data_2019601 _cell_angle_alpha 116.476 _cell_angle_beta 95.018 _cell_angle_gamma 90.263 _cell_length_a 9.0240 _cell_length_b 17.5656 _cell_length_c 18.9610 _exptl_crystal_F_000 968.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file fg3323IIsup3.hkl _[local]_cod_data_source_block II _shelx_title ' s4 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.53 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 379.86 465.94 32.01 o 2 0 0 6775.32 7221.11 132.19 o 3 0 0 772.16 804.89 16.01 o 4 0 0 35.38 43.93 8.51 o 5 0 0 771.46 733.62 20.34 o 6 0 0 14.59 15.01 11.73 o 7 0 0 221.43 221.70 22.91 o 8 0 0 178.84 178.99 21.09 o 9 0 0 17.43 15.23 17.38 o 10 0 0 138.16 134.09 30.39 o 11 0 0 76.24 59.27 36.72 o -11 1 0 15.61 26.09 25.28 o -10 1 0 280.12 264.70 31.39 o -9 1 0 7.19 10.81 35.58 o -8 1 0 99.57 93.38 19.71 o -7 1 0 156.31 146.56 17.80 o -6 1 0 1.13 7.66 11.96 o -5 1 0 25.36 34.34 11.30 o -4 1 0 2414.70 2394.06 30.23 o -3 1 0 2187.86 2062.26 24.42 o -2 1 0 2933.78 2853.58 23.13 o -1 1 0 4.87 12.44 3.86 o 1 1 0 6847.12 6700.39 217.11 o 2 1 0 3697.54 3517.84 43.16 o 3 1 0 724.54 736.95 15.34 o 4 1 0 65.77 74.53 12.90 o 5 1 0 189.99 183.42 14.05 o 6 1 0 1.88 -2.78 11.26 o 7 1 0 262.42 289.95 20.90 o 8 1 0 50.42 53.31 16.35 o 9 1 0 15.49 66.10 22.19 o 10 1 0 36.93 2.91 20.51 o 11 1 0 93.36 147.14 36.34 o -11 2 0 0.42 -3.26 26.43 o -10 2 0 35.91 27.82 22.70 o -9 2 0 61.30 107.36 23.43 o -8 2 0 4.74 2.61 17.35 o -7 2 0 34.55 10.53 19.22 o -6 2 0 69.71 77.67 15.07 o -5 2 0 793.99 856.80 22.33 o -4 2 0 1222.13 1180.76 21.46 o -3 2 0 897.27 1089.24 28.64 o -2 2 0 90.83 81.88 6.54 o -1 2 0 890.91 904.97 21.52 o 0 2 0 34994.51 37259.30 956.56 o 1 2 0 770.58 706.19 9.29 o 2 2 0 6022.35 5701.16 108.10 o 3 2 0 9.80 10.91 5.27 o 4 2 0 70.93 102.94 7.71 o 5 2 0 153.71 156.35 9.54 o 6 2 0 545.85 521.61 35.45 o 7 2 0 257.68 233.18 20.14 o 8 2 0 64.59 73.27 19.25 o 9 2 0 156.36 175.19 26.05 o 10 2 0 323.92 274.13 38.47 o 11 2 0 44.76 61.22 64.58 o -11 3 0 10.12 34.85 40.65 o -10 3 0 279.24 284.42 29.86 o -9 3 0 281.49 290.59 26.66 o -8 3 0 86.55 75.63 18.20 o -7 3 0 26.27 18.27 19.21 o -6 3 0 0.22 -15.43 20.43 o -5 3 0 743.30 801.02 21.15 o -4 3 0 2336.53 2407.92 38.88 o -3 3 0 124.25 133.77 9.69 o -2 3 0 4094.25 4363.88 62.33 o -1 3 0 667.64 768.85 23.83 o 0 3 0 536.11 600.30 8.96 o 1 3 0 114.57 151.89 3.93 o 2 3 0 480.06 449.05 8.90 o 3 3 0 1795.91 1821.26 20.60 o 4 3 0 638.78 612.79 13.51 o 5 3 0 2.83 15.13 7.93 o 6 3 0 3.99 11.25 11.70 o 7 3 0 19.19 9.97 33.99 o 8 3 0 50.94 47.06 17.42 o 9 3 0 56.74 61.47 29.00 o 10 3 0 16.57 44.80 27.51 o 11 3 0 71.83 54.52 50.85 o -11 4 0 132.55 169.64 33.07 o -10 4 0 190.62 212.51 27.54 o -9 4 0 22.60 19.54 19.76 o -8 4 0 701.46 731.95 29.42 o -7 4 0 395.73 386.35 21.77 o -6 4 0 324.36 309.13 18.65 o -5 4 0 1702.15 1925.61 58.69 o -4 4 0 903.47 914.98 18.47 o -3 4 0 106.94 90.38 6.44 o -2 4 0 12157.02 13469.94 128.52 o -1 4 0 5.56 6.87 5.96 o 0 4 0 7619.52 8241.43 37.35 o 1 4 0 38.52 34.05 3.63 o 2 4 0 100.29 107.33 6.76 o 3 4 0 174.62 165.71 7.70 o 4 4 0 324.51 290.59 10.68 o 5 4 0 2.99 9.22 7.65 o 6 4 0 107.62 105.19 21.06 o 7 4 0 552.20 517.83 24.27 o 8 4 0 314.03 301.68 36.47 o 9 4 0 140.24 160.54 29.51 o 10 4 0 92.82 121.73 33.52 o 11 4 0 124.80 143.96 38.52 o -11 5 0 2.99 -3.94 20.12 o -10 5 0 67.69 70.31 27.28 o -9 5 0 523.96 528.18 30.40 o -8 5 0 109.33 94.36 18.94 o -7 5 0 116.25 109.08 16.82 o -6 5 0 20.95 -7.15 16.13 o -5 5 0 688.69 743.63 24.58 o -4 5 0 427.45 423.90 12.01 o -3 5 0 93.52 96.28 7.35 o -2 5 0 313.87 275.05 7.31 o -1 5 0 6975.91 7535.54 73.44 o 0 5 0 680.90 673.23 23.30 o 1 5 0 12921.93 12806.85 89.69 o 2 5 0 179.26 174.52 5.90 o 3 5 0 647.18 682.68 14.45 o 4 5 0 105.20 108.16 8.98 o 5 5 0 58.70 47.97 9.32 o 6 5 0 0.35 -0.72 11.95 o 7 5 0 90.62 80.46 18.32 o 8 5 0 37.59 20.19 22.34 o 9 5 0 127.79 107.88 27.75 o 10 5 0 12.02 30.22 30.78 o 11 5 0 98.15 72.15 37.89 o -10 6 0 0.21 0.90 22.68 o -9 6 0 23.45 16.38 16.82 o -8 6 0 2.18 4.73 19.57 o -7 6 0 298.55 292.46 21.57 o -6 6 0 1993.73 1980.97 36.66 o -5 6 0 874.34 860.74 27.73 o -4 6 0 785.80 843.47 20.91 o -3 6 0 2861.65 2810.33 31.25 o -2 6 0 9358.98 9726.36 54.60 o -1 6 0 152.58 174.71 9.16 o 0 6 0 414.68 533.19 9.66 o 1 6 0 1431.53 1563.15 22.02 o 2 6 0 6993.12 6836.99 62.87 o 3 6 0 367.34 435.37 14.72 o 4 6 0 169.61 159.91 10.61 o 5 6 0 3.35 16.18 8.43 o 6 6 0 546.49 476.12 21.81 o 7 6 0 387.16 467.52 57.17 o 8 6 0 36.28 47.89 23.04 o 9 6 0 73.35 32.12 23.46 o 10 6 0 17.60 45.68 32.94 o 11 6 0 26.20 48.70 39.15 o -10 7 0 0.15 15.28 33.67 o -9 7 0 67.27 69.68 36.42 o -8 7 0 261.73 242.09 24.18 o -7 7 0 0.78 28.58 29.06 o -6 7 0 79.17 68.40 15.09 o -5 7 0 672.10 647.54 24.94 o -4 7 0 1.11 1.95 7.41 o -3 7 0 6.51 23.23 7.87 o -2 7 0 4033.64 3851.65 43.87 o -1 7 0 4426.21 4606.87 71.05 o 0 7 0 213.83 230.84 9.57 o 1 7 0 3289.37 2931.15 27.17 o 2 7 0 117.46 119.92 7.39 o 3 7 0 810.56 839.20 13.76 o 4 7 0 3.98 3.63 9.51 o 5 7 0 962.82 903.53 20.34 o 6 7 0 85.30 48.34 15.44 o 7 7 0 1279.17 1265.90 71.65 o 8 7 0 144.25 83.35 28.92 o 9 7 0 403.48 421.29 38.82 o 10 7 0 3.94 39.87 30.69 o -10 8 0 0.46 2.86 34.87 o -9 8 0 90.92 109.08 41.36 o -8 8 0 155.90 153.51 33.43 o -7 8 0 1344.98 1343.66 45.15 o -6 8 0 385.44 407.45 30.92 o -5 8 0 802.67 840.25 23.77 o -4 8 0 104.84 72.47 9.44 o -3 8 0 101.35 124.15 9.51 o -2 8 0 66.00 96.52 13.28 o -1 8 0 618.87 601.77 17.81 o 0 8 0 134.74 156.66 8.51 o 1 8 0 20.66 27.00 6.87 o 2 8 0 208.43 155.58 10.43 o 3 8 0 43.21 42.90 7.67 o 4 8 0 1544.33 1559.18 17.84 o 5 8 0 17.57 26.55 12.37 o 6 8 0 785.66 795.87 31.56 o 7 8 0 534.34 544.10 53.85 o 8 8 0 587.05 710.77 43.20 o 9 8 0 31.90 42.88 28.37 o 10 8 0 124.99 155.64 43.70 o -10 9 0 0.00 17.10 43.14 o -9 9 0 36.03 55.56 32.16 o -8 9 0 384.77 418.94 48.83 o -7 9 0 289.99 326.57 36.88 o -6 9 0 115.91 132.24 27.44 o -5 9 0 173.22 77.00 31.55 o -4 9 0 51.99 74.55 14.33 o -3 9 0 1235.34 1345.99 32.84 o -2 9 0 2129.99 2222.80 32.35 o -1 9 0 350.34 320.69 13.97 o 0 9 0 599.63 584.88 15.46 o 1 9 0 3810.19 3858.48 55.98 o 2 9 0 89.98 111.92 10.86 o 3 9 0 20.30 40.51 8.40 o 4 9 0 58.32 58.86 9.45 o 5 9 0 228.23 227.32 16.51 o 6 9 0 10.66 20.74 21.01 o 7 9 0 127.04 108.32 24.80 o 8 9 0 6.60 -2.60 21.98 o 9 9 0 86.70 86.85 36.69 o 10 9 0 34.01 61.06 35.14 o -9 10 0 15.57 68.60 36.70 o -8 10 0 1005.47 1022.77 48.04 o -7 10 0 517.66 461.31 65.20 o -6 10 0 128.78 130.73 30.27 o -5 10 0 361.74 453.95 32.08 o -4 10 0 60.36 49.85 14.11 o -3 10 0 420.19 420.73 28.17 o -2 10 0 739.10 814.13 21.58 o -1 10 0 126.69 122.29 13.78 o 0 10 0 1064.75 1161.90 28.32 o 1 10 0 0.00 12.71 7.86 o 2 10 0 623.66 612.10 16.44 o 3 10 0 382.18 359.99 12.64 o 4 10 0 27.90 36.82 14.24 o 5 10 0 25.77 40.30 13.38 o 6 10 0 131.78 119.96 19.24 o 7 10 0 4.41 1.60 27.31 o 8 10 0 31.39 15.46 24.55 o 9 10 0 45.28 18.17 30.92 o 10 10 0 93.29 159.87 48.77 o -9 11 0 150.03 202.21 46.20 o -8 11 0 115.67 98.02 58.01 o -7 11 0 50.05 49.55 27.37 o -6 11 0 546.66 534.74 37.29 o -5 11 0 15.18 5.80 21.61 o -4 11 0 394.66 436.39 21.68 o -3 11 0 108.45 133.18 16.53 o -2 11 0 1338.70 1301.28 27.90 o -1 11 0 528.91 582.39 23.22 o 0 11 0 641.70 682.69 29.60 o 1 11 0 644.94 600.12 20.52 o 2 11 0 37.40 42.85 11.21 o 3 11 0 54.42 66.98 20.41 o 4 11 0 247.31 233.49 25.17 o 5 11 0 268.24 270.14 28.80 o 6 11 0 15.49 16.22 17.08 o 7 11 0 36.06 26.83 25.79 o 8 11 0 0.02 17.73 44.67 o -9 12 0 0.32 10.21 33.22 o -8 12 0 233.25 212.55 39.35 o -7 12 0 479.33 469.51 40.03 o -6 12 0 51.63 74.67 42.89 o -5 12 0 10.84 51.33 34.60 o -4 12 0 97.92 144.72 18.08 o -3 12 0 10.05 10.26 15.98 o -2 12 0 602.44 558.22 23.39 o -1 12 0 3290.76 3156.22 111.46 o 0 12 0 846.18 819.82 26.04 o 1 12 0 267.67 273.37 18.72 o 2 12 0 1199.83 1161.45 47.61 o 3 12 0 194.10 182.73 21.68 o 4 12 0 29.56 29.06 16.50 o 5 12 0 357.14 373.68 47.66 o 6 12 0 22.48 21.55 19.27 o 7 12 0 29.83 59.12 37.96 o 8 12 0 24.77 26.12 54.65 o 9 12 0 0.54 17.95 41.17 o -8 13 0 8.97 26.44 35.37 o -7 13 0 143.72 131.35 36.76 o -6 13 0 771.10 728.92 43.39 o -5 13 0 0.08 16.13 24.99 o -4 13 0 389.27 413.36 24.69 o -3 13 0 2.70 2.84 16.41 o -2 13 0 676.90 629.71 25.65 o -1 13 0 41.70 29.01 21.02 o 0 13 0 348.32 383.63 27.24 o 1 13 0 59.28 87.50 21.19 o 2 13 0 11.88 34.08 18.34 o 3 13 0 61.12 86.63 28.87 o 4 13 0 0.70 7.94 31.05 o 5 13 0 1000.73 1027.02 40.49 o 6 13 0 351.64 414.45 29.07 o 7 13 0 0.81 -0.15 31.81 o 8 13 0 13.87 -1.40 31.24 o -8 14 0 4.94 15.21 35.21 o -7 14 0 2.04 24.85 33.28 o -6 14 0 135.78 169.32 34.43 o -5 14 0 103.89 122.31 31.85 o -4 14 0 217.37 226.47 24.07 o -3 14 0 116.65 134.72 20.50 o -2 14 0 8.29 10.91 19.53 o -1 14 0 337.96 351.54 21.78 o 0 14 0 96.42 122.63 19.12 o 1 14 0 291.59 266.28 34.55 o 2 14 0 639.35 660.26 55.00 o 3 14 0 157.19 166.24 24.84 o 4 14 0 14.64 5.31 21.75 o 5 14 0 273.45 300.63 101.97 o 6 14 0 165.52 160.23 25.89 o 7 14 0 100.17 86.85 66.04 o -7 15 0 7.00 33.04 33.83 o -6 15 0 273.80 222.29 41.69 o -5 15 0 0.20 -27.65 39.61 o -4 15 0 175.46 180.31 25.17 o -3 15 0 13.17 22.54 28.95 o -2 15 0 311.69 303.29 28.24 o -1 15 0 143.92 169.59 22.16 o 0 15 0 964.36 957.52 54.77 o 1 15 0 133.23 129.90 26.93 o 2 15 0 11.50 11.84 32.92 o 3 15 0 635.88 666.87 37.39 o 4 15 0 0.68 8.28 22.06 o 5 15 0 280.24 305.75 34.77 o 6 15 0 73.27 120.30 29.52 o 7 15 0 7.46 62.83 65.88 o -7 16 0 35.65 -13.37 48.66 o -6 16 0 2.11 2.03 29.93 o -5 16 0 270.73 272.48 40.66 o -4 16 0 264.80 226.95 26.10 o -3 16 0 1206.44 1326.80 47.82 o -2 16 0 453.96 407.61 25.98 o -1 16 0 287.54 334.07 30.11 o 0 16 0 94.80 82.54 23.94 o 1 16 0 58.65 48.95 22.78 o 2 16 0 28.27 14.15 22.13 o 3 16 0 268.99 181.34 30.03 o 4 16 0 54.58 38.93 26.14 o 5 16 0 245.17 280.42 34.94 o 6 16 0 3.31 7.75 28.63 o -6 17 0 50.28 116.72 69.66 o -5 17 0 70.27 57.35 36.95 o -4 17 0 101.73 89.18 31.63 o -3 17 0 52.83 86.79 25.01 o -2 17 0 588.80 593.51 61.43 o -1 17 0 252.93 244.14 31.24 o 0 17 0 357.75 409.75 33.02 o 1 17 0 128.13 153.46 45.79 o 2 17 0 5.29 20.16 23.70 o 3 17 0 566.37 578.20 40.51 o 4 17 0 106.81 73.78 28.90 o 5 17 0 5.50 46.10 34.09 o 6 17 0 2.12 -34.18 36.05 o -6 18 0 22.75 -6.61 62.10 o -5 18 0 15.95 10.85 51.83 o -4 18 0 21.67 18.52 25.86 o -3 18 0 132.40 136.77 30.77 o -2 18 0 182.22 200.19 35.95 o -1 18 0 465.66 555.83 42.63 o 0 18 0 211.46 208.56 35.53 o 1 18 0 1.91 17.02 25.96 o 2 18 0 43.37 46.37 28.74 o 3 18 0 21.06 32.92 29.90 o 4 18 0 285.08 321.89 52.82 o 5 18 0 310.64 364.40 58.28 o -5 19 0 27.36 29.29 65.81 o -4 19 0 132.31 127.83 48.12 o -3 19 0 28.07 -2.79 36.09 o -2 19 0 448.96 361.20 37.75 o -1 19 0 0.53 21.85 36.97 o 0 19 0 323.63 354.02 39.38 o 1 19 0 0.24 25.32 33.46 o 2 19 0 0.59 3.24 26.64 o 3 19 0 13.30 -5.27 32.39 o -2 20 0 5.77 8.40 36.51 o -1 20 0 152.43 260.32 54.04 o 0 20 0 27.92 56.07 42.78 o 1 20 0 61.55 35.94 42.81 o 0 -21 1 22.20 51.87 48.73 o 1 -21 1 18.59 51.25 43.35 o 2 -21 1 45.09 42.74 37.28 o -3 -20 1 10.71 6.19 38.73 o -2 -20 1 4.00 -14.74 37.43 o -1 -20 1 39.65 9.05 37.39 o 1 -20 1 297.87 326.51 48.35 o 2 -20 1 40.71 24.90 40.06 o 3 -20 1 162.16 161.86 41.94 o 4 -20 1 22.02 90.17 42.39 o -4 -19 1 39.65 42.28 42.47 o -3 -19 1 65.18 43.45 35.49 o -2 -19 1 2.14 -0.19 46.40 o -1 -19 1 0.38 5.93 27.75 o 0 -19 1 23.58 42.46 27.84 o 1 -19 1 1.04 34.18 26.45 o 2 -19 1 167.85 155.91 55.42 o 3 -19 1 180.59 197.40 37.07 o 4 -19 1 113.49 61.63 30.76 o 5 -19 1 24.16 10.62 57.90 o -4 -18 1 34.52 57.90 56.41 o -3 -18 1 15.69 33.23 30.11 o -1 -18 1 218.75 238.94 33.41 o 0 -18 1 12.72 -12.83 34.11 o 1 -18 1 838.91 892.94 43.37 o 2 -18 1 334.92 279.94 33.86 o 3 -18 1 9.33 -7.58 24.68 o 4 -18 1 0.23 5.49 37.73 o 5 -18 1 166.45 144.54 41.87 o 6 -18 1 4.90 32.39 58.93 o -6 -17 1 249.42 243.63 51.64 o -5 -17 1 9.63 44.11 66.84 o -4 -17 1 74.10 88.48 30.89 o -3 -17 1 10.54 29.76 25.76 o -2 -17 1 112.88 88.86 26.83 o -1 -17 1 1.21 5.72 26.01 o 0 -17 1 61.91 102.35 27.96 o 1 -17 1 92.24 71.77 27.12 o 2 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-33.04 56.45 o -7 -14 1 29.05 18.33 49.92 o -6 -14 1 163.69 174.25 28.23 o -5 -14 1 234.26 203.94 26.23 o -4 -14 1 214.59 285.94 28.98 o -3 -14 1 0.03 10.25 20.67 o -2 -14 1 685.56 645.47 33.72 o -1 -14 1 15.50 21.92 14.46 o 0 -14 1 443.78 478.26 30.23 o 1 -14 1 317.18 306.93 21.04 o 2 -14 1 23.44 -3.64 13.28 o 3 -14 1 541.67 572.38 26.38 o 4 -14 1 8.28 19.80 21.60 o 5 -14 1 486.09 503.41 37.41 o 6 -14 1 145.98 98.53 32.45 o 7 -14 1 25.66 29.19 32.81 o 8 -14 1 85.51 82.72 40.73 o -8 -13 1 91.39 108.79 40.64 o -7 -13 1 0.42 10.81 26.18 o -6 -13 1 62.46 54.67 16.57 o -5 -13 1 16.00 19.87 28.61 o -4 -13 1 22.73 26.28 37.96 o -3 -13 1 133.30 158.13 35.27 o -2 -13 1 50.98 13.61 18.59 o -1 -13 1 1098.49 1075.11 33.80 o 0 -13 1 2235.82 2272.97 104.88 o 1 -13 1 380.81 354.83 27.85 o 2 -13 1 793.07 805.33 34.48 o 3 -13 1 184.99 186.94 31.98 o 4 -13 1 31.27 20.31 15.72 o 5 -13 1 51.95 68.34 38.35 o 6 -13 1 895.97 921.70 42.93 o 7 -13 1 20.17 45.85 29.65 o 8 -13 1 3.45 65.46 47.78 o -9 -12 1 7.10 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