#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:12 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180895 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/35/2103560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103560_Fobs loop_ _publ_author_name 'Wheatley, Paul S.' 'Lough, Alan J.' 'Ferguson, George' 'Burchell, Colin J.' 'Glidewell, Christopher' _publ_section_title ; Ethane-1,2-diphosphonic acid as a building block in supramolecular chemistry; a pillared-layer framework and framework-encapsulated cations ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 95 _journal_page_last 102 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.291 _cell_angle_gamma 90.000 _cell_length_a 7.3914 _cell_length_b 9.3343 _cell_length_c 9.3590 _exptl_crystal_F_000 292.00 _reflns_d_resolution_high 0.7721 _cod_data_source_file na011118sup2.hkl _cod_data_source_block 18 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 18 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4171.41 4070.04 154.74 o 2 0 0 4877.92 4760.88 175.06 o 3 0 0 619.27 578.31 25.01 o 4 0 0 110.04 121.91 10.94 o 5 0 0 337.42 314.16 31.26 o 6 0 0 635.95 647.08 43.76 o 7 0 0 794.66 867.46 70.33 o 8 0 0 142.99 104.72 32.82 o 9 0 0 49.24 39.07 28.13 o 1 1 0 481.44 489.22 14.07 o 2 1 0 0.07 -1.56 1.56 o 3 1 0 244.99 273.52 10.94 o 4 1 0 106.61 84.40 6.25 o 5 1 0 383.65 397.00 26.57 o 6 1 0 270.86 290.72 21.88 o 7 1 0 84.86 96.91 20.32 o 8 1 0 7.15 -15.63 15.63 o 9 1 0 78.27 60.96 25.01 o 0 2 0 3058.31 2847.78 107.85 o 1 2 0 847.99 900.28 20.32 o 2 2 0 478.00 536.11 15.63 o 3 2 0 1187.54 1220.70 34.39 o 4 2 0 4.94 18.76 6.25 o 5 2 0 34.28 45.33 17.19 o 6 2 0 2.75 35.95 21.88 o 7 2 0 61.10 51.58 21.88 o 8 2 0 105.38 107.85 23.44 o 1 3 0 2622.95 2703.98 87.53 o 2 3 0 2337.20 2397.63 67.21 o 3 3 0 1502.29 1556.74 39.07 o 4 3 0 3127.90 3330.74 100.03 o 5 3 0 702.77 745.55 37.51 o 6 3 0 552.48 559.55 34.39 o 7 3 0 64.39 93.78 18.76 o 8 3 0 10.27 18.76 18.76 o 0 4 0 384.11 404.82 21.88 o 1 4 0 584.22 636.14 21.88 o 2 4 0 0.96 3.13 1.56 o 3 4 0 112.78 107.85 9.38 o 4 4 0 536.33 553.30 32.82 o 5 4 0 16.86 17.19 9.38 o 6 4 0 44.92 34.39 15.63 o 7 4 0 13.10 42.20 29.70 o 8 4 0 13.99 15.63 34.39 o 1 5 0 12.02 17.19 6.25 o 2 5 0 5.27 7.81 4.69 o 3 5 0 742.64 817.45 28.13 o 4 5 0 587.83 640.83 26.57 o 5 5 0 0.39 1.56 12.50 o 6 5 0 169.16 160.99 17.19 o 7 5 0 119.87 129.73 23.44 o 8 5 0 13.66 9.38 20.32 o 0 6 0 301.19 267.27 17.19 o 1 6 0 405.67 401.69 15.63 o 2 6 0 423.08 415.76 18.76 o 3 6 0 186.46 203.19 15.63 o 4 6 0 54.83 60.96 7.81 o 5 6 0 0.00 3.13 20.32 o 6 6 0 101.48 126.60 31.26 o 7 6 0 18.67 37.51 15.63 o 1 7 0 28.97 28.13 7.81 o 2 7 0 134.56 132.85 14.07 o 3 7 0 1.79 4.69 12.50 o 4 7 0 44.26 18.76 10.94 o 5 7 0 49.65 53.14 18.76 o 6 7 0 34.68 62.52 18.76 o 7 7 0 5.12 25.01 42.20 o 0 8 0 7.65 28.13 12.50 o 1 8 0 46.48 59.39 9.38 o 2 8 0 20.84 -1.56 9.38 o 3 8 0 64.00 93.78 39.07 o 4 8 0 42.71 26.57 10.94 o 5 8 0 2.40 3.13 12.50 o 6 8 0 4.47 9.38 23.44 o 1 9 0 77.66 40.64 14.07 o 2 9 0 37.42 34.39 12.50 o 3 9 0 28.42 43.76 23.44 o 4 9 0 73.58 53.14 20.32 o 5 9 0 8.94 -9.38 17.19 o 6 9 0 60.05 48.45 31.26 o 0 10 0 40.65 32.82 15.63 o 1 10 0 269.10 268.84 29.70 o 2 10 0 178.03 146.92 25.01 o 3 10 0 15.63 14.07 18.76 o 4 10 0 30.95 17.19 29.70 o 5 10 0 3.13 25.01 39.07 o 1 11 0 7.14 7.81 15.63 o 2 11 0 0.42 -7.81 31.26 o 3 11 0 0.76 -25.01 29.70 o 0 12 0 0.52 25.01 32.82 o 1 12 0 4.64 -9.38 18.76 o -9 1 1 14.02 32.82 20.32 o -8 1 1 5.48 40.64 17.19 o -7 1 1 40.62 45.33 12.50 o -6 1 1 661.27 683.03 35.95 o -5 1 1 642.90 637.70 31.26 o -4 1 1 239.35 212.57 14.07 o -3 1 1 262.96 217.26 10.94 o -2 1 1 11.84 15.63 4.69 o -1 1 1 859.08 773.68 18.76 o 0 1 1 634.46 581.43 14.07 o 1 1 1 8444.52 7908.75 132.85 o 2 1 1 29.49 46.89 3.13 o 3 1 1 27.32 32.82 3.13 o 4 1 1 65.83 56.27 6.25 o 5 1 1 118.94 115.66 17.19 o 6 1 1 10.40 -1.56 12.50 o 7 1 1 0.02 20.32 21.88 o 8 1 1 22.21 14.07 18.76 o -9 2 1 196.27 234.45 42.20 o -8 2 1 2.41 -1.56 31.26 o -7 2 1 511.22 561.12 42.20 o -6 2 1 251.36 279.78 29.70 o -5 2 1 10.86 17.19 73.46 o -4 2 1 114.91 118.79 10.94 o -3 2 1 536.64 518.91 17.19 o -2 2 1 79.28 51.58 6.25 o -1 2 1 2481.83 2427.33 67.21 o 0 2 1 4431.25 4120.05 89.09 o 1 2 1 1156.47 1025.32 20.32 o 2 2 1 172.70 214.13 6.25 o 3 2 1 10.71 14.07 3.13 o 4 2 1 71.16 76.59 7.81 o 5 2 1 491.77 475.15 40.64 o 6 2 1 351.00 314.16 25.01 o 7 2 1 265.18 254.77 32.82 o 8 2 1 85.16 60.96 28.13 o -9 3 1 30.68 14.07 23.44 o -8 3 1 40.91 20.32 17.19 o -7 3 1 13.68 23.44 15.63 o -6 3 1 77.51 50.02 14.07 o -5 3 1 124.11 129.73 15.63 o -4 3 1 11.47 4.69 6.25 o -3 3 1 1245.29 1284.78 46.89 o -2 3 1 452.63 467.34 17.19 o -1 3 1 6.73 7.81 1.56 o 0 3 1 53.86 50.02 3.13 o 1 3 1 695.00 765.87 18.76 o 2 3 1 246.16 262.58 7.81 o 3 3 1 60.88 68.77 6.25 o 4 3 1 1.33 6.25 4.69 o 5 3 1 718.24 658.02 35.95 o 6 3 1 138.04 107.85 15.63 o 7 3 1 25.52 40.64 18.76 o 8 3 1 21.81 37.51 20.32 o -8 4 1 110.91 110.97 21.88 o -7 4 1 101.02 195.37 50.02 o -6 4 1 6.36 14.07 14.07 o -5 4 1 162.75 184.43 17.19 o -4 4 1 5.20 -1.56 4.69 o -3 4 1 985.36 1037.83 32.82 o -2 4 1 585.47 595.50 17.19 o -1 4 1 2.95 9.38 3.13 o 0 4 1 51.89 68.77 4.69 o 1 4 1 144.75 120.35 4.69 o 2 4 1 136.72 148.48 6.25 o 3 4 1 0.78 7.81 4.69 o 4 4 1 2.42 3.13 6.25 o 5 4 1 188.56 232.89 23.44 o 6 4 1 20.01 7.81 10.94 o 7 4 1 53.21 59.39 15.63 o 8 4 1 91.84 78.15 21.88 o -8 5 1 13.83 25.01 23.44 o -7 5 1 150.15 203.19 34.39 o -6 5 1 122.16 170.37 26.57 o -5 5 1 813.18 954.99 50.02 o -4 5 1 611.95 598.63 29.70 o -3 5 1 752.51 720.54 28.13 o -2 5 1 900.55 894.03 29.70 o -1 5 1 154.93 151.61 10.94 o 0 5 1 1.86 0.00 3.13 o 1 5 1 1299.44 1369.18 42.20 o 2 5 1 867.33 912.79 34.39 o 3 5 1 1957.93 2078.78 71.90 o 4 5 1 1111.57 1144.11 42.20 o 5 5 1 835.49 948.74 57.83 o 6 5 1 316.44 315.72 28.13 o 7 5 1 2.95 17.19 12.50 o 8 5 1 3.24 29.70 42.20 o -8 6 1 3.73 17.19 20.32 o -7 6 1 6.57 3.13 20.32 o -6 6 1 38.84 10.94 12.50 o -5 6 1 73.83 60.96 15.63 o -4 6 1 537.83 564.24 25.01 o -3 6 1 100.53 106.28 14.07 o -2 6 1 72.75 73.46 6.25 o -1 6 1 459.67 392.31 15.63 o 0 6 1 79.09 29.70 6.25 o 1 6 1 2.89 1.56 4.69 o 2 6 1 110.03 120.35 9.38 o 3 6 1 54.55 28.13 9.38 o 4 6 1 305.95 298.53 18.76 o 5 6 1 96.50 75.02 14.07 o 6 6 1 23.61 23.44 10.94 o 7 6 1 19.23 10.94 39.07 o -7 7 1 344.25 336.04 37.51 o -6 7 1 94.87 81.28 17.19 o -5 7 1 135.19 107.85 17.19 o -4 7 1 35.64 53.14 14.07 o -3 7 1 342.10 390.75 29.70 o -2 7 1 138.91 150.05 15.63 o -1 7 1 100.65 53.14 9.38 o 0 7 1 33.02 26.57 3.13 o 1 7 1 16.98 26.57 7.81 o 2 7 1 134.37 142.23 14.07 o 3 7 1 115.40 123.48 15.63 o 4 7 1 278.61 268.84 25.01 o 5 7 1 5.64 14.07 12.50 o 6 7 1 163.67 168.80 42.20 o 7 7 1 83.45 29.70 35.95 o -7 8 1 1.03 26.57 26.57 o -6 8 1 8.36 6.25 15.63 o -5 8 1 5.89 9.38 14.07 o -4 8 1 0.53 -14.07 14.07 o -3 8 1 478.61 486.09 35.95 o -2 8 1 449.51 562.68 29.70 o -1 8 1 1865.00 1927.17 79.71 o 0 8 1 712.24 715.85 34.39 o 1 8 1 1158.10 1237.89 54.70 o 2 8 1 1105.02 1156.62 59.39 o 3 8 1 55.20 64.08 14.07 o 4 8 1 6.90 23.44 14.07 o 5 8 1 145.90 132.85 43.76 o 6 8 1 129.90 193.81 56.27 o -6 9 1 0.01 -9.38 26.57 o -5 9 1 90.53 140.67 26.57 o -4 9 1 0.36 23.44 20.32 o -3 9 1 1.33 -6.25 14.07 o -2 9 1 10.46 25.01 12.50 o -1 9 1 10.65 10.94 17.19 o 0 9 1 41.78 25.01 10.94 o 1 9 1 8.98 -7.81 14.07 o 2 9 1 0.73 10.94 15.63 o 3 9 1 17.41 14.07 12.50 o 4 9 1 0.12 42.20 26.57 o 5 9 1 4.33 9.38 23.44 o -5 10 1 27.27 4.69 20.32 o -4 10 1 65.17 57.83 26.57 o -3 10 1 115.19 121.91 21.88 o -2 10 1 133.68 139.11 31.26 o -1 10 1 130.93 148.48 20.32 o 0 10 1 63.00 59.39 15.63 o 1 10 1 99.09 76.59 21.88 o 2 10 1 171.50 253.21 45.33 o 3 10 1 45.90 64.08 32.82 o 4 10 1 7.19 -17.19 26.57 o -3 11 1 224.40 250.08 50.02 o -2 11 1 82.86 85.96 21.88 o -1 11 1 3.88 17.19 20.32 o 0 11 1 29.97 34.39 17.19 o 1 11 1 24.18 40.64 15.63 o 2 11 1 244.21 218.82 57.83 o 3 11 1 513.86 481.40 117.22 o -1 12 1 22.97 18.76 21.88 o 0 12 1 22.34 -6.25 31.26 o -9 0 2 58.61 35.95 35.95 o -8 0 2 3.78 118.79 57.83 o -7 0 2 23.66 95.34 109.41 o -6 0 2 38.51 25.01 18.76 o -5 0 2 898.33 859.65 51.58 o -4 0 2 2133.98 2227.27 126.60 o -3 0 2 818.44 767.43 34.39 o -2 0 2 3754.79 3468.29 112.54 o -1 0 2 10191.26 9578.03 326.67 o 0 0 2 1960.67 2102.23 68.77 o 1 0 2 8787.87 8468.30 221.95 o 2 0 2 428.57 512.66 20.32 o 3 0 2 296.11 273.52 10.94 o 4 0 2 11.45 1.56 7.81 o 5 0 2 464.64 467.34 43.76 o 6 0 2 1458.94 1581.75 100.03 o 7 0 2 185.89 211.00 37.51 o 8 0 2 278.46 317.29 54.70 o -9 1 2 31.55 28.13 31.26 o -8 1 2 249.41 225.07 31.26 o -7 1 2 70.42 65.65 17.19 o -6 1 2 836.27 800.25 37.51 o -5 1 2 383.31 346.98 35.95 o -4 1 2 15.41 14.07 6.25 o -3 1 2 734.30 850.27 28.13 o -2 1 2 241.58 228.20 9.38 o -1 1 2 284.53 237.58 7.81 o 0 1 2 1118.12 1114.42 26.57 o 1 1 2 775.42 806.51 18.76 o 2 1 2 23.75 23.44 3.13 o 3 1 2 104.67 117.22 6.25 o 4 1 2 23.27 25.01 6.25 o 5 1 2 292.46 267.27 31.26 o 6 1 2 8.53 -3.13 12.50 o 7 1 2 9.83 37.51 25.01 o 8 1 2 6.53 -17.19 21.88 o -9 2 2 155.28 159.43 28.13 o -8 2 2 5.75 15.63 15.63 o -7 2 2 48.90 20.32 12.50 o -6 2 2 224.74 225.07 17.19 o -5 2 2 899.55 951.86 37.51 o -4 2 2 1823.25 1952.18 65.65 o -3 2 2 744.54 762.74 23.44 o -2 2 2 3397.64 3496.42 103.16 o -1 2 2 1.73 1.56 1.56 o 0 2 2 461.27 454.83 12.50 o 1 2 2 1.62 1.56 1.56 o 2 2 2 17.43 23.44 3.13 o 3 2 2 39.92 46.89 4.69 o 4 2 2 44.27 40.64 7.81 o 5 2 2 9.24 15.63 7.81 o 6 2 2 0.05 1.56 14.07 o 7 2 2 3.68 21.88 17.19 o 8 2 2 75.47 39.07 18.76 o -9 3 2 31.32 73.46 29.70 o -8 3 2 335.61 340.73 35.95 o -7 3 2 75.26 101.59 20.32 o -6 3 2 838.03 790.88 42.20 o -5 3 2 969.32 1020.64 50.02 o -4 3 2 120.54 89.09 9.38 o -3 3 2 743.61 762.74 23.44 o -2 3 2 74.10 54.70 6.25 o -1 3 2 5.54 9.38 3.13 o 0 3 2 932.28 1005.01 23.44 o 1 3 2 1533.01 1597.38 40.64 o 2 3 2 3058.68 3196.32 60.96 o 3 3 2 1075.28 1078.47 28.13 o 4 3 2 966.16 1012.82 31.26 o 5 3 2 1153.56 1216.01 48.45 o 6 3 2 7.25 -12.50 12.50 o 7 3 2 15.16 20.32 18.76 o 8 3 2 11.07 -15.63 39.07 o -8 4 2 40.22 40.64 20.32 o -7 4 2 110.61 50.02 15.63 o -6 4 2 23.43 21.88 15.63 o -5 4 2 24.30 23.44 9.38 o -4 4 2 236.74 192.25 18.76 o -3 4 2 59.21 46.89 7.81 o -2 4 2 159.04 162.55 9.38 o -1 4 2 397.62 401.69 15.63 o 0 4 2 224.84 223.51 7.81 o 1 4 2 17.43 23.44 3.13 o 2 4 2 513.72 553.30 17.19 o 3 4 2 160.64 175.06 9.38 o 4 4 2 45.77 48.45 6.25 o 5 4 2 0.01 9.38 12.50 o 6 4 2 256.84 290.72 31.26 o 7 4 2 37.98 43.76 18.76 o 8 4 2 4.05 14.07 20.32 o -8 5 2 208.23 236.01 32.82 o -7 5 2 264.33 317.29 34.39 o -6 5 2 44.29 56.27 15.63 o -5 5 2 92.50 81.28 10.94 o -4 5 2 14.02 15.63 6.25 o -3 5 2 147.08 162.55 12.50 o -2 5 2 354.80 359.49 14.07 o -1 5 2 1434.14 1506.73 50.02 o 0 5 2 68.08 54.70 4.69 o 1 5 2 23.70 29.70 3.13 o 2 5 2 646.87 689.28 18.76 o 3 5 2 62.73 51.58 6.25 o 4 5 2 36.45 31.26 7.81 o 5 5 2 24.64 15.63 10.94 o 6 5 2 6.63 -1.56 12.50 o 7 5 2 135.31 198.50 84.40 o -8 6 2 55.50 31.26 20.32 o -7 6 2 46.38 114.10 39.07 o -6 6 2 16.29 9.38 14.07 o -5 6 2 55.33 50.02 14.07 o -4 6 2 172.32 193.81 14.07 o -3 6 2 119.91 123.48 17.19 o -2 6 2 1314.36 1245.71 46.89 o -1 6 2 300.56 309.47 17.19 o 0 6 2 412.00 390.75 18.76 o 1 6 2 420.12 393.87 14.07 o 2 6 2 192.10 181.31 7.81 o 3 6 2 8.76 17.19 6.25 o 4 6 2 151.57 151.61 20.32 o 5 6 2 268.90 300.10 25.01 o 6 6 2 93.79 125.04 31.26 o 7 6 2 241.31 287.59 64.08 o -7 7 2 24.89 -1.56 17.19 o -6 7 2 58.73 51.58 17.19 o -5 7 2 75.25 92.22 25.01 o -4 7 2 244.59 345.42 57.83 o -3 7 2 195.33 192.25 20.32 o -2 7 2 0.14 4.69 12.50 o -1 7 2 323.25 309.47 23.44 o 0 7 2 142.56 118.79 10.94 o 1 7 2 21.55 18.76 4.69 o 2 7 2 72.80 57.83 6.25 o 3 7 2 257.93 284.47 23.44 o 4 7 2 80.43 73.46 12.50 o 5 7 2 32.68 20.32 56.27 o 6 7 2 0.37 14.07 25.01 o -7 8 2 2.48 -3.13 26.57 o -6 8 2 1.80 34.39 18.76 o -5 8 2 0.12 3.13 12.50 o -4 8 2 5.72 31.26 26.57 o -3 8 2 3.37 -9.38 10.94 o -2 8 2 180.15 179.74 21.88 o -1 8 2 3.70 23.44 12.50 o 0 8 2 3.31 1.56 10.94 o 1 8 2 61.08 40.64 12.50 o 2 8 2 73.16 54.70 12.50 o 3 8 2 26.80 26.57 10.94 o 4 8 2 0.09 -10.94 31.26 o 5 8 2 29.53 29.70 32.82 o 6 8 2 0.58 -6.25 28.13 o -6 9 2 36.44 28.13 23.44 o -5 9 2 74.22 65.65 21.88 o -4 9 2 181.08 225.07 26.57 o -3 9 2 244.19 250.08 21.88 o -2 9 2 19.22 20.32 15.63 o -1 9 2 1.09 -3.13 9.38 o 0 9 2 83.65 71.90 14.07 o 1 9 2 7.13 6.25 9.38 o 2 9 2 152.54 192.25 21.88 o 3 9 2 291.56 409.50 81.28 o 4 9 2 48.50 76.59 40.64 o 5 9 2 3.19 51.58 45.33 o -5 10 2 93.31 37.51 23.44 o -4 10 2 24.61 29.70 18.76 o -3 10 2 53.16 60.96 29.70 o -2 10 2 289.52 301.66 42.20 o -1 10 2 91.02 73.46 31.26 o 0 10 2 262.81 215.69 26.57 o 1 10 2 63.87 54.70 20.32 o 2 10 2 116.85 109.41 29.70 o 3 10 2 0.03 14.07 26.57 o 4 10 2 121.31 170.37 35.95 o -3 11 2 7.53 -10.94 18.76 o -2 11 2 147.10 120.35 25.01 o -1 11 2 28.46 3.13 25.01 o 0 11 2 34.84 53.14 37.51 o 1 11 2 13.12 4.69 25.01 o 2 11 2 2.46 35.95 37.51 o 3 11 2 7.10 3.13 43.76 o -9 1 3 74.17 76.59 26.57 o -8 1 3 98.06 95.34 20.32 o -7 1 3 145.24 170.37 20.32 o -6 1 3 176.79 234.45 26.57 o -5 1 3 457.45 454.83 28.13 o -4 1 3 0.17 20.32 7.81 o -3 1 3 409.56 493.91 23.44 o -2 1 3 1378.03 1356.68 42.20 o -1 1 3 73.58 115.66 4.69 o 0 1 3 147.98 114.10 4.69 o 1 1 3 204.92 250.08 6.25 o 2 1 3 341.11 318.85 9.38 o 3 1 3 55.22 57.83 4.69 o 4 1 3 133.09 125.04 9.38 o 5 1 3 98.64 100.03 12.50 o 6 1 3 40.07 20.32 9.38 o 7 1 3 98.63 71.90 14.07 o 8 1 3 1.65 32.82 34.39 o -9 2 3 4.87 14.07 17.19 o -8 2 3 81.63 48.45 15.63 o -7 2 3 16.61 31.26 14.07 o -6 2 3 132.97 112.54 15.63 o -5 2 3 496.17 545.49 26.57 o -4 2 3 294.65 281.34 14.07 o -3 2 3 25.28 18.76 7.81 o -2 2 3 6.80 -1.56 3.13 o -1 2 3 2365.66 2342.93 73.46 o 0 2 3 1622.40 1591.13 34.39 o 1 2 3 24.02 15.63 3.13 o 2 2 3 0.12 0.00 1.56 o 3 2 3 22.01 25.01 3.13 o 4 2 3 23.67 20.32 7.81 o 5 2 3 233.58 254.77 15.63 o 7 2 3 75.13 109.41 26.57 o 8 2 3 65.92 68.77 37.51 o -9 3 3 73.67 106.28 26.57 o -8 3 3 0.13 35.95 17.19 o -7 3 3 66.05 56.27 18.76 o -6 3 3 386.57 325.10 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