#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180858 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018983_Fobs loop_ _publ_author_name 'Wu, Xiang-Wen' 'Xin, Meng-Meng' 'Ma, Jian-Ping' 'Wu, Zhen-Hua' 'Dong, Yu-Bin' _publ_section_title ; The coordination chemistry of two symmetric double-armed oxadiazole-bridged organic ligands with copper salts ; _journal_coeditor_code OV3026 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 601 _journal_page_last 605 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 96.709 _cell_angle_beta 102.843 _cell_angle_gamma 108.464 _cell_length_a 9.2604 _cell_length_b 12.5973 _cell_length_c 15.6232 _exptl_crystal_F_000 884.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file ov3026IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 81205em in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 23673.96 25260.56 434.33 o 2 0 0 1172.02 1229.11 74.99 o 3 0 0 28628.57 28080.98 505.77 o 4 0 0 33797.80 33548.59 611.18 o 5 0 0 2583.18 2723.66 95.50 o 6 0 0 897.48 985.06 98.43 o 7 0 0 1569.65 1602.46 86.46 o 8 0 0 3373.29 3116.03 131.15 o 9 0 0 876.52 852.01 83.67 o 10 0 0 4.38 27.69 25.94 o -10 1 0 47.37 25.74 35.34 o -9 1 0 114.63 230.68 49.96 o -8 1 0 13.01 19.52 33.05 o -7 1 0 3168.92 2922.17 115.61 o -6 1 0 140.01 150.66 31.32 o -5 1 0 4985.59 4835.82 135.30 o -4 1 0 16494.50 16521.94 325.11 o -3 1 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