#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/33/2103303.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103303_Fobs loop_ _publ_author_name 'Yufit, D. S.' 'Kozhushkov, S. I.' 'Howard, J. A. K.' 'de Meijere, A.' _publ_section_title ; Crystal structure of 5-oxatricyclo[5.1.0.0^1,3^]octane-4-one: two polymorphs in one crystal ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 673 _journal_page_last 676 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.614 _cell_angle_gamma 90.000 _cell_length_a 9.9533 _cell_length_b 8.1831 _cell_length_c 7.8129 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.7068 _[local]_cod_data_source_file an0591sup2.hkl _[local]_cod_data_source_block b #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 62.56 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 237.14 253.16 1.73 o 2 0 0 3914.32 4296.39 84.87 o 3 0 0 409.16 448.35 14.53 o 5 0 0 702.97 743.79 6.24 o 6 0 0 1035.88 982.83 5.75 o 7 0 0 10.02 12.05 0.85 o 9 0 0 9.78 8.23 1.76 o 10 0 0 11.86 14.10 1.92 o 11 0 0 0.83 1.60 1.28 o 1 1 0 967.02 941.61 33.42 o 2 1 0 118.10 123.14 1.19 o 3 1 0 358.43 374.03 2.03 o 5 1 0 176.66 191.46 2.92 o 6 1 0 132.34 116.73 1.03 o 7 1 0 397.65 435.93 14.53 o 9 1 0 6.58 9.63 1.14 o 10 1 0 35.10 29.30 1.53 o 11 1 0 11.29 14.39 1.32 o 1 2 0 281.33 311.79 4.92 o 2 2 0 641.57 595.72 4.79 o 3 2 0 309.02 333.50 3.88 o 5 2 0 59.80 54.16 1.16 o 6 2 0 111.38 112.28 1.56 o 7 2 0 13.99 10.54 1.29 o 9 2 0 161.86 136.00 3.06 o 10 2 0 3.31 3.91 0.82 o 11 2 0 49.99 43.91 2.49 o 1 3 0 0.11 1.00 0.46 o 2 3 0 738.68 765.68 9.70 o 3 3 0 0.41 0.41 0.25 o 5 3 0 179.53 184.10 2.96 o 6 3 0 70.80 67.48 1.90 o 7 3 0 63.12 68.90 6.73 o 9 3 0 28.54 24.24 0.97 o 10 3 0 54.48 58.66 2.03 o 11 3 0 30.50 30.14 1.53 o 1 4 0 9.98 15.35 0.92 o 2 4 0 394.54 419.54 4.20 o 3 4 0 0.15 0.50 0.19 o 5 4 0 5.21 5.18 0.47 o 6 4 0 154.82 132.16 3.48 o 7 4 0 26.38 24.72 1.17 o 9 4 0 3.03 5.05 0.68 o 10 4 0 167.68 159.30 2.80 o 11 4 0 78.46 86.09 2.58 o 1 5 0 2.11 1.32 0.37 o 2 5 0 117.00 123.33 1.91 o 3 5 0 17.73 19.22 0.84 o 5 5 0 235.88 220.91 4.53 o 6 5 0 79.65 74.34 1.46 o 7 5 0 112.30 110.31 12.75 o 9 5 0 0.55 -0.04 0.62 o 10 5 0 5.57 6.99 0.90 o 11 5 0 7.07 12.44 2.86 o 1 6 0 5.31 5.94 0.51 o 2 6 0 220.46 215.81 2.39 o 3 6 0 51.91 52.84 1.38 o 5 6 0 37.88 39.83 1.07 o 6 6 0 32.55 30.91 1.03 o 7 6 0 0.07 0.21 0.50 o 9 6 0 6.13 6.73 1.28 o 10 6 0 73.00 78.80 2.43 o 11 6 0 26.06 28.90 2.02 o 1 7 0 198.74 194.68 4.67 o 2 7 0 286.36 260.54 3.26 o 3 7 0 1117.27 1039.05 17.76 o 5 7 0 76.13 74.83 2.32 o 6 7 0 6.52 6.12 0.68 o 7 7 0 2.89 7.43 1.48 o 9 7 0 109.13 118.45 2.52 o 10 7 0 25.21 26.93 1.55 o 1 8 0 56.10 51.16 2.24 o 2 8 0 35.64 27.11 1.35 o 3 8 0 0.24 0.76 2.14 o 5 8 0 189.16 185.50 7.25 o 6 8 0 2.48 2.09 0.95 o 7 8 0 38.60 36.70 2.23 o 9 8 0 4.02 8.33 2.56 o 1 9 0 102.20 110.61 4.05 o 2 9 0 21.99 21.41 1.42 o 3 9 0 4.26 5.04 1.26 o 5 9 0 7.49 7.12 1.04 o 6 9 0 44.18 48.06 2.72 o 7 9 0 2.09 2.26 0.98 o 1 10 0 12.22 17.21 1.59 o 2 10 0 0.35 0.11 0.92 o 3 10 0 33.26 31.83 2.84 o 5 10 0 1.30 1.62 0.98 o 6 10 0 5.57 3.20 1.92 o 1 11 0 24.79 23.97 2.14 o 2 11 0 4.75 3.84 1.36 o 3 11 0 37.52 42.38 3.04 o -13 1 1 2.87 4.49 1.92 o -11 1 1 13.96 14.17 2.56 o -10 1 1 0.43 0.69 0.82 o -9 1 1 209.21 210.77 3.38 o -7 1 1 71.53 67.01 1.08 o -6 1 1 0.35 1.15 0.21 o -5 1 1 124.88 164.00 3.27 o -3 1 1 1754.39 1733.56 19.17 o -2 1 1 157.32 145.26 1.69 o -1 1 1 2826.47 2785.15 27.40 o 1 1 1 2326.33 2302.06 28.23 o 2 1 1 276.87 276.57 1.25 o 3 1 1 2631.58 2625.78 20.13 o 5 1 1 527.37 551.90 4.33 o 6 1 1 1.07 2.51 0.34 o 7 1 1 34.13 27.66 1.22 o 9 1 1 121.46 115.46 2.59 o 10 1 1 34.54 32.66 1.53 o 11 1 1 0.19 -0.92 0.92 o -11 2 1 0.55 0.94 0.83 o -10 2 1 60.83 60.54 2.57 o -9 2 1 212.99 197.34 2.68 o -7 2 1 305.87 280.77 4.15 o -6 2 1 14.02 13.49 0.62 o -5 2 1 45.01 58.89 1.21 o -3 2 1 326.56 370.73 2.79 o -2 2 1 2261.62 2394.01 24.94 o -1 2 1 0.40 0.32 0.23 o 1 2 1 6.76 8.73 0.63 o 2 2 1 2056.86 2135.45 24.58 o 3 2 1 79.64 81.50 1.84 o 5 2 1 9.32 9.19 0.83 o 6 2 1 30.95 36.79 1.10 o 7 2 1 468.29 430.80 5.54 o 9 2 1 36.90 28.42 1.17 o 10 2 1 17.81 21.04 1.41 o 11 2 1 38.86 47.97 1.97 o -11 3 1 0.00 0.35 0.85 o -10 3 1 6.38 4.75 0.71 o -9 3 1 119.50 104.81 1.79 o -7 3 1 30.74 26.97 2.57 o -6 3 1 17.30 19.09 1.20 o -5 3 1 359.59 390.23 3.92 o -3 3 1 13.08 12.11 0.49 o -2 3 1 892.35 967.19 10.22 o -1 3 1 322.96 340.99 5.20 o 1 3 1 279.50 275.83 7.21 o 2 3 1 44.79 44.34 0.58 o 3 3 1 182.71 203.43 6.57 o 5 3 1 31.35 31.25 1.03 o 6 3 1 55.59 64.20 1.76 o 7 3 1 2.23 4.58 1.16 o 9 3 1 4.13 2.87 0.69 o 10 3 1 13.52 16.19 1.09 o 11 3 1 1.28 1.60 0.85 o -11 4 1 2.40 1.60 0.75 o -10 4 1 59.52 60.87 1.71 o -9 4 1 54.90 56.91 1.44 o -7 4 1 76.00 77.22 2.98 o -6 4 1 100.12 110.48 2.17 o -5 4 1 397.12 420.87 4.02 o -3 4 1 9.79 14.51 1.72 o -2 4 1 553.35 569.87 13.15 o -1 4 1 1.14 1.28 0.32 o 1 4 1 289.83 273.33 4.90 o 2 4 1 7.11 10.64 0.56 o 3 4 1 87.23 95.67 10.14 o 5 4 1 53.04 51.89 1.28 o 6 4 1 1.39 2.35 0.51 o 7 4 1 1.64 1.27 0.83 o 9 4 1 79.09 78.28 1.75 o 10 4 1 0.03 0.10 0.82 o 11 4 1 0.29 1.50 0.92 o -11 5 1 5.54 6.60 1.16 o -10 5 1 0.44 0.96 0.63 o -9 5 1 3.09 3.07 0.78 o -7 5 1 683.39 659.06 14.06 o -6 5 1 52.09 49.12 1.16 o -5 5 1 579.09 551.09 9.58 o -3 5 1 3.20 3.99 0.44 o -2 5 1 65.66 80.67 1.43 o -1 5 1 387.35 396.97 4.95 o 1 5 1 333.07 380.94 16.46 o 2 5 1 0.28 1.00 0.27 o 3 5 1 0.26 0.21 0.37 o 5 5 1 454.62 397.11 11.79 o 6 5 1 6.20 11.95 1.13 o 7 5 1 238.76 214.05 2.60 o 9 5 1 67.07 74.30 2.50 o 10 5 1 11.70 11.83 1.10 o 11 5 1 9.02 8.31 1.22 o -11 6 1 3.94 3.18 1.25 o -10 6 1 1.37 0.84 0.78 o -9 6 1 32.63 33.02 2.03 o -7 6 1 0.97 4.13 0.80 o -6 6 1 372.10 326.36 8.09 o -5 6 1 1.51 0.83 0.56 o -3 6 1 177.43 160.37 1.77 o -2 6 1 124.22 114.55 1.47 o -1 6 1 41.43 48.99 3.46 o 1 6 1 766.29 748.30 22.02 o 2 6 1 9.82 8.82 0.70 o 3 6 1 164.81 148.37 2.05 o 5 6 1 0.18 0.16 0.48 o 6 6 1 422.62 366.98 3.67 o 7 6 1 24.94 26.26 4.26 o 9 6 1 15.10 20.10 1.29 o 10 6 1 0.00 -0.89 0.89 o -10 7 1 1.94 1.58 0.94 o -9 7 1 0.02 0.29 0.89 o -7 7 1 7.95 7.78 0.80 o -6 7 1 39.44 38.50 1.35 o -5 7 1 2.53 1.60 0.60 o -3 7 1 3.96 9.21 2.77 o -2 7 1 106.92 108.47 2.42 o -1 7 1 36.78 42.77 1.19 o 1 7 1 15.13 22.01 1.34 o 2 7 1 105.45 103.82 2.96 o 3 7 1 4.44 7.62 1.12 o 5 7 1 15.55 13.95 1.34 o 6 7 1 60.68 56.77 2.54 o 7 7 1 1.72 2.72 0.80 o 9 7 1 15.97 18.45 1.35 o -9 8 1 65.56 63.48 2.86 o -7 8 1 0.99 2.45 0.79 o -6 8 1 24.16 23.02 1.65 o -5 8 1 33.44 35.85 1.53 o -3 8 1 3.59 2.48 0.60 o -2 8 1 12.99 13.56 0.83 o -1 8 1 0.11 4.30 2.92 o 1 8 1 31.84 26.15 1.12 o 2 8 1 2.85 2.27 0.59 o 3 8 1 28.37 26.44 1.71 o 5 8 1 34.00 40.29 3.45 o 6 8 1 25.53 26.95 1.62 o 7 8 1 0.12 0.50 0.79 o 9 8 1 49.38 48.70 3.52 o -7 9 1 18.14 21.63 1.53 o -6 9 1 14.89 15.05 1.97 o -5 9 1 109.85 113.73 3.55 o -3 9 1 51.96 49.21 2.07 o -2 9 1 0.69 2.09 1.09 o -1 9 1 24.57 23.99 1.43 o 1 9 1 28.70 25.12 1.29 o 2 9 1 2.49 5.61 1.09 o 3 9 1 52.19 50.75 1.78 o 5 9 1 66.11 69.62 2.28 o 6 9 1 22.67 22.81 1.66 o 7 9 1 0.00 -1.60 1.60 o -5 10 1 8.93 13.89 2.67 o -3 10 1 2.17 -0.12 0.85 o -2 10 1 2.69 3.36 1.13 o -1 10 1 0.88 0.07 1.00 o 1 10 1 29.18 31.38 2.08 o 2 10 1 2.88 1.92 0.92 o 3 10 1 34.52 33.07 1.78 o 5 10 1 1.89 3.12 1.23 o -3 11 1 1.54 2.34 1.84 o -2 11 1 53.78 58.31 3.84 o -1 11 1 1.57 2.88 1.92 o 1 11 1 6.01 5.19 1.76 o 2 11 1 19.07 19.69 1.92 o 3 11 1 0.65 0.64 1.92 o -13 0 2 0.39 -1.60 1.60 o -11 0 2 43.10 42.61 2.88 o -10 0 2 41.34 34.60 2.56 o -9 0 2 9.40 8.33 1.60 o -7 0 2 74.21 77.24 1.66 o -6 0 2 496.94 513.69 15.35 o -5 0 2 299.56 355.97 7.54 o -3 0 2 356.26 328.01 8.22 o -2 0 2 3656.41 3775.12 117.22 o -1 0 2 662.65 621.12 13.78 o 1 0 2 295.58 255.23 14.12 o 2 0 2 26.79 37.75 1.02 o 3 0 2 402.42 374.12 6.34 o 5 0 2 83.25 84.44 2.08 o 6 0 2 179.82 173.65 6.57 o 7 0 2 316.80 317.66 8.97 o 9 0 2 5.15 7.32 1.30 o 10 0 2 0.36 1.02 1.23 o 11 0 2 1.32 6.09 2.24 o -13 1 2 9.87 10.25 1.54 o -11 1 2 0.43 0.48 0.91 o -10 1 2 61.17 58.63 2.37 o -9 1 2 6.64 8.48 0.87 o -7 1 2 289.78 314.14 5.59 o -6 1 2 247.22 271.62 3.88 o -5 1 2 46.92 59.06 1.55 o -3 1 2 42.21 38.63 0.57 o -2 1 2 92.29 105.98 1.45 o -1 1 2 2458.19 2477.65 33.71 o 1 1 2 731.79 764.96 8.98 o 2 1 2 522.12 525.98 3.98 o 3 1 2 32.93 48.71 4.86 o 5 1 2 752.91 761.66 5.94 o 6 1 2 361.42 316.97 3.87 o 7 1 2 464.88 462.70 16.03 o 9 1 2 26.37 23.59 1.41 o 10 1 2 4.83 9.41 1.22 o 11 1 2 26.60 27.34 1.64 o -13 2 2 6.53 10.15 2.24 o -11 2 2 7.49 8.77 1.16 o -10 2 2 12.54 15.47 1.39 o -9 2 2 335.51 323.48 6.20 o -7 2 2 127.29 121.15 2.60 o -6 2 2 14.62 14.85 0.59 o -5 2 2 18.26 16.89 0.85 o -3 2 2 748.97 808.80 4.06 o -2 2 2 1299.45 1285.66 7.90 o -1 2 2 281.66 266.39 53.08 o 1 2 2 19.48 24.18 0.79 o 2 2 2 160.59 146.24 2.25 o 3 2 2 12.48 16.30 0.65 o 5 2 2 0.58 0.49 0.37 o 6 2 2 49.32 46.02 1.34 o 7 2 2 15.18 21.68 6.32 o 9 2 2 65.13 55.60 2.76 o 10 2 2 1.00 2.34 0.98 o 11 2 2 12.07 20.79 7.05 o -13 3 2 0.00 -0.32 2.24 o -11 3 2 86.96 84.83 3.98 o -10 3 2 16.09 14.00 0.96 o -9 3 2 2.95 0.77 0.53 o -7 3 2 2.43 2.14 0.53 o -6 3 2 22.43 27.33 0.71 o -5 3 2 374.92 363.69 3.85 o -3 3 2 12.39 9.83 0.43 o -2 3 2 359.98 414.48 6.87 o -1 3 2 369.47 364.81 4.31 o 1 3 2 0.19 1.02 0.18 o 2 3 2 152.11 133.47 3.86 o 3 3 2 0.97 0.00 0.26 o 5 3 2 21.05 28.08 2.03 o 6 3 2 66.08 69.35 2.87 o 7 3 2 78.27 84.15 5.38 o 9 3 2 18.66 16.34 1.07 o 10 3 2 55.01 52.72 3.89 o 11 3 2 0.08 0.72 1.04 o -11 4 2 74.70 83.21 2.12 o -10 4 2 75.41 74.49 1.66 o -9 4 2 11.73 14.14 0.83 o -7 4 2 19.35 21.75 1.24 o -6 4 2 303.77 309.40 2.91 o -5 4 2 58.25 58.73 0.96 o -3 4 2 94.29 111.66 10.94 o -2 4 2 716.65 753.52 11.67 o -1 4 2 0.82 4.53 0.62 o 1 4 2 9.11 10.33 0.50 o 2 4 2 0.65 1.32 0.27 o 3 4 2 121.74 110.00 8.53 o 5 4 2 31.86 26.91 2.96 o 6 4 2 24.21 16.34 0.87 o 7 4 2 36.32 55.51 12.58 o 9 4 2 5.74 6.75 0.93 o 10 4 2 89.91 89.49 2.19 o 11 4 2 30.92 31.72 2.88 o -11 5 2 53.67 53.30 1.88 o -10 5 2 0.43 -0.62 0.62 o -9 5 2 4.55 3.69 0.62 o -7 5 2 70.76 74.80 9.40 o -6 5 2 278.61 284.78 7.11 o -5 5 2 288.05 283.02 2.67 o -3 5 2 152.60 152.85 1.73 o -2 5 2 104.55 103.20 1.91 o -1 5 2 172.05 183.97 4.01 o 1 5 2 26.00 24.45 2.34 o 2 5 2 70.01 68.16 1.16 o 3 5 2 0.03 0.88 0.52 o 5 5 2 42.18 34.91 1.14 o 6 5 2 17.99 21.32 0.91 o 7 5 2 26.79 29.48 3.38 o 9 5 2 6.51 6.41 0.99 o 10 5 2 0.99 1.58 1.36 o -11 6 2 0.10 1.56 0.83 o -10 6 2 36.14 32.91 1.48 o -9 6 2 23.52 22.29 1.43 o -7 6 2 3.95 3.19 0.71 o -6 6 2 10.14 8.93 1.12 o -5 6 2 0.44 -0.07 0.63 o -3 6 2 43.64 46.22 1.78 o -2 6 2 304.32 297.72 10.54 o -1 6 2 20.44 20.21 1.65 o 1 6 2 31.28 36.00 1.29 o 2 6 2 289.86 274.69 3.25 o 3 6 2 220.14 207.00 4.52 o 5 6 2 39.44 43.93 4.16 o 6 6 2 0.47 0.21 0.74 o 7 6 2 9.95 8.50 1.04 o 9 6 2 17.95 16.36 1.22 o 10 6 2 72.12 78.18 4.49 o -10 7 2 17.93 20.10 2.27 o -9 7 2 86.54 86.55 3.04 o -7 7 2 19.93 20.58 1.13 o -6 7 2 0.18 -0.69 0.69 o -5 7 2 83.39 74.72 2.74 o -3 7 2 782.68 694.55 24.48 o -2 7 2 129.95 111.75 3.61 o -1 7 2 110.47 126.16 19.22 o 1 7 2 24.65 26.43 1.25 o 2 7 2 219.08 193.07 2.57 o 3 7 2 297.35 303.19 4.00 o 5 7 2 3.69 4.02 0.92 o 6 7 2 0.87 -0.21 0.79 o 7 7 2 2.51 0.37 0.73 o 9 7 2 27.68 30.20 2.72 o -10 8 2 39.00 47.42 3.52 o -9 8 2 0.06 -0.21 0.98 o -7 8 2 1.22 1.81 1.23 o -6 8 2 0.10 0.92 0.89 o -5 8 2 2.80 4.18 0.91 o -3 8 2 81.91 75.03 2.63 o -2 8 2 34.98 31.19 1.39 o -1 8 2 90.40 94.72 1.84 o 1 8 2 0.79 0.32 0.91 o 2 8 2 115.20 111.56 2.46 o 3 8 2 86.49 90.72 5.65 o 5 8 2 233.24 237.15 4.06 o 6 8 2 19.47 18.23 1.27 o 7 8 2 20.75 19.67 2.59 o -7 9 2 4.79 8.06 1.69 o -6 9 2 76.58 87.72 5.45 o -5 9 2 72.50 74.03 3.15 o -3 9 2 3.05 1.31 1.23 o -2 9 2 1.17 3.23 0.85 o -1 9 2 7.27 7.90 0.83 o 1 9 2 77.42 78.85 1.91 o 2 9 2 6.35 8.92 0.94 o 3 9 2 5.27 8.64 1.08 o 5 9 2 20.95 23.04 1.32 o 6 9 2 20.97 23.36 1.48 o 7 9 2 7.99 8.65 2.56 o -6 10 2 0.09 0.64 2.24 o -5 10 2 1.39 1.16 1.46 o -3 10 2 77.95 83.06 3.05 o -2 10 2 2.32 4.17 1.60 o -1 10 2 0.11 -0.96 1.60 o 1 10 2 35.06 40.82 1.78 o 2 10 2 10.28 10.18 1.16 o 3 10 2 5.45 8.24 1.22 o -3 11 2 17.90 24.99 2.88 o -2 11 2 2.17 2.24 1.92 o 1 11 2 10.08 12.50 2.56 o 2 11 2 2.18 -1.92 1.92 o -13 1 3 0.38 -1.13 1.13 o -11 1 3 27.41 23.48 1.92 o -10 1 3 56.53 57.52 1.78 o -9 1 3 234.70 247.16 6.75 o -7 1 3 362.73 331.92 5.98 o -6 1 3 18.86 21.45 0.88 o -5 1 3 0.42 0.53 0.25 o -3 1 3 38.70 40.43 1.00 o -2 1 3 937.97 888.66 21.13 o -1 1 3 168.73 190.01 4.20 o 1 1 3 40.42 43.59 0.71 o 2 1 3 132.28 141.73 1.37 o 3 1 3 1024.09 1078.01 16.50 o 5 1 3 327.40 327.82 3.77 o 6 1 3 8.90 14.89 1.01 o 7 1 3 13.88 10.57 1.28 o 9 1 3 25.83 23.79 1.41 o 10 1 3 40.92 40.69 1.91 o 11 1 3 1.20 5.13 1.92 o -13 2 3 36.73 32.53 2.04 o -11 2 3 40.14 41.96 1.66 o -10 2 3 13.40 18.95 1.22 o -9 2 3 244.92 245.30 2.63 o -7 2 3 28.72 25.48 0.89 o -6 2 3 4.85 5.90 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322.57 361.37 3.92 o -3 4 3 29.14 27.18 0.99 o -2 4 3 1508.86 1467.97 17.72 o -1 4 3 57.79 59.08 1.43 o 1 4 3 109.03 112.71 6.09 o 2 4 3 0.00 -0.16 0.26 o 3 4 3 15.11 19.67 1.84 o 5 4 3 21.83 26.81 1.07 o 6 4 3 4.77 4.38 0.71 o 7 4 3 0.50 1.60 0.65 o 9 4 3 6.07 4.51 1.28 o 10 4 3 7.20 7.70 1.36 o -11 5 3 4.95 7.94 1.80 o -10 5 3 24.30 24.00 1.24 o -9 5 3 5.30 5.86 0.81 o -7 5 3 284.07 262.02 8.69 o -6 5 3 67.38 63.53 2.22 o -5 5 3 89.41 90.73 1.60 o -3 5 3 55.88 55.31 1.62 o -2 5 3 10.41 12.06 0.64 o -1 5 3 7.12 10.82 0.79 o 1 5 3 19.71 27.33 0.97 o 2 5 3 0.00 -0.42 0.42 o 3 5 3 2.48 3.98 0.97 o 5 5 3 114.21 102.20 4.23 o 6 5 3 73.22 62.51 1.85 o 7 5 3 6.91 4.71 1.04 o 9 5 3 51.35 59.25 2.20 o 10 5 3 1.06 1.92 1.92 o -11 6 3 21.50 22.84 1.66 o -10 6 3 19.09 20.25 1.51 o -9 6 3 40.96 45.63 1.83 o -7 6 3 26.47 31.01 1.60 o -6 6 3 116.26 122.55 3.66 o -5 6 3 1.72 5.08 0.82 o -3 6 3 58.48 62.97 1.36 o -2 6 3 32.80 29.34 1.49 o -1 6 3 105.27 83.53 2.87 o 1 6 3 813.95 714.48 17.25 o 2 6 3 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