#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/47/2104787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104787_Fobs loop_ _publ_author_name 'Tumanov, N. A.' 'Boldyreva, E. V.' 'Kolesov, B. A.' 'Kurnosov, A. V.' 'Quesada Cabrera, R.' _publ_section_title ; Pressure-induced phase transitions in L-alanine, revisited ; _journal_coeditor_code GP5038 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 458 _journal_page_last 471 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.6084 _cell_length_b 5.5521 _cell_length_c 11.8571 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.6850 _[local]_cod_data_source_file gp50383.5GPasup7.hkl _[local]_cod_data_source_block 3.5GPa #BEGIN Tags that were not found in dictionaries: _shelx_title ' LALA37_F IN P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 63.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 961.09 1015.65 45.66 o 4 0 0 6.15 5.51 2.96 o 6 0 0 84.92 146.90 22.27 o 8 0 0 0.41 -1.81 12.55 o 2 1 0 1194.68 1227.29 39.19 o 3 1 0 1.98 3.41 1.50 o 4 1 0 95.78 120.96 9.66 o 5 1 0 138.27 128.06 6.19 o 6 1 0 34.14 31.46 4.30 o 7 1 0 0.03 4.27 5.18 o 8 1 0 0.36 -7.84 22.61 o 3 2 0 348.98 329.55 14.48 o 4 2 0 51.18 52.21 3.77 o 5 2 0 47.17 51.93 4.75 o 6 2 0 35.65 23.06 5.87 o 1 0 1 453.34 483.24 12.90 o 2 0 1 1354.12 1373.92 20.89 o 3 0 1 25.25 26.74 1.47 o 4 0 1 96.70 97.20 2.93 o 5 0 1 82.85 85.65 3.20 o 6 0 1 1.49 1.96 4.13 o 7 0 1 141.83 146.10 6.41 o 8 0 1 1.58 1.39 9.19 o -8 1 1 0.67 -8.22 22.60 o -7 1 1 35.03 35.77 5.70 o -6 1 1 1.19 0.36 3.87 o -5 1 1 70.03 70.23 3.44 o -4 1 1 293.10 298.78 8.59 o -3 1 1 21.64 22.00 1.57 o -2 1 1 935.05 930.51 29.56 o -1 1 1 77.14 78.19 4.00 o 0 1 1 150.86 141.03 17.34 o 1 1 1 76.95 78.77 7.77 o 2 1 1 934.68 932.81 45.29 o 3 1 1 21.67 18.45 1.57 o 4 1 1 292.54 278.65 9.17 o 5 1 1 69.97 78.45 4.43 o 6 1 1 1.16 4.99 4.06 o 7 1 1 35.04 35.88 5.30 o 8 1 1 0.65 0.18 17.46 o -7 2 1 15.52 22.74 10.56 o -6 2 1 2.56 6.64 7.53 o -5 2 1 72.58 74.68 7.64 o -4 2 1 120.54 118.22 7.83 o -3 2 1 66.13 68.98 4.30 o -2 2 1 661.25 649.62 52.81 o 2 2 1 661.11 731.27 20.13 o 3 2 1 66.26 74.16 7.23 o 4 2 1 120.88 112.16 12.01 o 5 2 1 72.66 58.04 8.99 o 6 2 1 2.55 1.35 6.15 o 7 2 1 15.53 10.35 8.96 o 1 0 2 381.42 198.25 20.70 o 2 0 2 198.32 203.09 8.63 o 3 0 2 273.18 256.80 6.59 o 4 0 2 27.55 26.04 2.06 o 5 0 2 139.51 144.97 5.28 o 6 0 2 9.82 15.38 4.10 o 7 0 2 4.85 6.95 5.14 o 8 0 2 4.03 16.87 13.92 o -8 1 2 10.04 1.16 15.77 o -7 1 2 14.28 15.57 6.37 o -6 1 2 1.94 4.25 4.46 o -5 1 2 54.86 58.41 3.93 o -4 1 2 8.23 5.77 1.82 o -3 1 2 194.55 208.07 9.36 o -2 1 2 134.99 124.06 7.62 o -1 1 2 57.82 70.87 1.30 o 0 1 2 4079.37 4572.89 104.17 o 1 1 2 57.79 64.63 3.10 o 2 1 2 135.00 136.38 7.60 o 3 1 2 194.86 186.73 7.88 o 4 1 2 8.23 7.39 1.77 o 5 1 2 54.83 62.24 3.48 o 6 1 2 1.95 -1.15 4.37 o 7 1 2 14.29 19.29 6.16 o 8 1 2 9.98 17.69 12.98 o -7 2 2 8.51 11.12 10.80 o -6 2 2 29.57 30.59 7.00 o -5 2 2 42.79 37.72 5.21 o -4 2 2 35.73 36.45 3.69 o -3 2 2 126.56 131.61 5.91 o -2 2 2 328.49 346.30 18.33 o -1 2 2 98.31 83.84 7.87 o 0 2 2 939.58 1121.44 32.60 o 1 2 2 98.46 102.82 3.57 o 2 2 2 328.59 353.47 19.31 o 3 2 2 126.39 120.39 11.34 o 4 2 2 35.63 35.64 4.16 o 5 2 2 42.91 29.70 5.23 o 6 2 2 29.50 28.72 5.91 o 7 2 2 8.56 10.04 8.45 o -5 3 2 8.67 18.30 14.06 o -4 3 2 107.27 106.05 7.46 o -3 3 2 153.94 171.29 11.01 o -2 3 2 13.19 13.21 8.21 o 3 3 2 153.93 158.88 6.02 o 4 3 2 107.46 103.82 6.69 o 5 3 2 8.68 9.09 7.38 o 6 3 2 3.83 13.98 18.93 o 2 0 3 510.20 422.31 23.48 o 3 0 3 88.80 82.43 4.43 o 4 0 3 14.14 13.81 2.12 o 5 0 3 47.43 46.73 3.52 o 6 0 3 0.00 0.75 4.21 o 7 0 3 15.52 13.70 5.59 o -8 1 3 6.12 4.68 20.35 o -7 1 3 98.26 126.74 9.62 o -6 1 3 5.49 8.14 5.91 o -5 1 3 213.24 230.78 6.50 o -4 1 3 105.85 117.93 4.22 o -3 1 3 36.87 35.44 2.45 o -2 1 3 230.23 218.12 7.52 o -1 1 3 745.29 832.30 18.54 o 0 1 3 16.17 13.46 0.95 o 1 1 3 745.03 843.41 21.46 o 2 1 3 230.03 215.90 7.74 o 3 1 3 37.02 31.40 1.93 o 4 1 3 105.86 106.61 3.67 o 5 1 3 213.34 211.74 5.59 o 6 1 3 5.48 5.51 5.18 o 7 1 3 98.25 96.54 8.12 o -7 2 3 14.14 24.96 10.92 o -6 2 3 7.90 8.68 6.21 o -5 2 3 24.18 24.61 5.25 o -4 2 3 49.44 49.94 3.82 o -3 2 3 14.92 23.31 3.44 o -2 2 3 17.44 17.68 1.76 o -1 2 3 306.04 305.34 13.22 o 0 2 3 827.43 819.45 24.07 o 1 2 3 305.80 320.37 13.30 o 2 2 3 17.46 19.62 2.23 o 3 2 3 14.90 11.13 2.83 o 4 2 3 49.36 43.33 3.61 o 5 2 3 24.08 22.97 4.36 o 6 2 3 7.91 9.07 5.66 o 7 2 3 14.07 12.71 8.09 o -6 3 3 6.31 5.49 12.58 o -5 3 3 8.45 8.17 7.98 o -4 3 3 25.24 23.07 4.96 o -3 3 3 31.02 27.40 3.52 o -2 3 3 346.50 351.85 17.07 o -1 3 3 217.64 243.71 12.72 o 0 3 3 144.12 164.30 6.84 o 1 3 3 217.65 237.55 7.44 o 2 3 3 346.36 357.38 17.03 o 3 3 3 30.82 30.00 4.11 o 4 3 3 25.32 22.72 4.86 o 5 3 3 8.48 3.44 5.69 o 6 3 3 6.28 9.54 9.08 o 7 3 3 19.89 21.33 20.95 o 3 0 4 389.59 364.07 8.59 o 4 0 4 28.88 27.14 2.76 o 5 0 4 60.72 57.72 4.60 o 6 0 4 20.55 21.17 4.93 o 7 0 4 1.10 10.12 9.86 o -7 1 4 18.12 22.63 8.69 o -6 1 4 9.89 17.45 6.35 o -5 1 4 57.21 58.96 5.30 o -4 1 4 62.58 67.91 3.68 o -3 1 4 84.01 81.15 4.29 o -2 1 4 681.17 732.82 15.39 o -1 1 4 348.27 339.93 9.86 o 0 1 4 1345.12 1260.54 57.97 o 1 1 4 348.27 304.81 28.18 o 2 1 4 680.96 685.21 23.70 o 3 1 4 83.88 77.92 5.03 o 4 1 4 62.52 53.67 3.59 o 5 1 4 57.13 53.88 4.80 o 6 1 4 9.89 5.45 4.89 o 7 1 4 18.09 17.79 7.24 o -7 2 4 8.48 13.90 9.08 o -6 2 4 13.68 15.88 8.15 o -5 2 4 2.96 2.53 4.86 o -4 2 4 19.63 21.19 3.98 o -3 2 4 262.95 276.36 7.82 o -2 2 4 14.02 12.27 1.51 o -1 2 4 16.67 18.49 1.61 o 0 2 4 44.40 56.71 5.20 o 1 2 4 16.82 13.90 1.54 o 2 2 4 13.94 13.17 1.90 o 3 2 4 263.03 253.85 11.25 o 4 2 4 19.66 17.19 3.68 o 5 2 4 2.97 1.69 4.43 o 6 2 4 13.62 15.06 7.36 o 7 2 4 8.44 10.65 7.99 o -7 3 4 2.37 11.31 14.21 o -6 3 4 7.46 9.97 9.64 o -5 3 4 87.22 79.50 8.55 o -4 3 4 7.83 2.98 5.00 o -3 3 4 111.10 95.15 7.01 o -2 3 4 7.88 8.59 3.04 o -1 3 4 28.07 28.30 2.84 o 0 3 4 42.32 40.74 3.01 o 1 3 4 28.11 28.10 3.18 o 2 3 4 7.94 8.27 3.69 o 3 3 4 110.94 105.53 12.46 o 4 3 4 7.84 6.85 5.19 o 5 3 4 87.22 83.35 12.17 o 6 3 4 7.44 1.04 7.61 o 7 3 4 2.37 8.83 10.13 o -4 4 4 25.15 30.05 15.52 o -3 4 4 10.58 5.38 14.01 o -2 4 4 14.39 9.72 8.91 o -1 4 4 25.34 32.05 5.76 o 0 4 4 22.06 21.26 7.92 o 1 4 4 25.46 29.51 5.30 o 2 4 4 14.33 17.94 6.30 o 3 4 4 10.60 20.23 7.99 o 4 4 4 25.29 31.69 15.69 o 4 0 5 112.40 108.82 7.40 o 5 0 5 104.61 102.00 10.71 o 6 0 5 21.17 14.61 19.24 o -7 1 5 14.35 23.24 11.00 o -6 1 5 1.15 2.67 7.09 o -5 1 5 35.44 34.39 6.48 o -4 1 5 111.89 118.45 6.11 o -3 1 5 106.37 107.95 4.56 o -2 1 5 91.82 89.82 3.18 o -1 1 5 218.27 231.29 8.60 o 0 1 5 450.87 317.64 43.94 o 1 1 5 218.29 236.06 8.89 o 2 1 5 91.76 77.54 5.35 o 3 1 5 106.24 102.81 6.30 o 4 1 5 111.65 100.97 5.50 o 5 1 5 35.49 32.10 5.16 o 6 1 5 1.17 3.84 6.81 o 7 1 5 14.30 10.60 10.34 o -7 2 5 17.83 22.20 9.43 o -6 2 5 0.89 -1.19 8.39 o -5 2 5 18.84 20.82 6.36 o -4 2 5 53.07 55.35 4.04 o -3 2 5 25.57 26.80 2.63 o -2 2 5 227.29 214.75 8.42 o -1 2 5 244.22 262.35 7.94 o 0 2 5 7.63 7.93 1.69 o 1 2 5 243.69 233.69 9.46 o 2 2 5 227.00 221.36 4.45 o 3 2 5 25.53 21.25 2.45 o 4 2 5 53.08 44.87 3.59 o 5 2 5 18.79 15.99 5.73 o 6 2 5 0.88 5.91 7.37 o 7 2 5 17.82 21.10 8.03 o -7 3 5 5.92 0.03 12.95 o -6 3 5 5.52 8.47 8.66 o -5 3 5 18.07 18.38 6.71 o -4 3 5 144.03 143.89 6.23 o -3 3 5 14.52 9.78 4.08 o -2 3 5 274.05 242.06 14.24 o -1 3 5 12.33 10.50 2.62 o 0 3 5 85.22 79.55 4.49 o 1 3 5 12.36 9.77 3.02 o 2 3 5 274.06 278.23 17.32 o 3 3 5 14.49 10.63 4.04 o 4 3 5 144.20 132.64 12.30 o 5 3 5 18.04 17.23 6.24 o 6 3 5 5.56 5.22 7.83 o 7 3 5 5.90 6.27 10.34 o -5 4 5 3.26 13.08 19.80 o -4 4 5 0.64 2.06 8.45 o -3 4 5 26.26 19.12 6.50 o -2 4 5 102.58 109.56 8.34 o -1 4 5 43.58 55.57 9.12 o 0 4 5 8.37 4.75 5.10 o 1 4 5 43.49 50.95 7.83 o 2 4 5 102.76 98.37 9.29 o 3 4 5 26.20 22.66 6.46 o 4 4 5 0.64 2.83 7.58 o 5 4 5 3.25 3.85 10.29 o 6 4 5 13.41 5.19 18.56 o -7 1 6 13.70 12.04 12.08 o -6 1 6 0.14 -3.49 8.19 o -5 1 6 30.73 30.75 5.79 o -4 1 6 41.88 43.82 4.89 o -3 1 6 5.76 5.69 3.48 o -2 1 6 146.32 153.67 4.60 o -1 1 6 0.18 0.90 2.67 o 0 1 6 40.34 34.70 4.74 o 1 1 6 0.18 -0.22 3.18 o 2 1 6 146.08 137.27 5.87 o 3 1 6 5.83 7.92 2.74 o 4 1 6 41.85 34.10 4.24 o 5 1 6 30.76 22.82 5.35 o 6 1 6 0.14 1.87 8.87 o 7 1 6 13.70 7.99 13.20 o -7 2 6 6.83 6.85 9.60 o -6 2 6 39.78 41.32 9.08 o -5 2 6 16.43 15.89 6.82 o -4 2 6 23.56 27.01 5.32 o -3 2 6 91.64 105.92 5.06 o -2 2 6 158.78 175.18 4.07 o -1 2 6 35.66 40.03 2.82 o 0 2 6 1063.71 1125.53 29.42 o 1 2 6 35.70 37.09 2.99 o 2 2 6 158.92 160.14 8.69 o 3 2 6 91.56 93.11 4.24 o 4 2 6 23.67 23.61 4.32 o 5 2 6 16.48 18.53 5.98 o 6 2 6 39.80 42.07 7.72 o 7 2 6 6.83 -0.48 9.41 o -6 3 6 3.08 -0.30 9.27 o -5 3 6 11.08 11.43 6.99 o -4 3 6 60.61 62.36 5.49 o -3 3 6 48.24 43.02 3.90 o -2 3 6 64.14 67.80 3.45 o -1 3 6 1.73 4.71 2.78 o 0 3 6 1.02 3.21 2.99 o 1 3 6 1.72 2.89 2.76 o 2 3 6 64.16 65.80 3.97 o 3 3 6 48.15 40.94 4.04 o 4 3 6 60.75 61.79 8.08 o 5 3 6 11.14 14.35 6.45 o 6 3 6 3.12 5.36 8.16 o -5 4 6 40.53 33.79 11.02 o -4 4 6 0.36 -0.87 8.34 o -3 4 6 38.24 38.37 6.81 o -2 4 6 11.15 9.12 5.45 o -1 4 6 40.39 37.25 4.89 o 0 4 6 117.82 101.61 10.72 o 1 4 6 40.38 34.46 5.36 o 2 4 6 11.15 5.89 7.07 o 3 4 6 38.24 36.18 6.00 o 4 4 6 0.36 1.47 6.41 o 5 4 6 40.51 42.42 8.57 o 6 4 6 42.76 36.14 12.22 o -5 1 7 37.71 47.59 9.95 o -4 1 7 2.24 1.80 5.30 o -3 1 7 16.99 15.74 4.26 o -2 1 7 38.01 38.73 6.75 o 2 1 7 38.10 48.23 9.39 o 3 1 7 16.95 14.66 4.61 o 4 1 7 2.28 12.34 7.17 o 5 1 7 37.65 36.99 17.11 o -7 2 7 19.66 47.15 17.45 o -6 2 7 2.04 3.15 8.73 o -5 2 7 29.18 32.83 7.05 o -4 2 7 110.69 124.57 6.75 o -3 2 7 44.37 47.19 4.90 o -2 2 7 109.94 107.43 5.59 o -1 2 7 56.20 56.80 3.34 o 0 2 7 332.57 311.91 14.66 o 1 2 7 56.27 52.58 2.96 o 2 2 7 109.95 90.48 7.66 o 3 2 7 44.32 44.57 4.04 o 4 2 7 110.79 99.59 11.22 o 5 2 7 29.12 25.62 6.65 o 6 2 7 2.03 0.32 7.11 o 7 2 7 19.63 12.37 19.08 o -6 3 7 7.99 11.59 9.11 o -5 3 7 3.28 3.31 7.05 o -4 3 7 27.65 31.69 5.59 o -3 3 7 31.16 36.61 4.09 o -2 3 7 81.33 79.68 4.50 o -1 3 7 107.48 115.91 4.64 o 0 3 7 68.55 66.08 3.77 o 1 3 7 107.26 110.04 4.86 o 2 3 7 81.24 78.28 4.40 o 3 3 7 31.05 31.07 3.84 o 4 3 7 27.65 23.86 4.99 o 5 3 7 3.30 3.83 6.26 o 6 3 7 8.02 14.18 7.87 o -5 4 7 5.54 11.65 10.82 o -4 4 7 9.35 9.45 7.19 o -3 4 7 22.09 12.90 7.19 o -2 4 7 54.29 53.28 5.44 o -1 4 7 72.55 69.60 5.55 o 0 4 7 5.72 5.88 4.59 o 1 4 7 72.44 64.22 5.93 o 2 4 7 54.31 53.98 8.00 o 3 4 7 22.14 23.77 6.97 o 4 4 7 9.43 12.62 6.53 o 5 4 7 5.54 6.73 9.37 o 6 4 7 5.29 -1.03 19.05 o -3 5 7 2.35 -1.17 19.27 o -2 5 7 7.23 -0.99 9.77 o -1 5 7 11.98 6.55 10.02 o 0 5 7 7.67 5.87 8.50 o 1 5 7 11.94 6.50 7.24 o 2 5 7 7.28 8.90 8.34 o 3 5 7 2.35 1.04 8.96 o 4 5 7 28.56 31.44 18.67 o -6 2 8 5.08 5.83 12.91 o -5 2 8 28.67 24.75 8.24 o -4 2 8 2.90 1.08 6.22 o -3 2 8 233.96 250.16 8.47 o -2 2 8 54.87 51.57 5.87 o -1 2 8 7.71 8.36 3.87 o 0 2 8 0.01 -0.82 3.70 o 1 2 8 7.74 7.10 3.50 o 2 2 8 54.77 52.25 5.64 o 3 2 8 233.79 226.08 12.11 o 4 2 8 2.88 0.65 5.74 o 5 2 8 28.65 20.30 7.11 o 6 2 8 5.10 10.97 13.03 o -6 3 8 8.66 7.46 9.31 o -5 3 8 28.27 31.19 7.56 o -4 3 8 0.62 -0.75 7.86 o -3 3 8 26.18 29.66 4.82 o -2 3 8 47.47 43.91 4.77 o -1 3 8 73.71 79.01 5.01 o 0 3 8 17.28 19.24 4.04 o 1 3 8 73.65 76.93 5.17 o 2 3 8 47.48 51.60 4.80 o 3 3 8 26.22 28.00 4.93 o 4 3 8 0.63 1.40 6.32 o 5 3 8 28.28 22.28 6.49 o 6 3 8 8.65 7.11 7.55 o -5 4 8 1.55 3.52 9.75 o -4 4 8 9.90 14.23 8.40 o -3 4 8 16.72 15.58 7.66 o -2 4 8 24.38 18.62 5.10 o -1 4 8 32.78 25.82 5.23 o 0 4 8 5.15 7.86 5.01 o 1 4 8 32.87 32.31 5.20 o 2 4 8 24.46 24.64 5.18 o 3 4 8 16.72 17.58 7.43 o 4 4 8 9.92 12.12 7.82 o 5 4 8 1.57 3.14 9.03 o -4 5 8 5.47 1.12 20.87 o -3 5 8 16.93 4.56 14.00 o -2 5 8 6.33 9.74 8.39 o -1 5 8 9.35 12.08 8.55 o 0 5 8 0.32 -1.17 8.56 o 1 5 8 9.39 9.77 7.29 o 2 5 8 6.32 9.60 6.77 o 3 5 8 16.85 17.42 7.88 o 4 5 8 5.50 8.34 9.76 o -5 2 9 23.61 34.33 21.89 o -4 2 9 20.34 20.82 7.16 o -3 2 9 5.81 6.73 6.44 o -2 2 9 3.28 4.91 6.34 o -1 2 9 119.24 137.31 12.02 o 0 2 9 99.85 104.82 10.62 o 1 2 9 119.04 133.48 13.33 o 2 2 9 3.27 23.22 13.40 o 3 2 9 5.83 3.99 6.83 o 4 2 9 20.37 10.81 14.51 o -6 3 9 10.23 19.64 21.67 o -5 3 9 61.44 64.52 11.07 o -4 3 9 32.05 38.05 8.25 o -3 3 9 0.92 8.59 7.23 o -2 3 9 56.88 59.57 5.98 o -1 3 9 151.56 143.89 6.38 o 0 3 9 33.01 34.37 5.03 o 1 3 9 151.46 140.67 9.24 o 2 3 9 56.90 60.72 6.11 o 3 3 9 0.91 1.63 6.32 o 4 3 9 32.10 24.60 7.45 o 5 3 9 61.37 65.90 15.86 o -5 4 9 6.13 1.32 12.46 o -4 4 9 11.39 14.79 8.64 o -3 4 9 9.05 12.06 7.93 o -2 4 9 3.63 6.57 5.73 o -1 4 9 1.99 5.07 5.24 o 0 4 9 40.02 39.89 5.56 o 1 4 9 1.99 5.69 5.08 o 2 4 9 3.66 3.66 5.62 o 3 4 9 9.02 8.74 7.39 o 4 4 9 11.41 14.36 7.86 o 5 4 9 6.13 6.68 10.83 o -4 5 9 3.76 6.79 12.27 o -3 5 9 3.68 6.64 10.08 o -2 5 9 3.46 6.50 8.92 o -1 5 9 2.99 -1.15 7.14 o 0 5 9 4.79 6.01 7.08 o 1 5 9 2.98 0.13 6.88 o 2 5 9 3.44 0.41 7.25 o 3 5 9 3.72 3.57 8.66 o 4 5 9 3.76 3.52 10.01 o -5 3 10 5.58 12.01 12.54 o -4 3 10 2.28 0.96 9.86 o -3 3 10 26.91 31.59 9.34 o -2 3 10 70.63 76.96 9.00 o -1 3 10 26.60 25.14 5.91 o 0 3 10 4.89 7.91 6.66 o 1 3 10 26.61 22.96 7.16 o 2 3 10 70.71 66.52 6.76 o 3 3 10 26.88 27.28 7.11 o 4 3 10 2.28 3.50 9.54 o 5 3 10 5.60 -0.57 19.20 o -5 4 10 4.20 0.86 21.58 o -4 4 10 10.49 21.66 10.98 o -3 4 10 14.67 13.53 8.70 o -2 4 10 0.64 0.83 6.18 o -1 4 10 45.19 60.45 6.64 o 0 4 10 9.41 1.82 7.17 o 1 4 10 45.16 51.62 6.32 o 2 4 10 0.62 4.19 5.44 o 3 4 10 14.59 9.57 7.65 o 4 4 10 10.55 11.59 8.24 o -4 5 10 7.09 9.66 15.51 o -3 5 10 7.57 10.17 8.91 o -2 5 10 8.12 11.62 7.37 o -1 5 10 3.26 6.10 7.31 o 0 5 10 0.12 2.50 7.55 o 1 5 10 3.25 1.61 7.42 o 2 5 10 8.17 1.61 8.26 o 3 5 10 7.53 9.51 8.42 o 4 5 10 7.09 3.31 11.18 o -1 6 10 0.90 8.36 21.81 o 0 6 10 20.50 29.85 15.03 o 1 6 10 0.91 10.45 20.56 o -4 3 11 12.67 12.14 22.10 o -3 3 11 5.02 2.83 9.21 o -2 3 11 7.47 5.93 8.72 o -1 3 11 51.82 56.34 9.89 o 0 3 11 99.44 120.78 12.61 o 1 3 11 51.77 43.47 12.72 o 2 3 11 7.48 11.03 11.07 o -4 4 11 2.62 8.53 10.84 o -3 4 11 10.31 13.06 10.39 o -2 4 11 16.74 19.26 6.73 o -1 4 11 24.72 23.34 7.06 o 0 4 11 1.96 3.58 6.86 o 1 4 11 24.67 19.43 7.84 o 2 4 11 16.65 15.56 7.42 o 3 4 11 10.31 13.98 7.76 o 4 4 11 2.63 3.50 10.39 o -3 5 11 2.54 2.41 9.24 o -2 5 11 4.42 3.87 7.60 o -1 5 11 12.53 18.84 8.36 o 0 5 11 0.01 -5.98 8.09 o 1 5 11 12.56 16.51 8.29 o 2 5 11 4.42 -0.25 8.19 o 3 5 11 2.53 -2.64 8.43 o -1 6 11 1.29 16.33 18.23 o 0 6 11 0.15 -0.67 20.92 o 1 6 11 1.30 -0.71 21.09 o -3 4 12 7.70 15.56 10.52 o -2 4 12 6.55 10.25 10.11 o -1 4 12 22.72 30.74 11.61 o 0 4 12 46.07 41.93 9.59 o 1 4 12 22.72 26.70 9.32 o 2 4 12 6.59 6.78 10.62 o 3 4 12 7.66 2.51 21.07 o -2 5 12 19.34 18.90 9.70 o -1 5 12 4.51 9.57 8.81 o 0 5 12 8.07 8.68 8.02 o 1 5 12 4.50 2.84 8.94 o 2 5 12 19.36 15.47 8.99 o 0 4 13 19.60 3.79 21.44 o -1 5 13 5.35 2.32 19.93 o 0 5 13 0.08 -2.10 15.09 o 1 5 13 5.34 5.73 15.04 o