#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:33:17 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181867 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/97/2019704.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2019704 _cell_angle_alpha 121.630 _cell_angle_beta 97.831 _cell_angle_gamma 116.728 _cell_length_a 12.7399 _cell_length_b 15.6208 _cell_length_c 21.5890 _exptl_crystal_F_000 1122.40 _reflns_d_resolution_high 0.8460 _cod_data_source_file ku3140Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' w/o H at O_13' _shelx_refln_list_code 4 _shelx_f_calc_maximum 179.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 193.82 150.30 4.00 o 2 0 0 3850.76 4089.20 129.00 o 3 0 0 5535.66 5877.20 141.34 o 4 0 0 2666.27 2573.75 52.88 o 5 0 0 61.04 43.60 1.27 o 6 0 0 254.85 281.40 6.74 o 7 0 0 90.77 56.43 2.80 o 8 0 0 665.50 624.33 26.16 o 9 0 0 1354.38 1363.97 37.82 o 10 0 0 6.13 5.41 0.88 o 11 0 0 251.26 272.56 11.62 o -12 1 0 40.69 30.94 3.61 o -11 1 0 183.36 167.04 6.23 o -10 1 0 155.48 153.72 9.32 o -9 1 0 1100.11 1133.47 34.58 o -8 1 0 706.62 719.68 17.62 o -7 1 0 59.28 57.07 1.95 o -6 1 0 488.46 565.34 11.48 o -5 1 0 1892.12 2041.68 44.42 o -4 1 0 182.58 200.65 7.09 o -3 1 0 5730.73 5998.74 125.68 o -2 1 0 22908.61 18528.12 662.85 o -1 1 0 14211.70 10755.77 1281.00 o 0 1 0 762.96 666.86 32.50 o 1 1 0 792.95 663.36 19.08 o 2 1 0 95.66 109.43 2.66 o 3 1 0 187.60 174.73 3.66 o 4 1 0 1812.86 2026.79 36.68 o 5 1 0 234.95 207.41 4.61 o 6 1 0 140.51 139.93 3.63 o 7 1 0 353.38 353.47 11.04 o 8 1 0 365.71 390.74 10.45 o 9 1 0 1.06 0.46 0.74 o 10 1 0 37.31 46.08 4.96 o 11 1 0 83.98 68.41 3.89 o -12 2 0 11.64 13.72 2.10 o -11 2 0 0.01 0.14 0.84 o -10 2 0 60.15 51.44 2.36 o -9 2 0 1428.43 1399.68 40.68 o -8 2 0 591.95 608.37 14.82 o -7 2 0 9.65 8.70 1.08 o -6 2 0 335.07 401.96 8.95 o -5 2 0 4380.87 4286.68 81.94 o -4 2 0 205.92 216.02 5.35 o -3 2 0 9.01 -0.69 0.69 o -2 2 0 62.87 92.59 5.75 o -1 2 0 16632.50 14041.24 1073.16 o 0 2 0 16632.81 15460.10 617.20 o 1 2 0 816.10 795.05 18.11 o 2 2 0 9944.54 10617.08 270.88 o 3 2 0 8380.27 8600.66 156.37 o 4 2 0 349.03 380.49 17.62 o 5 2 0 41.80 41.21 1.33 o 6 2 0 613.23 628.21 15.30 o 7 2 0 0.00 0.36 0.68 o 8 2 0 1153.14 1146.27 42.80 o 9 2 0 5.82 5.52 0.97 o 10 2 0 71.48 72.82 3.97 o -13 3 0 0.11 2.69 1.01 o -12 3 0 667.82 706.27 21.78 o -11 3 0 670.88 629.02 17.67 o -10 3 0 1259.60 1266.01 37.65 o -9 3 0 894.75 921.31 22.47 o -8 3 0 29.94 30.50 1.04 o -7 3 0 1967.95 1952.40 39.59 o -6 3 0 582.18 630.31 12.33 o -5 3 0 1029.14 1047.31 20.65 o -4 3 0 5243.74 5474.08 104.39 o -3 3 0 7907.42 7794.42 175.58 o -2 3 0 21552.27 21374.10 1419.19 o -1 3 0 6492.02 6506.15 256.29 o 0 3 0 204.35 201.76 6.70 o 1 3 0 3523.44 3637.82 92.46 o 2 3 0 1388.73 1390.98 31.06 o 3 3 0 571.07 504.40 11.11 o 4 3 0 14.60 14.97 0.76 o 5 3 0 69.75 55.62 2.05 o 6 3 0 155.55 142.54 4.35 o 7 3 0 749.49 764.01 21.35 o 8 3 0 1.88 1.82 0.86 o 9 3 0 61.87 46.87 3.03 o -13 4 0 174.08 183.95 10.51 o -12 4 0 126.71 109.01 5.59 o -11 4 0 9.49 5.97 1.15 o -10 4 0 382.40 384.70 14.65 o -9 4 0 1758.39 1786.06 36.14 o -8 4 0 103.81 111.83 2.52 o -7 4 0 381.51 323.79 6.97 o -6 4 0 10245.09 10612.02 224.34 o -5 4 0 1287.61 1397.32 27.92 o -4 4 0 5928.30 6005.12 156.17 o -3 4 0 728.57 668.44 16.66 o -2 4 0 2659.61 2586.39 75.28 o -1 4 0 50.05 43.09 1.02 o 0 4 0 3320.74 3377.68 64.43 o 1 4 0 25.15 18.97 1.21 o 2 4 0 68.97 50.93 2.03 o 3 4 0 216.05 210.03 5.10 o 4 4 0 166.14 130.14 4.94 o 5 4 0 2598.23 2614.76 81.05 o 6 4 0 0.69 1.07 0.66 o 7 4 0 63.16 61.49 2.85 o 8 4 0 9.45 9.01 2.10 o -13 5 0 296.29 283.30 13.13 o -12 5 0 6.60 1.80 1.44 o -11 5 0 32.92 35.99 1.96 o -10 5 0 664.53 607.08 19.64 o -9 5 0 92.66 95.79 2.43 o -8 5 0 1520.94 1427.69 27.88 o -7 5 0 5877.70 6021.06 143.88 o -6 5 0 3.63 8.59 0.60 o -5 5 0 4211.65 4458.91 97.51 o -4 5 0 4813.47 4799.53 87.75 o -3 5 0 4078.60 3756.05 78.91 o -2 5 0 673.88 617.80 13.97 o -1 5 0 2436.81 2364.07 50.90 o 0 5 0 519.51 537.50 11.23 o 1 5 0 63.17 78.32 1.90 o 2 5 0 4714.85 4833.96 105.12 o 3 5 0 824.26 829.74 21.34 o 4 5 0 70.18 69.19 2.65 o 5 5 0 26.33 27.87 1.34 o 6 5 0 78.43 59.32 2.23 o 7 5 0 262.53 259.59 16.07 o 8 5 0 20.06 11.72 2.10 o -14 6 0 144.45 140.19 5.79 o -13 6 0 6.60 2.40 0.99 o -12 6 0 195.68 184.00 11.01 o -11 6 0 105.81 99.51 3.39 o -10 6 0 18.03 12.77 1.58 o -9 6 0 2533.64 2479.97 54.01 o -8 6 0 990.73 951.32 19.94 o -7 6 0 5749.88 6277.82 124.08 o -6 6 0 82.56 75.87 1.64 o -5 6 0 1776.05 1853.13 68.21 o -4 6 0 1225.92 1242.64 25.02 o -3 6 0 105.37 81.32 3.92 o -2 6 0 4563.20 4706.27 144.54 o -1 6 0 79.21 59.57 2.05 o 0 6 0 2307.29 2369.98 47.39 o 1 6 0 136.22 130.15 3.23 o 2 6 0 990.76 1004.30 23.37 o 3 6 0 217.43 225.29 7.76 o 4 6 0 716.26 721.92 20.04 o 5 6 0 32.25 37.51 2.05 o 6 6 0 1086.98 1116.69 65.49 o 7 6 0 0.48 1.80 1.20 o -14 7 0 79.59 68.80 4.53 o -13 7 0 0.33 1.35 0.82 o -12 7 0 118.35 104.32 3.60 o -11 7 0 68.33 60.88 2.21 o -10 7 0 3.27 5.11 0.80 o -9 7 0 66.18 64.17 2.37 o -8 7 0 0.34 1.04 0.41 o -7 7 0 58.48 57.83 1.43 o -6 7 0 174.00 165.23 3.09 o -5 7 0 31.97 20.77 1.99 o -4 7 0 970.98 993.11 22.12 o -3 7 0 2169.01 2188.30 46.71 o -2 7 0 3053.56 3212.82 69.13 o -1 7 0 150.70 124.30 5.07 o 0 7 0 174.12 157.31 4.22 o 1 7 0 60.52 58.57 1.89 o 2 7 0 160.28 159.54 6.34 o 3 7 0 670.97 684.49 22.95 o 4 7 0 563.35 532.96 17.61 o 5 7 0 1.00 2.76 1.15 o 6 7 0 52.10 44.49 3.00 o -14 8 0 18.03 11.24 1.37 o -13 8 0 26.79 27.57 1.69 o -12 8 0 1445.85 1423.59 33.66 o -11 8 0 137.72 131.71 3.83 o -10 8 0 1160.95 1169.95 56.53 o -9 8 0 1208.86 1169.62 31.23 o -8 8 0 192.35 178.44 5.49 o -7 8 0 53.24 53.23 2.06 o -6 8 0 192.59 138.87 3.33 o -5 8 0 945.76 863.48 20.46 o -4 8 0 4767.47 4782.10 118.67 o -3 8 0 879.61 826.23 32.39 o -2 8 0 26.63 21.80 0.87 o -1 8 0 607.62 637.35 15.38 o 0 8 0 3867.51 4095.19 98.01 o 1 8 0 22.00 13.26 1.79 o 2 8 0 0.37 1.88 0.77 o 3 8 0 131.66 128.17 4.29 o 4 8 0 1.53 3.74 1.15 o 5 8 0 80.21 98.49 13.67 o -14 9 0 3.81 4.40 1.65 o -13 9 0 696.29 732.85 20.45 o -12 9 0 45.03 48.79 2.10 o -11 9 0 0.57 1.01 0.63 o -10 9 0 352.15 306.53 9.99 o -9 9 0 27.12 31.50 1.79 o -8 9 0 3.83 3.95 0.76 o -7 9 0 961.80 1005.35 25.09 o -6 9 0 74.60 62.70 1.79 o -5 9 0 484.09 470.70 10.85 o -4 9 0 1880.71 1862.90 43.53 o -3 9 0 36.78 32.22 1.62 o -2 9 0 72.93 66.52 6.11 o -1 9 0 682.97 683.73 24.72 o 0 9 0 75.24 76.75 3.60 o 1 9 0 148.87 143.93 7.32 o 2 9 0 66.63 55.53 3.43 o 3 9 0 503.96 483.47 36.65 o 4 9 0 217.13 208.79 14.12 o -14 10 0 248.56 273.79 8.02 o -13 10 0 137.64 138.54 7.36 o -12 10 0 233.11 257.60 7.45 o -11 10 0 9.57 12.50 1.37 o -10 10 0 10.64 7.82 1.95 o -9 10 0 517.67 488.49 36.05 o -8 10 0 1515.47 1488.66 39.45 o -7 10 0 184.05 210.89 6.46 o -6 10 0 3.16 2.37 0.83 o -5 10 0 694.48 652.42 17.37 o -4 10 0 1666.71 1606.46 37.71 o -3 10 0 369.71 349.44 13.09 o -2 10 0 346.71 325.46 8.92 o -1 10 0 19.32 19.29 1.32 o 0 10 0 666.20 642.50 20.29 o 1 10 0 191.78 177.18 9.46 o 2 10 0 70.41 75.07 3.93 o 3 10 0 154.75 164.93 11.72 o -14 11 0 164.28 187.86 5.62 o -13 11 0 3.21 4.53 0.92 o -12 11 0 729.89 787.93 21.80 o -11 11 0 1177.44 1174.26 34.54 o -10 11 0 391.51 429.83 14.46 o -9 11 0 4.59 2.94 0.89 o -8 11 0 563.11 542.11 15.99 o -7 11 0 154.84 172.13 4.41 o -6 11 0 11.70 9.20 1.67 o -5 11 0 8.59 9.54 0.86 o -4 11 0 28.34 25.49 1.99 o -3 11 0 538.01 517.63 14.16 o -2 11 0 659.35 604.27 16.47 o -1 11 0 101.29 103.74 3.89 o 0 11 0 12.48 13.59 1.83 o 1 11 0 1.22 2.23 1.16 o -14 12 0 21.46 23.08 1.78 o -13 12 0 15.79 26.71 3.55 o -12 12 0 160.47 178.43 5.77 o -11 12 0 75.32 81.52 6.47 o -10 12 0 243.57 295.19 22.83 o -9 12 0 105.98 104.96 4.39 o -8 12 0 75.63 78.26 3.47 o -7 12 0 717.83 740.26 29.47 o -6 12 0 704.85 674.97 20.49 o -5 12 0 117.24 92.30 6.25 o -4 12 0 17.80 23.34 1.99 o -3 12 0 361.60 340.56 11.03 o -2 12 0 169.70 160.69 7.08 o -1 12 0 0.06 2.45 1.44 o 0 12 0 32.42 37.71 3.19 o -14 13 0 278.55 291.41 10.62 o -13 13 0 0.66 0.77 0.94 o -12 13 0 81.12 80.60 4.11 o -11 13 0 67.27 78.20 5.97 o -10 13 0 75.06 90.38 3.62 o -9 13 0 93.91 86.96 3.03 o -8 13 0 231.83 197.74 6.93 o -7 13 0 259.94 244.33 12.36 o -6 13 0 0.59 1.02 0.90 o -5 13 0 13.33 17.12 2.70 o -4 13 0 33.03 30.81 2.13 o -3 13 0 325.48 372.55 19.04 o -2 13 0 21.97 26.52 2.43 o -13 14 0 51.34 55.73 2.43 o -12 14 0 25.15 17.31 1.66 o -11 14 0 47.05 59.91 2.79 o -10 14 0 249.32 234.81 10.66 o -9 14 0 114.83 126.48 6.16 o -8 14 0 0.61 1.70 0.93 o -7 14 0 20.73 16.08 1.85 o -6 14 0 166.62 168.54 14.12 o -5 14 0 10.23 16.17 1.87 o -4 14 0 895.88 901.78 31.92 o -3 14 0 323.85 259.26 19.53 o -11 15 0 26.05 27.29 2.12 o -10 15 0 40.03 63.69 5.41 o -9 15 0 9.12 14.42 1.88 o -8 15 0 14.27 9.01 2.10 o -7 15 0 75.59 61.09 3.89 o -6 15 0 1.28 3.00 1.50 o 9 -16 1 0.22 0.60 1.20 o 5 -15 1 69.47 59.18 4.66 o 6 -15 1 43.40 86.36 5.18 o 7 -15 1 233.29 311.16 16.86 o 8 -15 1 56.02 71.26 4.73 o 9 -15 1 296.87 264.08 14.61 o 10 -15 1 57.79 46.45 2.74 o 11 -15 1 20.30 16.06 2.16 o 12 -15 1 13.09 7.51 1.50 o 3 -14 1 56.63 48.35 2.96 o 4 -14 1 230.92 243.45 14.92 o 5 -14 1 14.89 12.70 1.72 o 6 -14 1 174.80 225.51 12.51 o 7 -14 1 57.85 62.06 3.43 o 8 -14 1 37.42 30.98 2.08 o 9 -14 1 554.97 543.33 17.85 o 10 -14 1 1.65 -0.30 1.06 o 11 -14 1 3.28 3.15 0.92 o 12 -14 1 64.70 80.94 3.25 o 13 -14 1 121.45 93.12 3.33 o 1 -13 1 448.80 427.90 20.48 o 2 -13 1 129.70 126.65 5.05 o 3 -13 1 190.18 220.61 8.27 o 4 -13 1 20.89 37.64 6.16 o 5 -13 1 279.49 265.22 8.78 o 6 -13 1 430.88 431.79 11.71 o 7 -13 1 1080.17 1111.88 32.69 o 8 -13 1 357.24 384.56 11.38 o 9 -13 1 4.06 1.69 0.82 o 10 -13 1 36.17 26.95 2.25 o 11 -13 1 646.69 700.90 22.55 o 12 -13 1 142.67 131.30 6.58 o 13 -13 1 6.35 12.18 1.49 o 14 -13 1 54.19 61.27 2.91 o -1 -12 1 37.46 52.57 5.11 o 0 -12 1 0.06 0.38 1.13 o 1 -12 1 98.25 86.71 4.45 o 2 -12 1 60.97 50.76 4.39 o 3 -12 1 152.91 91.58 5.65 o 4 -12 1 117.18 103.58 4.23 o 5 -12 1 692.80 690.65 24.37 o 6 -12 1 35.89 33.80 1.71 o 7 -12 1 186.56 209.59 6.07 o 8 -12 1 912.52 948.53 23.91 o 9 -12 1 840.90 829.59 22.67 o 10 -12 1 193.69 216.87 7.51 o 11 -12 1 0.04 2.52 0.88 o 12 -12 1 83.10 67.28 3.17 o 13 -12 1 29.77 21.95 2.55 o 14 -12 1 6.49 7.76 1.08 o -2 -11 1 204.15 221.54 11.03 o -1 -11 1 42.76 53.48 5.41 o 0 -11 1 33.01 30.23 2.22 o 1 -11 1 160.65 139.45 4.95 o 2 -11 1 2.32 5.20 0.91 o 3 -11 1 656.92 693.90 24.74 o 4 -11 1 276.32 285.22 10.41 o 5 -11 1 404.71 340.50 15.89 o 6 -11 1 144.82 137.38 4.91 o 7 -11 1 1976.92 2009.30 71.12 o 8 -11 1 373.10 380.21 18.09 o 9 -11 1 171.71 153.16 4.91 o 10 -11 1 113.40 97.65 4.38 o 11 -11 1 294.02 337.84 15.22 o 12 -11 1 47.11 44.38 2.21 o 13 -11 1 513.74 586.91 19.65 o 14 -11 1 4.08 2.31 0.91 o -3 -10 1 1.94 2.76 1.58 o -2 -10 1 9.47 2.87 1.66 o -1 -10 1 5.67 7.06 1.14 o 0 -10 1 146.90 132.17 5.89 o 1 -10 1 72.16 73.15 4.03 o 2 -10 1 71.02 61.29 5.41 o 3 -10 1 643.14 583.19 13.79 o 4 -10 1 9.38 5.78 0.79 o 5 -10 1 2982.24 2912.85 76.91 o 6 -10 1 48.35 45.87 1.55 o 7 -10 1 482.02 505.87 14.03 o 8 -10 1 522.03 515.93 14.08 o 9 -10 1 1.25 2.80 1.34 o 10 -10 1 3.47 8.41 1.04 o 12 -10 1 152.76 191.43 5.72 o 13 -10 1 16.43 16.82 1.45 o 14 -10 1 31.55 16.63 1.67 o -4 -9 1 9.65 16.19 1.55 o -3 -9 1 6.02 1.52 1.12 o -2 -9 1 442.48 465.95 17.62 o -1 -9 1 120.49 136.89 4.18 o 0 -9 1 1461.93 1476.85 37.37 o 1 -9 1 502.80 469.84 11.39 o 2 -9 1 902.63 913.17 24.53 o 3 -9 1 548.98 566.13 15.27 o 4 -9 1 1215.59 1150.00 26.15 o 5 -9 1 223.49 208.79 6.12 o 6 -9 1 245.50 273.29 6.32 o 7 -9 1 291.18 262.51 5.68 o 8 -9 1 139.26 125.85 3.37 o 9 -9 1 21.76 21.94 2.08 o 10 -9 1 269.65 256.12 10.84 o 11 -9 1 1392.26 1471.71 45.12 o 12 -9 1 214.35 215.02 5.88 o 13 -9 1 9.50 21.88 2.42 o 14 -9 1 204.06 242.67 18.33 o -5 -8 1 261.83 311.76 10.32 o -4 -8 1 454.62 439.37 17.24 o -3 -8 1 53.72 58.45 2.69 o -2 -8 1 733.70 739.38 22.05 o -1 -8 1 1177.65 1224.68 36.60 o 0 -8 1 548.47 531.82 12.89 o 1 -8 1 506.28 485.89 10.61 o 2 -8 1 338.19 326.43 8.70 o 3 -8 1 1761.87 1856.24 40.93 o 4 -8 1 445.26 369.35 12.89 o 5 -8 1 1094.49 1041.89 22.20 o 6 -8 1 3.73 3.65 0.50 o 7 -8 1 73.22 65.78 2.10 o 8 -8 1 13.93 11.60 0.73 o 9 -8 1 131.41 114.32 4.37 o 10 -8 1 122.65 150.79 5.58 o 11 -8 1 25.41 20.73 1.32 o 12 -8 1 0.06 0.99 0.85 o 13 -8 1 311.02 317.06 9.81 o 14 -8 1 14.92 13.43 1.75 o -6 -7 1 29.26 23.80 3.03 o -5 -7 1 155.23 126.34 7.11 o -4 -7 1 30.46 39.10 1.80 o -3 -7 1 252.95 244.10 6.89 o -2 -7 1 7.60 3.34 0.77 o -1 -7 1 346.91 338.92 8.34 o 0 -7 1 116.56 106.34 2.62 o 1 -7 1 365.43 381.72 9.14 o 2 -7 1 1719.01 1692.48 33.50 o 3 -7 1 2935.21 2850.33 66.88 o 4 -7 1 703.67 750.16 15.12 o 5 -7 1 656.26 612.99 12.54 o 6 -7 1 242.45 288.77 6.82 o 7 -7 1 116.80 113.29 2.46 o 8 -7 1 247.13 216.96 5.21 o 9 -7 1 356.31 313.42 7.39 o 10 -7 1 159.84 158.86 5.02 o 11 -7 1 376.99 380.55 8.55 o 12 -7 1 913.69 934.26 25.35 o 13 -7 1 454.71 432.25 16.47 o 14 -7 1 21.16 23.09 2.09 o -7 -6 1 3.26 3.03 1.22 o -6 -6 1 1.54 2.11 0.97 o -5 -6 1 153.15 143.51 5.41 o -4 -6 1 437.68 428.13 12.69 o -3 -6 1 1052.77 1026.92 23.54 o -2 -6 1 16.87 25.95 0.98 o -1 -6 1 52.93 47.54 1.39 o 0 -6 1 85.23 108.18 2.88 o 1 -6 1 1854.86 1969.96 73.43 o 2 -6 1 350.90 422.64 16.54 o 3 -6 1 1939.80 2140.12 60.97 o 4 -6 1 104.54 153.81 5.39 o 5 -6 1 768.67 765.00 20.45 o 6 -6 1 2028.21 2176.18 44.54 o 7 -6 1 3587.33 3493.21 72.26 o 8 -6 1 332.20 356.32 7.60 o 9 -6 1 132.39 109.28 3.95 o 10 -6 1 41.16 40.86 2.63 o 11 -6 1 41.39 31.70 1.45 o 12 -6 1 23.56 25.25 1.45 o 14 -6 1 36.58 50.74 3.07 o -8 -5 1 0.73 0.57 1.35 o -7 -5 1 68.63 60.04 7.06 o -6 -5 1 29.88 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65.19 5.41 o -3 -9 24 6.33 4.61 1.00 o -2 -9 24 44.95 51.07 4.51 o -1 -9 24 29.65 27.85 2.24 o 0 -9 24 63.81 64.55 3.18 o 1 -9 24 51.25 58.88 4.81 o -6 -8 24 156.45 186.56 14.12 o -5 -8 24 4.24 3.30 1.20 o -4 -8 24 22.21 23.76 3.61 o -3 -8 24 106.78 96.00 6.31 o -2 -8 24 42.04 48.45 3.10 o -1 -8 24 534.14 523.09 21.10 o 0 -8 24 77.65 83.83 4.56 o 1 -8 24 85.46 79.61 6.31 o -6 -7 24 0.34 2.40 1.20 o -5 -7 24 86.42 71.28 11.27 o -4 -7 24 31.56 22.53 2.09 o -3 -7 24 122.55 135.12 5.83 o -2 -7 24 470.74 490.73 19.90 o -1 -7 24 0.86 0.38 0.77 o 0 -7 24 532.40 582.76 28.27 o -6 -6 24 35.86 40.56 3.61 x -5 -6 24 153.73 143.99 9.93 o -4 -6 24 81.73 78.82 3.64 o -3 -6 24 454.47 471.33 19.15 o -2 -6 24 85.08 90.17 4.78 o -1 -6 24 89.36 81.69 4.66 o -6 -5 24 87.97 85.92 6.91 o -5 -5 24 2.04 0.14 1.09 o -4 -5 24 190.24 210.61 9.92 o -3 -5 24 348.85 300.90 14.89 o -5 -4 24 27.88 21.63 2.70 o -4 -4 24 226.02 257.46 19.23 o -1 -12 25 312.88 331.37 24.33 o 0 -12 25 40.25 27.04 2.70 o -2 -11 25 77.39 55.88 4.51 o -1 -11 25 75.31 88.32 6.91 o 0 -11 25 31.65 44.76 3.91 o -3 -10 25 17.77 27.04 2.70 o -2 -10 25 4.34 10.51 1.80 o -1 -10 25 137.19 132.84 18.93 o -4 -9 25 235.92 272.18 20.13 o -3 -9 25 220.12 225.92 16.82 o -2 -9 25 36.02 42.24 2.74 o -1 -9 25 2.27 9.61 2.10 o -4 -8 25 5.57 2.40 0.90 o -3 -8 25 0.47 0.79 1.05 o -2 -8 25 59.69 64.89 5.41 o -1 -8 25 117.66 102.74 8.11 o -3 -7 25 1.32 1.20 1.20 o