#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180858 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018995.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018995_Fobs loop_ _publ_author_name 'Baldo, Bianca' 'Cruz, Carlos' 'Venegas-Yazigi, Diego' 'Vega, Andres' 'Paredes-Garc\'ia, Ver\'onica' _publ_section_title ; catena-Poly[tris(\m~3~-acetylacetonato)nickelate(II)sodium(I)] ; _journal_coeditor_code SK3482 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 506 _journal_page_last 508 _journal_volume 69 _journal_year 2013 _space_group_IT_number 167 _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 16.1327 _cell_length_b 16.1327 _cell_length_c 11.6842 _exptl_crystal_F_000 1359.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file sk3482Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R-3c in R-3c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 346.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z+1/2' 'x-y, -y, -z+1/2' '-x, -x+y, -z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+5/6' 'x-y+2/3, -y+1/3, -z+5/6' '-x+2/3, -x+y+1/3, -z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+7/6' 'x-y+1/3, -y+2/3, -z+7/6' '-x+1/3, -x+y+2/3, -z+7/6' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z-1/2' '-x+y, y, z-1/2' 'x, x-y, z-1/2' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z-1/6' '-x+y+2/3, y+1/3, z-1/6' 'x+2/3, x-y+1/3, z-1/6' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+1/6' '-x+y+1/3, y+2/3, z+1/6' 'x+1/3, x-y+2/3, z+1/6' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 120117.80 128084.85 269.03 o 0 3 0 14176.62 14842.75 245.52 o -2 4 0 15329.62 15990.16 56.05 o -1 5 0 37748.34 39502.43 229.39 o -3 6 0 9086.59 8300.11 93.05 o 0 6 0 13500.73 12655.83 225.59 o -2 7 0 10877.97 10186.07 76.01 o -4 8 0 12064.40 11089.71 122.33 o -1 8 0 7860.41 7271.35 55.39 o -3 9 0 35446.73 36773.30 143.49 o 0 9 0 1788.22 1685.32 29.43 o -5 10 0 43067.84 44808.01 260.88 o -2 10 0 16411.18 16380.74 126.38 o -4 11 0 34088.29 36868.30 236.48 o -1 11 0 6670.96 6387.60 58.72 o -6 12 0 24984.19 25077.14 301.79 o -3 12 0 13935.69 14652.74 104.99 o 0 12 0 3367.07 3307.97 62.47 o -5 13 0 20040.13 20355.93 133.30 o -2 13 0 2758.85 2752.90 51.72 o -7 14 0 8112.86 7959.94 104.95 o -4 14 0 10037.52 10472.67 80.02 o -1 14 0 1286.34 1212.22 39.67 o -6 15 0 4285.71 4408.71 52.78 o -3 15 0 1979.37 1844.36 49.90 o 0 15 0 7727.88 7877.39 171.20 o -8 16 0 1817.15 1761.62 55.40 o -5 16 0 1248.05 1237.22 47.40 o -2 16 0 4281.84 4298.10 94.36 o -7 17 0 910.92 976.75 39.28 o -4 17 0 2043.63 2178.63 59.41 o -1 17 0 4328.47 4291.40 92.66 o -9 18 0 8763.02 9478.78 118.89 o -6 18 0 106.09 133.44 22.31 o -3 18 0 3377.58 3560.01 90.17 o -8 19 0 1451.60 1508.62 51.35 o -5 19 0 2697.13 2926.32 94.81 o -2 3 1 21909.33 23055.09 63.44 o -1 4 1 41521.04 44507.56 322.81 o -3 5 1 1929.44 1847.52 17.07 o -5 6 1 6049.95 6178.68 27.91 o -2 6 1 4928.12 4794.34 39.53 o -4 7 1 2032.94 2170.32 29.53 o -1 7 1 91.32 66.32 6.19 o -6 8 1 385.99 403.56 11.14 o -3 8 1 7.60 22.96 6.51 o -8 9 1 56.04 86.91 8.06 o -5 9 1 230.79 281.82 9.71 o -2 9 1 326.90 361.96 11.84 o -7 10 1 313.48 229.76 11.62 o -4 10 1 893.35 943.07 16.48 o -1 10 1 0.41 6.20 6.86 o -9 11 1 1462.43 1424.93 24.80 o -6 11 1 254.08 207.07 11.81 o -3 11 1 5.31 -1.22 7.57 o -11 12 1 8.99 6.45 12.01 o -8 12 1 33.11 43.59 10.11 o -5 12 1 233.59 205.96 13.32 o -2 12 1 104.99 132.19 14.78 o -10 13 1 1677.47 1647.20 35.49 o -7 13 1 522.71 463.49 23.11 o -4 13 1 25.83 22.69 10.31 o -1 13 1 22.15 12.27 11.59 o -12 14 1 108.45 115.24 18.22 o -9 14 1 5.39 -10.72 10.70 o -6 14 1 614.90 597.27 21.62 o -3 14 1 298.99 305.43 18.11 o -14 15 1 91.17 98.68 19.32 o -11 15 1 350.22 360.63 24.06 o -8 15 1 413.49 389.62 20.65 o -5 15 1 1771.88 1767.55 39.00 o -2 15 1 1112.26 1125.29 43.38 o -13 16 1 20.44 19.68 17.41 o -10 16 1 295.98 279.46 24.44 o -7 16 1 1.26 8.71 12.11 o -4 16 1 408.34 400.59 26.70 o -1 16 1 96.03 87.59 23.10 o -15 17 1 3.89 -8.12 19.03 o -12 17 1 541.11 496.26 31.61 o -9 17 1 46.45 60.20 16.16 o -6 17 1 766.34 728.28 30.93 o -3 17 1 1775.03 1804.21 60.73 o -14 18 1 4.09 8.54 18.68 o -11 18 1 529.61 523.96 31.17 o -8 18 1 80.00 113.36 18.92 o -5 18 1 88.48 92.59 20.61 o -2 18 1 12.88 57.44 32.72 o -13 19 1 534.45 618.27 37.95 o -10 19 1 172.42 123.31 30.42 o -7 19 1 2.86 -3.68 18.36 o 0 1 2 36825.43 37491.70 617.51 o -2 2 2 345.51 296.32 9.53 o -1 3 2 45279.46 47869.86 347.77 o -3 4 2 6666.25 7084.75 36.42 o 0 4 2 67807.78 72674.97 932.22 o -5 5 2 53.04 24.15 7.22 o -2 5 2 1130.20 1001.52 11.99 o -4 6 2 400.47 248.63 9.13 o -1 6 2 49363.10 54956.19 426.47 o -6 7 2 2447.59 2517.43 21.27 o -3 7 2 8087.69 7493.93 63.78 o 0 7 2 36849.57 38670.33 600.58 o -8 8 2 53.83 179.33 13.31 o -5 8 2 4362.74 4538.75 31.49 o -2 8 2 3668.31 3529.22 49.24 o -7 9 2 54.99 100.32 10.37 o -4 9 2 7871.11 7516.42 54.59 o -1 9 2 7317.41 6860.50 79.76 o -9 10 2 6997.74 7049.02 64.85 o -6 10 2 13201.10 14341.38 75.32 o -3 10 2 328.55 289.53 12.58 o 0 10 2 1657.27 1617.51 48.91 o -11 11 2 9432.05 9816.31 103.74 o -8 11 2 4852.46 4949.18 44.16 o -5 11 2 6318.26 6229.39 45.46 o -2 11 2 2574.98 2675.69 35.10 o -10 12 2 6578.94 6801.64 62.74 o -7 12 2 7368.47 7469.72 58.02 o -4 12 2 2648.84 2574.85 32.20 o -1 12 2 2500.61 2406.59 45.17 o -12 13 2 6291.94 6335.19 70.18 o -9 13 2 4735.08 4568.50 60.32 o -6 13 2 1242.26 1185.68 38.66 o -3 13 2 1275.32 1251.85 41.08 o 0 13 2 311.06 303.59 31.67 o -14 14 2 3104.76 2941.51 99.31 o -11 14 2 3573.56 3461.50 54.69 o -8 14 2 430.25 453.25 21.82 o -5 14 2 4842.16 4896.19 74.43 o -2 14 2 125.14 148.96 16.79 o -13 15 2 896.54 943.00 36.69 o -10 15 2 151.66 170.58 19.44 o -7 15 2 3079.83 3157.09 46.86 o -4 15 2 2560.34 2492.29 48.91 o -1 15 2 3435.26 3621.05 75.84 o -15 16 2 552.89 537.42 36.47 o -12 16 2 127.50 86.73 17.92 o -9 16 2 149.70 145.31 18.87 o -6 16 2 5311.12 5140.56 71.69 o -3 16 2 2551.17 2590.43 82.77 o 0 16 2 563.21 581.64 59.12 o -17 17 2 1210.59 1242.14 76.99 o -14 17 2 70.73 64.87 20.13 o -11 17 2 56.27 101.45 20.06 o -8 17 2 1358.80 1441.25 54.43 o -5 17 2 1258.12 1216.23 39.16 o -2 17 2 1361.04 1394.79 95.28 o -13 18 2 116.50 115.88 21.83 o -10 18 2 295.38 334.00 27.01 o -7 18 2 1045.89 1056.86 43.13 o -4 18 2 2702.47 2947.30 169.85 o -12 19 2 202.04 263.91 26.12 o -9 19 2 1757.05 1830.58 55.98 o -6 19 2 633.21 717.86 42.79 o -1 2 3 688.75 587.11 9.47 o -2 4 3 66.49 62.25 5.47 o -4 5 3 631.22 715.33 12.28 o -1 5 3 517.53 545.43 16.17 o -3 6 3 3878.82 4338.77 42.55 o -5 7 3 2648.63 2873.86 29.43 o -2 7 3 7780.13 8201.14 83.62 o -7 8 3 36.95 29.40 6.76 o -4 8 3 3958.21 4190.50 37.30 o -1 8 3 6821.57 6467.14 45.37 o -6 9 3 206.20 170.77 10.31 o -3 9 3 629.77 612.13 15.54 o -8 10 3 69.85 67.54 11.96 o -5 10 3 787.91 753.18 18.05 o -2 10 3 385.99 294.80 12.96 o -10 11 3 81.62 61.30 14.16 o -7 11 3 69.70 80.73 11.14 o -4 11 3 1897.24 1968.82 30.86 o -1 11 3 1011.00 972.58 21.86 o -9 12 3 530.27 625.23 24.48 o -6 12 3 110.92 150.08 12.70 o -3 12 3 46.24 62.61 10.31 o -11 13 3 6.15 -16.67 12.24 o -8 13 3 371.56 364.19 20.64 o -5 13 3 42.57 29.47 10.29 o -2 13 3 4258.27 4358.54 57.76 o -13 14 3 13.69 -5.36 13.60 o -10 14 3 4.55 7.26 14.71 o -7 14 3 374.68 339.24 21.45 o -4 14 3 826.97 835.71 26.08 o -1 14 3 111.78 139.94 17.35 o -12 15 3 17.07 24.72 15.71 o -9 15 3 94.05 98.75 17.38 o -6 15 3 5.78 5.75 11.44 o -3 15 3 20.85 36.41 14.14 o -14 16 3 1013.40 971.20 39.89 o -11 16 3 52.89 58.54 16.39 o -8 16 3 13.99 15.89 15.69 o -5 16 3 147.49 168.51 18.78 o -2 16 3 903.26 859.35 37.69 o -16 17 3 1110.77 1130.99 52.00 o -13 17 3 68.56 60.97 19.60 o -10 17 3 143.10 128.44 20.09 o -7 17 3 252.84 224.24 22.64 o -4 17 3 1.54 -6.63 15.53 o -1 17 3 10.09 -4.16 19.26 o -15 18 3 269.47 235.18 27.80 o -12 18 3 101.23 53.75 19.03 o -9 18 3 83.42 75.42 19.07 o -6 18 3 106.29 120.14 25.13 o -3 18 3 16.70 -10.02 21.30 o -11 19 3 30.22 -2.19 20.51 o -8 19 3 15.69 19.50 21.07 o -1 1 4 1077.69 803.20 16.64 o 0 2 4 41.34 109.46 8.22 o -2 3 4 19294.04 18219.36 75.41 o -4 4 4 26519.91 27800.43 182.96 o -1 4 4 69223.92 74145.48 538.57 o -3 5 4 27755.28 28216.00 217.71 o 0 5 4 112005.96 120004.64 1345.90 o -5 6 4 22386.30 22429.37 97.65 o -2 6 4 57727.26 61984.18 569.19 o -7 7 4 22588.75 24268.02 143.35 o -4 7 4 18481.89 18807.33 141.72 o -1 7 4 24052.87 23302.88 174.48 o -6 8 4 17495.74 17656.65 146.77 o -3 8 4 15475.46 15710.03 99.30 o 0 8 4 47650.73 51443.45 910.57 o -8 9 4 10351.06 10066.49 82.94 o -5 9 4 15115.49 15149.93 111.53 o -2 9 4 15695.60 15303.52 122.49 o -10 10 4 18719.53 19194.63 160.09 o -7 10 4 8369.33 8005.70 65.27 o -4 10 4 5753.61 5479.38 76.89 o -1 10 4 26058.88 27470.63 308.41 o -9 11 4 14697.76 14725.13 91.17 o -6 11 4 1513.11 1594.56 29.82 o -3 11 4 352.39 266.22 14.68 o 0 11 4 10427.37 9952.60 132.42 o -11 12 4 19904.26 20732.23 190.13 o -8 12 4 1273.31 1231.34 31.10 o -5 12 4 1334.62 1301.40 31.28 o -2 12 4 1074.16 1037.27 26.50 o -13 13 4 13376.32 14178.38 297.42 o -10 13 4 5360.28 5270.51 60.25 o -7 13 4 838.19 769.41 26.95 o -4 13 4 3645.81 3711.80 63.50 o -1 13 4 4798.96 4619.77 75.23 o -12 14 4 5409.58 5140.31 62.63 o -9 14 4 3802.51 3907.20 66.31 o -6 14 4 6573.21 6646.75 99.85 o -3 14 4 7757.60 7998.20 96.55 o 0 14 4 5143.98 5243.77 94.07 o -14 15 4 3703.36 3823.50 66.32 o -11 15 4 5132.16 5069.56 62.89 o -8 15 4 4891.99 4991.49 67.36 o -5 15 4 11873.48 12043.24 147.17 o -2 15 4 4016.22 4111.31 81.78 o -16 16 4 770.39 862.04 64.93 o -13 16 4 1999.79 2032.77 59.57 o -10 16 4 6352.33 6552.44 83.25 o -7 16 4 3636.88 3460.54 76.86 o -4 16 4 5573.54 5476.17 109.42 o -1 16 4 1916.38 1998.98 70.67 o -15 17 4 57.41 52.57 20.92 o -12 17 4 3917.10 4093.83 68.44 o -9 17 4 1910.84 1886.61 49.45 o -6 17 4 6332.71 6399.42 114.97 o -3 17 4 1452.05 1412.42 54.97 o -14 18 4 1676.57 1862.72 72.83 o -11 18 4 1291.33 1270.60 45.20 o -8 18 4 3121.34 3265.32 84.57 o -5 18 4 3245.01 3254.80 112.95 o -10 19 4 2118.42 2079.62 62.44 o -1 3 5 680.48 714.03 15.82 o -3 4 5 556.29 446.62 10.77 o -2 5 5 7137.07 7920.50 50.88 o -4 6 5 2627.78 2636.96 28.46 o -1 6 5 302.72 267.86 9.75 o -6 7 5 11.13 9.55 8.42 o -3 7 5 653.70 526.79 15.13 o -5 8 5 919.37 891.92 20.70 o -2 8 5 834.95 813.08 21.15 o -7 9 5 520.59 480.16 20.65 o -4 9 5 182.77 189.51 12.52 o -1 9 5 229.55 236.87 15.41 o -9 10 5 136.24 164.42 16.85 o -6 10 5 981.80 1055.20 27.51 o -3 10 5 733.19 699.46 23.44 o -8 11 5 2.75 9.74 12.15 o -5 11 5 2293.87 2159.91 35.00 o -2 11 5 48.67 35.52 11.53 o -10 12 5 137.63 139.14 16.69 o -7 12 5 136.81 98.98 15.19 o -4 12 5 6.94 0.57 10.09 o -1 12 5 869.92 810.61 28.18 o -12 13 5 1500.56 1453.90 38.43 o -9 13 5 11.09 10.86 12.77 o -6 13 5 2223.87 2111.60 44.22 o -3 13 5 1.13 -3.69 11.36 o -11 14 5 84.49 63.44 15.79 o -8 14 5 525.87 478.88 24.62 o -5 14 5 0.02 11.41 12.30 o -2 14 5 1924.31 1845.96 49.47 o -13 15 5 1188.17 1073.92 37.65 o -10 15 5 105.57 136.64 18.00 o -7 15 5 127.95 104.89 17.14 o -4 15 5 355.71 318.58 25.50 o -1 15 5 574.14 558.96 34.08 o -15 16 5 233.19 207.03 25.31 o -12 16 5 430.04 400.26 29.99 o -9 16 5 388.91 374.97 26.81 o -6 16 5 86.20 77.87 20.70 o -3 16 5 0.06 -10.68 22.10 o -14 17 5 7.36 13.91 19.42 o -11 17 5 9.71 -2.01 16.73 o -8 17 5 426.14 421.63 41.50 o -5 17 5 16.12 19.62 20.08 o -2 17 5 56.78 40.98 25.02 o -13 18 5 17.01 39.03 19.46 o -10 18 5 73.38 65.51 20.40 o -7 18 5 52.05 24.35 23.42 o 0 0 6 97.10 120.25 20.69 o -1 2 6 556.53 541.16 12.75 o -3 3 6 7653.02 7680.59 53.15 o 0 3 6 4575.65 4315.52 43.60 o -2 4 6 9131.93 9421.67 46.22 o -4 5 6 39410.66 41833.12 167.18 o -1 5 6 509.22 422.28 11.82 o -6 6 6 12805.68 12326.74 104.87 o -3 6 6 4995.50 4419.39 42.15 o 0 6 6 189.85 205.81 17.46 o -5 7 6 8502.90 8251.61 75.54 o -2 7 6 535.60 500.71 16.28 o -7 8 6 10059.40 9636.36 87.56 o -4 8 6 3025.97 2821.98 33.91 o -1 8 6 1943.13 1791.97 37.78 o -9 9 6 16262.20 17703.79 146.04 o -6 9 6 4335.06 4315.30 51.92 o -3 9 6 2640.67 2741.17 33.45 o 0 9 6 2680.03 2731.01 62.54 o -8 10 6 1362.95 1324.89 32.63 o -5 10 6 1592.36 1439.66 29.59 o -2 10 6 2447.29 2459.79 39.36 o -10 11 6 1358.26 1377.22 35.27 o -7 11 6 32.55 24.60 13.29 o -4 11 6 61.85 87.47 13.62 o -1 11 6 10378.14 10524.93 161.64 o -12 12 6 923.36 950.49 47.13 o -9 12 6 1133.95 1065.97 32.27 o -6 12 6 29.01 35.66 12.57 o -3 12 6 1016.82 995.71 41.66 o 0 12 6 11784.96 11717.26 211.84 o -11 13 6 87.36 80.52 16.74 o -8 13 6 1168.07 1155.26 33.51 o -5 13 6 111.00 110.82 16.02 o -2 13 6 2878.82 2760.72 46.60 o -13 14 6 854.84 930.32 35.60 o -10 14 6 4020.20 4066.57 73.49 o -7 14 6 1035.33 1066.31 52.89 o -4 14 6 1323.28 1237.63 40.00 o -1 14 6 3140.07 3152.25 60.67 o -15 15 6 1401.02 1409.67 62.35 o -12 15 6 2218.86 2179.98 48.08 o -9 15 6 3138.22 3097.95 64.85 o -6 15 6 2252.10 2250.09 49.50 o -3 15 6 549.97 629.27 35.15 o 0 15 6 1812.03 1659.26 82.95 o -14 16 6 595.91 551.33 31.09 o -11 16 6 4978.34 4912.93 71.07 o -8 16 6 393.02 422.00 28.87 o -5 16 6 1624.73 1550.84 61.44 o -2 16 6 138.35 203.36 29.48 o -13 17 6 1269.16 1272.67 47.30 o -10 17 6 1469.27 1463.34 50.45 o -7 17 6 278.41 297.11 33.56 o -4 17 6 383.08 361.31 35.78 o -9 18 6 604.43 580.15 46.23 o -2 3 7 202.51 200.63 10.01 o -1 4 7 124.90 125.03 9.57 o -3 5 7 413.76 379.93 14.92 o -5 6 7 2025.59 1947.02 37.49 o -2 6 7 266.56 275.31 14.00 o -4 7 7 2.93 8.40 9.56 o -1 7 7 50.30 75.32 12.11 o -6 8 7 5523.54 5667.25 56.49 o -3 8 7 1096.39 898.15 23.27 o -8 9 7 334.63 295.19 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102.32 o -3 4 8 23053.63 23960.05 105.68 o 0 4 8 1969.22 1825.32 37.38 o -5 5 8 29652.84 30945.76 183.56 o -2 5 8 2406.88 2400.91 41.47 o -4 6 8 11625.66 11584.23 82.06 o -1 6 8 3505.99 3352.75 45.85 o -6 7 8 14213.62 13996.42 97.91 o -3 7 8 9018.20 8985.89 87.04 o 0 7 8 674.04 665.54 34.40 o -8 8 8 15478.48 15852.92 143.40 o -5 8 8 8138.64 8132.25 72.62 o -2 8 8 2434.66 2279.03 39.99 o -7 9 8 3944.53 3591.23 49.89 o -4 9 8 17397.07 17692.91 116.22 o -1 9 8 3116.25 3447.98 51.33 o -9 10 8 8176.75 8376.54 90.67 o -6 10 8 8841.58 8951.58 122.98 o -3 10 8 7925.44 7849.14 187.61 o 0 10 8 8435.27 7474.55 113.30 o -11 11 8 19.54 37.16 22.27 o -8 11 8 4883.11 4671.26 61.97 o -5 11 8 16218.33 16131.02 166.17 o -2 11 8 7679.73 7399.67 107.54 o -10 12 8 1355.03 1343.55 43.13 o -7 12 8 6880.09 6607.31 98.31 o -4 12 8 8543.11 8489.99 129.48 o -1 12 8 5250.16 5051.34 67.34 o -12 13 8 15.95 31.12 16.37 o -9 13 8 5271.29 5145.50 113.18 o -6 13 8 4828.81 4788.54 89.47 o -3 13 8 5428.93 5440.87 93.06 o 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