#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018273.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018273_Fobs loop_ _publ_author_name 'Schwarzer, Anke' 'Weber, Edwin' _publ_section_title ; Three new fluorinated N-phenyl-substituted pentacyclic ethanoanthracenedicarboximides ; _journal_coeditor_code EG3076 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o457 _journal_page_last o460 _journal_volume 67 _journal_year 2011 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.2586 _cell_length_b 24.1036 _cell_length_c 8.4301 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file eg3076IIcsup4.hkl _[local]_cod_data_source_block IIc #BEGIN Tags that were not found in dictionaries: _shelx_title ' ansc79_1m in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 339.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31321.54 47461.54 2255.62 o 4 0 0 4118.69 4241.17 267.22 o 6 0 0 86261.43 130222.56 6187.19 o 8 0 0 1610.61 1646.52 129.88 o 10 0 0 1192.97 1210.89 124.04 o 12 0 0 1.63 -23.31 113.13 o 14 0 0 6176.09 6420.51 308.90 o 16 0 0 6889.25 7386.92 571.41 o 18 0 0 1002.11 684.87 182.93 o 20 0 0 829.30 598.86 420.92 o 22 0 0 46.74 -178.27 197.17 o 1 1 0 12292.80 -8.85 16.79 o 3 1 0 228.52 245.11 22.83 o 5 1 0 22035.71 25916.00 648.19 o 7 1 0 11120.20 11211.08 311.45 o 9 1 0 68.08 -14.36 48.33 o 11 1 0 9259.27 9545.97 282.12 o 13 1 0 3316.76 3113.36 134.67 o 15 1 0 822.88 926.65 79.06 o 17 1 0 801.09 725.72 130.28 o 19 1 0 657.67 544.18 125.06 o 21 1 0 14.53 -28.42 166.95 o 2 2 0 1622.79 1461.38 55.36 o 4 2 0 3018.10 2973.43 86.71 o 6 2 0 6654.18 6677.86 180.81 o 8 2 0 10585.13 10724.25 304.81 o 10 2 0 9222.27 9424.30 282.92 o 12 2 0 535.54 518.28 133.09 o 14 2 0 826.61 811.80 98.94 o 16 2 0 674.29 753.24 99.22 o 18 2 0 1065.73 985.00 228.03 o 20 2 0 26.80 -5.67 119.21 o 22 2 0 195.78 376.07 137.52 o 1 3 0 18560.96 20695.27 420.05 o 3 3 0 32153.76 39881.99 873.54 o 5 3 0 1652.10 1399.99 63.20 o 7 3 0 2846.50 3175.31 121.56 o 9 3 0 16030.07 16410.38 528.12 o 11 3 0 1060.43 1178.40 117.35 o 13 3 0 1739.21 1697.13 149.14 o 15 3 0 820.45 703.03 166.82 o 17 3 0 2500.54 2783.51 181.29 o 19 3 0 3156.60 3176.73 247.64 o 21 3 0 197.29 53.51 132.34 o 0 4 0 6753.05 6120.56 205.43 o 2 4 0 10642.66 10298.07 227.42 o 4 4 0 4318.91 3908.93 140.16 o 6 4 0 28272.71 31050.80 641.98 o 8 4 0 6776.39 6866.69 228.96 o 10 4 0 302.51 277.31 89.46 o 12 4 0 3598.77 3589.85 231.49 o 14 4 0 1015.82 859.43 122.57 o 16 4 0 809.71 655.62 95.03 o 18 4 0 748.13 723.39 145.80 o 20 4 0 2855.33 2464.83 230.15 o 22 4 0 236.54 331.15 163.12 o 1 5 0 10263.73 10274.17 213.06 o 3 5 0 23614.04 27083.30 683.06 o 5 5 0 3265.96 3295.42 238.47 o 7 5 0 9476.97 9283.79 244.56 o 9 5 0 3309.48 3378.98 154.35 o 11 5 0 29.41 9.39 66.03 o 13 5 0 360.93 383.33 94.48 o 15 5 0 490.84 422.61 102.12 o 17 5 0 689.27 721.82 110.08 o 19 5 0 240.43 209.14 126.38 o 21 5 0 1.46 93.25 136.26 o 0 6 0 13366.04 13536.56 423.02 o 2 6 0 18166.55 19813.38 419.97 o 4 6 0 4516.53 4471.59 161.30 o 6 6 0 18152.97 18728.20 506.17 o 8 6 0 11754.79 12617.07 321.24 o 10 6 0 8520.99 8142.60 276.10 o 12 6 0 231.12 180.04 80.07 o 14 6 0 1662.22 1755.24 160.33 o 16 6 0 136.52 260.44 103.43 o 18 6 0 2522.89 2592.22 228.99 o 20 6 0 45.46 150.22 135.85 o 22 6 0 9.49 57.10 139.41 o 1 7 0 599.35 661.37 57.67 o 3 7 0 11194.03 10849.02 281.24 o 5 7 0 5.42 -49.98 49.98 o 7 7 0 9530.18 8758.35 273.82 o 9 7 0 12401.17 11964.90 361.29 o 11 7 0 26507.35 28347.88 766.73 o 13 7 0 689.40 543.90 108.14 o 15 7 0 181.43 -47.75 80.95 o 17 7 0 1477.50 1552.83 249.23 o 19 7 0 35.96 88.66 126.71 o 21 7 0 5.15 139.30 140.29 o 0 8 0 10239.88 9806.21 545.64 o 2 8 0 8114.61 7471.52 193.22 o 4 8 0 8752.84 7994.87 382.92 o 6 8 0 5951.35 5190.34 218.86 o 8 8 0 29000.94 30715.93 804.77 o 10 8 0 397.40 463.51 88.83 o 12 8 0 305.77 120.70 68.88 o 14 8 0 1.49 122.47 157.36 o 16 8 0 1012.01 1032.94 156.70 o 18 8 0 336.63 330.51 134.71 o 20 8 0 2.27 -50.00 118.88 o 1 9 0 3324.17 3480.75 153.13 o 3 9 0 529.81 330.15 87.03 o 5 9 0 442.66 483.95 83.43 o 7 9 0 20734.53 21355.36 675.65 o 9 9 0 2046.96 2226.68 135.84 o 11 9 0 328.31 301.97 79.49 o 13 9 0 111.99 64.60 79.88 o 15 9 0 146.21 35.94 83.32 o 17 9 0 216.87 142.30 109.57 o 19 9 0 55.13 -60.04 112.70 o 21 9 0 11.82 -116.07 134.32 o 0 10 0 1904.63 1678.94 233.76 o 2 10 0 9020.04 8728.94 282.60 o 4 10 0 161.64 144.10 72.03 o 6 10 0 22.60 -54.12 54.12 o 8 10 0 1390.33 1714.12 267.58 o 10 10 0 4661.38 4543.33 278.69 o 12 10 0 20.45 151.05 77.00 o 14 10 0 495.66 583.76 125.70 o 16 10 0 587.34 705.12 139.80 o 18 10 0 39.41 24.09 114.27 o 20 10 0 455.92 442.68 163.17 o 1 11 0 387.92 492.44 93.07 o 3 11 0 1240.66 1363.66 93.57 o 5 11 0 3313.39 3541.24 253.60 o 7 11 0 1516.09 1436.15 130.55 o 9 11 0 25.13 153.90 95.98 o 11 11 0 6119.86 5491.05 323.88 o 13 11 0 2.52 36.56 78.83 o 15 11 0 3352.38 3509.53 281.39 o 17 11 0 317.64 303.48 136.13 o 19 11 0 165.77 372.33 255.77 o 0 12 0 5146.55 5161.64 290.28 o 2 12 0 765.38 907.74 194.53 o 4 12 0 5346.59 5508.42 209.80 o 6 12 0 3.14 -2.74 66.58 o 8 12 0 669.74 739.95 194.19 o 10 12 0 9.21 11.90 87.61 o 12 12 0 8835.23 9085.87 328.06 o 14 12 0 846.77 730.20 125.47 o 16 12 0 1614.65 1486.65 184.70 o 18 12 0 86.97 201.18 157.43 o 20 12 0 211.38 300.86 156.64 o 1 13 0 2303.46 2228.45 142.16 o 3 13 0 29.86 -7.58 66.97 o 5 13 0 349.82 217.57 84.61 o 7 13 0 1071.58 1197.75 131.40 o 9 13 0 7.30 67.74 82.73 o 11 13 0 595.95 444.98 90.79 o 13 13 0 12925.71 13612.89 613.21 o 15 13 0 583.09 494.84 127.04 o 17 13 0 34.34 62.91 119.54 o 19 13 0 4057.07 4329.76 399.52 o 0 14 0 8718.25 7665.98 392.33 o 2 14 0 1563.82 1646.09 131.55 o 4 14 0 3273.48 3144.76 183.51 o 6 14 0 265.35 269.86 90.35 o 8 14 0 3818.76 3811.68 224.04 o 10 14 0 1481.69 1463.78 158.25 o 12 14 0 2492.85 2616.83 175.73 o 14 14 0 4119.18 3978.14 267.64 o 16 14 0 26.45 18.68 114.83 o 18 14 0 5087.07 5220.30 421.00 o 1 15 0 29.77 78.00 77.92 o 3 15 0 8932.40 8216.96 300.86 o 5 15 0 74.01 114.63 69.86 o 7 15 0 0.12 -91.28 132.63 o 9 15 0 3.13 95.14 140.11 o 11 15 0 158.11 71.66 77.28 o 13 15 0 917.06 1047.43 133.56 o 15 15 0 1109.38 1082.25 171.08 o 17 15 0 723.79 435.34 152.44 o 19 15 0 557.16 312.80 186.89 o 0 16 0 9988.96 9467.23 471.79 o 2 16 0 25.09 17.55 108.53 o 4 16 0 7602.87 8063.41 304.28 o 6 16 0 138.19 165.82 84.31 o 8 16 0 20.46 171.79 93.16 o 10 16 0 122.84 158.62 102.92 o 12 16 0 1974.74 2029.48 169.10 o 14 16 0 5020.94 4044.34 485.41 o 16 16 0 382.82 498.87 147.14 o 18 16 0 1.56 89.79 139.39 o 1 17 0 629.98 699.80 168.98 o 3 17 0 557.69 534.03 113.08 o 5 17 0 350.55 324.77 101.42 o 7 17 0 826.61 713.49 153.70 o 9 17 0 737.17 606.08 128.19 o 11 17 0 10.56 -55.87 106.63 o 13 17 0 24.24 19.73 105.83 o 15 17 0 312.59 532.16 197.55 o 17 17 0 110.57 144.43 146.93 o 0 18 0 3120.86 3101.55 652.19 o 2 18 0 2286.51 2541.48 245.37 o 4 18 0 247.83 299.76 182.27 o 6 18 0 8.38 16.81 135.61 o 8 18 0 937.41 676.07 122.55 o 10 18 0 106.44 192.75 119.90 o 12 18 0 0.60 40.87 94.88 o 14 18 0 46.47 12.36 120.23 o 16 18 0 862.93 688.78 287.53 o 1 19 0 86.44 83.12 94.73 o 3 19 0 49.69 55.21 94.70 o 5 19 0 355.99 269.30 142.00 o 7 19 0 22.29 40.41 119.34 o 9 19 0 387.39 267.71 115.64 o 11 19 0 1812.92 2068.61 439.29 o 13 19 0 15.21 112.28 123.52 o 15 19 0 310.58 293.01 146.58 o 17 19 0 7.93 53.41 139.42 o 0 20 0 3592.72 3575.09 316.66 o 2 20 0 80.05 119.00 129.29 o 4 20 0 5936.01 6413.85 380.51 o 6 20 0 1254.85 1321.38 165.67 o 8 20 0 3547.16 3600.48 283.38 o 10 20 0 466.43 271.19 120.10 o 12 20 0 2.54 -100.47 152.13 o 14 20 0 2810.13 2821.51 255.86 o 16 20 0 161.15 -97.83 138.83 o 1 21 0 923.72 1078.19 154.20 o 3 21 0 308.21 349.35 125.05 o 5 21 0 28.11 119.90 115.68 o 7 21 0 137.70 116.65 138.02 o 9 21 0 372.86 332.54 168.13 o 11 21 0 461.23 64.05 162.27 o 13 21 0 668.90 389.12 156.71 o 15 21 0 199.47 301.42 157.65 o 0 22 0 350.76 543.95 193.57 o 2 22 0 1.32 -104.84 104.84 o 4 22 0 2365.53 2277.59 205.73 o 6 22 0 174.47 142.93 160.28 o 8 22 0 473.13 536.98 213.91 o 10 22 0 33.77 -186.09 186.09 o 12 22 0 359.62 315.28 179.93 o 14 22 0 3535.67 3820.28 548.85 o 1 23 0 749.46 555.31 156.66 o 3 23 0 2277.94 2214.82 210.01 o 5 23 0 15.69 -35.53 120.65 o 7 23 0 179.76 338.27 535.18 o 9 23 0 4.19 161.53 218.38 o 11 23 0 543.41 523.49 272.90 o 13 23 0 894.87 812.86 244.17 o 0 24 0 85.03 -2.02 248.09 o 2 24 0 109.99 310.24 138.95 o 4 24 0 72.35 68.80 208.66 o 6 24 0 45.94 -50.10 188.62 o 8 24 0 1539.55 1799.28 572.07 o 10 24 0 60.82 350.52 280.47 o 12 24 0 105.88 -387.70 387.70 o 1 25 0 302.95 349.74 152.93 o 3 25 0 307.63 402.22 354.06 o 5 25 0 60.31 -87.51 170.66 o 7 25 0 1130.11 1054.61 302.11 o 9 25 0 141.69 113.12 503.01 o 11 25 0 162.92 -288.51 407.59 o 0 26 0 7.34 490.04 388.39 o 2 26 0 0.03 131.00 183.42 o 4 26 0 171.56 84.12 172.85 o 6 26 0 28.46 -121.95 376.53 o 8 26 0 78.81 -22.77 369.36 o 10 26 0 121.73 44.03 441.10 o 1 27 0 103.48 -216.76 377.99 o 3 27 0 156.42 498.21 287.62 o 5 27 0 1.41 603.72 288.15 o 7 27 0 95.77 -396.22 396.22 o 9 27 0 47.39 85.50 480.85 o 0 28 0 54.86 453.31 435.01 o 2 28 0 97.86 723.41 335.01 o 4 28 0 51.65 82.21 294.16 o 6 28 0 192.74 206.86 434.48 o 1 29 0 37.74 -268.26 268.26 o 3 29 0 111.55 97.71 344.54 o 1 1 1 860.42 740.58 23.55 o 2 1 1 2423.57 2185.35 49.09 o 3 1 1 11842.39 12452.65 192.98 o 4 1 1 91.74 45.34 23.47 o 5 1 1 22729.20 25617.77 487.00 o 6 1 1 8769.23 8955.22 193.88 o 7 1 1 26.31 42.66 26.33 o 8 1 1 189.89 236.76 35.93 o 9 1 1 225.87 235.97 36.51 o 10 1 1 1630.64 1784.05 70.12 o 11 1 1 139.84 186.71 39.69 o 12 1 1 102.88 106.27 37.90 o 13 1 1 171.98 49.08 39.07 o 14 1 1 0.72 23.15 38.97 o 15 1 1 4.24 67.97 43.31 o 16 1 1 271.29 271.04 61.23 o 17 1 1 1504.83 1633.71 102.36 o 18 1 1 242.51 106.89 103.70 o 19 1 1 33.45 -68.97 68.97 o 20 1 1 85.12 39.58 80.28 o 21 1 1 549.86 553.58 99.23 o 22 1 1 2.35 -48.49 82.35 o 1 2 1 30722.06 38186.68 495.01 o 2 2 1 12727.01 13026.12 208.59 o 3 2 1 2173.94 2278.43 56.37 o 4 2 1 3157.67 3035.50 74.78 o 5 2 1 222.11 175.52 33.79 o 6 2 1 5140.57 4953.99 124.82 o 7 2 1 682.32 723.31 54.04 o 8 2 1 717.38 607.75 56.06 o 9 2 1 1027.47 1112.06 67.99 o 10 2 1 59.17 4.17 38.07 o 11 2 1 79.11 -1.30 39.81 o 12 2 1 557.72 601.70 51.82 o 13 2 1 84.71 168.80 41.07 o 14 2 1 1545.40 1625.23 89.12 o 15 2 1 467.50 556.51 61.53 o 16 2 1 110.94 184.32 52.93 o 17 2 1 230.95 259.39 70.37 o 18 2 1 19.17 17.93 111.47 o 19 2 1 0.00 81.78 75.68 o 20 2 1 207.50 346.13 89.15 o 21 2 1 477.52 406.03 96.49 o 22 2 1 4.44 -15.20 84.80 o 1 3 1 20804.89 22948.00 358.05 o 2 3 1 15618.36 16142.18 286.85 o 3 3 1 33207.80 40632.77 700.41 o 4 3 1 29451.87 33556.04 523.97 o 5 3 1 16967.42 17699.38 308.47 o 6 3 1 6455.28 6157.99 130.45 o 7 3 1 286.84 222.19 38.31 o 8 3 1 2179.51 2206.70 79.13 o 9 3 1 9249.83 9542.56 210.50 o 10 3 1 863.11 1032.27 61.75 o 11 3 1 35.63 26.68 32.79 o 12 3 1 630.06 647.16 53.76 o 13 3 1 6163.40 5957.26 142.90 o 14 3 1 72.56 86.73 47.11 o 15 3 1 17.40 36.06 43.58 o 16 3 1 52.56 15.22 55.00 o 17 3 1 571.65 484.20 77.74 o 18 3 1 952.61 789.87 122.13 o 19 3 1 232.48 160.82 109.98 o 20 3 1 610.38 689.94 105.88 o 21 3 1 542.80 562.52 106.52 o 22 3 1 0.55 36.03 99.31 o 1 4 1 23104.04 24599.35 408.75 o 2 4 1 568.88 541.33 35.69 o 3 4 1 11889.13 11207.42 200.20 o 4 4 1 2057.72 1952.36 70.37 o 5 4 1 11378.19 11429.43 240.47 o 6 4 1 4.71 6.53 40.90 o 7 4 1 2628.97 2624.58 80.18 o 8 4 1 1702.54 1762.95 78.26 o 9 4 1 1568.55 1800.13 71.34 o 10 4 1 329.61 276.67 52.80 o 11 4 1 201.61 351.95 46.59 o 12 4 1 617.01 622.13 55.96 o 13 4 1 912.64 808.61 71.47 o 14 4 1 530.98 631.54 71.47 o 15 4 1 1.10 -36.23 44.71 o 16 4 1 491.01 465.21 71.69 o 17 4 1 292.17 255.66 125.90 o 18 4 1 158.41 193.42 75.44 o 19 4 1 26.11 77.30 83.02 o 20 4 1 76.53 -81.24 81.24 o 21 4 1 339.24 430.61 100.37 o 22 4 1 12.83 160.51 99.83 o 1 5 1 10.28 -15.68 30.78 o 2 5 1 14948.30 14883.24 277.09 o 3 5 1 11127.19 10951.64 228.26 o 4 5 1 117.25 163.65 31.09 o 5 5 1 2932.83 2749.37 83.72 o 6 5 1 1326.73 1313.61 66.07 o 7 5 1 1148.41 1307.64 65.22 o 8 5 1 3454.81 3431.88 129.70 o 9 5 1 86.31 19.02 44.91 o 10 5 1 758.84 740.05 60.70 o 11 5 1 995.92 888.60 72.83 o 12 5 1 851.29 782.68 70.70 o 13 5 1 109.48 84.01 47.69 o 14 5 1 1491.13 1511.39 95.65 o 15 5 1 61.74 -46.05 46.05 o 16 5 1 9.05 50.41 68.06 o 17 5 1 65.73 54.07 64.02 o 18 5 1 43.19 28.90 67.13 o 19 5 1 543.10 530.46 100.81 o 20 5 1 0.02 -31.83 85.71 o 21 5 1 136.30 73.87 93.70 o 22 5 1 108.44 123.66 98.72 o 1 6 1 23236.13 24760.73 446.81 o 2 6 1 10134.02 9410.71 180.22 o 3 6 1 47.77 16.18 34.09 o 4 6 1 103.75 7.93 23.57 o 5 6 1 1086.05 1098.38 55.88 o 6 6 1 25498.50 27921.46 509.34 o 7 6 1 180.65 263.37 42.20 o 8 6 1 1624.76 1479.33 67.79 o 9 6 1 4449.55 4217.41 117.12 o 10 6 1 1306.90 1334.20 70.63 o 11 6 1 474.68 455.20 55.35 o 12 6 1 920.36 941.07 80.55 o 13 6 1 540.95 512.10 71.08 o 14 6 1 569.79 672.70 79.58 o 15 6 1 242.12 169.36 72.51 o 16 6 1 103.82 100.55 62.77 o 17 6 1 5.55 -25.53 62.59 o 18 6 1 32.21 15.09 67.24 o 19 6 1 1.90 -20.29 80.10 o 20 6 1 82.98 64.38 93.63 o 21 6 1 224.22 123.94 100.55 o 1 7 1 1033.24 1009.19 48.76 o 2 7 1 20588.43 21230.28 370.53 o 3 7 1 7056.98 6780.23 143.40 o 4 7 1 34.09 10.55 32.75 o 5 7 1 75.48 124.85 34.43 o 6 7 1 6783.17 6305.23 149.24 o 7 7 1 372.68 259.12 79.49 o 8 7 1 7541.31 7606.43 167.57 o 9 7 1 136.75 71.96 39.15 o 10 7 1 1458.82 1416.87 94.73 o 11 7 1 43.17 77.25 42.89 o 12 7 1 59.10 75.08 44.63 o 13 7 1 649.47 768.90 76.66 o 14 7 1 250.35 263.36 63.86 o 15 7 1 1.96 17.98 54.88 o 16 7 1 3.52 -28.29 63.19 o 17 7 1 125.84 165.52 69.00 o 18 7 1 5.68 7.76 69.20 o 19 7 1 38.69 98.40 86.82 o 20 7 1 0.01 -85.21 114.04 o 21 7 1 2.66 -53.09 94.39 o 1 8 1 4681.30 4354.47 102.84 o 2 8 1 737.34 765.50 45.59 o 3 8 1 0.13 -23.00 28.43 o 4 8 1 902.68 888.76 85.17 o 5 8 1 2127.32 2080.16 78.34 o 6 8 1 4524.03 4317.76 161.30 o 7 8 1 1591.39 1484.62 75.14 o 8 8 1 1232.39 1248.36 68.94 o 9 8 1 275.99 356.83 63.97 o 10 8 1 517.38 439.54 54.35 o 11 8 1 9.90 105.66 54.82 o 12 8 1 400.17 330.86 54.81 o 13 8 1 161.72 66.41 86.55 o 14 8 1 412.42 399.41 79.16 o 15 8 1 16.68 -45.35 86.68 o 16 8 1 204.27 47.96 70.48 o 17 8 1 40.07 129.10 79.37 o 18 8 1 36.20 -2.87 68.91 o 19 8 1 485.27 348.58 107.85 o 20 8 1 15.51 53.01 92.76 o 21 8 1 204.70 283.45 107.62 o 1 9 1 10591.77 10304.76 195.45 o 2 9 1 8182.63 7813.38 157.08 o 3 9 1 12298.53 12002.99 220.62 o 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