#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180858 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018986.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2018986_Fobs
loop_
_publ_author_name
'He, Hua'
'Stoyko, Stanislav S.'
'Mar, Arthur'
'Bobev, Svilen'
_publ_section_title
;
 Ternary K~2~Zn~5~As~4~-type pnictides Rb~2~Cd~5~As~4~ and
 Rb~2~Zn~5~Sb~4~, and the solid solution Rb~2~Cd~5~(As,Sb)~4~
;
_journal_coeditor_code           OV3027
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              455
_journal_page_last               459
_journal_volume                  69
_journal_year                    2013
_space_group_IT_number           63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   12.6086
_cell_length_b                   7.6761
_cell_length_c                   12.6232
_exptl_crystal_F_000             1856.00
_reflns_d_resolution_high        0.7685
_cod_data_source_file            ov3027IIIsup4.hkl
_cod_data_source_block           III
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' Rb2Cd5As3Sb in Cmcm'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            970.44
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 134670.55 140980.97 1085.42 o
4 0 0 142952.22 145888.25 1295.30 o
6 0 0 941752.44 920219.75 11026.26 o
8 0 0 266293.25 272841.75 2859.18 o
10 0 0 36115.44 36827.48 756.79 o
12 0 0 93672.62 95616.96 1392.38 o
14 0 0 204057.88 206639.00 3503.42 o
16 0 0 831.78 708.00 247.77 o
1 1 0 26072.64 27155.73 287.45 o
3 1 0 585.63 650.49 54.35 o
5 1 0 31241.96 31831.92 384.28 o
7 1 0 147428.38 149501.55 1081.37 o
9 1 0 11453.33 11277.57 272.24 o
11 1 0 522.86 566.77 107.40 o
13 1 0 11073.61 11765.99 700.06 o
15 1 0 278.83 263.29 92.33 o
0 2 0 29359.34 31060.14 383.85 o
2 2 0 74303.50 77723.70 538.33 o
4 2 0 10132.57 10396.18 161.46 o
6 2 0 105328.53 104974.85 800.22 o
8 2 0 22487.72 22414.25 363.23 o
10 2 0 16621.68 16714.62 427.50 o
12 2 0 76139.71 75564.98 1029.09 o
14 2 0 42.12 285.80 112.61 o
16 2 0 36.42 -38.79 104.95 o
1 3 0 433145.94 432118.72 2383.64 o
3 3 0 39124.69 39123.23 512.81 o
5 3 0 317129.25 316737.22 1941.68 o
7 3 0 105760.73 106842.83 972.88 o
9 3 0 129980.34 130514.09 1203.82 o
11 3 0 19188.44 19638.53 516.21 o
13 3 0 50437.93 49820.58 979.59 o
15 3 0 46982.78 47057.94 1215.25 o
0 4 0 58460.49 58286.17 736.42 o
2 4 0 9582.41 9261.60 218.50 o
4 4 0 50581.10 50385.36 672.97 o
6 4 0 9812.30 10054.92 316.11 o
8 4 0 9630.69 9510.84 341.01 o
10 4 0 21610.44 21222.15 589.86 o
12 4 0 2935.05 3143.70 284.95 o
14 4 0 524.96 509.78 150.37 o
1 5 0 25204.10 25229.76 344.84 o
3 5 0 67992.26 65724.68 667.86 o
5 5 0 11882.42 12363.80 358.63 o
7 5 0 1025.01 1519.37 196.60 o
9 5 0 1099.29 1024.32 159.09 o
11 5 0 12137.41 12059.50 454.56 o
13 5 0 3194.06 3101.70 286.95 o
0 6 0 4748.09 4800.47 394.20 o
2 6 0 7279.23 7137.56 280.69 o
4 6 0 97047.67 95882.70 1115.36 o
6 6 0 2113.87 2249.40 199.80 o
8 6 0 2070.95 2169.96 236.23 o
10 6 0 66617.74 65879.65 1060.65 o
12 6 0 4619.46 4322.51 487.00 o
1 7 0 256.88 233.51 101.58 o
3 7 0 2178.70 1960.38 176.78 o
5 7 0 18125.22 17367.73 539.43 o
7 7 0 15891.27 15485.42 477.15 o
9 7 0 13056.16 12569.01 454.64 o
11 7 0 1373.31 1526.73 194.17 o
0 8 0 218680.08 219477.05 7529.77 o
2 8 0 86.00 143.29 82.94 o
4 8 0 1077.99 978.32 151.56 o
6 8 0 82351.05 83024.58 1201.20 o
8 8 0 14874.04 15189.80 497.55 o
1 9 0 14.46 154.35 98.17 o
3 9 0 641.36 629.50 147.02 o
5 9 0 9715.90 8978.30 515.68 o
7 9 0 8279.16 7675.42 477.88 o
1 1 1 496.67 581.65 34.60 o
3 1 1 2277.71 2505.97 60.50 o
5 1 1 9807.57 10198.70 139.28 o
7 1 1 36.05 27.90 24.71 o
9 1 1 10848.75 10632.99 189.27 o
11 1 1 6595.71 6821.40 180.80 o
13 1 1 2733.10 2590.83 170.25 o
15 1 1 9271.00 8937.12 334.54 o
0 2 1 28074.59 28546.42 285.70 o
2 2 1 57648.05 58272.38 314.35 o
4 2 1 157534.17 158158.00 994.66 o
6 2 1 2366.01 2387.44 102.48 o
8 2 1 84.98 112.90 31.05 o
10 2 1 59547.01 58761.83 518.50 o
12 2 1 5231.49 5199.64 200.69 o
14 2 1 3079.46 3264.13 235.03 o
16 2 1 6451.92 7028.95 351.79 o
1 3 1 11482.10 11879.31 143.69 o
3 3 1 305249.09 304721.12 1416.58 o
5 3 1 12067.02 12038.04 152.14 o
7 3 1 33254.08 32498.70 320.15 o
9 3 1 73630.48 72606.08 596.54 o
11 3 1 30950.37 30448.94 479.92 o
13 3 1 10966.75 10807.21 367.73 o
15 3 1 5866.10 6403.86 342.47 o
0 4 1 314.60 385.92 52.07 o
2 4 1 11.21 74.43 34.12 o
4 4 1 199.51 397.28 61.19 o
6 4 1 18.92 78.51 33.77 o
8 4 1 232.79 222.37 61.09 o
10 4 1 24.62 28.26 45.36 o
12 4 1 94.36 148.08 65.90 o
14 4 1 91.89 49.46 104.53 o
1 5 1 3636.24 3589.85 97.49 o
3 5 1 237300.28 234324.78 1129.65 o
5 5 1 29082.71 28730.40 425.01 o
7 5 1 768.85 768.57 87.80 o
9 5 1 83630.85 83151.60 796.27 o
11 5 1 32121.78 32506.95 531.14 o
13 5 1 853.22 961.55 115.15 o
0 6 1 1159.98 1158.48 93.79 o
2 6 1 19002.48 19157.23 281.86 o
4 6 1 45366.26 45327.52 517.26 o
6 6 1 197.54 324.11 64.43 o
8 6 1 293.98 272.67 64.21 o
10 6 1 21730.61 21407.26 410.05 o
12 6 1 4698.08 4352.64 246.67 o
1 7 1 1375.52 1273.41 114.59 o
3 7 1 4103.86 4092.89 187.80 o
5 7 1 259.22 368.13 87.71 o
7 7 1 1482.33 1630.12 130.63 o
9 7 1 8095.60 8240.19 326.58 o
11 7 1 1068.38 1267.14 106.22 o
0 8 1 41136.63 41507.18 997.65 o
2 8 1 17559.08 16840.76 405.69 o
4 8 1 9565.11 9225.50 329.65 o
6 8 1 25511.44 24734.88 463.19 o
8 8 1 17368.40 16894.94 371.23 o
1 9 1 1771.97 1859.69 183.67 o
3 9 1 1780.48 1508.94 158.23 o
5 9 1 1470.83 1157.09 127.36 o
7 9 1 1934.84 2066.78 159.17 o
0 0 2 146944.31 153375.33 1872.97 o
2 0 2 957.14 1120.98 98.97 o
4 0 2 298167.41 302506.69 1740.12 o
6 0 2 150320.86 148161.77 1025.42 o
8 0 2 27275.81 28123.18 416.55 o
10 0 2 163484.44 166890.91 1308.61 o
12 0 2 36155.77 36835.20 632.79 o
14 0 2 3774.41 3773.65 273.24 o
16 0 2 8010.64 8818.49 560.75 o
1 1 2 286.50 374.29 31.01 o
3 1 2 332306.84 333592.09 1563.54 o
5 1 2 793.52 688.05 54.26 o
7 1 2 23284.39 23273.63 264.67 o
9 1 2 3893.80 4191.91 144.43 o
11 1 2 51940.62 52549.16 569.35 o
13 1 2 802.33 979.74 134.49 o
15 1 2 284.52 492.17 162.75 o
0 2 2 46215.14 47389.88 428.76 o
2 2 2 292505.22 293569.03 1120.69 o
4 2 2 62178.56 62495.85 365.38 o
6 2 2 311.20 593.83 85.85 o
8 2 2 61811.87 61839.58 461.18 o
10 2 2 23010.54 23145.78 320.13 o
12 2 2 8648.88 8743.84 274.05 o
14 2 2 64.91 98.13 98.01 o
1 3 2 8606.67 8733.62 120.51 o
3 3 2 2099.66 2471.87 96.00 o
5 3 2 21624.53 21683.71 225.42 o
7 3 2 82207.02 82431.05 510.23 o
9 3 2 8857.08 8803.50 209.04 o
11 3 2 138.58 139.17 56.62 o
13 3 2 5355.87 5256.62 270.43 o
15 3 2 30.50 213.34 136.54 o
0 4 2 8510.67 8880.04 204.72 o
2 4 2 58032.69 58607.82 373.72 o
4 4 2 6170.06 6142.56 145.14 o
6 4 2 17539.91 17246.64 267.53 o
8 4 2 862.46 851.47 92.54 o
10 4 2 268.70 360.87 70.23 o
12 4 2 52385.86 52687.50 734.24 o
14 4 2 7408.07 7527.08 377.49 o
1 5 2 44275.00 44428.00 356.55 o
3 5 2 5126.38 5212.63 123.19 o
5 5 2 1001.25 1244.90 134.59 o
7 5 2 126750.82 125793.37 958.10 o
9 5 2 953.00 858.94 94.92 o
11 5 2 375.74 367.79 74.03 o
13 5 2 17906.99 17786.51 452.92 o
0 6 2 53072.09 52564.16 649.94 o
2 6 2 71082.98 71326.10 636.12 o
4 6 2 21107.56 20714.34 342.45 o
6 6 2 4297.71 3918.99 189.51 o
8 6 2 9849.74 10331.12 302.76 o
10 6 2 9859.35 9370.21 334.64 o
12 6 2 1707.45 1545.91 131.94 o
1 7 2 51.79 193.56 53.60 o
3 7 2 49867.08 50115.24 570.18 o
5 7 2 545.65 585.59 80.81 o
7 7 2 5407.03 5282.66 241.04 o
9 7 2 791.29 703.29 88.43 o
11 7 2 10545.11 10134.88 360.33 o
0 8 2 26469.35 26222.13 787.68 o
2 8 2 1985.74 1957.45 149.23 o
4 8 2 27109.59 26028.08 458.52 o
6 8 2 36263.98 35070.21 554.22 o
8 8 2 8392.76 8162.67 314.53 o
1 9 2 167.88 249.66 85.79 o
3 9 2 27112.49 27582.81 608.07 o
5 9 2 213.40 226.18 71.98 o
1 1 3 131.87 185.13 25.62 o
3 1 3 4200.22 4192.05 79.09 o
5 1 3 6039.66 6220.15 110.49 o
7 1 3 153.48 224.57 36.81 o
9 1 3 10868.04 10848.80 200.47 o
11 1 3 5586.18 5287.52 196.51 o
13 1 3 2256.90 1958.61 145.03 o
15 1 3 9644.46 9577.54 388.33 o
0 2 3 251250.02 255118.75 1392.85 o
2 2 3 11248.93 11087.47 133.46 o
4 2 3 5180.26 5073.01 99.37 o
6 2 3 92105.98 91988.37 535.19 o
8 2 3 49411.98 49088.34 405.95 o
10 2 3 3424.30 3411.97 140.70 o
12 2 3 4954.50 5030.44 240.28 o
14 2 3 28193.20 28647.43 564.11 o
1 3 3 277700.41 276302.88 1165.79 o
3 3 3 13660.21 13870.87 163.23 o
5 3 3 65131.95 64766.45 415.43 o
7 3 3 239900.30 240212.19 1290.60 o
9 3 3 0.47 45.60 51.05 o
11 3 3 2115.42 2199.56 167.07 o
13 3 3 74919.64 75379.26 906.59 o
15 3 3 3691.08 3256.83 279.57 o
0 4 3 814.44 865.52 82.96 o
2 4 3 2277.90 2404.34 119.20 o
4 4 3 2902.29 2808.41 96.13 o
6 4 3 1103.52 1156.26 86.51 o
8 4 3 299.00 391.53 81.02 o
10 4 3 815.77 737.05 94.53 o
12 4 3 1079.02 869.41 112.15 o
14 4 3 75.88 133.65 68.48 o
1 5 3 193248.31 193303.48 919.70 o
3 5 3 21.58 170.16 58.30 o
5 5 3 74132.75 73065.02 658.32 o
7 5 3 163382.22 163413.98 1133.47 o
9 5 3 2330.63 2309.42 160.83 o
11 5 3 9387.82 9058.05 361.18 o
13 5 3 62197.54 63582.24 861.08 o
0 6 3 124864.17 126750.89 1132.26 o
2 6 3 35995.91 35363.54 378.95 o
4 6 3 8523.23 8579.32 229.23 o
6 6 3 66195.95 65839.00 708.37 o
8 6 3 49063.34 48862.24 606.52 o
10 6 3 3180.31 3084.26 193.33 o
12 6 3 10562.81 10578.53 411.95 o
1 7 3 14937.05 14536.07 303.20 o
3 7 3 8864.87 8593.09 253.11 o
5 7 3 23585.66 23195.39 399.07 o
7 7 3 8611.10 8486.68 297.38 o
9 7 3 443.85 310.16 69.93 o
11 7 3 15758.52 15350.23 480.11 o
0 8 3 14253.82 13896.14 569.88 o
2 8 3 30423.86 31404.23 564.03 o
4 8 3 38929.83 38503.49 566.72 o
6 8 3 12337.33 12352.27 322.25 o
8 8 3 11545.09 11135.61 358.38 o
1 9 3 1923.30 1685.38 166.30 o
3 9 3 15762.76 16273.11 459.75 o
5 9 3 1431.65 1443.50 122.32 o
0 0 4 235566.38 233490.09 2088.72 o
2 0 4 451020.75 447054.41 2445.41 o
4 0 4 311840.31 314399.41 2757.39 o
6 0 4 10511.07 10027.79 251.63 o
8 0 4 30078.96 29514.84 391.36 o
10 0 4 123518.38 123897.42 1212.62 o
12 0 4 19056.91 18886.26 485.73 o
14 0 4 7807.60 8059.56 456.81 o
1 1 4 67289.23 68196.13 405.19 o
3 1 4 124158.59 122131.34 578.93 o
5 1 4 230391.23 229730.84 1049.46 o
7 1 4 4949.44 4946.49 133.87 o
9 1 4 106310.61 106685.84 752.71 o
11 1 4 42518.13 42468.66 480.48 o
13 1 4 2515.56 2378.72 161.07 o
15 1 4 10452.73 10129.24 388.55 o
0 2 4 145230.81 146491.67 1317.25 o
2 2 4 77504.37 77643.86 434.53 o
4 2 4 311063.00 309542.22 1227.30 o
6 2 4 13695.82 13287.88 180.36 o
8 2 4 45091.23 45308.23 409.28 o
10 2 4 166061.25 166345.89 1091.26 o
12 2 4 640.63 608.04 85.69 o
14 2 4 31887.72 32341.55 649.75 o
1 3 4 298.94 461.64 42.57 o
3 3 4 149949.61 149400.62 723.04 o
5 3 4 118.26 125.72 37.98 o
7 3 4 20361.66 20338.86 242.50 o
9 3 4 1345.60 1292.40 103.93 o
11 3 4 30136.69 30835.13 530.16 o
13 3 4 1147.90 1233.96 134.22 o
15 3 4 95.27 285.84 116.72 o
0 4 4 87924.31 87160.98 747.33 o
2 4 4 504.25 562.95 49.41 o
4 4 4 73697.45 74179.68 476.44 o
6 4 4 22624.15 22255.96 295.16 o
8 4 4 1729.88 1614.39 117.02 o
10 4 4 31906.83 32098.90 536.44 o
12 4 4 7716.19 7426.49 328.46 o
14 4 4 2434.78 2330.88 202.11 o
1 5 4 95672.56 95929.20 593.00 o
3 5 4 6417.77 6656.61 161.69 o
5 5 4 60172.69 59884.75 553.45 o
7 5 4 23978.32 24118.60 385.31 o
9 5 4 19754.35 19950.28 393.62 o
11 5 4 139.97 157.76 70.50 o
13 5 4 16086.17 16532.46 497.29 o
0 6 4 302.54 348.41 79.44 o
2 6 4 30.38 118.15 40.24 o
4 6 4 47361.11 46323.21 533.07 o
6 6 4 11194.82 11124.43 276.55 o
8 6 4 223.70 287.24 63.23 o
10 6 4 36817.52 36105.15 607.08 o
12 6 4 11110.24 11074.32 374.90 o
1 7 4 7266.13 7772.98 251.27 o
3 7 4 12936.54 12505.35 300.54 o
5 7 4 36012.19 35426.33 500.37 o
7 7 4 3510.77 3365.75 184.82 o
9 7 4 25682.10 25107.71 552.56 o
0 8 4 77194.96 77303.15 1409.35 o
2 8 4 23213.29 23517.17 485.69 o
4 8 4 13827.16 14362.53 348.03 o
6 8 4 17843.26 17785.49 388.13 o
8 8 4 65.57 96.66 88.57 o
1 9 4 2832.82 2775.06 216.12 o
3 9 4 4856.18 4938.53 300.48 o
5 9 4 18811.88 19568.24 440.29 o
1 1 5 2529.14 2738.28 79.52 o
3 1 5 10473.06 10787.73 163.28 o
5 1 5 690.38 693.10 52.62 o
7 1 5 1560.64 1739.84 76.96 o
9 1 5 17045.81 16807.49 274.92 o
11 1 5 1776.18 1722.51 119.17 o
13 1 5 504.25 461.33 76.52 o
15 1 5 11745.05 12012.71 423.65 o
0 2 5 93659.95 94408.51 773.26 o
2 2 5 771.40 860.95 66.64 o
4 2 5 32466.02 31737.77 271.74 o
6 2 5 30723.61 30869.63 286.41 o
8 2 5 14715.76 14886.32 235.98 o
10 2 5 15593.45 15222.28 293.46 o
12 2 5 132.24 180.48 64.81 o
14 2 5 12348.59 12003.92 454.68 o
1 3 5 59457.02 59073.50 408.20 o
3 3 5 106865.33 105771.75 592.05 o
5 3 5 1562.83 1631.92 81.01 o
7 3 5 74245.15 73197.56 537.14 o
9 3 5 20348.44 20595.45 376.05 o
11 3 5 6171.75 6146.58 283.62 o
13 3 5 25424.69 24621.17 576.67 o
0 4 5 1185.05 1340.21 109.47 o
2 4 5 1521.33 1625.95 90.15 o
4 4 5 2963.66 3023.97 144.41 o
6 4 5 1080.54 1143.11 88.89 o
8 4 5 265.63 281.69 57.32 o
10 4 5 1020.13 893.28 107.63 o
12 4 5 824.78 724.50 117.68 o
14 4 5 112.27 293.39 156.61 o
1 5 5 23135.61 22986.55 272.67 o
3 5 5 52417.30 52649.95 455.08 o
5 5 5 703.74 776.11 90.93 o
7 5 5 35017.02 34026.54 489.07 o
9 5 5 15557.09 15713.16 370.95 o
11 5 5 2197.25 2427.51 222.28 o
13 5 5 14724.04 15844.81 478.72 o
0 6 5 27167.40 26986.49 488.19 o
2 6 5 10.08 105.02 41.61 o
4 6 5 4431.37 4268.27 193.07 o
6 6 5 9536.17 9721.42 270.35 o
8 6 5 6451.40 6108.83 266.28 o
10 6 5 2444.28 2327.83 167.49 o
12 6 5 22.42 -88.15 105.87 o
1 7 5 651.49 596.54 77.02 o
3 7 5 45.44 81.34 49.90 o
5 7 5 4816.79 4633.15 217.70 o
7 7 5 77.41 291.13 62.52 o
9 7 5 1524.70 1407.44 126.09 o
0 8 5 3359.75 3800.73 364.43 o
2 8 5 101.58 125.19 71.77 o
4 8 5 901.81 939.43 90.17 o
6 8 5 1181.92 1454.54 174.72 o
8 8 5 411.80 500.89 81.04 o
1 9 5 170.61 82.01 78.69 o
3 9 5 7097.72 7260.28 372.84 o
5 9 5 187.92 175.35 72.94 o
0 0 6 587952.44 573626.00 4772.65 o
2 0 6 233958.23 231552.61 1702.77 o
4 0 6 32.69 104.08 58.54 o
6 0 6 478700.03 465528.50 3651.87 o
8 0 6 208727.05 207837.03 1798.99 o
10 0 6 6411.74 6801.20 337.03 o
12 0 6 144055.69 147372.00 1725.99 o
14 0 6 51337.80 51112.68 1027.36 o
1 1 6 26089.03 25784.50 232.58 o
3 1 6 77796.59 77167.30 542.65 o
5 1 6 16229.41 15749.00 192.21 o
7 1 6 150.24 347.07 67.39 o
9 1 6 3091.41 3165.55 163.64 o
11 1 6 11810.27 11477.61 284.33 o
13 1 6 2152.72 2287.70 282.05 o
15 1 6 4937.45 4541.15 279.66 o
0 2 6 203171.33 202935.45 1289.67 o
2 2 6 20547.43 20575.21 218.12 o
4 2 6 3011.41 3049.05 92.69 o
6 2 6 47000.54 46075.93 393.08 o
8 2 6 168.02 153.90 40.44 o
10 2 6 1140.74 1253.59 114.99 o
12 2 6 2742.39 3062.98 218.57 o
14 2 6 11423.26 11822.28 470.09 o
1 3 6 118912.72 118767.24 655.79 o
3 3 6 85907.30 85734.94 551.37 o
5 3 6 13134.44 12809.30 189.48 o
7 3 6 197821.62 197488.75 1039.93 o
9 3 6 8861.44 8640.40 298.77 o
11 3 6 17961.70 18002.92 442.16 o
13 3 6 33087.86 33790.17 696.04 o
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