#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:53 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180906 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/47/2104785.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104785_Fobs loop_ _publ_author_name 'Tumanov, N. A.' 'Boldyreva, E. V.' 'Kolesov, B. A.' 'Kurnosov, A. V.' 'Quesada Cabrera, R.' _publ_section_title ; Pressure-induced phase transitions in L-alanine, revisited ; _journal_coeditor_code GP5038 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 458 _journal_page_last 471 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.6729 _cell_length_b 5.6707 _cell_length_c 12.0465 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.6920 _cod_data_source_file gp50382.2GPasup5.hkl _cod_data_source_block 2.2GPa #BEGIN Tags that were not found in dictionaries: _shelx_title ' LALA22_FINE IN P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 66.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1767.01 1953.01 47.81 o 4 0 0 12.62 10.94 3.15 o 8 0 0 2.61 8.97 10.38 o 1 1 0 36.86 55.87 3.89 o 2 1 0 1979.65 2025.09 13.41 o 3 1 0 1.65 1.72 1.49 o 4 1 0 6.44 6.53 1.91 o 5 1 0 292.32 279.97 5.15 o 6 1 0 8.54 7.12 4.07 o 7 1 0 75.84 65.14 6.81 o 8 1 0 0.35 7.83 9.16 o 3 2 0 278.40 278.68 4.18 o 4 2 0 35.67 40.44 2.94 o 5 2 0 89.79 87.51 5.07 o 6 2 0 4.54 9.03 5.40 o 7 2 0 8.40 15.20 10.27 o 1 0 1 547.42 583.00 9.63 o 2 0 1 998.41 1013.21 13.25 o 3 0 1 55.59 58.88 1.66 o 4 0 1 88.98 91.06 3.11 o 5 0 1 0.90 3.70 2.80 o 6 0 1 33.81 33.45 4.71 o 7 0 1 84.12 96.06 6.98 o 8 0 1 0.28 5.37 7.32 o -8 1 1 7.81 11.98 13.24 o -7 1 1 20.18 22.17 6.15 o -6 1 1 4.32 4.79 4.12 o -5 1 1 6.89 7.50 3.31 o -4 1 1 342.09 342.19 5.35 o -3 1 1 88.35 87.43 2.02 o -2 1 1 508.53 512.09 5.32 o -1 1 1 92.81 96.46 2.05 o 0 1 1 165.44 177.18 3.38 o 1 1 1 92.64 99.18 1.59 o 2 1 1 508.32 507.29 6.74 o 3 1 1 88.30 86.98 2.26 o 4 1 1 341.52 325.74 4.83 o 5 1 1 6.89 8.10 3.12 o 6 1 1 4.28 5.21 4.29 o 7 1 1 20.18 23.95 6.40 o 8 1 1 7.79 8.81 13.02 o -7 2 1 0.42 6.10 10.70 o -6 2 1 40.49 52.20 7.18 o -5 2 1 14.58 22.76 4.71 o -4 2 1 147.25 143.37 4.57 o -3 2 1 83.64 81.77 3.00 o -2 2 1 478.53 496.24 8.06 o -1 2 1 161.47 143.92 7.95 o 1 2 1 161.78 153.73 5.81 o 2 2 1 478.31 492.11 5.86 o 3 2 1 83.83 81.53 3.25 o 4 2 1 147.47 140.03 5.64 o 5 2 1 14.64 17.74 4.71 o 6 2 1 40.38 27.83 6.76 o 7 2 1 0.42 9.17 9.03 o -5 3 1 29.61 20.58 16.41 o -4 3 1 84.51 76.64 11.88 o 4 3 1 84.53 90.43 10.39 o 5 3 1 29.62 40.71 17.22 o 1 0 2 283.22 193.17 4.63 o 2 0 2 177.64 194.75 4.37 o 3 0 2 232.95 234.72 3.00 o 4 0 2 47.16 46.03 2.51 o 5 0 2 210.41 210.53 4.39 o 6 0 2 1.38 3.06 4.43 o 7 0 2 85.92 97.37 7.07 o 8 0 2 0.30 7.63 9.30 o -8 1 2 12.31 29.99 16.77 o -7 1 2 11.57 12.93 6.60 o -6 1 2 1.72 4.07 4.38 o -5 1 2 215.09 217.19 4.96 o -4 1 2 1.65 2.97 1.85 o -3 1 2 204.88 222.78 3.24 o -2 1 2 255.55 260.85 7.82 o -1 1 2 57.85 67.62 1.43 o 0 1 2 4483.79 4364.30 62.68 o 1 1 2 57.91 68.24 1.27 o 2 1 2 255.57 270.57 7.34 o 3 1 2 205.26 198.21 7.58 o 4 1 2 1.66 2.30 1.89 o 5 1 2 215.14 213.03 5.23 o 6 1 2 1.70 5.01 4.52 o 7 1 2 11.57 13.44 6.19 o 8 1 2 12.22 13.28 16.13 o -7 2 2 7.72 5.49 9.88 o -6 2 2 26.67 22.43 6.59 o -5 2 2 100.91 97.08 5.70 o -4 2 2 4.76 4.16 3.22 o -3 2 2 182.65 171.04 4.98 o -2 2 2 565.53 600.25 8.64 o -1 2 2 145.01 141.77 2.55 o 0 2 2 1080.68 1203.40 20.88 o 1 2 2 145.15 138.78 3.01 o 2 2 2 565.57 593.07 7.53 o 3 2 2 182.52 183.18 4.06 o 4 2 2 4.75 4.98 3.55 o 5 2 2 100.93 90.21 6.28 o 6 2 2 26.65 19.88 5.86 o 7 2 2 7.77 8.69 8.46 o -6 3 2 12.07 10.66 10.67 o -5 3 2 1.89 7.72 6.83 o -4 3 2 27.43 28.30 5.40 o -3 3 2 104.31 108.86 4.17 o -2 3 2 58.37 60.85 4.12 o -1 3 2 97.85 97.63 9.30 o 0 3 2 5.33 1.66 4.80 o 1 3 2 97.93 95.88 5.44 o 2 3 2 58.38 54.49 4.09 o 3 3 2 104.35 95.58 4.62 o 4 3 2 27.50 24.01 5.15 o 5 3 2 1.91 1.65 5.86 o 6 3 2 12.14 10.01 8.33 o 2 0 3 273.82 258.10 4.22 o 3 0 3 0.20 1.70 1.89 o 4 0 3 12.86 13.20 2.20 o 5 0 3 54.18 54.99 3.99 o 6 0 3 0.01 4.08 4.62 o 7 0 3 28.21 21.91 6.05 o -8 1 3 0.78 2.52 16.24 o -7 1 3 78.72 94.60 8.58 o -6 1 3 14.57 11.80 6.32 o -5 1 3 59.11 69.96 4.77 o -4 1 3 77.73 81.01 3.86 o -3 1 3 45.25 45.96 2.10 o -2 1 3 202.50 197.96 3.13 o -1 1 3 797.76 807.37 21.10 o 0 1 3 18.71 16.33 0.99 o 1 1 3 797.40 847.91 13.85 o 2 1 3 202.32 194.36 4.86 o 3 1 3 45.41 40.57 1.94 o 4 1 3 77.76 75.88 3.78 o 5 1 3 59.19 61.92 4.81 o 6 1 3 14.56 7.15 5.88 o 7 1 3 78.67 79.87 9.21 o 8 1 3 0.78 17.82 21.02 o -7 2 3 14.52 14.91 11.78 o -6 2 3 4.35 2.97 6.42 o -5 2 3 2.51 5.63 5.28 o -4 2 3 88.15 93.72 3.79 o -3 2 3 109.88 108.24 2.66 o -2 2 3 38.57 40.81 1.96 o -1 2 3 354.41 370.29 5.95 o 0 2 3 855.03 777.42 24.54 o 1 2 3 354.24 380.51 8.61 o 2 2 3 38.62 39.52 2.12 o 3 2 3 109.89 108.46 3.43 o 4 2 3 88.08 86.61 4.37 o 5 2 3 2.51 7.85 4.99 o 6 2 3 4.35 5.06 6.18 o 7 2 3 14.53 12.67 9.88 o -7 3 3 9.74 21.37 16.72 o -6 3 3 3.30 12.85 9.89 o -5 3 3 0.41 3.41 7.20 o -4 3 3 51.25 49.09 4.86 o -3 3 3 77.09 71.73 3.77 o -2 3 3 343.24 324.05 8.86 o -1 3 3 269.40 296.36 5.44 o 0 3 3 122.73 131.79 4.56 o 1 3 3 269.44 278.54 4.96 o 2 3 3 343.11 337.82 5.28 o 3 3 3 76.72 76.04 4.18 o 4 3 3 51.39 49.38 5.92 o 5 3 3 0.41 3.26 6.22 o 6 3 3 3.24 7.47 8.54 o 7 3 3 9.76 7.28 10.88 o -4 4 3 60.27 59.16 17.08 o -3 4 3 124.57 105.72 14.75 o 2 4 3 19.25 25.26 6.98 o 3 4 3 124.52 118.33 8.82 o 4 4 3 60.39 46.23 11.86 o 3 0 4 560.30 510.67 16.19 o 4 0 4 96.52 93.71 3.51 o 5 0 4 218.89 215.29 5.91 o 6 0 4 0.77 4.86 5.42 o 7 0 4 24.71 25.80 14.34 o -7 1 4 15.88 18.80 8.65 o -6 1 4 6.04 6.57 6.59 o -5 1 4 90.57 93.10 6.15 o -4 1 4 42.15 44.27 3.80 o -3 1 4 75.24 80.28 3.61 o -2 1 4 772.12 735.45 10.45 o -1 1 4 238.36 221.62 5.11 o 0 1 4 1289.93 1197.34 47.88 o 1 1 4 238.36 243.05 6.72 o 2 1 4 771.78 752.90 15.04 o 3 1 4 75.09 68.92 3.90 o 4 1 4 42.05 39.07 4.50 o 5 1 4 90.44 86.27 6.17 o 6 1 4 6.04 3.77 5.76 o 7 1 4 15.94 14.35 8.86 o -7 2 4 40.40 45.78 10.40 o -6 2 4 1.83 4.03 8.12 o -5 2 4 23.90 28.92 5.15 o -4 2 4 0.81 5.08 4.00 o -3 2 4 176.52 187.04 4.91 o -2 2 4 24.22 27.60 1.81 o -1 2 4 24.78 23.76 1.81 o 0 2 4 22.03 17.04 2.21 o 1 2 4 24.89 23.54 1.84 o 2 2 4 24.15 27.19 2.20 o 3 2 4 176.60 170.13 5.29 o 4 2 4 0.82 7.16 4.14 o 5 2 4 23.94 15.92 4.90 o 6 2 4 1.82 1.75 7.83 o 7 2 4 40.28 37.43 11.72 o -7 3 4 4.52 12.70 11.76 o -6 3 4 2.06 4.29 9.01 o -5 3 4 108.61 107.69 7.84 o -4 3 4 5.16 4.59 5.12 o -3 3 4 51.29 53.74 3.62 o -2 3 4 9.78 10.95 2.99 o -1 3 4 29.91 29.39 2.65 o 0 3 4 98.58 88.32 3.93 o 1 3 4 29.91 23.48 3.27 o 2 3 4 9.80 8.60 2.73 o 3 3 4 51.26 50.05 4.60 o 4 3 4 5.13 1.53 4.60 o 5 3 4 108.67 108.97 8.31 o 6 3 4 2.06 4.14 8.54 o 7 3 4 4.53 5.25 9.82 o -5 4 4 9.47 10.91 13.55 o -4 4 4 4.88 5.16 8.87 o -3 4 4 14.11 12.30 6.80 o -2 4 4 47.34 50.88 6.73 o -1 4 4 17.28 16.61 5.00 o 0 4 4 16.40 14.82 4.82 o 1 4 4 17.37 17.20 4.64 o 2 4 4 47.25 48.56 6.91 o 3 4 4 14.13 10.12 5.74 o 4 4 4 4.92 3.74 7.79 o 5 4 4 9.45 6.57 8.15 o 6 4 4 24.29 36.29 24.34 o -7 1 5 4.93 11.95 9.29 o -6 1 5 0.18 5.95 7.28 o -5 1 5 28.02 35.20 6.77 o -4 1 5 114.43 118.13 5.51 o -3 1 5 56.95 62.95 4.28 o -2 1 5 40.67 38.07 2.92 o -1 1 5 257.86 265.67 7.04 o 0 1 5 391.92 380.58 20.10 o 1 1 5 257.93 260.37 10.10 o 2 1 5 40.60 39.15 2.82 o 3 1 5 56.85 53.65 3.65 o 4 1 5 114.18 108.71 7.27 o 5 1 5 28.04 23.90 5.72 o 6 1 5 0.18 2.53 7.66 o 7 1 5 4.91 11.65 12.66 o -7 2 5 22.00 23.14 10.23 o -6 2 5 20.52 18.32 8.58 o -5 2 5 42.49 39.52 6.54 o -4 2 5 47.66 52.35 4.04 o -3 2 5 82.02 84.55 3.48 o -2 2 5 110.27 102.22 2.83 o -1 2 5 273.81 270.77 8.49 o 0 2 5 9.15 9.24 0.99 o 1 2 5 273.25 274.79 6.48 o 2 2 5 110.06 109.32 4.73 o 3 2 5 81.89 83.26 3.31 o 4 2 5 47.62 44.13 4.29 o 5 2 5 42.45 38.19 6.90 o 6 2 5 20.43 15.65 8.24 o 7 2 5 21.94 16.86 9.58 o -7 3 5 1.20 7.83 11.69 o -6 3 5 4.27 5.03 9.03 o -5 3 5 2.94 4.27 7.24 o -4 3 5 209.43 218.20 6.84 o -3 3 5 50.86 54.00 4.94 o -2 3 5 250.47 252.23 6.09 o -1 3 5 14.50 14.59 2.57 o 0 3 5 121.50 110.39 4.85 o 1 3 5 14.54 12.86 2.98 o 2 3 5 250.53 256.18 5.60 o 3 3 5 50.82 57.10 5.18 o 4 3 5 209.75 197.34 7.15 o 5 3 5 2.92 8.74 7.12 o 6 3 5 4.26 4.78 8.70 o 7 3 5 1.19 2.53 9.91 o -6 4 5 26.47 28.10 16.20 o -5 4 5 15.10 20.02 9.54 o -4 4 5 15.52 14.92 7.33 o -3 4 5 51.96 49.41 6.10 o -2 4 5 98.31 105.72 6.27 o -1 4 5 47.40 50.31 5.09 o 0 4 5 6.06 5.44 4.53 o 1 4 5 47.30 49.66 5.51 o 2 4 5 98.47 93.39 6.43 o 3 4 5 51.85 45.13 6.74 o 4 4 5 15.56 13.99 6.54 o 5 4 5 15.12 16.64 8.49 o 6 4 5 26.49 26.54 11.22 o -1 5 5 37.10 41.90 11.79 o 0 5 5 10.20 9.84 8.17 o 1 5 5 37.00 32.72 10.68 o 2 5 5 12.75 5.55 17.46 o -6 1 6 5.35 7.33 7.61 o -5 1 6 84.55 84.73 7.14 o -4 1 6 60.54 62.17 5.30 o -3 1 6 25.61 32.81 4.20 o -2 1 6 141.95 139.36 8.83 o -1 1 6 3.17 3.12 5.03 o 2 1 6 141.77 145.15 10.10 o 3 1 6 25.70 26.29 3.40 o 4 1 6 60.61 57.78 5.81 o 5 1 6 84.60 84.63 11.89 o 6 1 6 5.38 10.88 12.73 o -7 2 6 0.13 4.02 10.27 o -6 2 6 29.75 26.61 9.21 o -5 2 6 8.46 12.01 6.61 o -4 2 6 11.14 8.63 5.22 o -3 2 6 90.14 97.32 4.97 o -2 2 6 158.95 165.57 7.49 o -1 2 6 27.96 32.11 2.67 o 0 2 6 1163.12 1044.95 48.22 o 1 2 6 28.01 29.77 2.48 o 2 2 6 158.99 166.03 9.16 o 3 2 6 90.10 88.11 4.59 o 4 2 6 11.17 8.55 4.52 o 5 2 6 8.49 8.72 6.96 o 6 2 6 29.77 22.39 8.61 o 7 2 6 0.13 5.34 12.06 o -7 3 6 24.67 36.29 17.53 o -6 3 6 14.19 17.20 9.45 o -5 3 6 4.24 2.51 7.65 o -4 3 6 4.01 8.08 5.19 o -3 3 6 34.70 33.50 3.89 o -2 3 6 168.86 170.73 4.98 o -1 3 6 8.37 11.84 2.55 o 0 3 6 1.14 5.37 2.88 o 1 3 6 8.36 9.22 2.28 o 2 3 6 168.85 167.75 4.74 o 3 3 6 34.67 34.81 4.06 o 4 3 6 4.04 4.96 4.86 o 5 3 6 4.26 7.08 6.87 o 6 3 6 14.30 12.91 8.87 o 7 3 6 24.68 22.54 16.14 o -6 4 6 23.13 17.14 12.92 o -5 4 6 37.47 41.80 7.44 o -4 4 6 6.24 6.23 6.91 o -3 4 6 15.56 15.58 6.06 o -2 4 6 22.64 24.99 4.79 o -1 4 6 45.78 46.01 5.11 o 0 4 6 99.96 93.99 5.35 o 1 4 6 45.74 49.61 5.14 o 2 4 6 22.66 24.14 5.10 o 3 4 6 15.58 18.04 6.08 o 4 4 6 6.26 9.70 5.76 o 5 4 6 37.46 35.89 8.70 o 6 4 6 23.14 16.94 9.75 o -4 5 6 0.67 1.64 13.69 o -3 5 6 9.92 9.65 10.08 o -2 5 6 1.49 4.47 9.13 o -1 5 6 67.94 67.68 9.98 o 0 5 6 0.93 3.58 7.58 o 1 5 6 68.04 77.20 8.62 o 2 5 6 1.51 4.07 8.09 o 3 5 6 9.89 14.56 10.74 o 4 5 6 0.67 3.12 10.00 o -4 1 7 21.55 16.55 11.39 o -6 2 7 8.10 6.69 9.15 o -5 2 7 25.44 35.05 7.71 o -4 2 7 131.90 133.26 7.58 o -3 2 7 50.45 55.18 6.80 o -2 2 7 121.33 111.26 9.25 o -1 2 7 48.12 51.95 4.21 o 0 2 7 306.73 273.72 12.82 o 1 2 7 48.19 54.62 3.36 o 2 2 7 121.36 107.93 8.20 o 3 2 7 50.35 44.04 5.26 o 4 2 7 132.09 115.51 8.65 o 5 2 7 25.36 27.87 8.04 o 6 2 7 8.13 7.62 8.66 o 7 2 7 2.85 2.07 20.65 o -6 3 7 12.54 18.07 10.08 o -5 3 7 22.89 15.02 7.56 o -4 3 7 28.16 28.93 5.68 o -3 3 7 68.48 66.82 4.46 o -2 3 7 46.59 52.15 4.45 o -1 3 7 112.87 110.90 5.20 o 0 3 7 79.53 79.64 4.06 o 1 3 7 112.64 112.61 6.02 o 2 3 7 46.51 44.77 4.95 o 3 3 7 68.26 71.28 4.98 o 4 3 7 28.14 24.65 5.42 o 5 3 7 22.92 20.02 7.15 o 6 3 7 12.53 7.38 9.59 o -6 4 7 10.31 7.11 13.65 o -5 4 7 0.09 9.68 8.79 o -4 4 7 13.91 17.14 7.30 o -3 4 7 34.51 37.89 7.43 o -2 4 7 54.04 63.05 5.78 o -1 4 7 95.63 88.38 5.50 o 0 4 7 16.29 17.30 3.96 o 1 4 7 95.53 88.35 5.43 o 2 4 7 54.05 60.16 5.80 o 3 4 7 34.58 32.29 7.34 o 4 4 7 13.99 16.08 7.01 o 5 4 7 0.09 2.32 7.90 o 6 4 7 10.26 6.93 15.87 o -5 5 7 8.73 16.47 23.36 o -4 5 7 30.47 34.62 12.14 o -3 5 7 1.34 4.05 10.52 o -2 5 7 6.09 8.12 7.59 o -1 5 7 24.53 28.81 7.45 o 0 5 7 3.47 5.01 7.20 o 1 5 7 24.48 22.43 6.60 o 2 5 7 6.13 5.79 7.78 o 3 5 7 1.33 2.71 8.35 o 4 5 7 30.48 26.47 10.47 o 5 5 7 8.76 2.77 13.63 o -5 2 8 1.99 2.50 8.22 o -4 2 8 13.49 14.23 7.03 o -3 2 8 165.04 169.56 10.76 o -2 2 8 66.49 71.12 5.75 o -1 2 8 5.34 6.81 3.90 o 0 2 8 1.65 2.34 3.59 o 1 2 8 5.39 5.79 3.65 o 2 2 8 66.34 58.47 5.86 o 3 2 8 165.02 178.60 12.55 o 4 2 8 13.46 15.18 8.47 o 5 2 8 2.01 1.70 11.99 o -6 3 8 3.29 3.52 11.37 o -5 3 8 66.23 79.67 9.71 o -4 3 8 6.01 7.36 7.54 o -3 3 8 30.99 36.04 5.86 o -2 3 8 48.68 48.64 5.23 o -1 3 8 56.22 56.28 6.73 o 0 3 8 27.48 30.37 5.19 o 1 3 8 56.14 63.85 4.92 o 2 3 8 48.69 44.96 5.64 o 3 3 8 31.08 28.47 5.57 o 4 3 8 5.99 7.53 6.43 o 5 3 8 66.26 63.80 10.03 o 6 3 8 3.29 2.53 10.36 o -6 4 8 6.22 2.38 23.81 o -5 4 8 6.17 5.81 11.64 o -4 4 8 9.43 9.49 8.69 o -3 4 8 20.86 26.71 8.57 o -2 4 8 44.51 41.70 5.55 o -1 4 8 31.71 31.96 5.68 o 0 4 8 13.94 14.94 5.01 o 1 4 8 31.81 32.60 5.65 o 2 4 8 44.60 40.27 5.50 o 3 4 8 20.85 26.47 8.25 o 4 4 8 9.43 8.61 8.34 o 5 4 8 6.17 5.71 8.81 o 6 4 8 6.23 3.17 21.85 o -5 5 8 1.24 0.94 22.26 o -4 5 8 11.98 14.48 11.62 o -3 5 8 16.13 11.80 8.75 o -2 5 8 5.36 10.70 5.97 o -1 5 8 8.80 11.27 7.33 o 0 5 8 1.54 7.64 7.56 o 1 5 8 8.83 12.01 6.02 o 2 5 8 5.34 7.54 7.25 o 3 5 8 16.07 14.18 8.89 o 4 5 8 12.01 13.23 10.01 o 5 5 8 1.22 2.28 16.11 o -2 6 8 14.13 17.47 23.52 o -1 6 8 6.26 8.93 14.60 o 0 6 8 23.66 31.94 12.39 o 1 6 8 6.26 7.55 12.14 o 2 6 8 14.23 12.80 16.03 o -6 3 9 0.74 2.43 17.17 o -5 3 9 37.15 43.81 11.21 o -4 3 9 38.63 41.65 8.72 o -3 3 9 2.04 4.77 7.14 o -2 3 9 44.55 46.84 8.21 o -1 3 9 160.69 154.59 12.26 o 0 3 9 48.39 43.12 5.56 o 1 3 9 160.58 151.30 11.07 o 2 3 9 44.57 46.15 6.38 o 3 3 9 2.05 4.25 7.74 o 4 3 9 38.71 24.29 10.51 o 5 3 9 37.12 46.53 12.14 o -5 4 9 8.08 10.32 11.12 o -4 4 9 3.06 11.46 9.07 o -3 4 9 4.15 9.06 8.25 o -2 4 9 2.09 4.40 5.73 o -1 4 9 0.59 2.23 5.25 o 0 4 9 52.24 51.12 5.54 o 1 4 9 0.59 5.27 5.25 o 2 4 9 2.11 5.93 5.69 o 3 4 9 4.14 8.16 7.88 o 4 4 9 3.07 3.07 8.69 o 5 4 9 8.13 9.26 12.40 o -4 5 9 1.38 3.06 11.11 o -3 5 9 2.69 9.94 9.19 o -2 5 9 5.94 9.51 6.48 o -1 5 9 8.78 9.17 6.71 o 0 5 9 6.77 2.82 8.07 o 1 5 9 8.77 8.19 6.80 o 2 5 9 5.92 14.09 7.10 o 3 5 9 2.70 2.33 8.98 o 4 5 9 1.37 6.48 9.69 o -3 6 9 0.27 2.45 24.47 o -2 6 9 4.45 14.82 12.42 o -1 6 9 8.07 12.47 11.11 o 0 6 9 5.60 11.42 12.75 o 1 6 9 8.04 15.04 11.77 o 2 6 9 4.44 1.77 11.23 o 3 6 9 0.26 8.98 13.51 o -4 3 10 2.22 7.86 10.13 o -3 3 10 17.26 16.23 9.40 o -2 3 10 91.54 106.89 14.68 o -1 3 10 21.91 25.34 9.03 o 0 3 10 3.03 11.07 10.30 o 1 3 10 21.92 26.30 10.60 o 2 3 10 91.57 107.53 17.30 o 4 3 10 2.22 1.90 19.01 o -5 4 10 6.74 7.67 16.69 o -4 4 10 15.74 18.67 11.60 o -3 4 10 13.45 10.49 8.98 o -2 4 10 3.44 5.61 6.40 o -1 4 10 37.21 43.38 6.54 o 0 4 10 7.96 14.05 7.21 o 1 4 10 37.18 40.71 7.01 o 2 4 10 3.42 2.51 6.25 o 3 4 10 13.39 15.57 8.73 o 4 4 10 15.82 23.50 10.80 o 5 4 10 6.74 6.87 13.34 o -4 5 10 9.06 11.75 10.36 o -3 5 10 15.23 19.87 10.19 o -2 5 10 5.37 4.41 7.42 o -1 5 10 6.41 12.08 7.33 o 0 5 10 0.65 5.71 8.13 o 1 5 10 6.41 10.93 7.87 o 2 5 10 5.43 6.94 7.28 o 3 5 10 15.18 12.11 9.65 o 4 5 10 9.03 10.27 10.12 o -2 6 10 14.22 4.22 13.10 o -1 6 10 0.88 8.05 11.00 o 0 6 10 17.04 17.58 9.86 o 1 6 10 0.89 5.01 11.27 o 2 6 10 14.21 19.13 10.18 o 3 6 10 4.28 2.36 23.63 o -4 4 11 2.55 6.76 11.54 o -3 4 11 6.08 9.37 10.44 o -2 4 11 9.23 10.90 8.50 o -1 4 11 35.65 48.33 9.67 o 0 4 11 6.05 9.83 8.97 o 1 4 11 35.60 30.37 8.23 o 2 4 11 9.16 9.51 10.92 o 3 4 11 6.08 3.00 21.33 o 4 4 11 2.53 15.63 21.23 o -3 5 11 0.00 8.45 11.72 o -2 5 11 3.02 7.84 8.81 o -1 5 11 15.70 13.64 8.37 o 0 5 11 2.49 6.88 8.33 o 1 5 11 15.73 17.79 8.39 o 2 5 11 3.01 6.77 9.63 o 3 5 11 0.00 3.60 9.71 o -1 6 11 2.64 11.73 11.41 o 0 6 11 0.00 4.23 10.14 o 1 6 11 2.64 4.79 13.33 o -1 4 12 22.92 24.23 15.34 o 0 4 12 45.77 45.27 16.73 o 2 4 12 10.80 14.72 21.36 o -3 5 12 3.21 17.74 22.80 o -2 5 12 25.67 27.53 11.85 o -1 5 12 4.50 15.47 13.09 o 0 5 12 7.03 6.64 11.03 o 1 5 12 4.49 2.49 10.94 o 2 5 12 25.70 30.13 13.07 o 0 5 13 0.07 15.98 22.90 o 1 5 13 3.48 8.59 23.92 o