#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180858 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018984.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2018984_Fobs
loop_
_publ_author_name
'He, Hua'
'Stoyko, Stanislav S.'
'Mar, Arthur'
'Bobev, Svilen'
_publ_section_title
;
 Ternary K~2~Zn~5~As~4~-type pnictides Rb~2~Cd~5~As~4~ and
 Rb~2~Zn~5~Sb~4~, and the solid solution Rb~2~Cd~5~(As,Sb)~4~
;
_journal_coeditor_code           OV3027
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              455
_journal_page_last               459
_journal_volume                  69
_journal_year                    2013
_space_group_IT_number           63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   12.4317
_cell_length_b                   7.5870
_cell_length_c                   12.5073
_exptl_crystal_F_000             1784.00
_reflns_d_resolution_high        0.7643
_cod_data_source_file            ov3027Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' Rb2Cd5As4 in Cmcm'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            929.88
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 126964.80 134582.08 2213.56 o
4 0 0 142036.22 149480.31 2644.20 o
6 0 0 864676.88 820247.62 12741.74 o
8 0 0 246422.31 251396.34 4587.48 o
10 0 0 27544.29 28115.16 1300.29 o
12 0 0 82678.16 85898.59 2457.54 o
14 0 0 202506.19 206555.59 5782.18 o
16 0 0 61.63 -748.64 748.64 o
1 1 0 24501.40 25431.44 310.45 o
3 1 0 281.26 345.72 105.50 o
5 1 0 27477.76 29733.80 531.30 o
7 1 0 145791.50 150444.41 2106.76 o
9 1 0 15641.84 15967.86 674.96 o
11 1 0 647.84 245.76 307.63 o
13 1 0 14619.07 14540.67 866.34 o
15 1 0 58.21 -491.21 491.21 o
0 2 0 13605.93 14435.22 396.18 o
2 2 0 75745.65 80619.25 945.06 o
4 2 0 9283.29 10125.18 478.21 o
6 2 0 76026.71 77214.18 1048.73 o
8 2 0 24571.35 24528.70 713.85 o
10 2 0 13901.12 13525.51 685.96 o
12 2 0 56966.58 54254.55 1359.78 o
14 2 0 155.71 359.17 468.23 o
1 3 0 429835.91 415700.25 4070.99 o
3 3 0 36271.59 36800.52 601.36 o
5 3 0 312219.66 312665.75 3255.34 o
7 3 0 108224.37 110970.43 1460.31 o
9 3 0 114645.53 114568.51 1903.87 o
11 3 0 16931.94 15047.44 790.42 o
13 3 0 52271.95 51729.57 1684.69 o
15 3 0 41234.52 39774.48 1683.16 o
0 4 0 36071.27 34002.54 1125.92 o
2 4 0 7087.07 7159.40 342.44 o
4 4 0 50207.82 52791.92 1472.48 o
6 4 0 2685.33 2627.04 302.19 o
8 4 0 6931.51 6753.62 411.29 o
10 4 0 26908.47 26860.75 1486.92 o
12 4 0 442.48 230.92 570.65 o
14 4 0 287.54 -631.97 631.97 o
1 5 0 20476.40 21156.92 613.80 o
3 5 0 68809.60 68833.65 1170.53 o
5 5 0 10699.15 10055.72 525.93 o
7 5 0 903.41 887.03 315.50 o
9 5 0 71.32 -362.62 362.62 o
11 5 0 12113.00 11109.84 926.95 o
13 5 0 4218.68 4651.99 963.25 o
0 6 0 11252.06 11436.38 1493.19 o
2 6 0 10022.68 9545.92 505.21 o
4 6 0 93339.52 91342.50 1657.39 o
6 6 0 285.72 800.12 336.21 o
8 6 0 3210.68 2971.31 502.53 o
10 6 0 63001.10 65337.68 3043.31 o
12 6 0 2477.09 2580.60 897.14 o
1 7 0 307.91 52.73 340.85 o
3 7 0 2376.77 1978.43 467.80 o
5 7 0 16838.56 17455.55 1069.45 o
7 7 0 12902.75 13610.74 822.34 o
9 7 0 11193.76 11185.23 1101.47 o
11 7 0 2074.39 2326.50 841.99 o
0 8 0 164413.14 145239.52 6203.67 o
2 8 0 122.21 62.89 518.90 o
4 8 0 137.97 -167.73 480.77 o
6 8 0 60570.75 57956.80 1921.21 o
8 8 0 11421.86 14513.97 1304.98 o
1 9 0 84.74 -103.66 744.00 o
3 9 0 2540.41 2480.43 1110.11 o
5 9 0 8503.22 8615.26 1653.10 o
1 1 1 298.42 200.52 46.39 o
3 1 1 283.21 288.78 76.17 o
5 1 1 6892.62 7108.97 178.72 o
7 1 1 50.04 68.28 119.52 o
9 1 1 3533.34 3239.37 279.22 o
11 1 1 5333.84 5384.75 364.78 o
13 1 1 703.73 1024.08 306.39 o
15 1 1 5229.53 6339.36 518.45 o
0 2 1 27332.84 27847.14 543.94 o
2 2 1 59484.19 59422.71 563.15 o
4 2 1 150873.62 152484.62 1190.27 o
6 2 1 4089.42 4888.55 191.95 o
8 2 1 5.87 35.06 142.35 o
10 2 1 63859.76 63495.82 954.81 o
12 2 1 2628.55 2715.81 328.40 o
14 2 1 4845.69 5039.94 444.11 o
1 3 1 10966.13 11020.39 257.43 o
3 3 1 253724.30 250466.83 1922.47 o
5 3 1 9447.63 10114.96 298.98 o
7 3 1 33515.42 33532.23 517.13 o
9 3 1 63558.00 61972.34 1045.55 o
11 3 1 29833.99 29128.64 717.36 o
13 3 1 13958.49 12510.48 615.15 o
15 3 1 3908.12 4788.67 605.48 o
0 4 1 747.73 760.21 176.19 o
2 4 1 11.13 112.57 116.08 o
4 4 1 122.49 200.40 129.90 o
6 4 1 261.45 335.86 151.95 o
8 4 1 104.68 266.41 184.47 o
10 4 1 112.11 -86.30 293.28 o
12 4 1 8.89 67.44 392.55 o
14 4 1 104.10 152.52 495.62 o
1 5 1 3736.79 4230.53 261.04 o
3 5 1 197883.23 194051.61 1709.31 o
5 5 1 28458.14 28588.13 555.70 o
7 5 1 838.35 909.46 214.10 o
9 5 1 66207.41 68573.65 1074.81 o
11 5 1 32371.41 33140.04 1049.41 o
13 5 1 1046.85 1840.96 602.98 o
0 6 1 2677.72 2946.99 355.13 o
2 6 1 17379.33 16677.19 454.22 o
4 6 1 42202.16 40614.46 755.52 o
6 6 1 98.15 344.31 223.12 o
8 6 1 183.41 173.78 255.33 o
10 6 1 23606.91 26114.76 1026.16 o
12 6 1 2374.24 2355.69 564.94 o
1 7 1 1923.81 1656.01 297.49 o
3 7 1 1043.92 1255.46 299.64 o
5 7 1 4.79 58.91 261.23 o
7 7 1 2455.10 2207.67 359.75 o
9 7 1 2859.73 2203.86 475.52 o
11 7 1 742.26 -239.01 497.04 o
0 8 1 35461.50 31979.32 1330.69 o
2 8 1 15563.82 13269.87 835.82 o
4 8 1 9340.91 7312.63 591.56 o
6 8 1 23238.47 23574.23 1070.54 o
8 8 1 13883.78 14972.74 919.66 o
1 9 1 938.12 1493.10 495.51 o
3 9 1 479.61 382.72 463.37 o
5 9 1 1049.52 1184.88 467.76 o
0 0 2 122988.12 128397.98 1849.69 o
2 0 2 2657.57 2566.01 150.11 o
4 0 2 262647.78 268555.62 2708.45 o
6 0 2 140889.02 144804.94 1939.12 o
8 0 2 29213.37 28655.26 799.68 o
10 0 2 159662.05 157538.11 2400.41 o
12 0 2 34559.33 32422.05 1092.99 o
14 0 2 7096.07 6951.47 1425.32 o
16 0 2 10233.40 9461.32 904.52 o
1 1 2 284.60 191.89 74.70 o
3 1 2 334076.62 336367.91 2333.97 o
5 1 2 327.16 184.12 102.95 o
7 1 2 20233.15 20774.40 347.67 o
9 1 2 6222.20 5869.78 325.57 o
11 1 2 48326.37 45994.96 841.27 o
13 1 2 46.28 284.04 279.81 o
15 1 2 110.28 -32.87 379.68 o
0 2 2 33174.31 34501.84 587.49 o
2 2 2 259625.53 260294.41 1926.97 o
4 2 2 51538.12 52490.26 595.08 o
6 2 2 1973.94 2263.55 158.38 o
8 2 2 49796.08 49941.69 645.26 o
10 2 2 17445.74 17335.69 541.96 o
12 2 2 12174.93 11209.12 501.89 o
14 2 2 187.58 102.53 376.57 o
1 3 2 9056.10 8880.40 216.61 o
3 3 2 1395.16 1535.39 157.50 o
5 3 2 19029.56 19635.93 348.42 o
7 3 2 82342.56 85935.21 875.76 o
9 3 2 10166.93 10165.26 401.38 o
11 3 2 273.15 234.60 276.77 o
13 3 2 7159.25 7422.81 564.33 o
15 3 2 28.49 191.06 525.12 o
0 4 2 13170.42 12879.74 389.02 o
2 4 2 66960.30 65606.72 707.25 o
4 4 2 9539.36 9222.96 313.56 o
6 4 2 8844.90 8792.28 319.13 o
8 4 2 2222.69 2598.28 240.28 o
10 4 2 812.42 442.87 276.60 o
12 4 2 35405.49 36267.80 1095.57 o
14 4 2 7387.57 8805.51 783.36 o
1 5 2 42729.94 42833.28 576.57 o
3 5 2 4658.58 5010.45 249.56 o
5 5 2 302.84 313.56 183.10 o
7 5 2 119921.91 121872.68 1343.13 o
9 5 2 1512.19 1500.06 333.10 o
11 5 2 373.24 -17.93 433.73 o
13 5 2 21033.05 23644.63 1115.92 o
0 6 2 41257.43 41104.27 1040.35 o
2 6 2 57463.13 55423.46 808.52 o
4 6 2 15563.28 15872.39 476.49 o
6 6 2 3117.86 3358.59 318.70 o
8 6 2 7658.50 8135.46 433.39 o
10 6 2 8090.88 9504.28 685.57 o
12 6 2 1446.22 1771.07 614.86 o
1 7 2 30.91 172.17 268.51 o
3 7 2 43603.20 42240.11 995.47 o
5 7 2 261.06 259.24 270.21 o
7 7 2 4131.51 4048.96 412.02 o
9 7 2 715.50 986.61 421.49 o
11 7 2 9988.86 9308.11 781.95 o
0 8 2 24916.22 24716.30 1347.80 o
2 8 2 2573.07 2326.43 429.42 o
4 8 2 19849.97 19644.36 944.72 o
6 8 2 32256.91 32666.37 1319.93 o
8 8 2 9485.10 11218.55 700.72 o
1 9 2 34.15 501.23 454.86 o
3 9 2 25539.74 25656.47 1217.38 o
5 9 2 116.64 -482.22 482.22 o
1 1 3 2017.89 1820.23 99.13 o
3 1 3 2125.59 2175.17 144.42 o
5 1 3 1359.86 1348.13 144.86 o
7 1 3 1488.68 1605.95 161.42 o
9 1 3 5469.93 5462.90 326.43 o
11 1 3 3432.92 2702.28 317.22 o
13 1 3 454.75 652.45 320.05 o
15 1 3 5771.91 5160.38 554.12 o
0 2 3 243307.27 239238.94 2431.72 o
2 2 3 9643.03 9661.86 243.71 o
4 2 3 4878.84 4861.35 182.45 o
6 2 3 95598.46 96584.53 902.37 o
8 2 3 42221.35 42714.28 615.89 o
10 2 3 5967.36 6239.61 468.52 o
12 2 3 6361.22 5908.87 429.97 o
14 2 3 28915.71 28003.01 1046.04 o
1 3 3 227745.83 225650.17 1679.18 o
3 3 3 13123.60 13190.66 328.82 o
5 3 3 51721.70 52956.11 608.28 o
7 3 3 206374.81 207793.47 1759.71 o
9 3 3 98.20 166.64 203.62 o
11 3 3 602.34 780.28 294.82 o
13 3 3 70536.33 69176.69 1649.33 o
15 3 3 3333.25 2823.63 622.22 o
0 4 3 1073.64 1111.43 181.70 o
2 4 3 3543.11 3910.30 235.48 o
4 4 3 3737.55 4025.48 215.88 o
6 4 3 840.44 838.00 181.71 o
8 4 3 729.35 820.45 209.97 o
10 4 3 1368.05 902.55 336.82 o
12 4 3 497.89 939.99 476.44 o
14 4 3 67.17 -362.67 526.77 o
1 5 3 159559.31 156244.02 1396.11 o
3 5 3 76.25 398.02 165.37 o
5 5 3 56433.97 56965.16 790.73 o
7 5 3 138543.31 140487.20 1549.27 o
9 5 3 2389.35 2352.73 378.77 o
11 5 3 4847.75 5131.39 600.12 o
13 5 3 52056.21 56232.99 1667.11 o
0 6 3 117338.40 115723.87 2205.31 o
2 6 3 27954.11 28396.15 834.00 o
4 6 3 5476.44 5222.21 329.19 o
6 6 3 64666.29 64519.18 961.96 o
8 6 3 40942.01 40737.08 844.52 o
10 6 3 979.26 462.87 474.90 o
12 6 3 10776.44 11904.21 857.83 o
1 7 3 10421.16 9405.56 546.64 o
3 7 3 12396.32 12058.48 557.74 o
5 7 3 16386.25 15677.90 602.15 o
7 7 3 4891.66 4335.20 402.18 o
9 7 3 2185.31 1572.46 428.32 o
11 7 3 12221.01 12350.66 836.56 o
0 8 3 12661.63 11670.28 1290.31 o
2 8 3 26501.03 26578.78 947.09 o
4 8 3 31831.44 30868.54 967.93 o
6 8 3 9919.86 9625.49 698.26 o
8 8 3 10743.98 10879.71 790.40 o
1 9 3 3214.59 3095.46 563.14 o
3 9 3 11159.37 11622.20 941.81 o
5 9 3 2008.55 2815.60 547.48 o
0 0 4 207484.03 204334.08 3004.69 o
2 0 4 414630.66 405542.81 3980.44 o
4 0 4 274786.91 271742.41 2815.68 o
6 0 4 9354.73 9614.00 411.64 o
8 0 4 25925.49 25268.31 706.58 o
10 0 4 118781.17 120527.85 2126.23 o
12 0 4 16810.69 15418.51 1080.95 o
14 0 4 11727.83 10294.71 1011.68 o
1 1 4 66695.09 66904.55 635.39 o
3 1 4 125309.28 128267.73 1040.97 o
5 1 4 212767.61 215921.36 1717.37 o
7 1 4 5559.98 5644.38 243.08 o
9 1 4 110748.11 110304.02 1308.90 o
11 1 4 39716.67 38423.68 897.77 o
13 1 4 731.65 603.91 359.10 o
15 1 4 10512.00 9893.38 685.56 o
0 2 4 161118.55 159255.75 1737.94 o
2 2 4 63211.81 63815.30 651.30 o
4 2 4 279508.84 279031.88 2067.98 o
6 2 4 19662.65 19632.94 406.59 o
8 2 4 35186.11 35925.80 553.71 o
10 2 4 144369.08 145440.44 1748.64 o
12 2 4 100.85 432.46 327.91 o
14 2 4 25750.64 25927.67 1077.72 o
1 3 4 359.65 446.18 125.34 o
3 3 4 151502.61 150226.00 1301.78 o
5 3 4 99.27 132.33 136.41 o
7 3 4 17553.42 17749.15 456.77 o
9 3 4 2373.09 2592.17 341.16 o
11 3 4 29342.56 29037.30 906.15 o
13 3 4 409.07 939.19 458.25 o
0 4 4 70938.91 70581.31 1002.29 o
2 4 4 756.93 813.53 168.11 o
4 4 4 80449.48 81154.69 931.89 o
6 4 4 13659.69 14468.39 439.50 o
8 4 4 460.36 473.60 223.86 o
10 4 4 38851.01 38151.92 1003.33 o
12 4 4 3297.92 3719.63 562.70 o
14 4 4 1517.20 1207.87 560.57 o
1 5 4 93456.02 90725.62 1003.23 o
3 5 4 4728.73 4629.33 276.06 o
5 5 4 62406.74 62979.89 857.19 o
7 5 4 26160.34 26479.62 608.36 o
9 5 4 15705.56 16137.07 869.41 o
11 5 4 18.18 268.19 456.61 o
13 5 4 19586.20 20451.71 1041.59 o
0 6 4 234.16 338.25 298.75 o
2 6 4 250.42 281.44 215.79 o
4 6 4 33071.57 32450.24 721.17 o
6 6 4 10060.13 10087.37 472.26 o
8 6 4 601.21 678.10 354.17 o
10 6 4 28456.30 29425.77 1724.10 o
12 6 4 9627.82 9486.70 809.30 o
1 7 4 6626.55 6148.56 447.85 o
3 7 4 12118.64 11442.68 733.22 o
5 7 4 31741.86 30531.33 936.92 o
7 7 4 2924.44 4411.81 549.02 o
9 7 4 20681.83 21220.68 924.08 o
0 8 4 69557.04 68042.99 2157.07 o
2 8 4 13731.24 12869.82 708.25 o
4 8 4 8812.71 9207.28 620.44 o
6 8 4 17960.48 19782.69 850.78 o
8 8 4 273.89 771.03 493.60 o
1 9 4 1271.96 1432.06 473.79 o
3 9 4 5249.03 4804.64 583.84 o
5 9 4 12204.30 13677.74 972.52 o
1 1 5 3995.62 3808.35 182.16 o
3 1 5 4366.04 4576.55 203.85 o
5 1 5 41.07 -58.94 123.70 o
7 1 5 2920.15 2987.88 241.27 o
9 1 5 8512.18 8210.37 375.89 o
11 1 5 1141.36 1178.02 312.84 o
13 1 5 43.30 238.13 364.46 o
15 1 5 7081.02 6824.00 721.91 o
0 2 5 91028.75 89301.39 1128.04 o
2 2 5 941.43 934.70 130.32 o
4 2 5 29559.36 29005.66 419.36 o
6 2 5 34055.97 33952.66 535.10 o
8 2 5 12279.56 12847.20 372.33 o
10 2 5 18237.22 17806.53 603.79 o
12 2 5 662.15 745.17 402.05 o
14 2 5 14030.88 13611.26 881.21 o
1 3 5 51974.06 50860.80 603.83 o
3 3 5 86319.08 87616.20 893.35 o
5 3 5 1546.95 1381.55 165.55 o
7 3 5 68641.38 67944.95 776.48 o
9 3 5 17611.02 18267.10 693.67 o
11 3 5 6683.25 6254.25 547.01 o
13 3 5 26958.79 26270.44 1073.29 o
0 4 5 939.74 983.37 186.47 o
2 4 5 1986.23 2081.70 190.72 o
4 4 5 3035.58 2998.74 246.83 o
6 4 5 625.07 666.44 200.44 o
8 4 5 525.19 606.83 247.00 o
10 4 5 1397.18 992.69 358.82 o
12 4 5 345.80 320.92 457.77 o
14 4 5 87.62 387.39 597.94 o
1 5 5 19988.07 18831.79 565.70 o
3 5 5 39828.65 39260.34 654.63 o
5 5 5 388.37 287.98 199.00 o
7 5 5 31447.88 31503.66 700.46 o
9 5 5 10641.96 10454.93 688.50 o
11 5 5 3035.98 2980.83 571.86 o
13 5 5 13329.03 14448.60 1216.50 o
0 6 5 28415.32 27679.60 1079.58 o
2 6 5 0.11 -147.58 220.07 o
4 6 5 4713.12 4584.58 368.70 o
6 6 5 11765.33 11203.94 514.87 o
8 6 5 5669.70 5879.33 497.30 o
10 6 5 3884.90 4813.73 644.97 o
1 7 5 343.28 511.98 304.30 o
3 7 5 660.03 421.16 313.66 o
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7 7 5 25.67 -346.48 378.46 o
9 7 5 69.14 374.37 543.00 o
0 8 5 2458.80 2695.20 723.52 o
2 8 5 103.59 457.97 422.74 o
4 8 5 636.82 720.07 459.10 o
6 8 5 1120.84 675.02 431.97 o
8 8 5 183.54 562.09 482.25 o
1 9 5 417.58 495.16 466.22 o
3 9 5 3889.24 5535.52 653.72 o
0 0 6 506265.47 483992.72 6783.54 o
2 0 6 222327.27 220390.50 2594.73 o
4 0 6 57.38 155.70 168.78 o
6 0 6 428010.91 418821.03 4329.04 o
8 0 6 192122.30 187318.88 2280.96 o
10 0 6 8269.53 8948.41 703.55 o
12 0 6 127447.16 128832.60 2580.06 o
14 0 6 53528.98 51956.82 1805.99 o
1 1 6 24530.45 23899.58 389.41 o
3 1 6 77690.20 77368.97 798.24 o
5 1 6 17499.98 17664.63 349.61 o
7 1 6 189.47 197.33 164.52 o
9 1 6 1391.12 1624.48 260.96 o
11 1 6 10919.52 10059.08 559.77 o
13 1 6 3679.80 3032.85 489.12 o
15 1 6 3534.45 3837.58 664.90 o
0 2 6 161250.91 156278.36 1807.96 o
2 2 6 18130.20 18391.70 419.98 o
4 2 6 2974.09 2939.27 192.55 o
6 2 6 31626.77 31954.99 538.98 o
8 2 6 21.57 121.70 194.19 o
10 2 6 1439.79 998.91 313.49 o
12 2 6 746.64 750.13 443.12 o
14 2 6 11053.13 9913.97 772.37 o
1 3 6 117271.23 117281.65 1103.98 o
3 3 6 79562.70 79128.66 858.46 o
5 3 6 14296.68 14591.57 389.44 o
7 3 6 191112.72 197703.50 2022.73 o
9 3 6 7136.90 7098.42 579.72 o
11 3 6 15505.04 15604.38 1170.78 o
13 3 6 34432.80 34032.62 1282.67 o
0 4 6 8596.31 9420.28 528.97 o
2 4 6 41312.09 40668.00 625.53 o
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