#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180907 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104802.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104802_Fobs loop_ _publ_author_name 'Vande Velde, Christophe M. L.' 'Tylleman, Beno\^it' 'Zeller, Matthias' 'Sergeyev, Sergey' _publ_section_title ; Structures of alkyl-substituted Tr\"oger's base derivatives illustrate the importance of Z' for packing in the absence of strong crystal synthons ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 472 _journal_page_last 481 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.713 _cell_angle_gamma 90.000 _cell_length_a 14.9437 _cell_length_b 33.2588 _cell_length_c 10.7536 _exptl_crystal_F_000 1992.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file ry5032beta3asup5.hkl _cod_data_source_block beta3a #BEGIN Tags that were not found in dictionaries: _shelx_title beta3a _shelx_refln_list_code 4 _shelx_f_calc_maximum 469.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 22660.17 21803.83 157.19 o 2 0 0 3433.13 3296.53 48.99 o 3 0 0 13977.44 13179.20 143.76 o 4 0 0 102.38 114.64 18.61 o 5 0 0 7512.81 6965.83 79.60 o 6 0 0 617.51 579.11 34.31 o 7 0 0 30.28 10.54 16.32 o 8 0 0 129.27 161.01 24.48 o 9 0 0 1074.83 1133.03 46.55 o 10 0 0 669.90 785.72 41.31 o 11 0 0 7456.27 7167.40 118.61 o 12 0 0 133.48 199.59 25.61 o 13 0 0 700.06 661.80 65.00 o 14 0 0 744.97 761.31 94.91 o 15 0 0 134.81 109.90 33.91 o 16 0 0 119.42 131.46 56.28 o 17 0 0 420.77 435.60 55.38 o 18 0 0 8.86 46.25 45.21 o 19 0 0 10.74 79.91 44.23 o 1 1 0 1.40 2.73 2.99 o 2 1 0 83.60 77.07 7.37 o 3 1 0 71.58 66.85 9.80 o 4 1 0 101.60 96.53 12.28 o 5 1 0 26.39 29.22 11.09 o 6 1 0 28.71 41.84 12.15 o 7 1 0 138.68 148.22 16.28 o 8 1 0 81.94 86.87 14.84 o 9 1 0 279.06 299.82 20.74 o 10 1 0 197.52 190.10 18.58 o 11 1 0 66.06 106.36 15.79 o 12 1 0 0.02 -1.72 7.63 o 13 1 0 0.24 -0.53 17.02 o 14 1 0 53.58 74.00 23.06 o 15 1 0 30.37 35.59 19.33 o 16 1 0 16.63 10.51 16.50 o 17 1 0 50.72 94.68 22.92 o 18 1 0 5.76 -26.41 34.39 o 19 1 0 3.34 11.51 28.90 o 0 2 0 129.14 85.07 15.72 o 1 2 0 5.60 2.55 3.70 o 2 2 0 16.06 16.83 6.42 o 3 2 0 64.76 49.70 9.63 o 4 2 0 0.55 0.11 10.36 o 5 2 0 10.78 7.19 10.21 o 6 2 0 21.63 26.71 11.20 o 7 2 0 4.28 1.43 14.16 o 8 2 0 13.59 -1.58 11.26 o 9 2 0 129.88 146.73 17.15 o 10 2 0 94.97 105.70 15.36 o 11 2 0 375.85 367.39 26.63 o 12 2 0 178.08 191.56 17.20 o 13 2 0 21.34 6.97 17.30 o 14 2 0 138.13 148.98 31.15 o 15 2 0 101.23 78.03 22.91 o 16 2 0 4.61 15.44 20.98 o 17 2 0 3.29 70.15 21.33 o 18 2 0 17.63 14.08 29.07 o 19 2 0 76.51 35.13 31.11 o 1 3 0 92703.58 90827.33 415.20 o 2 3 0 1108.70 1112.37 17.72 o 3 3 0 4347.74 4130.82 36.17 o 4 3 0 2826.48 2980.53 35.19 o 5 3 0 139.12 174.47 14.92 o 6 3 0 991.64 1087.37 27.84 o 7 3 0 1100.81 1190.63 30.64 o 8 3 0 1067.74 1170.42 37.65 o 9 3 0 18316.84 18890.22 132.85 o 10 3 0 152.41 235.62 20.55 o 11 3 0 513.03 530.02 26.16 o 12 3 0 3275.73 3334.53 59.90 o 13 3 0 7.29 17.19 12.60 o 14 3 0 3317.47 3167.85 88.86 o 15 3 0 326.95 335.56 37.05 o 16 3 0 8.32 16.94 22.41 o 17 3 0 723.27 763.38 63.62 o 18 3 0 14.93 15.33 20.80 o 19 3 0 50.61 42.00 53.39 o 0 4 0 327.95 258.08 15.46 o 1 4 0 157.64 145.58 9.41 o 2 4 0 12.85 7.50 7.53 o 3 4 0 1.54 -5.67 8.75 o 4 4 0 63.68 49.41 11.50 o 5 4 0 0.23 -4.52 9.66 o 6 4 0 4.36 -0.05 10.29 o 7 4 0 28.64 30.93 11.61 o 8 4 0 55.09 57.23 12.95 o 9 4 0 493.18 514.88 30.50 o 10 4 0 6.01 -9.13 13.74 o 11 4 0 91.83 86.61 13.36 o 12 4 0 510.05 469.48 23.47 o 13 4 0 175.95 154.73 20.77 o 14 4 0 535.77 566.74 47.89 o 15 4 0 221.14 214.01 30.44 o 16 4 0 74.43 101.28 27.06 o 17 4 0 0.63 51.40 55.63 o 18 4 0 1.21 5.24 19.83 o 19 4 0 18.57 49.33 29.51 o 1 5 0 67.73 70.31 8.68 o 2 5 0 79.14 77.25 9.70 o 3 5 0 8.49 15.68 9.59 o 4 5 0 14.44 9.95 10.22 o 5 5 0 3.70 7.06 10.47 o 6 5 0 117.79 103.17 14.61 o 7 5 0 45.25 20.63 11.54 o 8 5 0 107.58 105.86 15.21 o 9 5 0 74.01 76.67 14.56 o 10 5 0 5.17 20.83 15.34 o 11 5 0 155.17 126.03 14.84 o 12 5 0 14.00 -4.32 14.99 o 13 5 0 158.25 140.99 19.01 o 14 5 0 122.68 187.72 29.66 o 15 5 0 19.25 37.99 15.25 o 16 5 0 4.49 33.75 23.76 o 17 5 0 110.96 115.06 28.99 o 18 5 0 2.29 7.84 23.97 o 19 5 0 26.79 30.41 28.21 o 0 6 0 220191.36 214891.39 818.81 o 1 6 0 12751.97 12408.50 59.04 o 2 6 0 305.96 284.91 14.05 o 3 6 0 877.51 662.16 21.54 o 4 6 0 93.15 111.77 12.98 o 5 6 0 569.38 582.64 22.30 o 6 6 0 508.39 632.25 24.50 o 7 6 0 3691.87 4048.55 53.10 o 8 6 0 1398.35 1561.47 36.57 o 9 6 0 3610.31 3539.92 55.17 o 10 6 0 3618.66 3794.10 66.68 o 11 6 0 225.93 244.82 25.90 o 12 6 0 2257.57 2322.25 49.80 o 13 6 0 2737.25 2637.26 65.19 o 14 6 0 713.17 838.05 49.00 o 15 6 0 840.13 918.15 64.38 o 16 6 0 26.99 7.52 20.28 o 17 6 0 1586.99 1559.24 82.50 o 18 6 0 33.72 11.23 32.71 o 19 6 0 35.58 53.46 26.00 o 1 7 0 7.78 15.32 9.29 o 2 7 0 1.53 -8.97 8.97 o 3 7 0 16.38 13.24 10.13 o 4 7 0 57.05 65.74 11.74 o 5 7 0 465.23 491.37 20.90 o 6 7 0 278.14 292.80 18.97 o 7 7 0 358.02 352.17 21.57 o 8 7 0 47.01 42.75 11.65 o 9 7 0 70.03 80.37 15.00 o 10 7 0 124.86 117.53 16.37 o 11 7 0 142.89 170.43 17.87 o 12 7 0 55.07 55.08 10.11 o 13 7 0 0.72 4.72 11.56 o 14 7 0 20.73 19.93 17.10 o 15 7 0 127.13 127.57 40.74 o 16 7 0 220.60 239.95 39.91 o 17 7 0 84.98 157.52 34.77 o 18 7 0 8.94 29.30 22.50 o 19 7 0 19.14 -4.62 26.95 o 0 8 0 9.86 9.05 16.62 o 1 8 0 4.25 13.25 10.06 o 2 8 0 0.51 18.10 12.53 o 3 8 0 177.94 188.09 15.48 o 4 8 0 118.61 113.01 13.85 o 5 8 0 2.20 -2.84 9.84 o 6 8 0 6.74 27.31 11.42 o 7 8 0 95.28 92.11 14.74 o 8 8 0 9.53 20.21 11.14 o 9 8 0 95.51 95.98 15.23 o 10 8 0 19.57 27.44 11.01 o 11 8 0 102.80 133.53 16.56 o 12 8 0 382.66 391.80 32.24 o 13 8 0 92.67 96.62 15.74 o 14 8 0 67.56 99.43 19.05 o 15 8 0 25.00 87.60 26.17 o 16 8 0 31.85 53.19 26.41 o 17 8 0 24.20 83.53 26.34 o 18 8 0 3.39 13.89 35.39 o 1 9 0 1094.92 1146.17 25.71 o 2 9 0 490.75 461.03 21.38 o 3 9 0 3490.70 3419.10 40.23 o 4 9 0 4.26 18.93 11.01 o 5 9 0 1978.70 2138.46 37.31 o 6 9 0 373.74 478.31 23.23 o 7 9 0 1475.05 1435.68 35.13 o 8 9 0 8748.87 9035.66 84.55 o 9 9 0 5968.79 6333.16 74.94 o 10 9 0 1076.18 1186.65 35.79 o 11 9 0 8699.08 8261.80 92.57 o 12 9 0 700.18 758.37 38.84 o 13 9 0 159.75 144.16 17.85 o 14 9 0 889.75 927.53 65.17 o 15 9 0 359.33 392.19 49.85 o 16 9 0 705.33 686.36 66.45 o 17 9 0 378.67 358.68 50.60 o 18 9 0 423.38 414.10 48.58 o 0 10 0 342.73 301.74 27.18 o 1 10 0 420.16 374.65 20.98 o 2 10 0 796.90 718.23 29.07 o 3 10 0 468.62 429.73 20.19 o 4 10 0 152.80 151.86 14.57 o 5 10 0 121.48 124.38 16.81 o 6 10 0 737.08 739.34 26.70 o 7 10 0 296.19 313.91 21.95 o 8 10 0 143.84 140.58 17.03 o 9 10 0 32.25 55.01 13.01 o 10 10 0 68.83 66.47 13.22 o 11 10 0 70.50 96.50 13.17 o 12 10 0 7.37 44.07 13.43 o 13 10 0 12.90 20.24 11.53 o 14 10 0 14.35 39.94 37.22 o 15 10 0 16.10 23.44 23.18 o 16 10 0 7.38 1.32 22.38 o 17 10 0 60.79 31.62 25.72 o 18 10 0 10.28 7.92 27.14 o 1 11 0 297.47 284.34 19.80 o 2 11 0 38.81 18.94 9.30 o 3 11 0 98.27 83.36 15.52 o 4 11 0 117.67 114.15 14.02 o 5 11 0 0.49 3.69 10.39 o 6 11 0 31.66 40.15 12.57 o 7 11 0 248.70 256.04 20.25 o 8 11 0 48.09 63.02 13.66 o 9 11 0 31.66 42.56 12.76 o 10 11 0 203.05 254.43 19.71 o 11 11 0 193.05 211.03 19.68 o 12 11 0 6.84 7.98 11.50 o 13 11 0 292.54 325.87 42.86 o 14 11 0 109.86 145.45 33.06 o 15 11 0 87.48 109.55 31.14 o 16 11 0 49.10 37.63 25.44 o 17 11 0 162.02 155.93 48.61 o 18 11 0 4.51 16.36 20.50 o 0 12 0 95325.70 91043.23 738.94 o 1 12 0 22780.82 23144.53 213.65 o 2 12 0 38.54 34.65 9.65 o 3 12 0 13768.00 14419.45 95.64 o 4 12 0 12040.53 12608.85 94.18 o 5 12 0 1439.58 1566.01 34.83 o 6 12 0 66.88 81.99 14.71 o 7 12 0 2366.61 2556.14 46.50 o 8 12 0 3403.25 3471.26 55.81 o 9 12 0 243.82 285.27 22.71 o 10 12 0 3077.77 2896.03 55.49 o 11 12 0 280.56 279.18 24.69 o 12 12 0 4.60 11.19 10.18 o 13 12 0 1.06 21.84 17.19 o 14 12 0 2532.64 2450.67 96.85 o 15 12 0 15.07 41.95 24.25 o 16 12 0 4.99 40.89 24.52 o 17 12 0 182.13 203.50 37.40 o 18 12 0 249.49 222.67 54.92 o 1 13 0 58.30 84.24 22.71 o 2 13 0 910.44 852.27 25.35 o 3 13 0 566.77 548.80 25.21 o 4 13 0 5.40 16.92 12.62 o 5 13 0 776.73 805.04 27.85 o 6 13 0 344.14 354.05 22.55 o 7 13 0 9.28 11.47 10.91 o 8 13 0 10.12 11.41 9.82 o 9 13 0 1.38 -10.36 10.36 o 10 13 0 44.86 57.06 13.43 o 11 13 0 187.92 181.35 16.87 o 12 13 0 64.90 45.74 12.50 o 13 13 0 6.13 6.75 15.75 o 14 13 0 2.34 22.53 11.01 o 15 13 0 134.30 143.70 48.60 o 16 13 0 83.92 83.63 29.78 o 17 13 0 24.05 31.37 29.34 o 18 13 0 36.00 44.34 22.60 o 0 14 0 187.53 186.86 25.78 o 1 14 0 28.14 32.64 12.01 o 2 14 0 147.12 187.15 14.57 o 3 14 0 437.39 474.61 24.29 o 4 14 0 376.68 394.76 24.57 o 5 14 0 21.48 10.56 12.02 o 6 14 0 18.44 15.00 11.36 o 7 14 0 183.26 213.40 19.54 o 8 14 0 20.38 11.04 11.86 o 9 14 0 440.86 468.77 26.01 o 10 14 0 15.10 5.36 9.22 o 11 14 0 51.24 39.66 11.27 o 12 14 0 247.38 271.97 33.41 o 13 14 0 75.27 88.99 25.70 o 14 14 0 0.27 93.78 32.25 o 15 14 0 41.05 97.22 28.91 o 16 14 0 3.86 0.67 21.63 o 17 14 0 23.97 35.88 22.83 o 18 14 0 7.99 24.66 19.78 o 1 15 0 626.67 651.32 24.32 o 2 15 0 8549.90 8806.01 76.62 o 3 15 0 6302.52 6519.28 76.72 o 4 15 0 36.81 47.27 14.03 o 5 15 0 10908.49 12082.20 104.21 o 6 15 0 524.07 502.15 24.82 o 7 15 0 557.20 556.98 26.06 o 8 15 0 228.45 282.16 22.52 o 9 15 0 127.76 125.13 15.85 o 10 15 0 1533.81 1498.57 41.93 o 11 15 0 1840.04 1734.32 52.04 o 12 15 0 2704.67 2671.78 78.85 o 13 15 0 11.41 28.86 16.26 o 14 15 0 1514.50 1443.68 58.82 o 15 15 0 55.50 103.52 28.19 o 16 15 0 553.85 646.07 61.97 o 17 15 0 48.31 68.43 31.84 o 18 15 0 118.19 128.32 58.29 o 0 16 0 26.26 -0.24 14.95 o 1 16 0 0.04 0.13 9.89 o 2 16 0 108.46 199.65 20.16 o 3 16 0 673.14 716.92 28.60 o 4 16 0 1001.89 1023.44 35.54 o 5 16 0 123.90 143.75 18.48 o 6 16 0 16.91 9.12 10.63 o 7 16 0 73.84 74.64 13.97 o 8 16 0 0.40 12.72 11.43 o 9 16 0 330.78 332.06 24.94 o 10 16 0 8.39 16.07 11.14 o 11 16 0 211.83 241.14 32.36 o 12 16 0 55.35 94.66 22.54 o 13 16 0 0.33 23.67 16.12 o 14 16 0 24.85 45.61 17.85 o 15 16 0 70.69 71.02 36.96 o 16 16 0 33.16 64.12 20.68 o 17 16 0 11.83 69.18 23.69 o 1 17 0 79.33 95.62 13.83 o 2 17 0 483.87 505.58 24.95 o 3 17 0 0.01 -3.93 10.83 o 4 17 0 119.10 147.93 17.99 o 5 17 0 15.91 19.83 11.38 o 6 17 0 142.43 157.35 20.01 o 7 17 0 6.31 19.16 10.33 o 8 17 0 21.92 2.77 9.38 o 9 17 0 19.09 20.97 11.99 o 10 17 0 234.65 216.23 17.75 o 11 17 0 51.56 62.21 22.29 o 12 17 0 168.01 161.54 27.40 o 13 17 0 160.00 111.54 23.19 o 14 17 0 126.55 137.32 21.15 o 15 17 0 51.87 61.43 22.61 o 16 17 0 10.08 46.32 28.98 o 17 17 0 33.16 10.47 18.02 o 0 18 0 25617.89 27916.42 219.49 o 1 18 0 10025.79 11021.04 91.23 o 2 18 0 174.15 280.68 17.72 o 3 18 0 2251.44 2276.61 45.90 o 4 18 0 3616.04 4040.26 62.48 o 5 18 0 640.87 691.35 30.03 o 6 18 0 1276.05 1325.66 40.48 o 7 18 0 594.51 532.07 30.14 o 8 18 0 1468.23 1437.16 39.28 o 9 18 0 338.24 381.10 24.28 o 10 18 0 2.99 16.84 10.32 o 11 18 0 14.99 24.83 17.30 o 12 18 0 238.44 260.23 32.81 o 13 18 0 186.11 190.28 36.16 o 14 18 0 794.51 731.33 58.04 o 15 18 0 959.58 1000.94 64.68 o 16 18 0 1400.91 1445.23 76.90 o 17 18 0 25.77 101.84 40.13 o 1 19 0 5.54 168.94 19.96 o 2 19 0 155.73 208.84 14.34 o 3 19 0 49.67 36.57 12.69 o 4 19 0 288.52 327.84 24.75 o 5 19 0 86.66 103.40 16.92 o 6 19 0 128.39 135.71 18.71 o 7 19 0 0.06 5.07 10.33 o 8 19 0 10.50 18.11 10.16 o 9 19 0 17.32 28.40 8.62 o 10 19 0 186.54 206.33 22.94 o 11 19 0 241.48 236.95 31.79 o 12 19 0 208.11 166.57 29.17 o 13 19 0 120.76 123.51 21.72 o 14 19 0 26.40 33.66 13.38 o 15 19 0 0.13 60.98 35.16 o 16 19 0 229.96 277.11 60.58 o 17 19 0 111.75 216.72 55.80 o 0 20 0 321.86 321.24 29.07 o 1 20 0 795.67 708.52 26.39 o 2 20 0 904.35 839.05 28.05 o 3 20 0 408.13 430.93 25.04 o 4 20 0 202.95 264.10 20.98 o 5 20 0 111.45 116.37 16.98 o 6 20 0 34.78 31.29 12.44 o 7 20 0 25.45 71.16 37.45 o 8 20 0 3.08 28.48 11.82 o 9 20 0 0.00 32.04 11.90 o 10 20 0 249.50 255.52 24.92 o 11 20 0 48.65 32.52 17.55 o 12 20 0 29.28 24.69 19.40 o 13 20 0 75.32 109.63 19.81 o 14 20 0 143.28 133.95 18.36 o 15 20 0 0.20 14.02 35.04 o 16 20 0 8.61 56.45 39.31 o 17 20 0 11.49 79.75 40.93 o 1 21 0 0.27 16.84 8.57 o 2 21 0 59.56 57.89 9.19 o 3 21 0 1445.80 1526.93 49.29 o 4 21 0 462.70 479.68 34.47 o 5 21 0 495.08 564.74 28.78 o 6 21 0 519.20 467.30 28.42 o 7 21 0 1206.28 1277.02 42.30 o 8 21 0 9554.92 8660.51 109.24 o 9 21 0 7468.95 7019.93 101.84 o 10 21 0 355.32 459.59 38.31 o 11 21 0 61.23 96.61 21.56 o 12 21 0 810.36 801.70 45.05 o 13 21 0 274.00 291.02 29.94 o 14 21 0 23.63 19.64 20.02 o 15 21 0 3215.34 3223.75 152.64 o 16 21 0 237.25 189.12 56.08 o 0 22 0 0.34 2.72 11.85 o 1 22 0 150.28 157.86 16.46 o 2 22 0 484.86 438.39 22.04 o 3 22 0 261.60 303.97 29.95 o 4 22 0 42.16 67.87 15.15 o 5 22 0 0.80 8.67 12.33 o 6 22 0 104.06 106.52 16.08 o 7 22 0 100.52 91.66 16.01 o 8 22 0 3.29 44.43 17.75 o 9 22 0 281.76 234.33 23.63 o 10 22 0 0.09 17.68 9.87 o 11 22 0 3.42 17.54 16.73 o 12 22 0 159.51 161.19 33.18 o 13 22 0 514.74 472.03 55.04 o 14 22 0 549.96 619.99 55.95 o 15 22 0 120.65 156.67 48.76 o 16 22 0 147.49 186.76 53.62 o 1 23 0 1.88 15.17 8.75 o 2 23 0 4.86 6.13 13.65 o 3 23 0 3.46 -2.40 14.91 o 4 23 0 4.03 18.12 8.85 o 5 23 0 0.68 20.46 8.76 o 6 23 0 33.52 57.19 16.70 o 7 23 0 104.71 108.08 14.66 o 8 23 0 86.94 101.33 14.86 o 9 23 0 206.52 162.78 24.56 o 10 23 0 195.98 165.00 18.30 o 11 23 0 126.41 136.97 49.15 o 12 23 0 127.32 110.63 28.86 o 13 23 0 33.69 26.23 19.52 o 14 23 0 19.65 0.43 25.93 o 15 23 0 292.73 308.92 65.79 o 16 23 0 30.55 84.30 46.30 o 0 24 0 179.45 203.44 25.67 o 1 24 0 64.65 77.65 10.87 o 2 24 0 1172.22 1098.69 33.70 o 3 24 0 220.78 237.96 27.92 o 4 24 0 987.24 920.86 34.30 o 5 24 0 466.91 446.91 27.07 o 6 24 0 1768.78 1866.42 50.16 o 7 24 0 3953.14 3531.14 70.38 o 8 24 0 2299.83 2023.58 54.80 o 9 24 0 242.27 370.68 36.59 o 10 24 0 266.50 256.77 29.74 o 11 24 0 16.92 24.17 20.64 o 12 24 0 307.32 276.83 41.92 o 13 24 0 1190.17 1142.58 69.16 o 14 24 0 474.61 536.55 48.44 o 15 24 0 620.61 819.87 96.99 o 16 24 0 2782.63 2906.40 150.46 o 1 25 0 170.96 201.18 14.63 o 2 25 0 31.91 42.67 16.25 o 3 25 0 92.47 113.67 25.99 o 4 25 0 65.11 50.15 10.36 o 5 25 0 74.70 95.42 14.14 o 6 25 0 4.62 -7.90 13.53 o 7 25 0 71.37 43.89 18.79 o 8 25 0 0.06 4.04 13.87 o 9 25 0 16.85 11.17 13.70 o 10 25 0 3.42 56.32 23.32 o 11 25 0 3.06 34.75 20.23 o 12 25 0 1.70 33.25 32.55 o 13 25 0 44.41 51.57 24.00 o 14 25 0 300.04 283.40 44.87 o 15 25 0 450.81 496.94 78.90 o 0 26 0 507.30 435.62 30.21 o 1 26 0 501.15 488.08 22.46 o 2 26 0 56.91 41.62 6.62 o 3 26 0 1.60 19.48 10.31 o 4 26 0 1.21 8.42 20.72 o 5 26 0 1.35 -7.14 14.72 o 6 26 0 9.66 21.94 15.94 o 7 26 0 52.39 72.14 19.72 o 8 26 0 115.11 127.02 23.40 o 9 26 0 21.54 40.95 15.34 o 10 26 0 98.42 88.03 27.45 o 11 26 0 29.49 35.73 20.55 o 12 26 0 58.66 45.37 32.75 o 13 26 0 170.68 197.77 34.48 o 14 26 0 38.27 -27.02 40.77 o 15 26 0 224.59 199.41 54.26 o 1 27 0 126.22 130.15 19.35 o 2 27 0 1328.77 1225.86 47.35 o 3 27 0 283.78 311.23 32.62 o 4 27 0 617.53 653.78 40.36 o 5 27 0 999.23 1073.81 48.41 o 6 27 0 1569.54 1575.96 58.83 o 7 27 0 4633.00 4463.88 98.43 o 8 27 0 11182.83 10105.91 150.78 o 9 27 0 1055.12 1146.38 53.22 o 10 27 0 103.60 97.26 28.68 o 11 27 0 312.62 323.54 44.15 o 12 27 0 62.28 90.25 24.58 o 13 27 0 845.44 948.08 64.72 o 14 27 0 86.18 60.62 33.57 o 15 27 0 1742.95 1781.04 115.55 o 0 28 0 3927.26 3534.70 123.21 o 1 28 0 1452.23 1273.72 44.78 o 2 28 0 75.06 102.44 17.14 o 3 28 0 8.49 -7.51 12.35 o 4 28 0 36.52 46.94 14.77 o 5 28 0 23.41 59.55 17.19 o 6 28 0 100.81 115.30 25.08 o 7 28 0 0.20 47.80 18.01 o 8 28 0 6.05 139.95 29.08 o 9 28 0 58.97 43.20 21.91 o 10 28 0 45.90 64.48 30.33 o 11 28 0 19.51 33.91 23.74 o 12 28 0 0.17 24.97 34.13 o 13 28 0 53.52 109.46 28.98 o 14 28 0 3.51 8.55 16.36 o 1 29 0 23.42 78.01 21.30 o 2 29 0 157.83 188.35 34.33 o 3 29 0 135.34 143.93 20.13 o 4 29 0 36.07 18.05 11.28 o 5 29 0 90.83 141.70 25.75 o 6 29 0 9.21 19.64 14.05 o 7 29 0 244.17 192.81 28.31 o 8 29 0 54.12 111.90 21.64 o 9 29 0 12.54 3.47 11.81 o 10 29 0 21.69 46.56 37.03 o 11 29 0 46.18 16.31 22.28 o 12 29 0 13.97 12.40 27.45 o 13 29 0 16.57 49.95 17.93 o 14 29 0 36.02 37.21 22.05 o 0 30 0 324.42 526.56 64.71 o 1 30 0 2932.16 2339.65 73.77 o 2 30 0 1634.00 1371.64 68.18 o 3 30 0 627.66 646.71 59.53 o 4 30 0 73.76 84.38 20.08 o 5 30 0 595.48 654.65 41.88 o 6 30 0 71.14 79.02 19.51 o 7 30 0 112.77 97.64 21.27 o 8 30 0 201.76 196.64 28.78 o 9 30 0 143.11 135.40 22.04 o 10 30 0 10.77 12.73 20.44 o 11 30 0 58.31 28.50 24.49 o 12 30 0 0.38 16.80 32.40 o 13 30 0 295.73 159.93 41.53 o 14 30 0 85.73 72.01 24.57 o 1 31 0 1027.34 1126.93 58.23 o 2 31 0 1167.33 1175.63 64.75 o 3 31 0 370.65 308.37 43.96 o 4 31 0 33.14 18.74 28.71 o 5 31 0 0.39 19.99 21.58 o 6 31 0 0.02 5.93 10.00 o 7 31 0 7.45 11.60 12.00 o 8 31 0 80.64 73.85 18.02 o 9 31 0 288.81 233.44 27.90 o 10 31 0 333.96 302.78 42.94 o 11 31 0 96.95 55.30 25.26 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