#------------------------------------------------------------------------------ #$Date: 2018-01-17 08:22:48 +0200 (Wed, 17 Jan 2018) $ #$Revision: 205301 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/08/2020898.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020898 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.1217 _cell_length_b 9.8397 _cell_length_c 21.9142 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.8443 _cod_data_source_file qs3064Isup2.hkl _cod_data_source_block I _shelx_title ' 16275_1_opfinal in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.42 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 760.32 676.30 34.39 o 4 0 0 22.56 31.44 22.68 o 6 0 0 358.06 450.89 75.38 o 2 1 0 491.49 409.35 16.81 o 4 1 0 39.25 28.81 15.63 o 6 1 0 899.98 1058.28 82.95 o 0 2 0 3082.82 3944.96 226.83 o 2 2 0 2.42 -9.22 9.22 o 4 2 0 139.81 116.52 17.84 o 2 3 0 1128.60 1063.19 40.19 o 4 3 0 990.10 906.22 59.32 o 0 4 0 2720.43 3072.25 182.74 o 2 4 0 4251.24 3961.26 145.35 o 4 4 0 79.39 50.12 27.44 o 2 5 0 2654.41 2647.81 90.60 o 4 5 0 0.64 22.42 27.82 o 0 6 0 1364.46 1714.18 114.41 o 2 6 0 375.38 382.73 31.89 o 4 6 0 263.18 242.45 30.67 o 2 7 0 2.15 -19.21 29.86 o 4 7 0 149.20 162.81 32.68 o 0 8 0 18.27 24.19 37.17 o 2 8 0 29.72 -9.71 25.57 o 4 8 0 117.64 89.46 31.44 o 2 9 0 9.73 4.73 27.49 o 0 10 0 0.32 -16.64 80.54 o 2 10 0 14.78 -3.27 30.16 o 1 1 1 2830.71 2417.70 54.72 o 2 1 1 206.14 200.86 9.16 o 3 1 1 6.10 -7.85 7.85 o 4 1 1 7.01 -1.83 9.55 o 5 1 1 2.10 15.44 18.54 o 6 1 1 212.43 268.18 29.93 o 0 2 1 6986.58 9308.68 281.02 o 1 2 1 104.86 109.16 8.37 o 2 2 1 465.25 489.54 14.72 o 3 2 1 0.43 -8.30 8.30 o 4 2 1 45.00 42.87 10.66 o 5 2 1 318.73 363.98 25.27 o 1 3 1 2998.29 3111.20 77.41 o 2 3 1 150.23 154.76 15.33 o 3 3 1 0.20 0.65 7.94 o 4 3 1 48.84 54.52 13.48 o 5 3 1 118.78 123.16 20.77 o 0 4 1 2.34 -1.41 28.35 o 1 4 1 1244.28 1314.40 40.15 o 2 4 1 153.55 164.00 10.97 o 3 4 1 58.56 55.07 11.09 o 4 4 1 372.65 347.65 25.46 o 5 4 1 0.50 -20.66 20.66 o 1 5 1 3.78 3.58 13.60 o 2 5 1 1543.88 1520.56 43.77 o 3 5 1 43.07 47.92 16.19 o 4 5 1 591.14 536.81 28.98 o 5 5 1 15.25 36.75 23.41 o 0 6 1 646.61 814.45 45.51 o 1 6 1 170.47 216.04 17.81 o 2 6 1 416.14 414.20 19.60 o 3 6 1 93.92 80.94 17.59 o 4 6 1 0.04 20.13 18.53 o 5 6 1 14.72 -17.96 24.54 o 1 7 1 182.16 243.26 20.20 o 2 7 1 13.02 3.93 17.72 o 3 7 1 700.25 612.34 31.25 o 4 7 1 39.81 40.03 19.80 o 0 8 1 526.24 660.96 44.82 o 1 8 1 34.36 77.95 19.13 o 2 8 1 254.66 227.24 21.76 o 3 8 1 129.05 90.98 22.10 o 4 8 1 53.40 40.98 21.99 o 1 9 1 0.48 -13.81 19.94 o 2 9 1 514.30 508.40 33.88 o 3 9 1 11.02 -9.91 19.84 o 0 10 1 163.41 181.38 34.71 o 1 10 1 297.57 265.07 26.03 o 2 10 1 98.50 132.03 22.74 o 3 10 1 30.47 7.44 20.35 o 1 11 1 6.03 -17.64 22.40 o 0 0 2 5008.85 4126.86 165.31 o 1 0 2 61.56 49.69 7.64 o 2 0 2 37.55 38.70 9.84 o 3 0 2 33.80 28.90 13.39 o 4 0 2 50.93 34.67 16.46 o 5 0 2 751.96 779.55 37.90 o 6 0 2 57.86 79.62 38.34 o 1 1 2 3630.59 3204.66 78.22 o 2 1 2 862.37 765.29 21.22 o 3 1 2 60.81 50.43 8.58 o 4 1 2 1.76 -2.86 9.73 o 5 1 2 438.86 441.61 23.08 o 6 1 2 20.97 22.35 23.31 o 0 2 2 10.71 8.84 8.99 o 1 2 2 21147.68 25201.16 634.97 o 2 2 2 6.22 12.78 7.29 o 3 2 2 67.81 70.24 9.27 o 4 2 2 148.78 176.23 11.95 o 5 2 2 86.46 119.32 20.09 o 1 3 2 3861.53 4067.65 104.81 o 2 3 2 779.91 741.04 25.24 o 3 3 2 213.51 190.31 11.73 o 4 3 2 49.46 42.27 12.65 o 5 3 2 77.30 99.91 20.65 o 0 4 2 956.30 989.60 44.60 o 1 4 2 774.17 860.73 27.13 o 2 4 2 347.79 362.24 15.04 o 3 4 2 79.16 65.59 11.46 o 4 4 2 335.31 350.00 26.88 o 5 4 2 34.94 43.25 22.17 o 1 5 2 0.34 -2.56 9.57 o 2 5 2 572.88 542.96 21.58 o 3 5 2 1199.39 1074.74 38.53 o 4 5 2 52.46 39.57 20.69 o 5 5 2 94.82 77.29 25.58 o 0 6 2 90.17 154.90 24.22 o 1 6 2 54.13 51.98 11.18 o 2 6 2 269.37 256.53 16.61 o 3 6 2 266.47 258.86 21.12 o 4 6 2 2.57 3.85 18.33 o 5 6 2 42.86 51.64 23.69 o 1 7 2 14.37 27.58 16.45 o 2 7 2 39.19 51.47 16.98 o 3 7 2 154.02 166.32 20.81 o 4 7 2 14.68 -4.10 19.15 o 0 8 2 388.63 470.59 38.27 o 1 8 2 296.01 351.92 24.80 o 2 8 2 246.82 223.98 21.80 o 3 8 2 21.71 23.36 19.81 o 4 8 2 0.48 -21.32 21.32 o 1 9 2 10.94 9.76 20.20 o 2 9 2 137.78 152.43 22.11 o 3 9 2 47.39 34.61 21.14 o 0 10 2 1.56 -11.31 30.44 o 1 10 2 20.55 23.42 30.62 o 2 10 2 4.00 -1.06 21.00 o 3 10 2 3.23 -30.21 30.21 o 1 11 2 22.22 45.29 22.97 o 1 1 3 491.14 437.62 13.07 o 2 1 3 873.23 833.50 23.90 o 3 1 3 153.56 157.49 9.98 o 4 1 3 72.57 68.99 12.06 o 5 1 3 9.80 19.95 14.73 o 0 2 3 5177.50 5726.92 173.86 o 1 2 3 161.74 182.76 10.50 o 2 2 3 46.43 66.78 9.98 o 3 2 3 68.80 73.54 10.09 o 4 2 3 105.21 117.38 11.89 o 5 2 3 119.46 119.70 22.43 o 1 3 3 1126.66 1090.37 32.01 o 2 3 3 134.27 134.23 11.26 o 3 3 3 284.91 260.40 14.61 o 4 3 3 0.60 -2.21 14.99 o 5 3 3 246.52 239.42 24.92 o 0 4 3 7.67 13.83 14.38 o 1 4 3 33.19 54.54 9.40 o 2 4 3 247.18 213.68 12.25 o 3 4 3 55.25 68.78 13.75 o 4 4 3 182.07 215.57 19.79 o 5 4 3 17.95 8.62 22.45 o 1 5 3 561.25 659.69 25.07 o 2 5 3 404.53 441.41 18.85 o 3 5 3 192.74 172.09 13.28 o 4 5 3 0.31 -18.28 18.28 o 5 5 3 1.42 -18.17 31.68 o 0 6 3 1107.42 1377.86 68.14 o 1 6 3 201.78 201.63 13.63 o 2 6 3 6.61 16.99 10.60 o 3 6 3 702.38 607.18 29.78 o 4 6 3 2.47 -21.49 21.49 o 5 6 3 0.72 37.25 23.55 o 1 7 3 138.53 143.50 20.80 o 2 7 3 148.17 137.82 15.04 o 3 7 3 1073.72 945.27 40.35 o 4 7 3 6.02 -20.59 20.59 o 0 8 3 326.11 312.11 33.41 o 1 8 3 68.30 65.71 18.64 o 2 8 3 135.05 144.40 20.32 o 3 8 3 42.36 44.76 20.14 o 4 8 3 78.53 56.08 22.53 o 1 9 3 223.36 236.93 23.64 o 2 9 3 17.60 17.75 20.03 o 3 9 3 41.96 37.01 20.85 o 0 10 3 20.00 4.24 30.56 o 1 10 3 361.20 349.49 27.42 o 2 10 3 144.24 122.64 30.02 o 1 11 3 162.45 163.44 25.19 o 0 0 4 12213.85 11320.94 523.01 o 1 0 4 19.15 18.19 8.67 o 2 0 4 2053.31 1905.18 61.31 o 3 0 4 260.27 288.51 20.47 o 4 0 4 2.30 -9.13 27.53 o 5 0 4 32.46 62.93 22.41 o 1 1 4 1068.23 802.29 23.32 o 2 1 4 106.09 94.21 8.55 o 3 1 4 171.94 161.48 10.86 o 4 1 4 100.82 116.27 12.47 o 5 1 4 115.39 103.47 16.39 o 0 2 4 434.36 430.48 16.13 o 1 2 4 2287.03 2049.51 51.98 o 2 2 4 391.49 375.10 15.20 o 3 2 4 0.33 -2.07 10.27 o 4 2 4 369.30 390.61 21.81 o 5 2 4 268.61 347.67 25.74 o 1 3 4 2833.56 2841.48 74.52 o 2 3 4 2221.04 2222.26 59.76 o 3 3 4 0.03 -6.11 10.98 o 4 3 4 399.21 428.36 20.02 o 5 3 4 20.07 69.46 20.34 o 0 4 4 174.15 215.79 14.95 o 1 4 4 374.59 385.91 14.28 o 2 4 4 488.88 465.30 17.81 o 3 4 4 18.88 -10.82 10.82 o 4 4 4 143.58 144.53 17.62 o 5 4 4 31.58 23.59 24.95 o 1 5 4 72.87 88.30 11.78 o 2 5 4 54.56 70.25 10.69 o 3 5 4 4.50 -9.10 11.11 o 4 5 4 2.49 1.21 18.71 o 5 5 4 20.50 9.51 25.16 o 0 6 4 505.59 704.15 40.44 o 1 6 4 472.66 529.05 19.93 o 2 6 4 64.54 57.52 10.30 o 3 6 4 268.74 267.39 21.64 o 4 6 4 0.79 15.26 25.90 o 5 6 4 28.30 11.05 26.28 o 1 7 4 7.15 22.01 12.07 o 2 7 4 116.66 131.92 15.27 o 3 7 4 1703.01 1553.36 58.22 o 4 7 4 33.01 -1.22 22.67 o 0 8 4 92.15 141.99 34.23 o 1 8 4 0.06 -16.47 16.47 o 2 8 4 2.93 -7.94 17.84 o 3 8 4 439.61 401.02 25.21 o 4 8 4 142.73 84.65 23.33 o 1 9 4 151.23 159.48 22.09 o 2 9 4 40.74 19.93 18.80 o 3 9 4 12.60 -24.58 24.58 o 0 10 4 5.97 -11.24 35.17 o 1 10 4 209.80 196.77 24.01 o 2 10 4 4.63 -19.74 19.74 o 1 11 4 260.69 258.58 26.66 o 1 1 5 9.45 2.22 4.87 o 2 1 5 60.19 63.71 8.08 o 3 1 5 1140.65 1119.69 31.11 o 4 1 5 80.17 86.44 11.86 o 5 1 5 0.17 -3.03 17.58 o 0 2 5 0.34 -2.32 8.98 o 1 2 5 751.20 710.06 19.39 o 2 2 5 43.31 41.96 9.16 o 3 2 5 75.20 65.40 11.35 o 4 2 5 0.10 16.45 12.66 o 5 2 5 0.16 5.65 16.57 o 1 3 5 1034.32 1117.83 28.59 o 2 3 5 14.66 8.16 9.35 o 3 3 5 45.76 44.35 10.64 o 4 3 5 26.63 17.14 13.18 o 5 3 5 47.26 96.97 21.10 o 0 4 5 3.72 -6.17 9.37 o 1 4 5 1159.70 1288.92 32.32 o 2 4 5 1051.17 1066.42 32.94 o 3 4 5 35.69 17.81 10.96 o 4 4 5 23.24 38.83 14.26 o 5 4 5 71.83 75.11 24.02 o 1 5 5 18.33 37.16 8.91 o 2 5 5 27.71 30.68 10.71 o 3 5 5 278.86 278.65 15.99 o 4 5 5 397.49 425.37 26.89 o 5 5 5 85.31 42.52 27.25 o 0 6 5 31.90 23.11 12.09 o 1 6 5 7.72 11.74 9.53 o 2 6 5 321.17 355.51 18.82 o 3 6 5 135.16 100.39 18.55 o 4 6 5 56.99 69.13 22.03 o 5 6 5 14.34 20.72 27.07 o 1 7 5 19.19 3.25 12.15 o 2 7 5 44.13 37.08 14.42 o 3 7 5 48.49 74.58 19.47 o 4 7 5 15.88 -7.93 21.17 o 0 8 5 547.72 628.67 37.26 o 1 8 5 155.08 131.08 19.44 o 2 8 5 67.07 67.93 18.25 o 3 8 5 12.03 10.34 19.47 o 4 8 5 60.97 44.39 28.56 o 1 9 5 248.27 267.81 31.38 o 2 9 5 295.47 257.73 22.79 o 3 9 5 5.44 46.58 22.43 o 0 10 5 6.70 35.19 29.24 o 1 10 5 65.49 59.82 21.52 o 2 10 5 123.43 116.22 24.62 o 1 11 5 159.95 123.73 25.71 o 0 0 6 3562.02 2798.63 133.23 o 1 0 6 349.50 311.27 15.98 o 2 0 6 1.84 -9.35 11.97 o 3 0 6 1595.05 1655.00 66.80 o 4 0 6 22.67 12.06 18.04 o 5 0 6 24.20 30.65 22.28 o 1 1 6 1.72 -6.46 6.46 o 2 1 6 11.52 12.54 7.52 o 3 1 6 1488.84 1462.86 38.07 o 4 1 6 0.00 15.62 12.11 o 5 1 6 6.69 16.97 15.41 o 0 2 6 1618.21 1411.91 46.09 o 1 2 6 85.26 72.92 7.00 o 2 2 6 100.66 111.08 10.61 o 3 2 6 351.97 358.14 16.69 o 4 2 6 14.77 2.65 12.86 o 5 2 6 12.91 -7.97 16.41 o 1 3 6 582.78 590.82 15.88 o 2 3 6 33.55 27.39 10.35 o 3 3 6 38.33 30.65 10.48 o 4 3 6 84.13 66.68 13.98 o 5 3 6 24.68 40.15 30.29 o 0 4 6 117.22 107.18 10.75 o 1 4 6 17.55 20.52 6.60 o 2 4 6 464.88 470.14 17.71 o 3 4 6 87.10 86.27 11.89 o 4 4 6 251.48 221.68 17.08 o 5 4 6 133.26 108.95 24.61 o 1 5 6 1384.32 1491.11 37.55 o 2 5 6 473.20 473.69 19.18 o 3 5 6 84.48 90.01 12.81 o 4 5 6 117.37 140.56 20.90 o 5 5 6 3.78 -0.01 23.91 o 0 6 6 248.86 290.77 17.39 o 1 6 6 94.17 112.33 11.05 o 2 6 6 428.67 397.87 18.44 o 3 6 6 71.29 78.37 15.26 o 4 6 6 0.22 -18.44 18.44 o 1 7 6 44.97 46.42 10.70 o 2 7 6 236.44 253.42 16.73 o 3 7 6 48.00 40.95 17.84 o 4 7 6 3.82 1.81 26.74 o 0 8 6 6.36 -16.16 20.00 o 1 8 6 37.98 59.42 16.25 o 2 8 6 452.37 405.96 26.58 o 3 8 6 5.63 2.12 20.26 o 4 8 6 10.98 4.26 21.77 o 1 9 6 0.37 -7.47 17.99 o 2 9 6 293.24 223.50 22.07 o 3 9 6 0.46 -22.32 22.32 o 0 10 6 8.10 -30.14 30.14 o 1 10 6 25.57 1.72 20.50 o 2 10 6 29.96 47.04 22.20 o 1 11 6 95.96 70.72 24.16 o 1 1 7 297.95 283.64 11.67 o 2 1 7 1282.43 1218.09 33.41 o 3 1 7 35.17 42.64 9.09 o 4 1 7 48.79 31.19 13.91 o 5 1 7 7.55 3.53 16.36 o 0 2 7 766.25 655.83 24.75 o 1 2 7 238.92 245.54 11.19 o 2 2 7 1032.38 986.53 31.04 o 3 2 7 72.19 64.20 11.43 o 4 2 7 264.66 257.73 18.56 o 5 2 7 39.57 46.01 17.74 o 1 3 7 635.93 673.32 17.18 o 2 3 7 9.50 13.47 8.63 o 3 3 7 25.08 13.71 10.53 o 4 3 7 216.37 211.00 25.16 o 5 3 7 21.21 35.84 19.71 o 0 4 7 751.15 872.67 31.12 o 1 4 7 188.06 207.55 9.24 o 2 4 7 64.14 72.40 11.31 o 3 4 7 11.15 28.45 11.20 o 4 4 7 3.69 5.10 14.03 o 5 4 7 98.19 67.25 23.40 o 1 5 7 43.86 30.80 8.23 o 2 5 7 108.82 130.26 11.71 o 3 5 7 8.92 21.52 11.85 o 4 5 7 124.87 94.71 20.18 o 5 5 7 24.04 12.56 26.04 o 0 6 7 1111.12 1129.32 37.45 o 1 6 7 139.59 141.03 10.67 o 2 6 7 77.08 74.79 13.41 o 3 6 7 45.42 49.99 16.94 o 4 6 7 13.51 -19.03 19.03 o 1 7 7 2.12 10.66 11.72 o 2 7 7 12.71 16.29 13.79 o 3 7 7 0.14 10.12 18.66 o 4 7 7 22.17 -10.24 27.92 o 0 8 7 10.00 -14.48 16.50 o 1 8 7 216.27 225.19 19.02 o 2 8 7 45.65 52.54 16.07 o 3 8 7 20.25 -0.72 21.88 o 4 8 7 29.52 22.33 22.81 o 1 9 7 68.46 57.28 18.77 o 2 9 7 70.75 66.27 21.02 o 3 9 7 181.86 223.20 26.34 o 0 10 7 50.86 83.13 30.16 o 1 10 7 168.02 136.10 24.26 o 2 10 7 180.50 160.59 24.10 o 1 11 7 4.29 -23.00 41.40 o 0 0 8 14184.43 14444.99 816.49 o 1 0 8 1280.38 1092.42 41.29 o 2 0 8 548.80 568.90 27.75 o 3 0 8 6.52 10.22 14.47 o 4 0 8 20.84 45.49 18.56 o 5 0 8 72.52 59.08 30.40 o 1 1 8 878.69 750.34 20.49 o 2 1 8 78.21 83.92 7.81 o 3 1 8 61.80 61.13 9.07 o 4 1 8 250.86 221.84 16.00 o 5 1 8 1.44 -17.61 17.61 o 0 2 8 253.56 243.52 16.00 o 1 2 8 9.15 15.97 6.75 o 2 2 8 324.59 315.26 12.93 o 3 2 8 32.26 23.65 10.93 o 4 2 8 56.24 58.08 15.31 o 5 2 8 0.09 -15.02 24.24 o 1 3 8 12.40 17.87 7.19 o 2 3 8 189.21 205.04 11.33 o 3 3 8 33.08 40.54 12.03 o 4 3 8 20.86 14.14 15.52 o 5 3 8 33.78 42.68 22.73 o 0 4 8 44.51 50.47 10.18 o 1 4 8 1250.03 1262.77 29.85 o 2 4 8 745.75 778.85 22.86 o 3 4 8 3.33 7.49 11.06 o 4 4 8 256.14 284.51 20.56 o 5 4 8 18.90 -0.18 22.47 o 1 5 8 85.06 98.51 9.20 o 2 5 8 362.33 370.89 16.17 o 3 5 8 206.37 204.97 16.28 o 4 5 8 3.05 10.91 21.42 o 5 5 8 9.45 -7.85 23.64 o 0 6 8 57.24 75.09 12.48 o 1 6 8 117.92 130.52 10.28 o 2 6 8 4.58 1.73 11.35 o 3 6 8 0.02 -7.33 15.43 o 4 6 8 54.03 43.63 20.21 o 1 7 8 64.87 73.35 12.24 o 2 7 8 60.60 56.18 14.16 o 3 7 8 284.74 285.60 23.92 o 4 7 8 3.14 -21.91 31.42 o 0 8 8 262.13 264.58 21.41 o 1 8 8 138.27 146.27 15.04 o 2 8 8 35.83 35.78 15.57 o 3 8 8 71.23 56.18 20.62 o 1 9 8 14.08 19.38 16.00 o 2 9 8 73.64 55.18 20.13 o 3 9 8 0.09 -4.68 22.81 o 0 10 8 74.89 19.07 27.63 o 1 10 8 530.36 496.21 27.38 o 2 10 8 0.44 21.13 20.43 o 1 1 9 279.53 272.96 10.69 o 2 1 9 159.47 162.09 10.37 o 3 1 9 317.88 296.23 15.36 o 4 1 9 0.58 -4.52 14.07 o 5 1 9 6.87 45.20 20.91 o 0 2 9 206.15 219.05 13.88 o 1 2 9 270.37 279.89 10.16 o 2 2 9 369.69 383.85 13.91 o 3 2 9 27.26 32.36 11.38 o 4 2 9 86.52 68.87 15.64 o 5 2 9 74.09 67.75 19.23 o 1 3 9 1247.68 1277.42 29.90 o 2 3 9 0.17 -7.02 7.02 o 3 3 9 0.02 1.39 11.74 o 4 3 9 82.04 99.00 16.90 o 5 3 9 188.47 196.34 22.45 o 0 4 9 164.80 174.02 12.24 o 1 4 9 108.60 118.15 9.15 o 2 4 9 0.97 -8.68 8.68 o 3 4 9 41.18 19.77 12.05 o 4 4 9 0.93 -6.51 15.94 o 5 4 9 7.61 -22.36 22.36 o 1 5 9 30.71 30.57 7.83 o 2 5 9 174.01 183.15 13.62 o 3 5 9 14.75 22.48 13.80 o 4 5 9 51.71 61.73 19.30 o 5 5 9 0.13 -4.12 23.77 o 0 6 9 1772.97 1967.12 58.36 o 1 6 9 377.91 406.14 15.44 o 2 6 9 12.55 24.77 12.73 o 3 6 9 53.44 59.88 15.33 o 4 6 9 30.17 46.58 25.91 o 1 7 9 5.99 11.71 11.17 o 2 7 9 58.98 63.99 14.01 o 3 7 9 149.87 130.24 24.20 o 4 7 9 7.05 -11.83 23.26 o 0 8 9 2.35 -5.17 15.98 o 1 8 9 11.94 9.30 12.45 o 2 8 9 3.13 7.96 15.45 o 3 8 9 0.90 9.75 22.83 o 1 9 9 4.34 -2.88 16.14 o 2 9 9 2.28 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