data_2019606 _cell_angle_alpha 90.000 _cell_angle_beta 109.044 _cell_angle_gamma 90.000 _cell_length_a 4.6078 _cell_length_b 26.3970 _cell_length_c 6.1228 _exptl_crystal_F_000 444.00 _reflns_d_resolution_high 0.8261 _cod_data_source_file fa3345Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AA in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 187.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17678.41 18284.05 123.50 o 4 0 0 806.59 855.63 16.52 o 1 1 0 8526.88 8806.65 68.93 o 3 1 0 192.08 200.37 4.17 o 5 1 0 55.23 53.03 10.16 o 2 2 0 3746.01 4037.71 24.28 o 4 2 0 815.65 858.38 19.08 o 1 3 0 780.62 789.92 35.51 o 3 3 0 149.00 156.28 4.07 o 5 3 0 412.44 408.95 13.35 o 0 4 0 1619.47 1496.74 21.00 o 2 4 0 7063.15 7147.01 79.24 o 4 4 0 2820.42 2906.38 29.57 o 1 5 0 1620.16 1580.27 13.59 o 3 5 0 25.56 22.81 2.02 o 5 5 0 94.48 97.61 5.95 o 0 6 0 9.84 14.28 3.18 o 2 6 0 2484.49 2590.22 36.36 o 4 6 0 1087.68 1067.38 16.16 o 1 7 0 368.75 281.31 4.83 o 3 7 0 1577.47 1518.43 35.59 o 5 7 0 212.58 217.87 8.61 o 0 8 0 2942.36 2852.48 26.55 o 2 8 0 405.81 438.81 8.02 o 4 8 0 329.50 347.20 8.97 o 1 9 0 1500.04 1259.39 47.82 o 3 9 0 1990.36 1878.11 51.05 o 5 9 0 328.33 306.60 13.74 o 0 10 0 48.37 45.02 2.77 o 2 10 0 29.14 27.48 3.50 o 4 10 0 16.24 21.18 3.17 o 1 11 0 18.24 5.88 1.53 o 3 11 0 111.01 98.68 4.54 o 0 12 0 1728.88 1674.09 18.73 o 2 12 0 7983.36 7911.45 284.99 o 4 12 0 2495.50 2478.98 85.42 o 1 13 0 5188.63 4715.09 36.82 o 3 13 0 1834.45 1786.73 23.44 o 0 14 0 577.89 669.03 15.39 o 2 14 0 2108.36 2100.20 47.98 o 4 14 0 1063.66 1004.30 27.12 o 1 15 0 851.51 882.57 11.88 o 3 15 0 25.29 33.53 3.28 o 0 16 0 9373.87 8698.16 82.58 o 2 16 0 4576.16 4247.78 107.47 o 4 16 0 1465.66 1425.66 68.64 o 1 17 0 2413.47 2260.39 22.66 o 3 17 0 310.15 291.52 13.92 o 0 18 0 3605.24 3568.47 36.46 o 2 18 0 1033.67 944.65 14.07 o 4 18 0 557.97 532.00 15.45 o 1 19 0 287.20 249.98 13.02 o 3 19 0 133.91 121.34 7.04 o 0 20 0 8689.67 8674.93 116.43 o 2 20 0 1603.80 1487.29 22.47 o 4 20 0 104.98 109.91 6.37 o 1 21 0 90.95 89.45 4.91 o 3 21 0 1.59 -1.63 1.69 o 0 22 0 3580.64 3669.56 60.99 o 2 22 0 1596.20 1531.74 27.96 o 1 23 0 385.43 386.01 9.02 o 3 23 0 10.18 10.51 2.75 o 0 24 0 1435.24 1462.95 34.51 o 2 24 0 2.86 0.76 2.05 o 1 25 0 1462.07 1488.24 49.79 o 3 25 0 701.20 693.72 15.96 o 0 26 0 3.86 6.29 4.48 o 2 26 0 181.60 187.63 7.28 o 1 27 0 95.81 105.58 20.08 o 0 28 0 791.70 819.97 26.80 o 2 28 0 363.10 392.71 10.78 o 1 29 0 1301.46 1359.78 31.06 o 0 30 0 1.11 0.11 3.80 o 1 31 0 336.02 362.67 18.14 o -5 1 1 2182.17 2278.46 33.20 o -3 1 1 1625.96 1563.51 14.64 o -1 1 1 5242.49 5848.55 76.33 o 1 1 1 35075.91 34637.32 464.09 o 3 1 1 2564.82 2627.87 35.26 o -4 2 1 403.77 424.83 12.61 o -2 2 1 0.49 2.79 0.95 o 0 2 1 1748.81 1857.06 14.04 o 2 2 1 226.89 278.76 7.22 o 4 2 1 21.08 29.19 5.05 o -5 3 1 1152.16 1126.45 18.02 o -3 3 1 3133.47 3140.41 27.49 o -1 3 1 1953.91 2034.19 13.70 o 1 3 1 44.03 70.57 1.96 o 3 3 1 281.46 300.86 11.46 o -4 4 1 713.29 703.87 15.09 o -2 4 1 937.22 843.15 8.50 o 0 4 1 13902.97 13758.65 168.68 o 2 4 1 6148.82 5887.10 37.23 o 4 4 1 561.97 572.30 14.72 o -5 5 1 392.82 405.17 10.60 o -3 5 1 5595.21 5574.25 37.62 o -1 5 1 14865.34 14598.06 122.04 o 1 5 1 615.86 511.87 5.31 o 3 5 1 926.69 929.03 16.17 o -4 6 1 14.14 18.31 2.85 o -2 6 1 263.76 250.67 4.28 o 0 6 1 2103.47 2069.67 31.96 o 2 6 1 2329.10 2352.31 19.01 o 4 6 1 1023.97 1024.69 15.99 o -5 7 1 222.32 223.05 9.51 o -3 7 1 140.05 135.96 4.93 o -1 7 1 1052.48 1115.54 9.12 o 1 7 1 1747.79 1753.48 62.84 o 3 7 1 44.82 41.08 2.97 o -4 8 1 1153.34 1144.74 24.73 o -2 8 1 11175.92 10956.66 64.62 o 0 8 1 9889.27 9145.69 103.80 o 2 8 1 4893.52 4825.07 33.84 o 4 8 1 2634.05 2570.02 75.71 o -5 9 1 64.04 65.74 10.26 o -3 9 1 735.13 742.34 15.01 o -1 9 1 3967.40 4067.26 72.32 o 1 9 1 216.07 232.55 7.19 o 3 9 1 336.74 341.83 7.96 o -4 10 1 276.94 264.13 10.60 o -2 10 1 552.58 508.57 6.28 o 0 10 1 657.41 553.67 11.25 o 2 10 1 1445.89 1392.13 56.87 o 4 10 1 868.70 848.92 14.84 o -5 11 1 13.46 16.84 3.37 o -3 11 1 2143.97 2168.07 61.92 o -1 11 1 5810.50 6052.07 110.04 o 1 11 1 14.49 34.86 3.01 o 3 11 1 213.06 211.59 8.97 o -4 12 1 936.24 927.21 25.85 o -2 12 1 2282.22 2257.03 46.91 o 0 12 1 3725.92 3327.83 42.07 o 2 12 1 2509.54 2228.09 97.58 o 4 12 1 778.70 756.68 15.57 o -5 13 1 1.43 0.09 2.39 o -3 13 1 2799.77 2770.82 62.02 o -1 13 1 6738.47 7033.82 43.58 o 1 13 1 6.18 4.47 1.64 o 3 13 1 358.15 362.82 9.46 o -4 14 1 644.54 603.69 27.09 o -2 14 1 1504.71 1572.01 32.95 o 0 14 1 3424.33 3324.20 49.68 o 2 14 1 1872.34 1725.34 63.45 o 4 14 1 381.32 347.92 20.44 o -3 15 1 1172.10 1129.63 28.26 o -1 15 1 2031.12 1950.43 15.83 o 1 15 1 695.66 615.65 15.44 o 3 15 1 237.63 242.56 7.24 o -4 16 1 36.21 38.66 3.95 o -2 16 1 48.59 46.46 3.45 o 0 16 1 581.53 573.81 7.42 o 2 16 1 407.58 380.02 8.36 o 4 16 1 0.93 -1.57 2.45 o -3 17 1 3011.99 2902.68 57.86 o -1 17 1 3506.74 3280.12 43.11 o 1 17 1 3392.74 3107.63 28.77 o 3 17 1 659.60 600.17 24.91 o -4 18 1 410.77 403.79 10.54 o -2 18 1 1044.54 991.92 21.69 o 0 18 1 413.79 393.52 6.36 o 2 18 1 2.63 5.26 2.10 o 4 18 1 1.37 -1.58 4.53 o -3 19 1 171.41 161.01 6.26 o -1 19 1 23.52 18.91 2.61 o 1 19 1 1805.66 1752.39 20.17 o 3 19 1 368.76 333.04 12.28 o -4 20 1 18.72 30.37 8.86 o -2 20 1 77.55 84.08 4.63 o 0 20 1 2689.05 2619.13 25.63 o 2 20 1 2112.33 1998.05 69.48 o -3 21 1 517.14 535.61 11.66 o -1 21 1 2968.86 2779.57 83.28 o 1 21 1 8007.29 7584.12 59.62 o 3 21 1 1913.94 1818.18 87.72 o -4 22 1 89.93 85.48 9.31 o -2 22 1 7.71 7.90 2.28 o 0 22 1 78.41 78.82 6.00 o 2 22 1 6.37 9.29 2.61 o -3 23 1 166.28 165.64 6.79 o -1 23 1 177.69 202.01 6.56 o 1 23 1 1.60 2.15 2.43 o 3 23 1 209.78 200.95 26.21 o -2 24 1 1083.20 1036.80 16.60 o 0 24 1 1042.70 1014.98 36.20 o 2 24 1 532.91 540.76 12.05 o -3 25 1 584.77 580.69 13.23 o -1 25 1 618.62 594.90 46.82 o 1 25 1 63.67 73.20 8.50 o -2 26 1 683.95 720.14 14.12 o 0 26 1 1070.23 1143.24 21.94 o 2 26 1 796.03 820.63 21.99 o -1 27 1 81.12 89.46 17.70 o 1 27 1 1.62 1.42 3.41 o -2 28 1 796.91 840.76 20.43 o 0 28 1 419.79 448.87 13.74 o 2 28 1 338.23 379.65 10.80 o -1 29 1 179.56 177.48 8.96 o 1 29 1 63.47 66.06 16.05 o 0 30 1 1040.86 1139.75 41.92 o -1 31 1 27.18 22.98 4.73 o -4 0 2 3748.36 3828.26 68.54 o -2 0 2 658.16 542.45 9.34 o 0 0 2 86.02 53.95 4.44 o 2 0 2 10776.54 11055.19 125.90 o -5 1 2 0.68 10.10 4.98 o -3 1 2 75.16 107.81 5.06 o -1 1 2 42.38 61.19 2.73 o 1 1 2 488.78 525.28 5.65 o 3 1 2 154.33 165.34 4.56 o -4 2 2 854.68 885.71 18.75 o -2 2 2 9.82 3.15 1.16 o 0 2 2 1034.09 1293.66 15.12 o 2 2 2 509.11 629.61 45.40 o 4 2 2 352.14 378.04 23.15 o -5 3 2 828.44 805.30 20.39 o -3 3 2 5244.10 5500.26 38.35 o -1 3 2 6390.79 6776.26 40.27 o 1 3 2 5397.01 5367.57 32.99 o 3 3 2 878.42 898.59 20.59 o -4 4 2 952.18 933.73 12.24 o -2 4 2 5763.04 6206.21 38.89 o 0 4 2 5171.14 5125.43 44.59 o 2 4 2 16.11 12.22 1.54 o 4 4 2 71.27 102.13 17.05 o -5 5 2 451.54 446.41 11.04 o -3 5 2 1417.74 1389.34 31.77 o -1 5 2 2474.90 2479.98 43.45 o 1 5 2 7956.88 8312.55 101.91 o 3 5 2 2664.47 2657.30 36.51 o -4 6 2 63.37 67.55 4.32 o -2 6 2 445.48 420.98 5.91 o 0 6 2 3852.42 3824.11 110.26 o 2 6 2 1.53 4.17 1.23 o 4 6 2 26.35 26.99 3.80 o -5 7 2 363.52 373.08 10.11 o -3 7 2 2840.65 2800.12 22.25 o -1 7 2 17027.48 17637.07 342.64 o 1 7 2 8779.94 8561.38 420.75 o 3 7 2 2336.39 2447.43 41.76 o -4 8 2 532.82 558.05 11.07 o -2 8 2 283.31 285.88 4.98 o 0 8 2 3787.15 3867.08 72.21 o 2 8 2 1.73 5.69 1.57 o 4 8 2 21.46 22.19 4.85 o -5 9 2 1563.38 1497.91 33.27 o -3 9 2 5191.15 5133.42 42.05 o -1 9 2 17749.95 17893.79 358.48 o 1 9 2 7549.44 7204.83 376.95 o 3 9 2 2272.31 2314.69 78.21 o -4 10 2 116.04 103.19 5.34 o -2 10 2 942.50 985.27 16.35 o 0 10 2 1155.36 1124.64 25.35 o 2 10 2 546.08 560.68 26.62 o 4 10 2 29.43 36.17 5.21 o -5 11 2 1221.62 1225.82 20.17 o -3 11 2 1411.65 1402.67 17.19 o -1 11 2 1545.63 1542.33 21.43 o 1 11 2 1415.07 1313.86 58.93 o 3 11 2 1083.64 1042.00 16.55 o -4 12 2 124.97 133.93 5.75 o -2 12 2 2436.96 2415.56 22.98 o 0 12 2 6641.12 6385.00 180.55 o 2 12 2 3.90 7.45 2.31 o 4 12 2 31.77 34.52 5.85 o -5 13 2 567.00 565.62 13.17 o -3 13 2 4066.90 4036.15 58.77 o -1 13 2 7848.77 7941.49 49.20 o 1 13 2 5124.69 4709.78 115.80 o 3 13 2 1533.86 1509.15 106.25 o -4 14 2 339.73 343.17 10.99 o -2 14 2 113.42 115.31 4.62 o 0 14 2 150.58 154.89 6.29 o 2 14 2 53.72 51.94 3.81 o 4 14 2 8.26 10.37 3.61 o -3 15 2 1.48 4.07 2.69 o -1 15 2 177.82 160.67 6.97 o 1 15 2 310.21 312.62 8.61 o 3 15 2 372.57 357.04 11.64 o -4 16 2 1312.49 1302.90 42.13 o -2 16 2 1764.47 1717.43 19.40 o 0 16 2 1454.93 1398.33 53.83 o 2 16 2 746.17 739.91 68.73 o -3 17 2 142.33 135.09 6.13 o -1 17 2 24.74 19.63 2.01 o 1 17 2 327.10 326.07 7.74 o 3 17 2 49.58 47.20 5.27 o -4 18 2 1291.51 1263.24 38.33 o -2 18 2 714.17 747.47 12.33 o 0 18 2 6.78 7.41 4.22 o 2 18 2 417.65 393.99 20.68 o -3 19 2 60.37 65.32 4.48 o -1 19 2 45.86 50.10 5.11 o 1 19 2 1049.16 996.69 14.58 o 3 19 2 827.16 793.00 73.10 o -4 20 2 951.18 985.33 29.23 o -2 20 2 269.67 307.17 8.03 o 0 20 2 175.83 164.48 11.25 o 2 20 2 2341.84 2391.74 87.68 o -3 21 2 944.94 932.02 22.08 o -1 21 2 850.71 859.66 37.44 o 1 21 2 1327.55 1251.94 17.19 o 3 21 2 523.76 501.35 15.19 o -4 22 2 513.99 534.67 12.92 o -2 22 2 904.48 974.31 15.37 o 0 22 2 1532.57 1562.01 33.41 o 2 22 2 1569.89 1590.02 27.17 o -3 23 2 753.74 712.93 23.74 o -1 23 2 808.53 750.43 35.10 o 1 23 2 285.35 272.88 12.21 o -2 24 2 477.91 454.80 10.71 o 0 24 2 469.38 472.24 12.95 o 2 24 2 46.24 53.62 5.79 o -3 25 2 1155.26 1175.60 19.23 o -1 25 2 2940.89 2898.42 134.62 o 1 25 2 2495.62 2485.57 59.32 o -2 26 2 1251.23 1217.68 18.78 o 0 26 2 2048.74 2017.57 85.53 o 2 26 2 144.57 158.43 8.83 o -1 27 2 410.94 456.37 13.77 o 1 27 2 400.49 411.71 36.13 o -2 28 2 100.52 107.17 21.86 o 0 28 2 0.43 0.32 4.73 o -1 29 2 1765.01 1881.36 100.67 o 1 29 2 837.02 900.32 30.56 o 0 30 2 86.87 108.86 12.55 o -5 1 3 83.33 84.44 6.88 o -3 1 3 4025.34 4226.30 30.46 o -1 1 3 2258.42 2329.62 16.63 o 1 1 3 498.97 478.63 11.31 o 3 1 3 3062.24 3232.79 83.96 o -4 2 3 231.02 230.05 5.97 o -2 2 3 1750.92 2154.01 30.12 o 0 2 3 256.48 298.26 5.14 o 2 2 3 21.94 18.02 4.19 o -5 3 3 79.07 81.18 5.36 o -3 3 3 599.73 664.49 12.01 o -1 3 3 2384.22 2765.14 67.99 o 1 3 3 1294.88 1189.64 33.42 o 3 3 3 338.90 516.14 20.19 o -4 4 3 2947.62 2856.64 24.74 o -2 4 3 6270.97 6636.45 41.92 o 0 4 3 1819.45 1890.38 64.82 o 2 4 3 1712.06 1732.21 64.70 o 4 4 3 302.72 388.66 21.64 o -5 5 3 1605.69 1536.83 38.03 o -3 5 3 1131.16 1096.07 12.01 o -1 5 3 4575.65 4933.64 55.18 o 1 5 3 5647.27 5571.46 145.34 o 3 5 3 303.56 367.02 18.02 o -4 6 3 312.49 296.23 7.95 o -2 6 3 322.83 309.16 6.36 o 0 6 3 879.72 922.90 36.29 o 2 6 3 1042.21 1053.24 31.32 o -5 7 3 145.15 127.25 6.30 o -3 7 3 1658.58 1660.14 15.82 o -1 7 3 642.60 705.60 7.62 o 1 7 3 1088.50 1138.27 28.23 o 3 7 3 21.71 27.54 6.86 o -4 8 3 2498.72 2373.54 25.91 o -2 8 3 7620.07 7660.04 118.22 o 0 8 3 13100.72 12974.19 456.50 o 2 8 3 2233.40 2297.17 99.23 o -5 9 3 8.71 12.37 3.04 o -3 9 3 5.98 8.02 1.74 o -1 9 3 1265.59 1308.92 11.81 o 1 9 3 1591.31 1677.86 71.00 o 3 9 3 44.30 51.46 7.82 o -4 10 3 2327.21 2264.34 31.63 o -2 10 3 2062.46 2098.68 26.89 o 0 10 3 1717.30 1633.18 60.48 o 2 10 3 319.08 321.37 9.84 o -5 11 3 44.95 44.56 4.81 o -3 11 3 113.08 108.39 4.72 o -1 11 3 613.27 580.34 7.43 o 1 11 3 2189.35 2269.25 41.99 o 3 11 3 79.47 84.11 10.34 o -4 12 3 1806.29 1784.24 26.68 o -2 12 3 4162.97 4192.31 45.75 o 0 12 3 2973.35 2865.30 106.77 o 2 12 3 874.51 977.69 24.27 o -5 13 3 66.60 67.18 5.30 o -3 13 3 711.33 711.79 11.87 o -1 13 3 260.61 270.88 5.30 o 1 13 3 3414.74 3500.96 160.46 o 3 13 3 323.15 312.50 19.13 o -4 14 3 128.23 128.87 5.94 o -2 14 3 1411.67 1419.26 14.21 o 0 14 3 1297.79 1310.47 43.17 o 2 14 3 1044.24 1120.04 21.31 o -3 15 3 70.80 88.70 9.43 o -1 15 3 84.49 75.45 2.90 o 1 15 3 1034.31 1046.34 16.80 o 3 15 3 558.04 548.72 65.96 o -4 16 3 3.13 2.17 2.16 o -2 16 3 38.54 35.86 3.17 o 0 16 3 211.84 204.33 6.43 o 2 16 3 272.72 295.18 15.29 o -3 17 3 3427.95 3370.64 94.12 o -1 17 3 4155.71 3952.93 29.41 o 1 17 3 1398.82 1370.96 19.19 o 3 17 3 696.41 684.17 23.56 o -4 18 3 137.85 152.92 6.69 o -2 18 3 400.83 387.48 8.81 o 0 18 3 463.33 409.85 18.32 o 2 18 3 126.15 134.12 16.63 o -3 19 3 743.74 724.23 13.34 o -1 19 3 397.39 437.34 9.08 o 1 19 3 6.80 8.01 3.09 o -4 20 3 668.05 665.15 18.48 o -2 20 3 1229.18 1362.53 18.30 o 0 20 3 233.92 218.71 8.50 o 2 20 3 341.60 375.69 26.58 o -3 21 3 2118.62 2258.43 26.72 o -1 21 3 1644.00 1860.15 35.26 o 1 21 3 746.93 758.32 17.49 o -2 22 3 360.57 346.71 10.27 o 0 22 3 86.87 76.78 7.78 o 2 22 3 28.43 25.84 6.86 o -3 23 3 32.13 36.22 4.18 o -1 23 3 248.15 290.71 16.60 o 1 23 3 309.62 343.77 16.77 o -2 24 3 1504.43 1538.10 26.55 o 0 24 3 1379.45 1385.90 37.25 o 2 24 3 487.10 555.97 39.50 o -3 25 3 161.21 163.23 7.25 o -1 25 3 824.69 836.28 29.18 o 1 25 3 805.40 809.84 26.58 o -2 26 3 186.58 213.56 16.88 o 0 26 3 589.80 642.52 25.45 o -1 27 3 2.07 0.43 4.94 o 1 27 3 137.11 125.77 13.61 o -2 28 3 157.56 177.80 16.81 o 0 28 3 747.82 880.42 30.88 o -1 29 3 135.15 129.68 13.86 o -4 0 4 1605.98 1627.79 24.72 o -2 0 4 14671.80 16507.79 151.90 o 0 0 4 9048.84 9146.51 115.04 o 2 0 4 1187.08 1229.17 28.18 o -5 1 4 56.37 54.27 4.64 o -3 1 4 327.41 353.46 6.64 o -1 1 4 29.46 22.83 3.18 o 1 1 4 28.67 33.10 3.62 o 3 1 4 2.75 8.41 4.00 o -4 2 4 111.78 131.34 5.35 o -2 2 4 3064.11 3601.61 56.92 o 0 2 4 4170.83 4237.96 123.32 o 2 2 4 987.02 990.10 17.75 o -5 3 4 303.05 286.49 15.42 o -3 3 4 1715.77 1714.69 28.25 o -1 3 4 2601.93 2750.31 24.58 o 1 3 4 175.61 163.07 10.72 o 3 3 4 141.30 161.88 11.80 o -4 4 4 2801.09 2761.56 24.64 o -2 4 4 4433.97 4770.96 66.69 o 0 4 4 5757.87 5823.60 213.91 o 2 4 4 2627.68 2532.51 32.13 o -5 5 4 180.94 186.00 8.36 o -3 5 4 320.78 331.46 6.55 o -1 5 4 13.71 8.30 2.34 o 1 5 4 18.25 25.17 3.35 o 3 5 4 254.36 276.92 16.21 o -4 6 4 2298.41 2203.75 30.81 o -2 6 4 87.93 73.58 3.17 o 0 6 4 71.63 75.75 7.07 o 2 6 4 1289.71 1273.66 39.70 o -5 7 4 349.10 362.30 15.88 o -3 7 4 42.89 59.51 3.85 o -1 7 4 91.97 97.44 4.36 o 1 7 4 884.57 862.03 46.24 o 3 7 4 332.53 392.36 20.47 o -4 8 4 21.58 27.49 3.27 o -2 8 4 1197.94 1169.20 12.15 o 0 8 4 237.00 242.64 15.23 o 2 8 4 409.94 386.49 17.49 o -5 9 4 974.75 936.91 24.65 o -3 9 4 1977.16 1891.47 17.96 o -1 9 4 1813.06 1855.39 49.99 o 1 9 4 1821.13 1720.37 109.44 o 3 9 4 167.75 228.98 16.88 o -4 10 4 46.36 45.40 3.92 o -2 10 4 0.05 1.47 1.62 o 0 10 4 2.34 6.10 2.42 o 2 10 4 54.13 47.62 7.64 o -5 11 4 283.72 256.00 8.79 o -3 11 4 838.43 833.22 11.16 o -1 11 4 469.12 509.73 14.15 o 1 11 4 244.78 226.21 12.44 o 3 11 4 37.88 45.53 10.31 o -4 12 4 1330.10 1282.26 18.23 o -2 12 4 249.90 236.90 6.73 o 0 12 4 1832.45 1836.05 75.09 o 2 12 4 2915.41 3082.23 61.41 o -3 13 4 1124.38 1125.47 28.43 o -1 13 4 3152.69 3146.76 48.52 o 1 13 4 1588.42 1463.09 34.26 o -4 14 4 831.48 835.88 18.61 o -2 14 4 5.37 4.14 2.01 o 0 14 4 123.36 111.66 4.84 o 2 14 4 1490.38 1616.97 43.04 o -3 15 4 19.53 25.27 3.06 o -1 15 4 3.27 8.90 5.64 o 1 15 4 2.68 3.51 2.70 o -4 16 4 2302.87 2344.62 44.27 o -2 16 4 5597.57 5734.42 59.53 o 0 16 4 3657.87 3284.08 284.44 o 2 16 4 1428.89 1587.17 40.59 o -3 17 4 1071.25 1146.05 21.59 o -1 17 4 832.68 872.08 29.29 o 1 17 4 160.94 176.39 7.05 o -4 18 4 99.06 102.00 5.98 o -2 18 4 2400.83 2332.93 32.44 o 0 18 4 2808.42 2626.12 141.06 o 2 18 4 450.34 485.72 17.20 o -3 19 4 4.79 5.32 5.46 o -1 19 4 55.26 37.76 3.51 o 1 19 4 237.61 232.56 8.31 o -2 20 4 1722.29 1758.16 28.03 o 0 20 4 1249.54 1204.81 46.08 o -3 21 4 81.86 94.78 10.00 o -1 21 4 154.63 196.32 13.82 o 1 21 4 3.21 3.13 3.09 o -2 22 4 869.78 945.98 20.26 o 0 22 4 728.62 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