 343.16 26.68 o -24 14 1 1502.53 1588.29 62.29 o -21 14 1 281.19 228.22 13.84 o -18 14 1 468.17 452.20 11.26 o -15 14 1 98.96 94.05 6.92 o -12 14 1 890.71 807.47 12.61 o -9 14 1 4680.43 5382.55 58.14 o -6 14 1 4119.13 4218.53 105.20 o -3 14 1 370.00 318.47 7.83 o 0 14 1 2585.97 2368.76 84.44 o 3 14 1 123.53 86.81 11.07 o 6 14 1 198.51 200.60 8.65 o 9 14 1 103.67 102.00 14.24 o 12 14 1 270.60 290.11 20.96 o -29 15 1 38.46 20.94 21.94 o -26 15 1 928.75 949.31 34.31 o -23 15 1 274.25 264.30 45.68 o -20 15 1 358.84 335.73 15.23 o -17 15 1 2.38 -1.19 6.64 o -14 15 1 116.82 101.80 18.00 o -11 15 1 9377.32 9997.68 121.81 o -8 15 1 5281.27 5463.40 87.21 o -5 15 1 1218.04 1120.92 16.55 o -2 15 1 246.11 191.71 13.84 o 1 15 1 2249.92 2271.11 96.90 o 4 15 1 17806.07 18978.53 329.45 o 7 15 1 79.39 84.88 29.07 o 10 15 1 258.03 190.70 16.55 o 13 15 1 96.08 52.34 20.49 o -31 16 1 1064.85 1199.20 48.47 o -28 16 1 10.58 9.10 19.93 o -25 16 1 4425.04 4794.93 127.35 o -22 16 1 1678.58 1756.61 77.52 o -19 16 1 821.18 838.85 18.43 o -16 16 1 5.35 14.53 7.12 o -13 16 1 126.54 111.24 13.84 o -10 16 1 4665.13 5385.28 70.60 o -7 16 1 5789.86 6247.78 125.97 o -4 16 1 74.86 58.80 8.31 o -1 16 1 4793.33 4966.33 150.88 o 2 16 1 2617.57 2641.01 35.23 o 5 16 1 310.31 319.96 13.84 o 8 16 1 562.61 548.16 21.53 o 11 16 1 206.51 238.42 21.27 o 14 16 1 71.48 29.68 24.41 o -30 17 1 753.21 826.33 74.75 o -27 17 1 1345.21 1482.56 45.59 o -24 17 1 0.58 -6.92 15.66 o -21 17 1 76.85 94.63 11.07 o -18 17 1 265.10 208.33 20.76 o -15 17 1 1200.39 1166.34 20.49 o -12 17 1 1911.34 2006.36 27.20 o -9 17 1 80.46 65.91 4.95 o -6 17 1 301.60 232.81 16.61 o -3 17 1 1853.04 1774.06 42.91 o 0 17 1 814.25 784.75 22.15 o 3 17 1 17087.06 17806.57 337.75 o 6 17 1 817.81 757.26 23.25 o 9 17 1 653.11 664.95 31.75 o 12 17 1 1151.03 1300.66 96.90 o -29 18 1 417.77 434.83 85.82 o -26 18 1 1199.50 1331.56 67.83 o -23 18 1 22.81 20.30 14.58 o -20 18 1 0.20 4.43 9.21 o -17 18 1 101.09 93.07 7.43 o -14 18 1 5280.27 5627.49 70.95 o -11 18 1 636.20 695.76 13.29 o -8 18 1 37.37 9.69 12.46 o -5 18 1 15.41 24.92 7.83 o -2 18 1 2.18 -7.83 7.83 o 1 18 1 273.66 265.70 26.30 o 4 18 1 1056.39 1081.73 27.41 o 7 18 1 46.28 52.04 16.61 o 10 18 1 4.70 -17.29 17.29 o 13 18 1 875.20 899.17 63.68 o -31 19 1 143.26 78.70 26.58 o -28 19 1 107.63 93.86 25.22 o -25 19 1 3830.38 4146.86 125.97 o -22 19 1 14.17 8.09 12.61 o -19 19 1 199.55 191.70 12.10 o -16 19 1 173.60 188.37 15.23 o -13 19 1 8.05 7.91 6.64 o -10 19 1 0.10 3.95 11.07 o -7 19 1 972.37 1003.23 22.45 o -4 19 1 414.63 389.02 15.66 o -1 19 1 2.42 -4.00 8.65 o 2 19 1 5154.43 5523.02 138.42 o 5 19 1 2325.58 2370.29 143.96 o 8 19 1 1871.44 1974.84 112.12 o 11 19 1 4.59 13.84 24.56 o -30 20 1 301.81 263.05 32.25 o -27 20 1 2572.74 2749.55 80.29 o -24 20 1 41.85 37.94 16.55 o -21 20 1 89.22 95.48 18.00 o -18 20 1 582.72 614.06 26.30 o -15 20 1 2591.11 2554.96 39.24 o -12 20 1 9.37 12.66 6.64 o -9 20 1 36.80 37.18 8.31 o -6 20 1 5133.08 5362.62 77.31 o -3 20 1 800.34 916.35 29.07 o 0 20 1 372.19 355.28 35.99 o 3 20 1 3564.55 3931.73 150.88 o 6 20 1 702.98 636.63 41.53 o 9 20 1 0.21 24.41 21.27 o -29 21 1 4.88 -6.66 25.09 o -26 21 1 165.09 170.01 23.49 o -23 21 1 470.43 448.87 23.25 o -20 21 1 211.47 170.94 14.58 o -17 21 1 5725.65 5901.67 101.05 o -14 21 1 354.55 340.25 15.23 o -11 21 1 16.70 8.31 7.83 o -8 21 1 905.53 879.11 20.49 o -5 21 1 1040.79 1088.43 23.95 o -2 21 1 115.70 113.15 12.61 o 1 21 1 668.07 662.08 25.45 o 4 21 1 598.06 561.32 42.91 o 7 21 1 1357.39 1472.52 66.44 o 10 21 1 132.48 142.58 45.68 o -31 22 1 3.90 23.22 29.18 o -28 22 1 55.49 93.28 24.56 o -25 22 1 1146.08 1192.08 35.07 o -22 22 1 445.37 419.86 27.68 o -19 22 1 2.33 -5.54 11.75 o -16 22 1 159.31 130.14 11.26 o -13 22 1 352.39 240.83 20.76 o -10 22 1 84.89 35.99 11.07 o -7 22 1 1134.64 1244.47 27.41 o -4 22 1 629.30 595.00 26.30 o -1 22 1 86.29 61.88 13.82 o 2 22 1 397.50 417.89 33.22 o 5 22 1 6.03 4.37 18.52 o 8 22 1 42.35 25.74 26.37 o -30 23 1 0.05 -13.13 38.76 o -27 23 1 0.00 3.81 29.07 o -24 23 1 1749.76 1869.11 44.90 o -21 23 1 1051.74 1094.20 31.90 o -18 23 1 377.10 358.20 41.53 o -15 23 1 761.27 701.31 20.49 o -12 23 1 625.99 470.49 34.61 o -9 23 1 734.19 676.88 30.45 o -6 23 1 11.79 14.60 10.63 o -3 23 1 408.68 445.04 33.22 o 0 23 1 165.52 166.44 18.52 o 3 23 1 680.83 657.47 31.14 o 6 23 1 749.73 727.93 67.83 o -29 24 1 540.94 552.02 39.81 o -26 24 1 533.77 569.72 30.30 o -23 24 1 3443.43 3747.70 132.89 o -20 24 1 498.62 496.84 24.41 o -17 24 1 789.61 766.29 24.41 o -14 24 1 11.01 8.31 9.79 o -11 24 1 212.22 231.84 13.70 o -8 24 1 284.23 243.98 16.55 o -5 24 1 626.38 650.21 56.75 o -2 24 1 6.32 -18.52 18.52 o 1 24 1 4.52 8.45 18.52 o 4 24 1 50.91 41.53 23.49 o -28 25 1 304.43 265.64 59.52 o -25 25 1 1691.72 1861.86 53.59 o -22 25 1 734.23 696.27 42.91 o -19 25 1 74.29 60.32 17.91 o -16 25 1 6.00 5.71 15.30 o -13 25 1 1083.51 984.98 63.68 o -10 25 1 1003.49 911.75 26.37 o -7 25 1 49.89 30.45 13.82 o -4 25 1 62.98 55.52 19.38 o -1 25 1 17.12 -8.96 20.49 o 2 25 1 73.05 51.94 24.41 o -27 26 1 303.05 256.59 31.90 o -24 26 1 1865.12 2028.73 55.77 o -21 26 1 82.73 94.21 19.58 o -18 26 1 102.73 147.35 29.07 o -15 26 1 374.53 339.45 21.27 o -12 26 1 248.60 273.09 19.93 o -9 26 1 2068.58 2173.17 146.73 o -6 26 1 512.39 502.57 30.30 o -3 26 1 172.41 167.39 22.53 o 0 26 1 165.28 114.71 21.94 o 3 26 1 82.22 37.84 29.07 o -26 27 1 407.56 417.23 35.23 o -23 27 1 39.96 34.77 35.99 o -20 27 1 261.41 258.37 51.22 o -17 27 1 557.91 557.92 58.14 o -14 27 1 1382.98 1392.94 40.97 o -11 27 1 0.05 -0.87 15.30 o -8 27 1 656.10 636.73 32.59 o -5 27 1 3.03 -17.05 24.41 o -2 27 1 98.94 80.29 24.41 o 1 27 1 29.67 2.77 49.83 o -25 28 1 41.82 49.34 51.22 o -22 28 1 37.91 56.50 26.37 o -19 28 1 203.87 215.48 27.93 o -16 28 1 36.02 14.40 18.43 o -13 28 1 19.90 13.99 18.52 o -10 28 1 190.64 203.40 45.68 o -7 28 1 13.75 9.27 22.45 o -4 28 1 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