#------------------------------------------------------------------------------
#$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $
#$Revision: 88054 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018985.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2018985_Fobs
loop_
_publ_author_name
'He, Hua'
'Stoyko, Stanislav S.'
'Mar, Arthur'
'Bobev, Svilen'
_publ_section_title
;
 Ternary K~2~Zn~5~As~4~-type pnictides Rb~2~Cd~5~As~4~ and
 Rb~2~Zn~5~Sb~4~, and the solid solution Rb~2~Cd~5~(As,Sb)~4~
;
_journal_coeditor_code           OV3027
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              455
_journal_page_last               459
_journal_volume                  69
_journal_year                    2013
_space_group_IT_number           63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   12.3975
_cell_length_b                   7.5516
_cell_length_c                   12.4514
_exptl_crystal_F_000             1712.00
_reflns_d_resolution_high        0.7496
_[local]_cod_data_source_file    ov3027IIsup3.hkl
_[local]_cod_data_source_block   II
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' Rb2Zn5Sb4 in Cmcm'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            810.92
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 70365.20 77536.55 1241.64 o
4 0 0 175618.77 177590.62 3428.22 o
6 0 0 657591.06 628859.69 8673.38 o
8 0 0 319182.94 322354.53 5130.20 o
10 0 0 13650.32 11656.15 811.28 o
12 0 0 147343.25 145626.52 3202.71 o
14 0 0 159505.86 162878.77 3665.08 o
16 0 0 700.33 1193.55 584.78 o
1 1 0 15824.32 16911.87 223.32 o
3 1 0 3101.35 3011.99 135.23 o
5 1 0 22580.01 24044.89 602.96 o
7 1 0 101179.85 102505.20 1270.45 o
9 1 0 9897.48 9287.17 492.43 o
11 1 0 4884.55 4603.08 403.78 o
13 1 0 1489.78 1677.77 300.13 o
15 1 0 16086.07 15066.30 802.67 o
0 2 0 135762.52 133805.64 1769.24 o
2 2 0 150738.61 154254.98 1482.82 o
4 2 0 3292.97 3622.11 174.16 o
6 2 0 342970.66 337688.56 3137.54 o
8 2 0 10174.33 9654.22 378.17 o
10 2 0 556.74 434.54 168.86 o
12 2 0 122176.83 124067.15 2042.29 o
14 2 0 3981.99 3996.70 389.18 o
16 2 0 2182.56 2396.20 403.41 o
1 3 0 212320.84 205981.02 2120.51 o
3 3 0 73299.43 76499.38 872.48 o
5 3 0 190718.36 192200.66 2049.05 o
7 3 0 33857.02 33159.25 600.20 o
9 3 0 170984.69 176258.77 2349.91 o
11 3 0 3122.91 2850.95 331.32 o
13 3 0 55802.73 54383.07 1463.53 o
15 3 0 17414.67 18008.31 1120.80 o
0 4 0 257616.08 243213.84 3444.16 o
2 4 0 3809.00 3797.62 235.16 o
4 4 0 81781.03 81823.66 1195.18 o
6 4 0 55295.02 56960.53 843.25 o
8 4 0 4704.21 5197.39 332.16 o
10 4 0 4267.44 3571.72 402.63 o
12 4 0 56581.16 54597.61 1436.35 o
14 4 0 8576.88 8217.02 700.17 o
1 5 0 926.30 885.46 110.66 o
3 5 0 134109.83 133691.50 2104.54 o
5 5 0 579.47 679.72 153.21 o
7 5 0 4273.16 4440.59 330.33 o
9 5 0 1189.40 1485.09 264.46 o
11 5 0 57447.98 58552.65 1479.91 o
13 5 0 3865.72 4696.31 611.74 o
0 6 0 10006.82 10752.73 888.72 o
2 6 0 140.74 436.29 130.07 o
4 6 0 87174.48 87171.05 1502.86 o
6 6 0 58414.76 59892.98 1099.77 o
8 6 0 944.84 1027.38 201.83 o
10 6 0 24321.41 25752.19 1198.71 o
12 6 0 13665.66 14012.04 1001.11 o
1 7 0 12136.21 11524.28 556.60 o
3 7 0 24365.89 24607.13 766.01 o
5 7 0 32525.29 32272.21 982.12 o
7 7 0 706.42 912.78 222.36 o
9 7 0 58417.39 58198.57 2070.18 o
11 7 0 618.83 1179.85 467.50 o
0 8 0 142211.19 149346.98 4060.48 o
2 8 0 4411.53 4858.57 453.55 o
4 8 0 1326.70 1429.78 259.87 o
6 8 0 30857.19 32546.76 1448.83 o
8 8 0 10057.35 10110.68 801.32 o
10 8 0 1708.49 1166.97 549.55 o
1 9 0 1513.54 1612.78 407.54 o
3 9 0 11447.77 12000.47 1065.88 o
5 9 0 1669.97 1598.74 341.68 o
7 9 0 12860.54 14745.78 958.51 o
0 10 0 103.95 374.18 327.24 o
2 10 0 2178.10 2459.34 508.26 o
1 1 1 145.26 171.64 43.55 o
3 1 1 100422.83 104736.59 709.61 o
5 1 1 2545.59 2566.55 100.74 o
7 1 1 607.68 692.71 96.41 o
9 1 1 72088.52 72723.72 921.85 o
11 1 1 587.82 605.16 122.79 o
13 1 1 5338.37 4847.64 305.25 o
15 1 1 36456.80 35465.25 809.00 o
0 2 1 30830.30 32601.16 412.59 o
2 2 1 15094.96 14816.72 206.50 o
4 2 1 64801.52 64684.50 545.46 o
6 2 1 4001.60 3938.39 146.36 o
8 2 1 2534.31 2472.69 142.73 o
10 2 1 21182.74 21091.36 608.09 o
12 2 1 2269.69 2009.78 197.90 o
14 2 1 3047.57 3068.62 252.08 o
16 2 1 587.95 436.19 209.45 o
1 3 1 9462.16 9507.98 186.39 o
3 3 1 335725.09 333151.16 2870.42 o
5 3 1 11640.40 11708.11 235.32 o
7 3 1 26297.67 27107.19 384.51 o
9 3 1 92322.57 91644.09 1068.17 o
11 3 1 27752.95 26866.92 713.85 o
13 3 1 6718.96 6331.00 401.51 o
15 3 1 15026.95 15592.55 717.87 o
0 4 1 1197.39 927.83 108.13 o
2 4 1 194.31 122.02 53.60 o
4 4 1 1988.50 1631.52 114.99 o
6 4 1 2961.32 2927.72 167.03 o
8 4 1 280.23 305.37 97.23 o
10 4 1 301.55 108.25 126.24 o
12 4 1 4742.85 4867.15 352.12 o
14 4 1 10.95 -196.26 196.26 o
1 5 1 2467.19 2384.68 130.97 o
3 5 1 185195.02 185356.97 1487.77 o
5 5 1 13430.14 13130.57 343.44 o
7 5 1 123.75 261.82 96.09 o
9 5 1 82701.76 84600.57 1183.50 o
11 5 1 14590.50 15328.42 618.52 o
13 5 1 618.65 899.52 228.58 o
0 6 1 7447.75 7031.29 503.87 o
2 6 1 7323.09 7009.51 257.74 o
4 6 1 15780.00 16149.92 392.67 o
6 6 1 12133.00 12210.01 368.64 o
8 6 1 372.69 511.48 121.39 o
10 6 1 5142.48 5770.09 394.75 o
12 6 1 14861.43 14931.55 782.43 o
1 7 1 1446.21 1211.93 142.60 o
3 7 1 20549.94 20338.70 545.37 o
5 7 1 158.26 174.96 107.26 o
7 7 1 886.61 771.04 142.55 o
9 7 1 26256.17 26222.12 833.51 o
11 7 1 414.57 441.93 233.00 o
0 8 1 69810.57 69816.98 1556.29 o
2 8 1 8306.13 9019.21 432.18 o
4 8 1 1054.77 977.15 165.40 o
6 8 1 42396.43 44451.06 940.99 o
8 8 1 16713.28 15793.71 738.36 o
10 8 1 298.88 340.55 246.83 o
1 9 1 2763.45 2467.19 278.51 o
3 9 1 16475.10 16184.37 645.18 o
5 9 1 288.27 500.86 171.54 o
7 9 1 4596.56 4959.18 407.71 o
0 10 1 22717.89 19936.25 1132.32 o
0 0 2 81301.90 88021.60 1120.84 o
2 0 2 253.61 410.74 151.90 o
4 0 2 381054.34 374678.38 3400.65 o
6 0 2 185643.09 191538.91 2029.46 o
8 0 2 369.10 476.23 126.76 o
10 0 2 94921.80 92984.15 1585.74 o
12 0 2 15760.05 15055.62 709.71 o
14 0 2 10.35 -156.16 174.26 o
16 0 2 5986.55 5536.70 561.36 o
1 1 2 128.98 164.89 48.46 o
3 1 2 133570.25 136280.61 896.96 o
5 1 2 503.92 384.08 61.95 o
7 1 2 23386.70 23820.54 344.48 o
9 1 2 4491.47 4815.14 265.93 o
11 1 2 71115.41 70030.78 980.66 o
13 1 2 2327.76 2226.51 207.16 o
15 1 2 1766.61 1661.80 221.02 o
0 2 2 93126.22 95755.45 1018.93 o
2 2 2 317931.78 323041.47 2321.48 o
4 2 2 35670.56 35936.27 367.59 o
6 2 2 1216.22 1190.11 91.31 o
8 2 2 29652.78 29824.15 427.01 o
10 2 2 66625.73 67388.26 918.23 o
12 2 2 333.02 216.80 154.38 o
14 2 2 1073.64 1380.98 213.53 o
16 2 2 58515.01 60023.75 1341.92 o
1 3 2 4.14 21.85 41.08 o
3 3 2 8279.80 8124.57 193.94 o
5 3 2 23019.42 23656.03 327.35 o
7 3 2 30807.30 30756.31 415.46 o
9 3 2 8491.17 8303.52 331.95 o
11 3 2 4701.74 4420.15 298.01 o
13 3 2 7199.19 7122.50 446.82 o
15 3 2 7922.24 8098.02 550.32 o
0 4 2 1935.88 1777.11 161.16 o
2 4 2 11816.63 11750.78 260.15 o
4 4 2 20386.40 20190.47 329.72 o
6 4 2 61455.00 61287.59 667.76 o
8 4 2 17618.78 17531.39 398.98 o
10 4 2 4548.15 4393.16 301.16 o
12 4 2 40058.93 39897.05 993.06 o
14 4 2 9506.69 9551.39 610.69 o
1 5 2 49007.73 48836.42 568.99 o
3 5 2 249.34 189.56 74.93 o
5 5 2 98.83 80.78 81.84 o
7 5 2 125636.95 126761.09 1212.28 o
9 5 2 5602.16 5862.54 347.84 o
11 5 2 8169.14 7581.53 481.17 o
13 5 2 3385.47 3152.45 358.38 o
0 6 2 94839.66 94522.39 1333.73 o
2 6 2 88492.30 86697.44 953.90 o
4 6 2 21786.78 21996.13 471.96 o
6 6 2 3247.15 3214.14 211.69 o
8 6 2 763.92 677.99 140.93 o
10 6 2 36419.87 36004.09 940.54 o
12 6 2 255.47 465.65 228.03 o
1 7 2 2929.70 2383.25 220.00 o
3 7 2 18212.00 17637.44 593.87 o
5 7 2 7972.74 8134.70 360.84 o
7 7 2 1489.80 1458.48 181.10 o
9 7 2 703.16 706.61 179.55 o
11 7 2 5060.11 4822.80 446.50 o
0 8 2 11586.84 10395.61 654.93 o
2 8 2 2158.07 1993.43 262.94 o
4 8 2 30962.56 30895.94 742.51 o
6 8 2 41604.49 40707.46 1014.24 o
8 8 2 2.58 -198.03 198.03 o
1 9 2 2880.99 3501.85 303.44 o
3 9 2 6853.99 6571.70 423.29 o
5 9 2 1899.22 2359.21 301.54 o
7 9 2 13007.70 13355.06 669.31 o
0 10 2 6712.00 6957.26 757.65 o
1 1 3 75599.91 78974.79 560.87 o
3 1 3 2486.83 2428.72 95.92 o
5 1 3 72639.72 72163.55 618.47 o
7 1 3 48714.06 49774.03 520.28 o
9 1 3 7144.48 6479.34 301.11 o
11 1 3 30617.07 28807.84 614.90 o
13 1 3 42004.87 41204.38 789.64 o
15 1 3 4909.28 5074.31 375.81 o
0 2 3 82085.31 81997.05 843.30 o
2 2 3 6.33 88.88 41.81 o
4 2 3 17577.19 17202.14 249.55 o
6 2 3 22777.93 22293.91 322.94 o
8 2 3 14957.18 14904.45 321.70 o
10 2 3 6798.45 6769.68 324.05 o
12 2 3 12.22 104.25 118.15 o
14 2 3 7105.33 6852.74 420.04 o
1 3 3 293263.50 281209.97 1785.97 o
3 3 3 14809.78 15251.32 254.73 o
5 3 3 81919.53 82493.10 717.61 o
7 3 3 251772.84 253290.75 1741.97 o
9 3 3 14.02 -8.83 91.58 o
11 3 3 8889.43 7903.23 413.84 o
13 3 3 85971.50 87851.11 1432.06 o
15 3 3 3624.13 3642.04 441.94 o
0 4 3 1298.66 1191.06 121.15 o
2 4 3 2598.99 2495.88 131.41 o
4 4 3 555.18 519.40 79.85 o
6 4 3 56.12 91.44 66.75 o
8 4 3 5429.40 5670.79 251.31 o
10 4 3 1391.36 1421.88 220.36 o
12 4 3 320.63 353.50 297.33 o
14 4 3 2350.53 1793.16 318.35 o
1 5 3 150644.88 146814.58 1168.87 o
3 5 3 9.15 205.93 71.02 o
5 5 3 76098.20 76257.27 888.49 o
7 5 3 125299.93 129055.12 1299.52 o
9 5 3 564.60 830.80 171.21 o
11 5 3 19304.90 18539.92 731.53 o
13 5 3 59117.70 60939.40 1646.70 o
0 6 3 42269.70 42157.16 910.63 o
2 6 3 42796.64 43412.27 670.16 o
4 6 3 22392.88 22786.50 482.50 o
6 6 3 20981.24 21164.13 496.55 o
8 6 3 42198.10 42672.52 787.05 o
10 6 3 16498.65 15873.71 685.77 o
12 6 3 2851.39 2279.25 330.10 o
1 7 3 26596.54 24547.43 613.04 o
3 7 3 3015.12 2746.93 233.39 o
5 7 3 36697.32 35132.78 698.53 o
7 7 3 19349.17 19256.33 583.32 o
9 7 3 156.50 210.75 170.55 o
11 7 3 22577.48 23005.92 863.25 o
0 8 3 2366.72 1932.40 321.89 o
2 8 3 42923.39 44676.90 870.31 o
4 8 3 65150.98 65863.02 1160.32 o
6 8 3 4122.19 4257.42 358.67 o
8 8 3 13629.57 13660.81 767.10 o
1 9 3 3433.31 3111.99 278.52 o
3 9 3 14209.17 14355.80 626.34 o
5 9 3 651.92 730.41 314.10 o
0 0 4 176999.61 180588.17 2285.58 o
2 0 4 529478.75 507454.62 7469.14 o
4 0 4 253880.98 247917.80 2249.99 o
6 0 4 1068.35 1087.68 134.07 o
8 0 4 19636.29 19185.62 553.15 o
10 0 4 196589.77 197948.52 2740.01 o
12 0 4 9240.70 8656.90 565.30 o
14 0 4 66.93 277.95 216.35 o
16 0 4 79850.49 81862.84 2008.50 o
1 1 4 34437.89 35201.64 355.79 o
3 1 4 51311.69 51616.29 495.78 o
5 1 4 143210.62 142756.33 1186.02 o
7 1 4 6015.56 6103.84 196.72 o
9 1 4 72614.50 72832.27 853.98 o
11 1 4 6470.39 5979.15 320.52 o
13 1 4 23984.33 24003.75 675.20 o
15 1 4 586.71 401.80 205.35 o
0 2 4 110365.99 115169.95 1138.73 o
2 2 4 88574.08 88429.45 733.30 o
4 2 4 406966.94 412406.06 2554.29 o
6 2 4 133.72 370.26 132.04 o
8 2 4 130779.10 130685.62 1127.92 o
10 2 4 133891.92 135133.38 1517.05 o
12 2 4 18.21 -28.09 115.52 o
14 2 4 44721.06 46017.07 969.28 o
1 3 4 12099.98 11920.25 217.52 o
3 3 4 62618.93 62184.86 600.04 o
5 3 4 2916.38 2699.57 135.59 o
7 3 4 51762.72 53044.36 588.40 o
9 3 4 2308.45 2169.32 189.16 o
11 3 4 53136.59 54346.00 1048.87 o
13 3 4 175.94 88.45 163.29 o
15 3 4 4286.40 4167.73 428.66 o
0 4 4 80108.55 80698.88 1025.89 o
2 4 4 53904.02 53496.68 605.84 o
4 4 4 8510.66 8175.87 229.02 o
6 4 4 3803.29 3654.34 245.50 o
8 4 4 6314.72 6543.33 296.54 o
10 4 4 4953.48 4588.63 373.70 o
12 4 4 11859.40 12127.23 625.29 o
14 4 4 256.65 161.99 259.08 o
1 5 4 113605.08 111078.37 1018.53 o
3 5 4 1536.99 1419.54 130.92 o
5 5 4 66396.27 66481.98 778.70 o
7 5 4 35668.66 37007.28 676.84 o
9 5 4 36440.71 36696.80 824.54 o
11 5 4 1200.38 998.11 212.80 o
13 5 4 49578.23 48971.78 1195.68 o
0 6 4 2682.25 2598.60 283.56 o
2 6 4 1149.30 1295.37 157.14 o
4 6 4 100020.97 97384.02 1135.33 o
6 6 4 34400.45 33145.62 629.42 o
8 6 4 4952.08 5197.30 320.32 o
10 6 4 35535.12 35677.76 956.58 o
12 6 4 5079.02 5035.47 577.94 o
1 7 4 1171.72 1109.07 161.19 o
3 7 4 162.54 216.47 110.09 o
5 7 4 1805.91 1869.51 214.90 o
7 7 4 20749.34 21241.52 647.22 o
9 7 4 13762.30 14341.45 715.43 o
11 7 4 6432.54 6416.16 531.84 o
0 8 4 69519.51 65875.80 1554.06 o
2 8 4 23325.55 23586.74 677.41 o
4 8 4 2907.41 2499.04 330.92 o
6 8 4 7242.14 7440.77 434.20 o
8 8 4 401.99 661.22 235.29 o
1 9 4 10003.39 10292.14 547.80 o
3 9 4 998.89 1254.44 240.33 o
5 9 4 27550.04 28588.30 872.57 o
1 1 5 186.15 54.96 46.67 o
3 1 5 68151.94 68724.70 626.75 o
5 1 5 2193.65 2104.54 140.84 o
7 1 5 939.67 797.70 94.81 o
9 1 5 54477.51 53782.65 701.36 o
11 1 5 980.64 1411.17 167.78 o
13 1 5 6383.68 6001.90 379.16 o
15 1 5 26794.45 27371.90 866.91 o
0 2 5 64470.96 66883.75 790.18 o
2 2 5 41.20 -2.00 43.00 o
4 2 5 13902.98 13849.82 237.13 o
6 2 5 20300.34 19888.81 323.81 o
8 2 5 13599.95 13456.79 347.58 o
10 2 5 4878.96 4576.93 288.68 o
12 2 5 27.48 77.66 165.11 o
14 2 5 7469.41 7417.27 508.37 o
1 3 5 52593.07 53582.04 542.21 o
3 3 5 130939.79 131054.38 1038.11 o
5 3 5 1284.45 1442.33 104.02 o
7 3 5 65553.97 65725.10 719.32 o
9 3 5 30351.76 30886.35 665.71 o
11 3 5 4411.27 4169.60 331.73 o
13 3 5 21917.41 21616.93 763.84 o
0 4 5 3384.53 3298.56 233.89 o
2 4 5 1140.77 1218.34 102.34 o
4 4 5 3754.30 3706.61 189.71 o
6 4 5 4393.10 4217.92 224.90 o
8 4 5 0.00 20.43 98.82 o
10 4 5 635.49 705.43 163.08 o
12 4 5 4798.29 4701.93 404.97 o
14 4 5 5.40 -208.22 208.22 o
1 5 5 19297.90 18757.95 399.76 o
3 5 5 42949.21 42576.43 584.49 o
5 5 5 3324.47 3087.94 198.08 o
7 5 5 24767.06 25292.59 662.38 o
9 5 5 18973.28 18582.22 641.01 o
11 5 5 0.88 115.25 166.11 o
13 5 5 12958.65 13007.32 882.14 o
0 6 5 732.13 594.98 165.76 o
2 6 5 547.56 636.38 127.00 o
4 6 5 170.50 158.86 109.91 o
6 6 5 170.00 126.69 115.01 o
8 6 5 3891.08 3445.07 290.01 o
10 6 5 34.78 99.47 179.77 o
12 6 5 2731.63 2860.73 430.06 o
1 7 5 2215.49 1866.04 212.82 o
3 7 5 3227.50 3018.62 253.46 o
5 7 5 7243.46 7224.21 409.22 o
7 7 5 1508.45 1097.24 179.87 o
9 7 5 8093.42 8015.84 556.96 o
0 8 5 15420.39 15072.82 803.19 o
2 8 5 1335.54 1003.58 193.49 o
4 8 5 6508.46 6102.39 407.83 o
6 8 5 7021.04 7051.81 451.34 o
8 8 5 588.26 1146.12 248.79 o
1 9 5 1596.36 1211.90 243.48 o
3 9 5 15992.31 16541.17 698.25 o
5 9 5 52.38 -25.59 186.79 o
0 0 6 472205.22 432662.19 5149.56 o
2 0 6 199171.70 201136.70 1899.88 o
4 0 6 5058.54 5060.50 230.44 o
6 0 6 542392.00 525506.31 4543.20 o
8 0 6 96395.84 96798.72 1404.28 o
10 0 6 195.90 594.04 404.62 o
12 0 6 122298.36 124143.87 3072.35 o
14 0 6 39569.50 39628.81 1179.70 o
1 1 6 12074.18 12039.00 207.25 o
3 1 6 30106.53 29515.65 384.91 o
5 1 6 7298.49 7049.24 224.04 o
7 1 6 1598.04 1230.97 121.73 o
9 1 6 18575.15 18160.68 453.83 o
11 1 6 27905.53 27660.53 694.41 o
13 1 6 9132.80 9528.11 486.68 o
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