#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103492.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103492_Fobs loop_ _publ_author_name 'W\'ojcik, Gra\.zyna' 'Mossakowska, Izabela' 'Holband, Jolanta' 'Bartkowiak, Wojciech' _publ_section_title ; Atomic thermal motions studied by variable-temperature X-ray diffraction and related to non-linear optical properties of crystalline meta-di-nitrobenzene ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 998 _journal_page_last 1004 _journal_volume 58 _journal_year 2002 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.0520 _cell_length_b 13.2240 _cell_length_c 3.7140 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.6862 _[local]_cod_data_source_file ns0009160sup4.hkl _[local]_cod_data_source_block 160 #BEGIN Tags that were not found in dictionaries: _shelx_title ' dnb160 in Pna2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 101.48 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -5 1.63 7.59 1.60 o 4 0 -5 62.03 81.11 2.23 o 0 1 -5 3.46 4.36 2.67 o 1 1 -5 8.06 13.03 2.53 o 2 1 -5 13.19 20.14 3.53 o 3 1 -5 5.83 5.88 1.19 o 4 1 -5 28.48 42.33 1.99 o 5 1 -5 8.45 7.85 1.18 o 7 1 -5 1.25 1.67 1.05 o 1 2 -5 0.36 1.52 0.53 o 2 2 -5 22.53 25.99 1.67 o 3 2 -5 10.74 9.47 1.30 o 4 2 -5 16.52 19.21 1.63 o 5 2 -5 2.38 2.80 0.99 o 6 2 -5 13.35 14.40 1.92 o 7 2 -5 16.13 15.35 1.95 o 0 3 -5 18.34 16.48 1.51 o 1 3 -5 0.31 1.34 0.85 o 2 3 -5 3.05 1.69 0.70 o 3 3 -5 0.78 1.13 0.60 o 4 3 -5 1.33 1.62 0.69 o 5 3 -5 0.35 0.51 0.64 o 6 3 -5 2.04 1.57 0.79 o 7 3 -5 5.11 3.13 1.23 o 1 4 -5 9.46 7.19 1.02 o 2 4 -5 10.03 7.08 1.18 o 3 4 -5 3.89 1.53 0.81 o 4 4 -5 1.48 1.16 0.67 o 5 4 -5 0.13 0.72 0.94 o 6 4 -5 2.09 1.50 1.12 o 0 5 -5 10.03 7.57 1.75 o 1 5 -5 0.88 0.33 0.53 o 2 5 -5 3.00 1.23 0.77 o 3 5 -5 6.80 4.07 1.00 o 4 5 -5 4.61 6.00 1.58 o 1 6 -5 1.32 0.52 0.82 o 2 6 -5 3.09 1.71 1.26 o 3 6 -5 4.22 2.54 1.28 o 2 7 -5 3.09 2.30 1.20 o 0 0 -4 41.74 43.41 4.03 o 2 0 -4 22.37 21.79 1.08 o 4 0 -4 138.08 146.28 3.32 o 6 0 -4 43.68 60.39 4.16 o 8 0 -4 125.57 119.51 13.44 o 10 0 -4 27.00 18.88 9.51 o 12 0 -4 25.22 16.96 10.37 o 1 1 -4 3.82 3.14 0.44 o 2 1 -4 10.37 10.27 0.61 o 3 1 -4 16.81 17.64 0.61 o 4 1 -4 6.72 9.12 0.83 o 5 1 -4 7.62 11.13 1.32 o 6 1 -4 308.96 373.55 3.29 o 7 1 -4 42.91 37.22 6.48 o 8 1 -4 2.09 3.62 0.72 o 9 1 -4 2.71 2.48 0.58 o 10 1 -4 0.12 0.52 0.54 o 11 1 -4 5.14 4.38 0.83 o 12 1 -4 2.35 1.53 0.82 o 13 1 -4 4.87 0.63 0.74 o 0 2 -4 87.05 97.43 5.56 o 1 2 -4 1.45 1.74 0.44 o 2 2 -4 0.26 2.22 0.61 o 3 2 -4 0.10 1.10 0.32 o 4 2 -4 5.69 5.19 0.62 o 5 2 -4 35.84 38.98 1.96 o 6 2 -4 2.05 5.56 1.34 o 7 2 -4 22.12 20.73 1.99 o 8 2 -4 15.36 13.04 1.32 o 9 2 -4 15.88 16.12 1.49 o 10 2 -4 0.05 1.73 0.52 o 11 2 -4 1.95 1.46 0.60 o 12 2 -4 12.31 8.99 2.30 o 13 2 -4 1.20 2.54 1.45 o 1 3 -4 23.29 24.67 1.14 o 2 3 -4 45.84 48.45 1.19 o 3 3 -4 6.31 6.01 0.74 o 4 3 -4 1.06 0.68 0.42 o 5 3 -4 22.53 22.45 1.02 o 6 3 -4 29.39 26.86 3.40 o 7 3 -4 4.37 5.10 0.68 o 8 3 -4 5.67 4.79 0.75 o 9 3 -4 11.89 9.76 1.49 o 10 3 -4 5.72 3.41 0.65 o 11 3 -4 7.51 5.25 1.25 o 12 3 -4 9.68 10.22 1.73 o 13 3 -4 0.65 1.69 0.94 o 0 4 -4 79.10 79.59 5.10 o 1 4 -4 14.83 14.46 1.31 o 2 4 -4 0.63 1.22 0.48 o 3 4 -4 8.17 10.14 1.25 o 4 4 -4 1.69 1.02 0.49 o 5 4 -4 11.61 12.59 0.79 o 6 4 -4 6.71 9.86 1.79 o 7 4 -4 16.53 16.57 1.63 o 8 4 -4 4.50 5.74 0.80 o 9 4 -4 1.25 1.10 0.48 o 10 4 -4 5.64 4.28 0.65 o 11 4 -4 1.41 3.84 1.32 o 12 4 -4 36.06 31.46 8.92 o 13 4 -4 0.82 5.63 1.47 o 1 5 -4 3.44 1.78 0.55 o 2 5 -4 13.60 11.06 1.00 o 3 5 -4 2.51 2.76 0.78 o 4 5 -4 1.99 1.53 0.89 o 5 5 -4 4.07 3.37 0.80 o 6 5 -4 38.54 44.17 1.50 o 7 5 -4 16.60 17.85 1.36 o 8 5 -4 4.08 4.16 0.69 o 9 5 -4 1.39 2.17 0.68 o 10 5 -4 7.01 4.65 0.89 o 11 5 -4 15.36 15.02 1.39 o 12 5 -4 1.23 3.72 1.40 o 0 6 -4 12.55 9.68 1.24 o 1 6 -4 1.42 0.97 0.46 o 2 6 -4 21.34 21.24 1.58 o 3 6 -4 0.45 1.01 0.55 o 4 6 -4 34.53 31.54 1.38 o 5 6 -4 2.54 1.37 0.88 o 6 6 -4 2.13 2.86 0.71 o 7 6 -4 12.66 12.37 1.14 o 8 6 -4 18.04 15.60 1.60 o 9 6 -4 0.53 1.66 0.57 o 10 6 -4 5.63 4.82 0.91 o 11 6 -4 3.44 3.31 0.99 o 1 7 -4 15.51 17.05 1.44 o 2 7 -4 7.31 5.36 1.05 o 3 7 -4 11.07 10.38 1.10 o 4 7 -4 6.50 5.66 1.08 o 5 7 -4 3.03 2.55 0.84 o 6 7 -4 53.13 53.50 2.01 o 7 7 -4 23.16 21.12 1.73 o 8 7 -4 1.05 1.54 0.70 o 9 7 -4 0.34 1.46 0.76 o 10 7 -4 0.24 0.94 0.65 o 0 8 -4 69.97 85.26 5.36 o 1 8 -4 21.55 23.31 1.62 o 2 8 -4 0.96 1.66 0.69 o 3 8 -4 13.81 14.19 1.13 o 4 8 -4 2.09 2.16 0.90 o 5 8 -4 16.92 16.15 1.23 o 6 8 -4 0.82 1.08 0.75 o 7 8 -4 6.93 8.00 1.09 o 8 8 -4 3.08 2.00 0.72 o 9 8 -4 1.30 0.79 0.67 o 10 8 -4 0.84 1.12 1.05 o 1 9 -4 58.89 63.01 2.01 o 2 9 -4 79.43 86.87 2.22 o 3 9 -4 3.55 2.64 0.66 o 4 9 -4 15.08 11.69 1.30 o 5 9 -4 3.64 1.63 0.89 o 6 9 -4 8.55 6.18 1.32 o 7 9 -4 3.00 1.44 0.67 o 8 9 -4 0.54 0.86 0.56 o 9 9 -4 4.89 2.90 1.33 o 0 10 -4 102.04 115.41 3.67 o 1 10 -4 27.01 32.21 1.84 o 2 10 -4 5.97 2.46 0.91 o 3 10 -4 9.13 7.49 1.25 o 4 10 -4 0.18 0.61 0.52 o 5 10 -4 0.14 1.38 0.83 o 6 10 -4 0.07 0.82 0.70 o 7 10 -4 6.25 2.69 2.38 o 8 10 -4 0.50 1.28 1.16 o 1 11 -4 34.48 39.74 1.89 o 2 11 -4 14.07 14.35 1.47 o 3 11 -4 1.30 1.01 0.78 o 4 11 -4 0.68 1.18 0.74 o 5 11 -4 2.67 1.89 0.82 o 0 12 -4 15.88 14.74 2.12 o 1 12 -4 0.35 0.98 0.71 o 2 12 -4 1.40 0.99 1.28 o 3 12 -4 1.71 0.51 0.82 o 4 12 -4 2.43 1.00 0.81 o 2 0 -3 39.09 39.09 1.21 o 4 0 -3 114.00 116.30 1.93 o 6 0 -3 457.29 517.52 29.36 o 8 0 -3 550.60 645.44 28.27 o 10 0 -3 11.33 8.68 0.83 o 12 0 -3 65.61 61.21 4.47 o 14 0 -3 25.30 17.16 7.58 o 16 0 -3 24.90 25.16 2.59 o 0 1 -3 63.80 76.09 1.38 o 1 1 -3 9.90 9.64 0.65 o 2 1 -3 83.26 96.46 3.25 o 3 1 -3 28.47 27.65 0.90 o 4 1 -3 268.49 288.36 12.50 o 5 1 -3 227.91 250.42 15.25 o 6 1 -3 28.03 35.01 2.35 o 7 1 -3 1.18 3.14 0.47 o 8 1 -3 214.45 228.93 28.59 o 9 1 -3 70.38 71.46 11.57 o 10 1 -3 19.19 14.09 2.67 o 11 1 -3 7.98 4.61 0.66 o 12 1 -3 26.65 23.70 1.04 o 13 1 -3 0.66 0.79 0.50 o 14 1 -3 15.78 15.83 0.97 o 15 1 -3 4.78 3.04 0.95 o 16 1 -3 3.03 1.75 0.80 o 1 2 -3 38.79 41.76 0.67 o 2 2 -3 20.90 20.67 0.71 o 3 2 -3 11.24 10.27 0.46 o 4 2 -3 130.19 151.04 3.89 o 5 2 -3 2.96 2.99 0.42 o 6 2 -3 120.10 140.63 2.07 o 7 2 -3 12.79 15.23 2.33 o 8 2 -3 80.27 84.23 13.96 o 9 2 -3 20.22 21.06 2.92 o 10 2 -3 2.52 1.94 0.49 o 11 2 -3 18.57 12.48 2.40 o 12 2 -3 22.46 18.51 1.48 o 13 2 -3 11.40 7.61 1.63 o 14 2 -3 17.84 20.19 1.52 o 15 2 -3 7.44 7.24 0.97 o 16 2 -3 21.93 18.07 1.47 o 0 3 -3 146.71 157.69 5.60 o 1 3 -3 13.58 12.31 0.45 o 2 3 -3 68.77 71.33 2.06 o 3 3 -3 23.81 26.98 1.03 o 4 3 -3 11.17 10.43 0.51 o 5 3 -3 10.81 11.15 0.66 o 6 3 -3 14.38 12.85 1.07 o 7 3 -3 77.52 79.33 3.85 o 8 3 -3 1.27 1.86 0.85 o 9 3 -3 47.32 53.57 1.43 o 10 3 -3 1.21 1.07 0.48 o 11 3 -3 4.70 3.77 0.55 o 12 3 -3 17.44 12.61 2.96 o 13 3 -3 11.33 7.21 1.32 o 14 3 -3 31.61 41.08 2.33 o 15 3 -3 5.41 4.55 0.74 o 16 3 -3 2.21 1.26 0.81 o 1 4 -3 71.36 78.74 2.18 o 2 4 -3 163.28 178.92 3.27 o 3 4 -3 30.43 31.96 0.70 o 4 4 -3 4.08 2.83 0.45 o 5 4 -3 23.37 22.97 0.76 o 6 4 -3 5.61 4.83 0.87 o 7 4 -3 7.00 7.67 1.12 o 8 4 -3 73.09 62.01 11.04 o 9 4 -3 34.35 31.47 7.30 o 10 4 -3 22.62 17.98 3.67 o 11 4 -3 11.21 7.59 1.68 o 12 4 -3 4.30 2.67 0.61 o 13 4 -3 6.81 6.73 0.93 o 14 4 -3 15.06 19.58 1.63 o 15 4 -3 2.41 2.25 0.64 o 16 4 -3 0.29 1.55 0.79 o 0 5 -3 166.24 202.56 12.33 o 1 5 -3 16.03 15.37 0.65 o 2 5 -3 18.41 15.40 0.88 o 3 5 -3 1.04 0.84 0.30 o 4 5 -3 25.36 26.30 0.82 o 5 5 -3 80.05 86.07 1.66 o 6 5 -3 4.27 7.40 1.48 o 7 5 -3 17.55 18.29 2.46 o 8 5 -3 37.93 39.68 2.31 o 9 5 -3 1.77 1.76 0.56 o 10 5 -3 1.20 1.44 0.67 o 11 5 -3 1.63 1.86 0.65 o 12 5 -3 14.92 9.23 2.29 o 13 5 -3 18.17 17.66 1.46 o 14 5 -3 3.85 3.39 0.82 o 15 5 -3 0.79 0.82 0.47 o 16 5 -3 7.38 1.53 1.19 o 1 6 -3 21.13 21.20 0.83 o 2 6 -3 4.58 4.22 0.53 o 3 6 -3 7.42 5.87 0.64 o 4 6 -3 63.51 59.44 1.38 o 5 6 -3 6.57 6.51 0.70 o 6 6 -3 130.72 141.47 3.58 o 7 6 -3 7.20 6.65 0.67 o 8 6 -3 66.10 70.32 2.42 o 9 6 -3 3.33 3.86 0.75 o 10 6 -3 24.16 23.24 1.59 o 11 6 -3 14.21 14.31 1.40 o 12 6 -3 4.64 4.27 1.15 o 13 6 -3 5.92 3.14 0.95 o 14 6 -3 3.64 2.36 0.79 o 15 6 -3 5.43 1.90 1.28 o 0 7 -3 6.89 5.61 1.02 o 1 7 -3 7.67 7.46 0.72 o 2 7 -3 0.61 0.66 0.35 o 3 7 -3 0.87 1.36 0.56 o 4 7 -3 58.37 58.48 1.31 o 5 7 -3 31.42 28.84 2.04 o 6 7 -3 0.20 1.24 0.49 o 7 7 -3 9.43 7.38 0.78 o 8 7 -3 17.80 15.16 1.40 o 9 7 -3 45.80 43.76 1.79 o 10 7 -3 7.66 5.88 0.95 o 11 7 -3 21.82 23.53 2.74 o 12 7 -3 29.45 31.37 1.84 o 13 7 -3 17.56 12.65 3.11 o 14 7 -3 1.22 1.19 0.53 o 1 8 -3 173.48 206.55 2.43 o 2 8 -3 34.07 32.10 1.19 o 3 8 -3 27.36 26.30 1.08 o 4 8 -3 57.27 52.74 1.32 o 5 8 -3 18.14 14.98 1.25 o 6 8 -3 1.71 2.02 0.58 o 7 8 -3 24.26 22.56 1.45 o 8 8 -3 8.06 8.75 0.95 o 9 8 -3 1.74 2.12 0.91 o 10 8 -3 5.68 6.14 1.12 o 11 8 -3 19.67 17.76 1.45 o 12 8 -3 3.29 2.01 0.90 o 13 8 -3 22.68 21.61 2.43 o 14 8 -3 12.10 1.33 1.15 o 0 9 -3 428.24 518.70 3.64 o 1 9 -3 11.21 15.11 0.92 o 2 9 -3 51.55 55.73 1.79 o 3 9 -3 38.05 41.01 1.36 o 4 9 -3 37.54 35.75 1.29 o 5 9 -3 11.00 9.61 0.85 o 6 9 -3 1.83 1.21 0.47 o 7 9 -3 7.36 6.36 0.75 o 8 9 -3 2.03 1.94 0.63 o 9 9 -3 11.95 9.72 1.27 o 10 9 -3 14.94 9.62 1.20 o 11 9 -3 5.27 2.99 0.75 o 12 9 -3 32.08 33.65 1.83 o 13 9 -3 8.65 0.55 0.90 o 1 10 -3 88.54 98.65 8.38 o 2 10 -3 80.54 80.36 3.07 o 3 10 -3 65.79 65.68 6.28 o 4 10 -3 29.65 25.38 1.14 o 5 10 -3 2.04 0.98 0.52 o 6 10 -3 12.07 10.38 2.08 o 7 10 -3 3.01 2.42 0.64 o 8 10 -3 20.61 17.58 3.40 o 9 10 -3 15.51 12.14 2.97 o 10 10 -3 24.98 25.84 1.70 o 11 10 -3 19.74 24.05 2.66 o 12 10 -3 0.10 0.89 0.67 o 0 11 -3 27.31 25.16 14.42 o 1 11 -3 48.49 49.93 1.72 o 2 11 -3 29.35 27.26 1.49 o 3 11 -3 13.17 9.55 1.20 o 4 11 -3 9.70 7.36 1.13 o 5 11 -3 7.75 6.98 0.92 o 6 11 -3 1.47 1.23 0.49 o 7 11 -3 21.46 18.76 1.42 o 8 11 -3 2.36 2.64 0.90 o 9 11 -3 11.28 10.60 1.27 o 10 11 -3 21.93 24.14 2.47 o 11 11 -3 2.15 0.88 0.65 o 1 12 -3 26.64 30.88 1.55 o 2 12 -3 2.53 1.86 0.75 o 3 12 -3 14.63 17.23 1.35 o 4 12 -3 2.64 1.96 0.87 o 5 12 -3 5.85 3.44 0.92 o 6 12 -3 13.53 13.15 1.25 o 7 12 -3 4.30 3.85 0.97 o 8 12 -3 7.57 6.23 1.15 o 9 12 -3 11.27 10.76 2.98 o 10 12 -3 0.42 1.70 1.12 o 0 13 -3 1.27 2.07 1.19 o 1 13 -3 3.97 3.06 0.96 o 2 13 -3 18.66 21.73 1.46 o 3 13 -3 0.67 1.43 0.75 o 4 13 -3 1.10 1.18 0.56 o 5 13 -3 4.70 2.60 0.59 o 6 13 -3 0.46 1.11 0.43 o 7 13 -3 7.02 7.58 0.95 o 8 13 -3 1.64 2.12 0.67 o 9 13 -3 2.23 2.82 1.33 o 1 14 -3 8.29 10.16 1.83 o 2 14 -3 9.29 6.88 2.44 o 3 14 -3 3.15 2.09 0.79 o 4 14 -3 11.08 8.19 3.01 o 5 14 -3 1.53 2.07 0.71 o 6 14 -3 2.77 2.49 0.75 o 7 14 -3 8.96 8.45 1.24 o 0 15 -3 41.06 56.57 2.71 o 1 15 -3 3.79 3.70 1.37 o 2 15 -3 0.60 1.13 0.99 o 3 15 -3 11.62 8.02 6.18 o 4 15 -3 10.67 6.70 2.41 o 5 15 -3 0.94 1.27 0.98 o 0 0 -2 69.56 70.57 2.26 o 2 0 -2 2721.52 2858.24 48.87 o 4 0 -2 801.28 874.69 4.20 o 6 0 -2 105.40 111.52 4.13 o 8 0 -2 465.02 463.46 15.43 o 10 0 -2 943.27 1044.11 62.06 o 12 0 -2 12.50 10.75 1.15 o 14 0 -2 32.97 33.57 1.49 o 16 0 -2 17.86 19.88 1.46 o 18 0 -2 5.56 3.48 1.43 o 1 1 -2 5.99 5.33 0.27 o 2 1 -2 360.19 380.24 5.37 o 3 1 -2 50.01 50.56 2.69 o 4 1 -2 636.35 645.48 38.43 o 5 1 -2 312.22 333.89 2.04 o 6 1 -2 69.19 57.72 8.29 o 7 1 -2 257.10 233.21 44.53 o 8 1 -2 142.73 129.93 23.70 o 9 1 -2 58.43 50.66 8.88 o 10 1 -2 63.52 61.30 7.34 o 11 1 -2 157.99 135.51 25.28 o 12 1 -2 15.97 16.60 0.82 o 13 1 -2 4.64 4.34 0.66 o 14 1 -2 39.76 36.82 1.10 o 15 1 -2 8.24 7.99 0.78 o 16 1 -2 97.87 114.37 2.43 o 17 1 -2 3.02 3.29 0.82 o 18 1 -2 2.23 1.59 0.75 o 19 1 -2 2.10 1.47 1.23 o 0 2 -2 217.31 216.92 4.05 o 1 2 -2 42.98 44.80 1.60 o 2 2 -2 53.78 61.96 1.28 o 3 2 -2 137.06 134.03 6.11 o 4 2 -2 391.90 407.28 15.00 o 5 2 -2 246.21 253.61 10.91 o 6 2 -2 216.10 214.98 28.09 o 7 2 -2 95.29 87.62 13.14 o 8 2 -2 8.35 7.72 1.39 o 9 2 -2 7.96 6.02 1.41 o 10 2 -2 352.30 318.19 60.49 o 11 2 -2 19.51 17.60 3.75 o 12 2 -2 30.13 22.08 4.82 o 13 2 -2 28.16 32.12 1.15 o 14 2 -2 17.05 19.71 1.42 o 15 2 -2 67.42 75.68 1.69 o 16 2 -2 2.39 3.08 0.97 o 17 2 -2 25.44 28.05 1.62 o 18 2 -2 7.35 6.02 0.92 o 1 3 -2 60.96 60.84 1.28 o 2 3 -2 549.80 546.73 17.64 o 3 3 -2 103.76 109.97 3.29 o 4 3 -2 985.86 1023.04 52.24 o 5 3 -2 20.26 16.43 2.35 o 6 3 -2 75.19 77.17 8.49 o 7 3 -2 116.65 107.38 16.42 o 8 3 -2 11.26 8.80 1.86 o 9 3 -2 35.50 25.61 4.13 o 10 3 -2 10.93 11.51 0.76 o 11 3 -2 2.69 1.80 0.60 o 12 3 -2 0.12 0.42 0.57 o 13 3 -2 14.29 13.76 1.28 o 14 3 -2 1.13 1.24 0.54 o 15 3 -2 3.32 4.11 1.08 o 16 3 -2 61.24 74.75 1.79 o 17 3 -2 12.65 13.10 1.29 o 18 3 -2 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13 1 0 133.11 138.03 2.42 o 2 2 0 505.29 335.51 1.60 o 3 2 0 1483.76 1396.67 15.98 o 4 2 0 260.83 223.46 1.08 o 5 2 0 639.22 580.64 10.89 o 6 2 0 7.23 4.71 1.06 o 7 2 0 349.25 304.65 86.62 o 8 2 0 25.55 38.46 1.15 o 9 2 0 123.15 135.62 2.08 o 10 2 0 19.01 18.65 0.88 o 11 2 0 106.68 106.38 1.34 o 12 2 0 278.61 298.12 3.57 o 13 2 0 163.41 173.21 2.64 o 3 3 0 773.72 733.36 2.89 o 4 3 0 266.59 261.58 2.42 o 5 3 0 247.37 229.02 1.30 o 6 3 0 3306.22 3437.84 35.94 o 7 3 0 394.35 375.88 1.85 o 8 3 0 0.02 0.34 0.29 o 9 3 0 78.39 85.24 1.73 o 10 3 0 41.01 44.47 5.28 o 11 3 0 17.36 15.65 0.76 o 12 3 0 29.60 27.55 1.57 o 13 3 0 17.12 14.73 1.49 o 14 3 0 70.88 78.31 2.19 o 1 4 0 90.67 80.92 0.95 o 2 4 0 531.76 458.43 2.12 o 4 4 0 0.01 4.41 0.77 o 5 4 0 310.68 303.51 2.66 o 6 4 0 122.82 115.81 2.10 o 7 4 0 60.29 58.96 1.42 o 8 4 0 70.99 89.56 2.01 o 9 4 0 90.67 99.62 1.29 o 10 4 0 236.84 243.74 1.90 o 11 4 0 31.86 31.86 0.98 o 12 4 0 11.38 9.62 1.25 o 13 4 0 1.43 1.83 0.86 o 14 4 0 1.79 3.07 1.08 o 1 5 0 174.24 169.45 4.29 o 2 5 0 1561.42 1556.55 27.03 o 3 5 0 142.47 134.55 1.32 o 4 5 0 170.55 170.71 1.48 o 5 5 0 33.41 48.35 1.63 o 6 5 0 175.53 226.21 2.51 o 7 5 0 359.66 404.37 3.29 o 8 5 0 528.58 543.10 2.52 o 9 5 0 0.47 1.85 0.59 o 10 5 0 0.85 0.79 0.47 o 11 5 0 24.13 26.58 1.68 o 12 5 0 27.87 27.94 1.82 o 13 5 0 149.21 140.90 2.72 o 14 5 0 13.26 12.88 1.49 o 15 5 0 26.00 20.53 1.59 o 0 6 0 3472.88 3688.93 5.57 o 1 6 0 6.50 5.86 0.79 o 2 6 0 266.81 258.30 1.19 o 3 6 0 20.16 16.44 1.80 o 4 6 0 2.48 2.57 0.65 o 5 6 0 51.36 44.89 1.00 o 6 6 0 0.06 1.21 0.73 o 7 6 0 69.99 66.80 1.86 o 8 6 0 3.56 3.25 0.78 o 9 6 0 18.58 16.06 1.26 o 10 6 0 0.89 0.06 0.71 o 11 6 0 2.76 1.13 0.91 o 12 6 0 152.88 140.58 3.00 o 13 6 0 7.22 9.58 1.54 o 14 6 0 11.16 16.19 1.67 o 15 6 0 1.06 0.44 0.74 o 18 6 0 0.00 5.40 1.76 o 1 7 0 1793.48 1944.39 16.41 o 2 7 0 124.17 141.64 1.98 o 3 7 0 112.66 107.35 0.94 o 4 7 0 106.12 97.84 1.66 o 5 7 0 37.23 38.71 2.89 o 6 7 0 10.47 12.57 0.87 o 7 7 0 209.44 204.90 2.01 o 8 7 0 11.34 14.21 3.53 o 9 7 0 2.88 1.16 0.81 o 10 7 0 7.30 2.45 0.92 o 11 7 0 15.28 12.00 1.39 o 12 7 0 17.61 19.48 1.93 o 13 7 0 2.82 4.90 1.49 o 14 7 0 26.63 27.46 2.20 o 15 7 0 8.36 13.50 3.33 o 16 7 0 1.73 2.64 1.33 o 17 7 0 12.59 16.29 2.16 o 18 7 0 0.57 3.63 1.68 o 0 8 0 68.00 83.12 1.15 o 1 8 0 49.36 42.43 0.77 o 2 8 0 141.79 143.46 1.31 o 3 8 0 127.68 119.63 1.90 o 4 8 0 218.98 213.87 2.38 o 5 8 0 18.93 17.76 1.01 o 6 8 0 2.02 2.59 0.70 o 7 8 0 615.71 609.71 3.25 o 8 8 0 371.10 376.54 5.08 o 9 8 0 524.72 538.25 3.49 o 10 8 0 23.75 21.60 2.76 o 11 8 0 24.79 25.67 3.82 o 12 8 0 68.97 61.06 4.17 o 13 8 0 97.46 102.68 2.18 o 14 8 0 8.73 7.88 1.49 o 15 8 0 8.08 8.94 1.16 o 16 8 0 2.86 3.17 0.91 o 17 8 0 0.79 2.59 1.38 o 1 9 0 0.05 0.62 0.37 o 2 9 0 17.47 16.89 0.83 o 3 9 0 22.12 22.40 1.05 o 4 9 0 51.60 52.66 1.53 o 5 9 0 14.84 14.62 1.43 o 6 9 0 555.38 556.00 20.63 o 7 9 0 1.54 9.20 4.14 o 8 9 0 275.70 277.12 8.76 o 9 9 0 17.70 18.17 1.35 o 10 9 0 3.91 5.07 2.68 o 11 9 0 16.27 15.81 1.44 o 12 9 0 85.15 92.08 3.38 o 13 9 0 2.32 2.87 1.25 o 14 9 0 1.29 2.26 1.16 o 15 9 0 1.97 2.82 0.93 o 16 9 0 0.11 2.57 0.79 o 17 9 0 1.50 2.45 1.42 o 2 10 0 62.83 53.46 1.33 o 3 10 0 91.34 83.31 1.72 o 4 10 0 180.32 177.89 2.46 o 5 10 0 1204.36 1252.55 4.82 o 6 10 0 46.04 45.84 1.91 o 7 10 0 305.26 330.89 10.11 o 8 10 0 252.09 263.60 2.70 o 9 10 0 77.82 81.17 1.97 o 10 10 0 39.85 38.25 3.88 o 11 10 0 1.47 1.29 1.03 o 12 10 0 4.62 6.39 1.69 o 13 10 0 40.96 41.10 3.32 o 14 10 0 25.74 31.19 1.73 o 15 10 0 26.35 30.14 1.76 o 16 10 0 7.66 11.89 1.53 o 5 11 0 26.65 22.94 1.22 o 6 11 0 197.09 211.46 2.41 o 7 11 0 104.17 110.27 3.46 o 8 11 0 191.61 203.78 3.70 o 9 11 0 30.67 34.85 1.56 o 10 11 0 11.68 12.56 2.07 o 11 11 0 0.55 2.07 1.24 o 12 11 0 38.73 43.45 2.25 o 13 11 0 14.38 16.94 1.42 o 14 11 0 28.19 30.50 1.73 o 15 11 0 27.77 37.07 1.93 o 16 11 0 0.16 2.86 1.02 o 5 12 0 3.32 4.33 1.50 o 6 12 0 52.71 50.68 2.65 o 7 12 0 29.57 29.59 2.30 o 8 12 0 9.43 11.20 1.09 o 9 12 0 49.90 57.65 1.79 o 10 12 0 29.54 30.96 2.86 o 11 12 0 4.55 3.50 0.94 o 12 12 0 0.44 1.23 0.79 o 13 12 0 19.87 23.63 1.69 o 14 12 0 2.68 3.36 1.17 o 15 12 0 5.35 6.04 1.18 o 5 13 0 39.78 41.15 2.59 o 6 13 0 69.26 66.96 2.72 o 7 13 0 1.55 3.75 1.42 o 8 13 0 17.25 21.77 2.17 o 9 13 0 3.52 4.09 1.90 o 10 13 0 0.86 0.51 1.00 o 11 13 0 17.08 15.78 2.01 o 12 13 0 0.07 0.62 0.63 o 13 13 0 13.03 11.51 1.35 o 14 13 0 8.26 7.33 1.19 o 15 13 0 3.40 2.96 1.33 o 5 14 0 0.56 2.00 1.35 o 6 14 0 2.20 2.31 1.36 o 7 14 0 29.94 35.88 2.65 o 8 14 0 9.91 13.39 2.07 o 9 14 0 4.23 6.72 2.11 o 10 14 0 4.05 3.56 1.72 o 11 14 0 22.61 20.20 2.32 o 12 14 0 11.84 14.13 2.16 o 13 14 0 0.12 1.14 1.13 o 4 15 0 9.99 5.13 1.90 o 5 15 0 0.38 2.81 1.63 o 6 15 0 54.48 61.72 3.02 o 7 15 0 0.85 4.72 1.63 o 8 15 0 36.64 45.14 2.84 o 9 15 0 17.94 18.31 2.15 o 10 15 0 25.35 26.68 2.82 o 11 15 0 17.12 14.64 2.13 o 4 16 0 44.95 48.24 3.08 o 5 16 0 42.90 47.74 3.14 o 6 16 0 3.31 5.82 2.05 o 7 16 0 7.44 6.28 1.70 o 8 16 0 3.83 4.57 1.61 o 9 16 0 28.21 33.87 2.87 o 10 16 0 0.07 -0.11 0.86 o 3 17 0 10.68 8.34 1.83 o 4 17 0 16.72 18.07 2.23 o 5 17 0 3.36 5.47 1.96 o 6 17 0 3.96 7.41 1.81 o 7 17 0 31.75 35.41 2.92 o 3 18 0 12.59 13.19 2.40 o 4 18 0 23.88 22.22 2.64 o 5 1 1 287.64 271.63 1.52 o 6 1 1 174.94 178.61 1.41 o 7 1 1 65.41 63.78 1.00 o 8 1 1 120.75 131.71 1.46 o 6 2 1 411.03 464.86 2.42 o 7 2 1 306.00 309.44 2.11 o 8 2 1 286.21 283.87 2.15 o 9 2 1 41.85 38.62 1.10 o 6 3 1 108.03 115.59 1.54 o 7 3 1 312.14 314.44 2.36 o 8 3 1 204.47 212.35 2.10 o 9 3 1 43.22 41.97 1.25 o 10 3 1 5.04 6.62 0.78 o 8 4 1 143.99 150.36 2.12 o 9 4 1 19.80 18.49 1.14 o 10 4 1 56.59 51.38 1.52 o 7 5 1 29.94 29.76 1.36 o 9 5 1 14.83 12.83 1.27 o 10 5 1 117.73 117.50 2.20 o 11 5 1 2.46 0.84 0.67 o 8 6 1 9.44 14.57 1.36 o 9 6 1 34.50 40.24 1.76 o 10 6 1 113.61 102.02 2.31 o 11 6 1 19.44 14.18 1.33 o 1 7 1 384.17 358.80 1.70 o 8 7 1 14.52 13.58 1.42 o 9 7 1 51.15 57.25 2.05 o 10 7 1 162.21 156.71 2.91 o 11 7 1 7.51 5.00 1.13 o 12 7 1 76.81 70.18 2.25 o 8 8 1 7.05 6.25 1.24 o 9 8 1 219.87 231.86 3.50 o 10 8 1 17.70 23.11 1.81 o 11 8 1 143.19 141.68 3.07 o 12 8 1 14.97 11.15 1.38 o 9 9 1 68.07 66.96 2.39 o 10 9 1 109.42 112.76 2.95 o 11 9 1 1.61 2.09 1.25 o 8 10 1 103.56 105.42 2.98 o 9 10 1 6.37 5.57 1.55 o 11 10 1 21.48 21.15 2.15 o 12 10 1 0.07 0.77 0.91 o 8 11 1 37.88 36.06 2.30 o 9 11 1 26.12 23.78 2.22 o 10 11 1 13.38 14.46 1.82 o 11 11 1 35.08 34.42 2.15 o 12 11 1 3.37 4.17 1.02 o 13 11 1 7.01 9.03 2.38 o 14 11 1 10.75 11.98 1.70 o 15 11 1 33.19 43.12 2.65 o 16 11 1 3.26 6.77 1.62 o 8 12 1 23.34 24.74 2.37 o 9 12 1 25.80 28.50 2.29 o 10 12 1 3.82 2.94 1.37 o 11 12 1 44.09 53.35 2.81 o 12 12 1 11.24 8.16 1.84 o 13 12 1 23.00 19.89 1.97 o 8 13 1 22.97 24.92 2.36 o 12 13 1 38.84 41.92 2.64 o 13 13 1 0.75 0.32 0.73 o 8 14 1 16.52 14.84 2.14 o 9 14 1 19.02 19.01 2.00 o 12 14 1 2.32 2.53 1.33 o 13 14 1 2.16 1.01 1.01 o 7 15 1 11.29 13.06 2.25 o 8 15 1 10.69 13.51 2.05 o 9 15 1 6.88 6.61 1.83 o 10 15 1 12.73 13.97 2.26 o 11 15 1 7.37 7.82 1.87 o 7 16 1 45.03 51.47 3.06 o 8 16 1 3.75 5.68 1.82 o 9 16 1 5.26 5.52 1.82 o 7 17 1 10.12 8.74 1.72 o 10 13 2 7.94 7.91 1.61 o 9 14 2 6.17 4.46 1.56 o 10 14 2 5.35 6.18 1.73 o 9 15 2 12.82 15.25 2.04 o 10 15 2 7.00 8.58 1.70 o