#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:59:06 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180885 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/25/2102587.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2102587_Fobs loop_ _publ_author_name 'Harada, Jun' 'Harakawa, Mayuko' 'Ogawa, Keiichiro' _publ_section_title ; Torsional vibration and central bond length of N-benzylideneanilines ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 578 _journal_page_last 588 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 134.151 _cell_angle_gamma 90.000 _cell_length_a 6.6193 _cell_length_b 30.3811 _cell_length_c 7.5764 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7101 _cod_data_source_file bk50072_90Ksup5.hkl _cod_data_source_block 2_90K #BEGIN Tags that were not found in dictionaries: _shelx_title ' N-benzylidene-4-carboxyaniline at 90K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4388.27 4471.45 43.77 o 3 0 0 242.72 244.55 2.97 o 4 0 0 87.04 112.25 1.84 o 5 0 0 0.69 1.63 0.58 o 6 0 0 51.10 49.15 1.46 o 1 1 0 2049.40 2032.67 16.33 o 2 1 0 131.57 133.81 1.47 o 3 1 0 293.98 344.07 2.98 o 4 1 0 4.21 2.10 0.33 o 5 1 0 159.09 128.22 1.54 o 6 1 0 0.01 0.48 0.54 o 0 2 0 1598.54 1083.68 20.40 o 1 2 0 1005.17 1062.28 8.28 o 2 2 0 140.06 175.43 1.48 o 3 2 0 764.84 818.58 6.05 o 4 2 0 107.10 103.66 1.35 o 5 2 0 32.81 32.28 0.78 o 6 2 0 32.49 33.17 1.00 o 1 3 0 20.05 23.07 1.93 o 2 3 0 996.05 1043.60 7.44 o 3 3 0 31.01 29.87 0.72 o 4 3 0 21.86 16.65 0.88 o 5 3 0 1.24 1.67 0.41 o 6 3 0 0.50 1.08 0.56 o 0 4 0 0.10 0.82 0.06 o 1 4 0 904.14 897.31 7.84 o 2 4 0 452.51 482.15 5.54 o 3 4 0 651.52 630.57 4.76 o 4 4 0 289.91 257.06 2.33 o 5 4 0 127.09 103.98 1.36 o 6 4 0 7.40 11.75 0.76 o 1 5 0 7749.44 7904.27 76.63 o 2 5 0 91.94 106.91 0.92 o 3 5 0 24.54 33.23 1.10 o 4 5 0 59.87 56.90 1.06 o 5 5 0 0.01 0.61 0.39 o 6 5 0 32.79 31.47 1.46 o 0 6 0 12.35 10.01 0.19 o 1 6 0 4860.68 5151.89 66.32 o 2 6 0 7.18 7.37 0.65 o 3 6 0 17.93 26.87 0.55 o 4 6 0 6.12 10.58 0.48 o 5 6 0 0.30 0.44 0.44 o 6 6 0 61.87 68.45 1.39 o 1 7 0 13048.58 13157.03 289.37 o 2 7 0 113.71 141.46 1.16 o 3 7 0 556.51 540.70 3.82 o 4 7 0 1.53 1.97 0.34 o 5 7 0 28.87 26.66 0.82 o 6 7 0 1.33 2.13 0.68 o 0 8 0 1628.22 1647.35 16.73 o 1 8 0 5161.37 5337.85 75.68 o 2 8 0 119.19 130.41 1.56 o 3 8 0 0.06 0.85 0.26 o 4 8 0 215.05 211.29 2.02 o 5 8 0 4.91 5.59 0.54 o 6 8 0 0.12 1.58 0.66 o 1 9 0 1146.23 1133.85 7.38 o 2 9 0 705.10 760.40 5.50 o 3 9 0 78.70 87.86 0.91 o 4 9 0 105.73 119.29 1.53 o 5 9 0 66.87 57.70 1.13 o 6 9 0 107.78 101.54 1.65 o 0 10 0 93.07 93.82 0.93 o 1 10 0 421.31 431.17 2.93 o 2 10 0 95.34 81.57 1.09 o 3 10 0 35.49 35.54 0.58 o 4 10 0 179.37 172.50 1.95 o 5 10 0 75.71 70.97 1.25 o 6 10 0 0.16 0.91 0.58 o 1 11 0 14.05 20.05 0.60 o 2 11 0 6.61 18.83 1.37 o 3 11 0 202.94 192.71 1.61 o 4 11 0 0.13 0.20 0.38 o 5 11 0 60.53 59.94 1.31 o 6 11 0 28.47 29.68 1.03 o 0 12 0 690.32 681.83 5.28 o 1 12 0 31.21 30.54 0.41 o 2 12 0 1825.76 1837.93 12.13 o 3 12 0 62.68 56.29 0.81 o 4 12 0 43.97 39.59 0.89 o 5 12 0 19.35 20.35 0.79 o 6 12 0 37.13 40.54 1.25 o 1 13 0 89.93 115.56 0.97 o 2 13 0 701.81 763.30 5.16 o 3 13 0 31.19 30.68 0.62 o 4 13 0 5.33 6.01 0.50 o 5 13 0 3.38 3.35 0.53 o 6 13 0 70.04 74.40 1.62 o 0 14 0 70.65 67.84 0.75 o 1 14 0 106.25 116.58 1.21 o 2 14 0 2070.11 2091.01 16.10 o 3 14 0 79.25 67.30 0.91 o 4 14 0 8.69 7.03 0.82 o 5 14 0 2.91 1.83 0.52 o 6 14 0 0.94 2.25 0.69 o 1 15 0 539.99 583.12 4.10 o 2 15 0 1040.80 1065.61 7.10 o 3 15 0 62.87 56.57 0.84 o 4 15 0 24.79 25.08 0.88 o 5 15 0 10.34 9.70 0.66 o 6 15 0 6.06 10.17 0.87 o 0 16 0 229.64 233.87 2.03 o 1 16 0 34.67 47.48 1.63 o 2 16 0 871.61 888.53 6.00 o 3 16 0 10.72 15.46 0.70 o 4 16 0 220.38 213.03 2.32 o 5 16 0 10.43 12.02 0.78 o 6 16 0 69.76 85.20 1.75 o 1 17 0 37.99 36.63 1.68 o 2 17 0 20.23 26.74 1.12 o 3 17 0 500.22 478.35 3.81 o 4 17 0 295.37 280.25 2.57 o 5 17 0 268.71 263.15 3.22 o 6 17 0 0.99 1.06 0.71 o 0 18 0 10.26 14.96 0.40 o 1 18 0 947.02 944.26 6.30 o 2 18 0 102.99 111.60 1.09 o 3 18 0 50.15 56.58 1.89 o 4 18 0 78.47 80.18 1.57 o 5 18 0 12.71 14.72 0.86 o 6 18 0 0.00 0.10 0.70 o 1 19 0 155.48 171.80 2.70 o 2 19 0 293.11 316.09 2.41 o 3 19 0 586.23 584.20 4.56 o 4 19 0 341.21 325.37 3.18 o 5 19 0 18.04 19.34 0.94 o 0 20 0 73.68 71.00 1.33 o 1 20 0 596.00 621.03 4.29 o 2 20 0 372.87 386.87 2.88 o 3 20 0 1168.78 1159.98 9.37 o 4 20 0 78.55 82.30 1.85 o 5 20 0 16.72 16.31 0.90 o 1 21 0 37.01 48.46 1.45 o 2 21 0 1.95 3.45 0.40 o 3 21 0 180.05 194.92 3.35 o 4 21 0 201.64 192.26 2.20 o 5 21 0 98.29 99.77 1.81 o 0 22 0 100.46 94.90 1.22 o 1 22 0 52.58 56.50 0.71 o 2 22 0 27.67 26.46 0.55 o 3 22 0 62.82 71.64 2.03 o 4 22 0 14.93 19.16 0.76 o 5 22 0 1.51 3.16 0.96 o 1 23 0 270.29 265.92 1.94 o 2 23 0 6.73 8.59 0.73 o 3 23 0 746.53 728.07 6.16 o 4 23 0 2.94 6.25 0.66 o 5 23 0 186.03 190.77 2.68 o 0 24 0 0.15 2.96 1.00 o 1 24 0 43.21 50.54 0.80 o 2 24 0 56.72 57.90 0.83 o 3 24 0 235.83 239.51 3.04 o 4 24 0 395.11 393.45 3.81 o 5 24 0 0.17 3.53 0.84 o 1 25 0 5.83 7.13 0.33 o 2 25 0 153.67 148.75 1.56 o 3 25 0 0.65 1.27 0.44 o 4 25 0 145.03 149.18 1.94 o 5 25 0 7.46 8.02 0.83 o 0 26 0 17.43 18.24 1.45 o 1 26 0 171.00 166.03 1.40 o 2 26 0 18.29 23.57 0.80 o 3 26 0 10.54 15.09 0.70 o 4 26 0 213.04 212.37 2.46 o 5 26 0 1.95 3.50 0.74 o 1 27 0 25.08 27.44 0.54 o 2 27 0 2.07 3.44 0.40 o 3 27 0 218.55 203.59 2.29 o 4 27 0 10.11 18.33 1.17 o 5 27 0 103.59 107.70 1.98 o 0 28 0 1.91 2.17 0.48 o 1 28 0 4.75 4.97 0.37 o 2 28 0 83.04 78.64 1.11 o 3 28 0 80.37 77.72 1.33 o 4 28 0 303.10 297.85 3.17 o 5 28 0 57.56 67.12 1.59 o 1 29 0 38.49 40.02 0.70 o 2 29 0 54.69 59.17 0.96 o 3 29 0 58.01 66.67 1.22 o 4 29 0 8.33 6.51 0.77 o 0 30 0 230.82 221.55 4.28 o 1 30 0 14.41 15.07 0.57 o 2 30 0 371.48 353.44 3.10 o 3 30 0 191.67 179.26 2.16 o 4 30 0 22.16 25.61 0.94 o 1 31 0 47.78 45.16 0.84 o 2 31 0 84.11 87.63 1.42 o 3 31 0 2.18 4.95 0.70 o 4 31 0 20.21 24.44 0.94 o 0 32 0 68.49 64.87 1.78 o 1 32 0 20.12 18.83 0.64 o 2 32 0 24.86 25.70 0.67 o 3 32 0 6.22 7.63 0.66 o 4 32 0 5.43 9.51 0.76 o 1 33 0 0.44 1.15 0.41 o 2 33 0 0.61 1.57 0.41 o 3 33 0 0.27 -0.01 0.53 o 4 33 0 11.96 18.93 0.99 o 0 34 0 129.07 123.32 2.62 o 1 34 0 31.91 31.79 0.99 o 2 34 0 18.56 19.28 0.71 o 3 34 0 1.10 3.85 0.61 o 4 34 0 127.73 130.00 2.10 o 1 35 0 75.16 71.54 1.41 o 2 35 0 12.86 16.61 0.69 o 3 35 0 102.32 97.45 1.61 o 0 36 0 489.27 467.52 6.88 o 1 36 0 23.48 28.02 0.98 o 2 36 0 130.50 135.00 1.67 o 3 36 0 15.87 23.38 0.82 o 1 37 0 131.25 128.44 2.01 o 2 37 0 109.86 107.61 2.69 o 3 37 0 1.45 4.97 0.67 o 0 38 0 148.45 143.74 3.07 o 1 38 0 232.80 227.27 3.62 o 2 38 0 6.03 10.89 0.79 o 3 38 0 3.65 5.59 0.79 o 1 39 0 154.68 156.98 2.34 o 2 39 0 13.93 17.32 1.04 o 0 40 0 435.87 424.07 6.60 o 1 40 0 3.57 10.07 0.82 o 2 40 0 54.26 55.65 1.39 o 1 41 0 4.45 6.14 0.79 o 0 42 0 126.37 140.23 4.30 o 1 42 0 7.85 11.04 0.91 o -7 1 1 0.23 2.17 0.72 o -6 1 1 336.58 316.33 2.95 o -5 1 1 148.01 148.84 1.86 o -4 1 1 117.37 110.11 1.20 o -3 1 1 30.59 23.19 0.70 o -2 1 1 84.31 77.23 0.90 o -1 1 1 295.68 283.17 2.10 o 0 1 1 2886.07 2939.74 17.92 o 1 1 1 15.81 11.84 0.30 o 2 1 1 754.75 803.09 5.89 o 3 1 1 324.21 357.12 2.97 o 4 1 1 52.86 47.48 0.88 o 5 1 1 117.19 101.53 1.49 o 6 1 1 21.32 24.02 1.13 o -7 2 1 217.93 228.58 2.74 o -6 2 1 60.99 68.56 1.13 o -5 2 1 325.69 266.85 2.46 o -4 2 1 1.10 0.94 0.29 o -3 2 1 602.35 631.15 4.67 o -2 2 1 288.70 272.37 1.80 o -1 2 1 2.63 3.49 0.13 o 0 2 1 3900.50 3959.22 49.13 o 1 2 1 217.62 231.15 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1.21 0.61 o -5 11 1 39.97 38.10 0.90 o -4 11 1 15.45 17.01 0.66 o -3 11 1 77.54 86.39 0.87 o -2 11 1 13.05 7.89 0.33 o -1 11 1 305.36 315.03 2.19 o 0 11 1 14.68 19.96 0.29 o 1 11 1 531.43 554.95 3.79 o 2 11 1 178.20 199.14 1.62 o 3 11 1 391.90 349.92 2.94 o 4 11 1 78.64 69.62 1.22 o 5 11 1 17.81 22.10 0.86 o -6 12 1 6.84 9.12 0.77 o -5 12 1 66.29 61.00 1.11 o -4 12 1 131.22 123.12 1.33 o -3 12 1 144.64 134.85 1.20 o -2 12 1 693.65 722.68 6.10 o -1 12 1 710.82 717.69 5.18 o 0 12 1 0.21 0.49 0.17 o 1 12 1 2138.27 2348.15 15.13 o 2 12 1 1.11 1.61 0.22 o 3 12 1 178.51 194.33 1.87 o 4 12 1 17.92 19.49 0.77 o 5 12 1 132.55 122.75 1.79 o -6 13 1 65.74 68.12 1.65 o -5 13 1 30.13 26.71 0.81 o -4 13 1 37.15 38.20 0.88 o -3 13 1 44.87 36.73 0.57 o -2 13 1 198.11 188.79 1.59 o -1 13 1 340.62 345.44 2.41 o 0 13 1 1182.60 1231.69 7.57 o 1 13 1 0.52 1.82 0.26 o 2 13 1 72.38 76.88 0.83 o 3 13 1 199.71 181.22 1.79 o 4 13 1 169.16 162.39 1.99 o 5 13 1 12.05 14.03 1.00 o -6 14 1 4.87 6.92 0.73 o -5 14 1 4.96 5.67 0.62 o -4 14 1 9.17 20.72 1.82 o -3 14 1 88.94 82.18 0.88 o -2 14 1 2929.33 3096.81 21.76 o -1 14 1 267.05 254.00 1.85 o 0 14 1 205.30 223.08 2.03 o 1 14 1 137.20 157.54 1.70 o 2 14 1 0.00 0.56 0.22 o 3 14 1 374.84 325.83 2.80 o 4 14 1 115.35 117.78 1.64 o 5 14 1 19.91 18.76 0.85 o -6 15 1 30.39 33.53 1.11 o -5 15 1 0.04 -0.06 0.49 o -4 15 1 1644.80 1609.50 11.54 o -3 15 1 52.64 64.15 0.77 o -2 15 1 4233.32 4422.34 28.57 o -1 15 1 99.25 94.68 1.02 o 0 15 1 434.63 435.27 3.02 o 1 15 1 928.30 999.22 6.65 o 2 15 1 0.69 0.38 0.22 o 3 15 1 116.73 114.06 1.50 o 4 15 1 28.66 31.93 0.91 o 5 15 1 52.40 50.15 1.18 o -6 16 1 115.19 124.15 2.05 o -5 16 1 102.41 98.40 1.65 o -4 16 1 2564.51 2473.25 17.43 o -3 16 1 182.40 184.90 1.57 o -2 16 1 115.67 126.38 2.29 o -1 16 1 217.38 214.08 1.63 o 0 16 1 80.68 75.91 0.76 o 1 16 1 105.92 120.68 2.17 o 2 16 1 67.88 64.75 0.79 o 3 16 1 13.69 14.16 0.54 o 4 16 1 189.18 178.51 2.67 o 5 16 1 1.94 1.78 0.60 o -6 17 1 33.79 37.70 1.18 o -5 17 1 31.29 29.59 0.97 o -4 17 1 247.13 255.76 6.15 o -3 17 1 208.50 187.41 1.60 o -2 17 1 273.99 281.91 2.12 o -1 17 1 477.31 493.96 3.16 o 0 17 1 14.77 20.82 1.21 o 1 17 1 8.83 10.54 0.57 o 2 17 1 0.07 1.67 0.26 o 3 17 1 5.21 6.59 0.45 o 4 17 1 94.15 89.62 1.44 o 5 17 1 0.40 0.69 0.65 o -6 18 1 94.96 99.09 1.84 o -5 18 1 16.35 16.66 0.82 o -4 18 1 12.24 14.99 0.73 o -3 18 1 117.37 109.51 1.12 o -2 18 1 264.81 268.04 2.05 o -1 18 1 67.21 84.88 0.78 o 0 18 1 767.98 771.10 4.81 o 1 18 1 333.00 332.59 2.48 o 2 18 1 130.54 119.33 1.18 o 3 18 1 29.64 26.52 0.69 o 4 18 1 8.12 9.00 0.65 o 5 18 1 6.07 7.10 0.80 o -6 19 1 7.42 11.94 1.08 o -5 19 1 18.55 19.54 0.87 o -4 19 1 8.06 9.40 0.55 o -3 19 1 45.07 52.23 1.23 o -2 19 1 39.39 43.05 0.61 o -1 19 1 446.44 453.15 2.96 o 0 19 1 13.41 36.40 1.40 o 1 19 1 21.96 24.21 0.91 o 2 19 1 64.97 52.14 0.86 o 3 19 1 2.82 0.97 0.37 o 4 19 1 42.46 38.28 1.00 o 5 19 1 7.15 7.10 0.82 o -6 20 1 138.97 144.28 2.30 o -5 20 1 61.23 59.89 1.32 o -4 20 1 134.43 126.04 1.62 o 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24 8 174.09 164.32 2.61 o -5 24 8 107.51 122.54 3.11 o -4 24 8 39.22 45.38 1.21 o -3 24 8 10.71 15.11 1.18 o -6 25 8 52.29 47.58 1.25 o -5 25 8 164.61 166.30 2.62 o -4 25 8 43.16 44.74 1.38 o -3 25 8 39.44 42.48 2.20 o -6 26 8 69.51 67.80 1.58 o -5 26 8 77.90 80.36 1.77 o -4 26 8 39.89 38.66 1.32 o -6 27 8 4.79 4.07 0.70 o -5 27 8 14.53 17.60 1.05 o -4 27 8 20.83 25.56 1.43 o -5 28 8 27.08 29.90 1.25 o -9 1 9 24.12 24.67 1.16 o -8 1 9 56.32 60.83 1.54 o -7 1 9 0.28 0.28 0.62 o -6 1 9 73.78 78.72 1.70 o -5 1 9 124.11 123.84 2.18 o -4 1 9 103.08 103.81 1.74 o -3 1 9 1.52 1.34 0.63 o -2 1 9 65.53 66.45 1.63 o -9 2 9 43.39 48.79 1.44 o -8 2 9 57.62 60.07 1.53 o -7 2 9 24.58 28.90 1.12 o -6 2 9 172.59 175.84 2.68 o -5 2 9 16.01 17.63 0.98 o -4 2 9 129.85 131.19 1.99 o -3 2 9 5.34 6.59 0.74 o -2 2 9 32.18 34.53 1.26 o -9 3 9 128.29 134.03 2.34 o -8 3 9 87.47 90.63 1.86 o -7 3 9 110.30 110.73 2.04 o -6 3 9 84.96 87.28 1.79 o -5 3 9 4.51 4.78 0.63 o -4 3 9 11.28 13.39 0.81 o -3 3 9 1.35 1.73 0.72 o -2 3 9 15.71 22.71 1.13 o -9 4 9 284.24 326.46 4.82 o -8 4 9 73.42 74.40 1.69 o -7 4 9 129.72 118.46 2.12 o -6 4 9 0.31 0.63 0.62 o -5 4 9 84.61 80.14 1.50 o -4 4 9 170.82 163.22 2.28 o -3 4 9 14.32 18.23 1.05 o -2 4 9 13.76 17.45 1.06 o -8 5 9 44.31 47.86 1.39 o -7 5 9 0.60 1.32 0.65 o -6 5 9 144.71 141.65 2.34 o -5 5 9 7.86 14.36 0.79 o -4 5 9 67.76 72.17 1.46 o -3 5 9 119.27 124.72 2.22 o -2 5 9 55.76 57.90 1.80 o -8 6 9 106.02 104.89 2.01 o -7 6 9 149.35 141.87 2.35 o -6 6 9 2.44 3.82 0.60 o -5 6 9 459.49 453.66 4.60 o -4 6 9 8.71 10.55 0.76 o -3 6 9 47.76 48.93 1.43 o -8 7 9 59.49 57.35 1.51 o -7 7 9 9.15 12.25 0.90 o -6 7 9 12.76 15.13 0.81 o -5 7 9 78.24 77.25 1.47 o -4 7 9 160.93 155.32 2.21 o -3 7 9 39.27 40.13 1.33 o -8 8 9 0.90 1.54 0.85 o -7 8 9 21.61 22.31 1.37 o -6 8 9 32.66 33.53 1.02 o -5 8 9 4.17 4.46 0.63 o -4 8 9 0.02 1.17 0.59 o -3 8 9 7.23 9.01 1.05 o -8 9 9 0.78 0.68 0.85 o -7 9 9 7.14 8.35 0.85 o -6 9 9 0.28 0.81 0.55 o -5 9 9 11.86 11.60 0.77 o -4 9 9 16.39 17.34 0.90 o -3 9 9 33.96 35.47 1.43 o -8 10 9 72.14 82.41 2.83 o -7 10 9 65.40 70.76 1.42 o -6 10 9 40.22 33.36 1.18 o -5 10 9 129.81 130.49 1.97 o -4 10 9 37.38 32.08 1.06 o -3 10 9 8.06 9.70 0.90 o -8 11 9 1.15 3.91 0.96 o -7 11 9 139.19 137.25 2.02 o -6 11 9 41.52 41.77 1.12 o -5 11 9 115.72 121.08 1.89 o -4 11 9 21.93 24.42 0.97 o -3 11 9 24.07 29.66 1.22 o -8 12 9 37.51 45.19 1.69 o -7 12 9 81.12 83.05 1.74 o -6 12 9 0.35 0.53 0.56 o -5 12 9 14.36 20.43 0.91 o -4 12 9 23.21 25.77 1.01 o -3 12 9 12.18 20.72 1.11 o -8 13 9 65.84 70.79 2.05 o -7 13 9 72.26 74.58 1.67 o -6 13 9 1.03 1.51 0.59 o -5 13 9 21.03 20.88 0.92 o -4 13 9 9.66 11.87 0.83 o -3 13 9 41.72 46.36 1.44 o -8 14 9 329.91 359.55 4.42 o -7 14 9 13.82 15.36 0.97 o -6 14 9 69.90 75.34 1.49 o -5 14 9 6.11 5.51 0.68 o -4 14 9 85.25 85.84 1.62 o -3 14 9 54.87 64.98 1.64 o -8 15 9 84.53 104.57 2.67 o -7 15 9 21.44 21.76 1.09 o -6 15 9 2.23 3.54 0.65 o -5 15 9 3.16 3.92 0.65 o -4 15 9 8.75 9.20 0.88 o -3 15 9 51.70 58.47 1.58 o -8 16 9 43.88 46.24 1.75 o -7 16 9 238.02 247.29 3.51 o -6 16 9 184.00 182.18 2.77 o -5 16 9 30.28 32.08 1.07 o -4 16 9 13.28 17.68 0.97 o -3 16 9 40.73 52.76 1.52 o -7 17 9 5.86 11.28 0.93 o -6 17 9 71.44 82.04 1.77 o -5 17 9 21.16 19.77 0.93 o -4 17 9 72.55 81.87 1.60 o -7 18 9 12.59 14.61 1.13 o -6 18 9 25.50 29.55 1.19 o -5 18 9 19.40 21.49 0.95 o -4 18 9 29.68 35.24 1.14 o -7 19 9 1.99 2.29 0.76 o -6 19 9 56.78 45.11 1.39 o -5 19 9 7.05 7.54 0.85 o -4 19 9 54.95 68.27 1.49 o -7 20 9 17.26 19.26 1.11 o -6 20 9 0.26 1.26 0.72 o -5 20 9 32.16 27.66 1.20 o -4 20 9 0.22 1.74 0.67 o -6 21 9 1.47 2.03 0.75 o -5 21 9 3.97 5.97 0.78 o -6 22 9 50.15 52.61 1.53 o -5 22 9 30.26 30.32 1.53 o -8 0 10 0.01 1.00 1.05 o -7 0 10 0.90 2.86 1.03 o -6 0 10 31.37 32.90 2.55 o -5 0 10 15.69 25.27 1.71 o -4 0 10 133.31 141.13 3.55 o -8 1 10 14.38 15.63 1.21 o -7 1 10 79.41 77.30 1.80 o -6 1 10 42.30 47.93 1.48 o -5 1 10 167.94 167.05 2.74 o -4 1 10 84.02 93.34 2.03 o -8 2 10 0.05 0.61 0.73 o -7 2 10 0.01 0.72 0.71 o -6 2 10 13.36 16.95 1.07 o -5 2 10 130.28 136.38 2.44 o -4 2 10 36.98 43.26 1.49 o -8 3 10 38.33 32.95 1.29 o -7 3 10 19.57 24.84 1.16 o -6 3 10 55.66 69.68 1.72 o -5 3 10 54.91 61.67 1.63 o -4 3 10 201.24 225.98 3.34 o -8 4 10 0.01 0.15 0.73 o -7 4 10 52.30 60.48 1.60 o -6 4 10 97.76 106.26 2.11 o -5 4 10 0.38 0.69 0.73 o -4 4 10 3.70 9.58 0.86 o -8 5 10 11.90 11.80 1.39 o -7 5 10 156.72 164.15 2.69 o -6 5 10 1.35 4.10 0.79 o -5 5 10 5.41 5.91 0.87 o -4 5 10 261.99 300.11 3.57 o -8 6 10 2.48 3.19 0.80 o -7 6 10 21.04 23.97 1.16 o -6 6 10 0.09 -0.43 0.68 o -5 6 10 49.04 49.57 1.51 o -4 6 10 271.04 292.79 3.52 o -8 7 10 16.95 21.11 1.16 o -7 7 10 41.86 42.99 1.41 o -6 7 10 4.35 5.10 0.82 o -5 7 10 1.75 7.31 0.78 o -8 8 10 12.54 15.68 1.06 o -7 8 10 47.01 49.46 1.48 o -6 8 10 3.51 4.34 0.81 o -5 8 10 330.66 347.57 4.78 o -7 9 10 86.98 89.98 1.94 o -6 9 10 44.33 48.86 1.49 o -5 9 10 191.02 192.93 2.65 o -7 10 10 9.17 11.48 0.96 o -6 10 10 139.58 142.78 2.18 o -5 10 10 304.23 337.46 3.85 o -7 11 10 44.89 44.06 1.43 o -6 11 10 0.61 2.52 0.67 o -5 11 10 39.99 50.50 1.35 o -7 12 10 18.05 16.29 1.07 o -6 12 10 84.12 88.75 1.69 o -5 12 10 33.65 26.11 1.10 o -7 13 10 12.32 15.41 1.03 o -6 13 10 50.03 51.39 1.32 o -5 13 10 13.35 16.15 1.09 o -6 14 10 191.90 197.72 2.68 o