#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:59:55 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180893 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/33/2103322.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103322_Fobs
loop_
_publ_author_name
'Saraswathi, N.T.'
'Vijayan, M.'
_publ_section_title
;
 X-ray studies on crystalline complexes involving amino acids and
 peptides. XXXIX. Crystal structures of malonic acid complexes of
 <small>DL</small>- and <small>L</small>-histidine. Preservation of
 aggregation pattern on reversal of chirality
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              734
_journal_page_last               739
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 96.202
_cell_angle_gamma                90.000
_cell_length_a                   5.3643
_cell_length_b                   25.3538
_cell_length_c                   8.3043
_exptl_crystal_F_000             544.00
_reflns_d_resolution_high        .8208
_cod_data_source_file            de0016DLsup2.hkl
_cod_data_source_block           DL
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '(DL-Histidine complexed with Malonic  acid)'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            119.12
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x+1/2, -y+1/2, z+1/2'
'-x, -y, -z'
'-x-1/2, y-1/2, -z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 4.96 11.83 1.11 o
4 0 0 175.99 193.25 5.61 o
6 0 0 39.87 34.50 2.84 o
1 1 0 384.78 373.30 4.43 o
2 1 0 4016.40 4304.63 22.39 o
3 1 0 102.24 117.83 3.65 o
4 1 0 46.38 45.70 3.09 o
5 1 0 2.99 -.98 2.36 o
6 1 0 .43 .93 1.89 o
0 2 0 3.32 1.54 .64 o
1 2 0 1400.63 1322.24 8.39 o
2 2 0 5502.24 5604.57 25.69 o
3 2 0 4.94 5.63 2.17 o
4 2 0 1.46 -2.94 2.94 o
5 2 0 70.86 76.56 3.76 o
6 2 0 24.61 25.13 2.63 o
1 3 0 827.20 756.11 6.69 o
2 3 0 4023.97 4157.15 22.00 o
3 3 0 108.03 89.43 2.67 o
4 3 0 15.22 22.44 2.23 o
5 3 0 257.52 245.61 7.80 o
6 3 0 81.42 75.51 3.62 o
0 4 0 825.40 826.00 5.84 o
1 4 0 23.30 19.56 .95 o
2 4 0 541.28 517.91 7.97 o
3 4 0 237.32 263.01 7.41 o
4 4 0 52.81 53.95 3.06 o
5 4 0 18.89 18.61 2.90 o
6 4 0 2.07 4.42 2.57 o
1 5 0 1861.90 1956.28 12.01 o
2 5 0 204.07 224.65 5.44 o
3 5 0 83.91 89.93 2.68 o
4 5 0 48.44 55.84 3.22 o
5 5 0 40.12 35.77 3.38 o
6 5 0 98.96 95.50 3.68 o
0 6 0 8499.10 8144.56 24.18 o
1 6 0 7.76 11.65 .83 o
2 6 0 .01 3.90 1.14 o
3 6 0 1.63 -.20 .95 o
4 6 0 93.40 96.54 3.70 o
5 6 0 .06 -.96 2.03 o
6 6 0 1.29 .21 .99 o
1 7 0 209.18 160.56 4.09 o
2 7 0 344.92 346.23 7.26 o
3 7 0 116.39 127.35 3.64 o
4 7 0 299.20 303.99 8.91 o
5 7 0 2.37 6.08 3.02 o
6 7 0 .03 -.93 1.56 o
0 8 0 367.22 418.16 6.06 o
1 8 0 1819.85 1872.88 14.06 o
2 8 0 1.36 .46 1.07 o
3 8 0 .24 1.40 1.59 o
4 8 0 355.93 358.36 9.67 o
5 8 0 11.29 11.79 2.45 o
6 8 0 58.58 60.67 2.93 o
1 9 0 318.22 308.07 6.14 o
2 9 0 2006.89 2243.96 19.21 o
3 9 0 185.76 179.68 5.40 o
4 9 0 591.92 582.81 14.29 o
5 9 0 94.01 97.21 4.24 o
6 9 0 22.99 28.04 2.14 o
0 10 0 540.02 466.29 7.27 o
1 10 0 1125.84 1108.32 12.13 o
2 10 0 1322.77 1421.80 16.28 o
3 10 0 330.36 335.08 9.36 o
4 10 0 22.87 31.71 2.65 o
5 10 0 10.51 7.59 3.55 o
6 10 0 73.58 84.29 3.09 o
1 11 0 414.94 427.81 8.07 o
2 11 0 1755.22 1788.52 18.85 o
3 11 0 .01 6.73 1.43 o
4 11 0 667.84 682.80 15.47 o
5 11 0 260.07 279.37 8.32 o
6 11 0 32.76 34.34 2.13 o
0 12 0 1171.84 1173.68 13.40 o
1 12 0 1346.26 1328.04 14.76 o
2 12 0 381.20 412.09 9.56 o
3 12 0 229.22 245.17 7.37 o
4 12 0 124.63 116.37 4.21 o
5 12 0 11.63 9.76 2.06 o
1 13 0 6.44 3.74 1.74 o
2 13 0 625.12 709.26 12.55 o
3 13 0 11.81 11.38 1.77 o
4 13 0 367.29 367.07 10.05 o
5 13 0 52.63 48.38 2.99 o
0 14 0 935.52 888.46 12.85 o
1 14 0 194.50 196.30 5.46 o
2 14 0 280.20 268.96 7.28 o
3 14 0 284.15 307.50 8.73 o
4 14 0 4.48 5.79 1.78 o
5 14 0 .16 -2.08 2.08 o
1 15 0 42.07 43.10 2.03 o
2 15 0 12.16 8.08 2.41 o
3 15 0 63.08 62.35 3.18 o
4 15 0 85.53 89.29 4.07 o
5 15 0 1.15 4.34 2.15 o
0 16 0 52.96 62.56 2.34 o
1 16 0 196.14 208.52 6.21 o
2 16 0 23.49 27.40 2.11 o
3 16 0 21.15 16.31 2.23 o
4 16 0 205.53 205.80 6.17 o
5 16 0 19.80 22.83 2.18 o
1 17 0 61.12 63.96 2.80 o
2 17 0 12.13 10.36 3.20 o
3 17 0 1.92 .33 1.44 o
4 17 0 266.10 257.78 7.56 o
5 17 0 56.57 58.39 2.88 o
0 18 0 926.34 948.05 16.17 o
1 18 0 5.19 5.01 2.43 o
2 18 0 106.75 117.23 3.93 o
3 18 0 6.22 7.48 2.83 o
4 18 0 69.99 66.12 3.50 o
5 18 0 .03 3.27 1.75 o
1 19 0 5.92 9.64 1.42 o
2 19 0 10.76 4.23 2.43 o
3 19 0 .75 -1.95 1.95 o
4 19 0 44.66 44.17 2.86 o
5 19 0 6.78 11.65 1.47 o
0 20 0 76.19 65.36 3.04 o
1 20 0 59.57 57.36 3.05 o
2 20 0 .42 -2.18 2.18 o
3 20 0 38.20 42.49 2.89 o
4 20 0 112.78 125.99 4.07 o
1 21 0 404.93 435.52 12.35 o
2 21 0 3.08 1.68 2.42 o
3 21 0 40.76 41.53 2.86 o
4 21 0 4.56 5.25 2.15 o
0 22 0 119.49 119.29 4.11 o
1 22 0 1.62 .34 1.42 o
2 22 0 107.10 109.22 4.35 o
3 22 0 87.00 96.54 3.70 o
4 22 0 16.61 21.75 2.00 o
1 23 0 53.61 50.84 2.97 o
2 23 0 59.66 64.60 3.45 o
3 23 0 33.05 25.47 2.31 o
4 23 0 .76 -1.70 1.70 o
0 24 0 657.58 663.21 15.25 o
1 24 0 371.62 396.51 10.18 o
2 24 0 166.87 170.76 5.10 o
3 24 0 .16 1.21 1.70 o
4 24 0 2.83 3.57 1.55 o
1 25 0 38.19 41.62 2.95 o
2 25 0 116.82 109.80 3.94 o
3 25 0 .21 -2.08 2.08 o
0 26 0 4.91 3.96 2.35 o
1 26 0 2.25 1.46 2.14 o
2 26 0 .55 1.75 1.83 o
3 26 0 11.97 13.46 1.68 o
1 27 0 23.26 22.50 2.17 o
2 27 0 .93 5.63 1.72 o
3 27 0 3.00 .42 1.10 o
0 28 0 14.59 13.71 1.84 o
1 28 0 34.77 31.48 2.34 o
2 28 0 49.12 42.23 2.27 o
1 29 0 9.55 11.51 1.46 o
2 29 0 21.17 23.35 1.69 o
0 30 0 119.41 120.64 3.69 o
1 30 0 77.82 73.20 2.76 o
-5 0 1 430.68 405.77 11.92 o
-3 0 1 2414.26 2411.21 20.60 o
-1 0 1 3229.07 2851.74 12.47 o
1 0 1 10527.59 10591.41 130.59 o
3 0 1 281.09 278.35 7.40 o
5 0 1 5.53 2.37 2.98 o
-6 1 1 44.61 42.40 2.89 o
-5 1 1 31.56 34.49 2.68 o
-4 1 1 297.95 314.64 8.35 o
-3 1 1 905.33 967.42 13.41 o
-2 1 1 1285.32 1285.99 11.63 o
-1 1 1 3678.60 3499.59 13.84 o
0 1 1 170.58 136.96 4.57 o
1 1 1 83.80 70.96 2.04 o
2 1 1 606.38 554.96 8.25 o
3 1 1 13.22 14.06 1.51 o
4 1 1 14.74 7.52 3.21 o
5 1 1 26.73 23.21 2.79 o
6 1 1 34.44 33.63 2.65 o
-6 2 1 31.36 25.95 2.60 o
-5 2 1 215.69 254.06 7.50 o
-4 2 1 61.54 58.28 2.98 o
-3 2 1 46.79 50.07 2.00 o
-2 2 1 46.11 35.61 1.36 o
-1 2 1 173.96 115.56 2.75 o
0 2 1 49.68 64.16 1.89 o
1 2 1 101.68 64.99 1.95 o
2 2 1 91.24 78.60 2.26 o
3 2 1 198.11 202.38 5.74 o
4 2 1 199.52 200.82 6.10 o
5 2 1 1.07 -.33 1.62 o
6 2 1 6.05 3.36 2.27 o
-6 3 1 57.82 50.56 3.06 o
-5 3 1 35.60 43.37 3.19 o
-4 3 1 267.35 263.22 7.85 o
-3 3 1 175.45 171.67 5.11 o
-2 3 1 152.35 155.37 4.36 o
-1 3 1 455.33 512.24 5.79 o
0 3 1 687.94 654.98 28.19 o
1 3 1 1337.27 1209.39 9.42 o
2 3 1 4051.06 3997.02 22.41 o
3 3 1 934.17 909.57 13.81 o
4 3 1 89.57 80.98 3.63 o
5 3 1 107.32 96.95 4.50 o
6 3 1 .00 1.86 2.14 o
-6 4 1 41.64 39.99 2.72 o
-5 4 1 8.92 4.09 3.12 o
-4 4 1 63.16 73.19 3.22 o
-3 4 1 1703.69 1746.91 18.62 o
-2 4 1 946.82 1021.10 11.20 o
-1 4 1 6062.35 6518.52 21.29 o
0 4 1 2428.52 2331.72 54.80 o
1 4 1 11702.72 11987.23 158.62 o
2 4 1 62.95 51.91 1.74 o
3 4 1 78.02 72.85 2.76 o
4 4 1 246.95 254.10 7.29 o
5 4 1 94.40 104.36 4.53 o
6 4 1 185.27 188.82 5.91 o
-6 5 1 11.49 9.59 2.75 o
-5 5 1 27.90 25.60 2.79 o
-4 5 1 167.79 169.53 5.07 o
-3 5 1 3.63 9.47 1.24 o
-2 5 1 131.54 126.49 3.63 o
-1 5 1 1170.49 1127.73 9.54 o
0 5 1 3173.06 2930.61 50.07 o
1 5 1 14190.18 15254.73 190.61 o
2 5 1 375.67 355.14 7.10 o
3 5 1 934.70 942.26 14.47 o
4 5 1 303.88 295.15 9.01 o
5 5 1 51.03 43.02 3.17 o
6 5 1 .37 2.73 2.20 o
-6 6 1 58.79 65.14 3.15 o
-5 6 1 235.15 225.16 7.26 o
-4 6 1 4.44 3.98 2.79 o
-3 6 1 81.31 71.14 2.49 o
-2 6 1 186.44 210.92 5.47 o
-1 6 1 561.23 562.06 7.03 o
0 6 1 797.36 682.21 4.99 o
1 6 1 12455.10 13042.78 37.14 o
2 6 1 646.33 662.36 10.05 o
3 6 1 20.57 23.67 1.83 o
4 6 1 205.09 199.11 6.07 o
5 6 1 .24 4.37 2.61 o
6 6 1 294.55 276.37 7.60 o
-6 7 1 154.69 146.73 4.23 o
-5 7 1 41.43 41.79 3.13 o
-4 7 1 1.95 3.12 2.23 o
-3 7 1 163.78 161.42 4.95 o
-2 7 1 9.56 14.88 1.09 o
-1 7 1 1251.11 1258.37 11.02 o
0 7 1 1384.23 1234.38 45.39 o
1 7 1 2389.76 2551.53 16.45 o
2 7 1 3270.30 3384.02 22.90 o
3 7 1 407.48 386.83 9.79 o
4 7 1 222.66 224.55 6.45 o
5 7 1 .25 2.98 2.55 o
6 7 1 12.87 15.88 1.93 o
-6 8 1 112.76 104.93 3.72 o
-5 8 1 1.08 9.31 3.07 o
-4 8 1 197.71 197.96 5.87 o
-3 8 1 87.77 103.26 3.14 o
-2 8 1 12.87 15.51 1.22 o
-1 8 1 539.55 494.70 7.49 o
0 8 1 2137.16 2075.65 22.25 o
1 8 1 361.49 365.18 6.69 o
2 8 1 309.54 283.63 7.02 o
3 8 1 68.11 72.50 2.86 o
4 8 1 382.45 384.05 10.28 o
5 8 1 153.80 159.18 5.09 o
6 8 1 118.84 119.60 3.53 o
-6 9 1 9.70 3.03 2.13 o
-5 9 1 112.87 112.20 4.56 o
-4 9 1 370.24 367.35 9.80 o
-3 9 1 118.11 108.26 3.36 o
-2 9 1 148.29 161.08 4.61 o
-1 9 1 1182.04 1252.46 12.42 o
0 9 1 241.10 251.56 5.55 o
1 9 1 355.54 441.48 7.63 o
2 9 1 111.59 114.22 3.45 o
3 9 1 742.39 788.01 14.36 o
4 9 1 403.84 427.42 12.24 o
5 9 1 13.55 12.59 3.82 o
6 9 1 1.30 -.87 1.56 o
-6 10 1 4.17 3.29 1.90 o
-5 10 1 85.07 88.27 4.04 o
-4 10 1 136.31 136.78 4.56 o
-3 10 1 62.79 77.98 2.97 o
-2 10 1 25.65 31.86 1.67 o
-1 10 1 68.60 92.11 2.71 o
0 10 1 163.94 147.00 2.86 o
1 10 1 366.36 425.20 7.77 o
2 10 1 55.12 54.05 2.07 o
3 10 1 245.40 249.64 7.44 o
4 10 1 191.28 193.25 5.98 o
5 10 1 147.33 147.52 4.73 o
6 10 1 .53 3.74 1.79 o
-6 11 1 9.75 10.15 1.41 o
-5 11 1 47.07 42.58 2.98 o
-4 11 1 16.73 14.77 2.43 o
-3 11 1 1.02 3.20 2.09 o
-2 11 1 25.99 24.33 1.66 o
-1 11 1 397.05 397.67 7.78 o
0 11 1 66.26 64.18 3.60 o
1 11 1 12.95 13.61 1.24 o
2 11 1 1096.30 1147.84 15.53 o
3 11 1 166.84 173.41 5.13 o
4 11 1 30.68 27.19 2.59 o
5 11 1 30.59 27.55 2.54 o
-6 12 1 1.76 .13 .75 o
-5 12 1 119.36 124.33 4.35 o
-4 12 1 7.60 9.18 3.14 o
-3 12 1 348.07 347.01 10.27 o
-2 12 1 65.81 75.04 2.44 o
-1 12 1 223.87 234.82 6.39 o
0 12 1 1424.31 1415.64 19.81 o
1 12 1 374.97 385.30 8.19 o
2 12 1 2.42 7.44 2.16 o
3 12 1 16.21 19.97 2.16 o
4 12 1 43.67 53.16 3.33 o
5 12 1 63.47 67.22 3.31 o
-5 13 1 2.16 -2.34 2.34 o
-4 13 1 158.62 142.19 4.65 o
-3 13 1 2.78 3.82 2.28 o
-2 13 1 2.08 2.49 1.80 o
-1 13 1 697.39 745.76 11.77 o
0 13 1 22.93 19.95 2.75 o
1 13 1 96.59 91.73 2.83 o
2 13 1 555.77 636.39 12.56 o
3 13 1 118.38 131.63 4.17 o
4 13 1 13.42 15.45 2.33 o
5 13 1 2.16 1.04 1.86 o
-5 14 1 .04 2.89 1.96 o
-4 14 1 3.94 3.74 2.73 o
-3 14 1 101.95 111.63 3.98 o
-2 14 1 202.83 197.61 6.24 o
-1 14 1 244.22 274.71 7.58 o
0 14 1 110.89 105.15 3.24 o
1 14 1 51.89 48.85 2.07 o
2 14 1 202.06 180.06 5.41 o
3 14 1 32.66 32.02 2.51 o
4 14 1 13.44 11.20 2.34 o
5 14 1 .30 7.55 2.18 o
-5 15 1 9.10 6.35 2.68 o
-4 15 1 78.95 72.27 3.77 o
-3 15 1 384.21 399.50 11.56 o
-2 15 1 766.50 764.05 14.52 o
-1 15 1 287.79 297.50 8.35 o
0 15 1 141.12 163.46 5.34 o
1 15 1 781.44 826.58 13.94 o
2 15 1 8.35 9.02 1.58 o
3 15 1 43.02 41.88 2.78 o
4 15 1 6.25 10.66 1.97 o
5 15 1 42.99 44.44 2.78 o
-5 16 1 92.24 93.40 3.77 o
-4 16 1 241.14 247.70 7.41 o
-3 16 1 89.54 93.40 3.77 o
-2 16 1 147.19 161.56 4.78 o
-1 16 1 561.81 557.52 11.76 o
0 16 1 23.54 16.07 1.45 o
1 16 1 287.54 292.86 7.60 o
2 16 1 11.55 7.78 1.68 o
3 16 1 431.37 425.80 12.21 o
4 16 1 .19 5.79 2.46 o
5 16 1 3.11 .61 1.49 o
-5 17 1 44.59 46.52 2.66 o
-4 17 1 1.82 2.87 2.05 o
-3 17 1 513.12 519.75 13.49 o
-2 17 1 30.74 32.47 2.38 o
-1 17 1 134.51 135.69 4.07 o
0 17 1 1463.84 1414.89 18.01 o
1 17 1 357.12 340.30 9.68 o
2 17 1 4.53 1.21 2.01 o
3 17 1 .09 -2.13 2.13 o
4 17 1 30.64 33.40 2.64 o
5 17 1 8.83 9.22 1.68 o
-5 18 1 2.18 2.47 1.80 o
-4 18 1 51.93 54.64 2.98 o
-3 18 1 20.73 15.83 2.24 o
-2 18 1 93.07 96.68 3.70 o
-1 18 1 598.29 614.85 13.35 o
0 18 1 16.04 22.02 2.04 o
1 18 1 174.68 180.75 5.42 o
2 18 1 13.29 9.55 1.87 o
3 18 1 484.54 495.74 13.18 o
4 18 1 112.34 116.22 4.06 o
5 18 1 16.44 14.57 1.74 o
-5 19 1 11.06 13.07 1.55 o
-4 19 1 10.65 14.98 1.87 o
-3 19 1 52.86 52.19 3.01 o
-2 19 1 296.96 299.08 8.84 o
-1 19 1 13.67 13.22 2.10 o
0 19 1 4.20 3.77 1.96 o
1 19 1 58.47 58.80 3.19 o
2 19 1 241.36 236.41 7.03 o
3 19 1 69.95 68.11 3.66 o
4 19 1 2.20 .80 1.68 o
5 19 1 2.83 4.01 1.59 o
-4 20 1 6.56 6.45 2.76 o
-3 20 1 354.62 358.86 9.68 o
-2 20 1 426.77 416.13 12.07 o
-1 20 1 80.88 75.28 3.50 o
0 20 1 .94 .18 1.24 o
1 20 1 106.14 96.29 3.70 o
2 20 1 175.93 167.61 5.05 o
3 20 1 5.80 7.77 2.81 o
4 20 1 20.57 29.55 2.27 o
-4 21 1 31.18 32.70 2.31 o
-3 21 1 16.63 19.61 2.50 o
-2 21 1 .51 -2.13 2.13 o
-1 21 1 153.30 152.47 4.81 o
0 21 1 323.57 315.96 11.23 o
1 21 1 149.02 139.47 4.60 o
2 21 1 31.85 30.51 2.60 o
3 21 1 16.94 12.97 2.03 o
4 21 1 31.41 33.71 2.50 o
-4 22 1 28.82 30.96 2.24 o
-3 22 1 71.46 73.42 3.46 o
-2 22 1 82.86 89.92 4.08 o
-1 22 1 18.65 23.41 2.41 o
0 22 1 4.71 4.30 2.86 o
1 22 1 2.46 1.02 2.09 o
2 22 1 130.38 116.52 4.50 o
3 22 1 243.66 222.77 6.62 o
4 22 1 12.42 12.92 1.84 o
-4 23 1 67.35 74.23 2.90 o
-3 23 1 190.71 173.60 5.31 o
-2 23 1 32.21 33.16 2.63 o
-1 23 1 16.14 18.32 2.24 o
0 23 1 303.59 297.22 6.39 o
1 23 1 .55 3.72 2.05 o
2 23 1 18.81 14.21 2.13 o
3 23 1 .34 3.64 1.82 o
4 23 1 6.04 5.69 1.83 o
-4 24 1 1.71 4.17 1.62 o
-3 24 1 15.73 13.36 1.96 o
-2 24 1 37.85 37.15 2.70 o
-1 24 1 18.56 14.16 2.28 o
0 24 1 56.02 54.38 2.38 o
1 24 1 333.67 349.46 9.55 o
2 24 1 30.42 32.47 2.68 o
3 24 1 18.40 15.72 1.97 o
-3 25 1 5.91 9.18 1.47 o
-2 25 1 29.98 28.54 2.58 o
-1 25 1 31.00 35.69 2.57 o
0 25 1 6.82 6.41 2.01 o
1 25 1 6.43 6.52 2.78 o
2 25 1 38.95 41.70 2.61 o
3 25 1 25.09 23.93 2.10 o
-3 26 1 17.64 13.31 1.72 o
-2 26 1 52.27 46.80 2.66 o
-1 26 1 62.60 61.61 3.27 o
0 26 1 75.99 87.01 2.70 o
1 26 1 .02 1.70 1.95 o
2 26 1 1.42 .72 1.58 o
3 26 1 8.35 10.45 1.52 o
-3 27 1 .76 -1.54 1.54 o
-2 27 1 24.76 26.84 2.16 o
-1 27 1 48.40 47.54 2.78 o
0 27 1 32.62 40.87 5.18 o
1 27 1 .01 1.77 1.61 o
2 27 1 65.84 76.09 3.17 o
3 27 1 45.48 54.25 2.38 o
-2 28 1 5.44 3.90 1.96 o
-1 28 1 111.85 107.83 3.91 o
0 28 1 48.90 46.50 1.85 o
1 28 1 1.52 3.46 1.90 o
2 28 1 .00 -1.17 1.31 o
-2 29 1 60.60 71.93 2.51 o
-1 29 1 338.60 366.91 8.76 o
0 29 1 102.53 109.45 2.49 o
1 29 1 1.06 2.51 1.54 o
2 29 1 8.59 8.27 1.43 o
-1 30 1 5.35 7.52 1.40 o
0 30 1 1.82 1.40 1.41 o
1 30 1 101.48 104.25 3.16 o
-6 0 2 20.78 21.13 2.16 o
-4 0 2 9.88 13.61 1.88 o
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0 0 2 307.48 329.40 3.28 o
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0 17 8 .92 .10 1.50 o
1 17 8 .18 2.66 1.58 o
-1 18 8 9.64 7.38 1.85 o
0 18 8 72.97 74.25 1.92 o
-3 0 9 12.75 9.72 1.43 o
-1 0 9 371.63 328.27 9.75 o
1 0 9 8.92 15.24 2.00 o
-3 1 9 13.59 15.88 1.61 o
-2 1 9 67.11 77.62 3.08 o
-1 1 9 11.23 13.81 1.90 o
0 1 9 84.61 85.73 2.80 o
1 1 9 37.95 34.65 2.45 o
2 1 9 24.46 24.53 2.00 o
-3 2 9 2.43 2.33 1.70 o
-2 2 9 190.10 180.41 5.60 o
-1 2 9 67.61 78.22 3.45 o
0 2 9 25.45 24.76 2.73 o
1 2 9 9.74 9.47 2.89 o
2 2 9 20.82 25.40 1.83 o
-3 3 9 12.13 21.13 1.73 o
-2 3 9 10.00 12.49 1.81 o
-1 3 9 33.64 33.24 2.48 o
0 3 9 5.05 5.90 1.66 o
1 3 9 209.29 217.37 6.54 o
2 3 9 9.49 11.70 1.52 o
-3 4 9 27.80 34.02 2.12 o
-2 4 9 2.53 .68 1.54 o
-1 4 9 15.98 18.90 1.81 o
0 4 9 24.85 27.91 2.69 o
1 4 9 4.20 .00 .05 o
2 4 9 4.53 3.93 1.73 o
-3 5 9 23.49 27.19 2.03 o
-2 5 9 1.41 3.57 1.52 o
-1 5 9 8.20 10.06 1.66 o
0 5 9 45.25 40.61 1.88 o
1 5 9 .47 2.96 1.80 o
2 5 9 8.87 5.79 1.91 o
-3 6 9 19.78 15.29 1.63 o
-2 6 9 13.20 16.53 1.86 o
-1 6 9 .23 -1.93 1.93 o
0 6 9 19.49 19.56 1.38 o
1 6 9 9.09 8.98 1.57 o
2 6 9 17.82 18.15 1.77 o
-3 7 9 .69 .60 1.02 o
-2 7 9 35.09 39.56 2.54 o
-1 7 9 30.98 34.97 2.47 o
0 7 9 11.41 10.84 1.60 o
1 7 9 21.35 26.42 2.07 o
-3 8 9 11.22 11.56 1.46 o
-2 8 9 29.53 33.63 2.26 o
-1 8 9 6.29 6.05 2.48 o
0 8 9 88.44 86.60 3.19 o
1 8 9 17.09 30.07 2.21 o
-2 9 9 4.61 3.82 1.42 o
-1 9 9 87.15 83.55 3.44 o
0 9 9 9.83 11.61 1.16 o
1 9 9 147.26 145.60 4.38 o
-2 10 9 80.41 77.40 2.96 o
-1 10 9 89.92 90.57 3.32 o
0 10 9 10.52 8.85 1.36 o
1 10 9 .03 -1.21 1.38 o
-2 11 9 182.11 181.17 4.89 o
-1 11 9 32.01 36.66 2.36 o
0 11 9 25.70 24.71 2.06 o
1 11 9 48.09 43.28 2.21 o
-2 12 9 .78 2.14 1.48 o
-1 12 9 37.88 33.95 2.11 o
0 12 9 44.13 49.21 2.31 o
-1 13 9 54.02 55.75 2.41 o
0 13 9 4.71 7.80 1.90 o
-1 14 9 4.91 2.14 1.55 o
0 0 10 7.69 10.58 1.14 o
-1 1 10 3.04 1.77 1.61 o
0 1 10 21.56 23.62 1.29 o
-1 2 10 20.82 19.67 1.73 o
0 2 10 107.37 112.42 2.57 o
-1 3 10 34.76 32.78 2.08 o
0 3 10 134.33 149.46 3.08 o
-1 4 10 20.20 20.82 1.78 o