#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/49/2104976.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104976_Fobs loop_ _publ_author_name 'Solanko, Katarzyna A.' 'Bond, Andrew D.' _publ_section_title ; Intermolecular interactions and unexpected isostructurality in the crystal structures of the dichlorobenzaldehyde isomers ; _journal_coeditor_code GP5044 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 437 _journal_page_last 445 _journal_volume 67 _journal_year 2011 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.849 _cell_angle_gamma 90.000 _cell_length_a 3.8094 _cell_length_b 14.8887 _cell_length_c 6.2014 _exptl_crystal_F_000 176.00 _reflns_d_resolution_high 0.8119 _[local]_cod_data_source_file gp50445sup4.hkl _[local]_cod_data_source_block 5 #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 70.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -17 0 116.00 132.68 5.70 o 1 -16 0 42.48 48.04 3.61 o 2 -16 0 6.07 6.30 3.10 o 1 -15 0 39.56 43.51 3.20 o 2 -15 0 33.51 25.86 4.74 o 0 -14 0 241.80 261.11 5.78 o 1 -14 0 18.80 19.52 1.58 o 2 -14 0 79.89 79.74 6.00 o 1 -13 0 59.31 63.68 1.80 o 2 -13 0 18.26 17.08 3.70 o 3 -13 0 6.49 4.60 4.19 o 0 -12 0 124.99 124.84 2.44 o 1 -12 0 530.74 539.65 7.92 o 2 -12 0 99.30 103.56 3.54 o 3 -12 0 36.69 36.74 3.55 o 1 -11 0 265.53 268.35 3.69 o 2 -11 0 386.54 388.26 8.27 o 3 -11 0 19.24 14.53 2.42 o 0 -10 0 16.45 17.12 1.00 o 1 -10 0 261.26 252.28 3.19 o 2 -10 0 505.70 507.36 8.82 o 3 -10 0 29.38 27.79 2.92 o 1 -9 0 101.81 95.74 1.46 o 2 -9 0 1.66 2.35 1.01 o 3 -9 0 42.72 39.47 2.74 o 4 -9 0 57.96 56.90 5.75 o 0 -8 0 14.36 19.10 0.91 o 1 -8 0 195.56 184.03 2.14 o 2 -8 0 513.79 498.66 7.43 o 3 -8 0 17.25 16.18 1.63 o 4 -8 0 39.61 42.83 4.57 o 1 -7 0 788.00 799.76 8.10 o 2 -7 0 149.66 153.60 2.42 o 3 -7 0 33.66 31.55 1.74 o 4 -7 0 36.33 41.54 4.09 o 0 -6 0 644.51 611.29 8.20 o 1 -6 0 1222.56 1217.87 12.34 o 2 -6 0 637.64 621.15 8.48 o 3 -6 0 77.32 75.09 2.87 o 4 -6 0 46.97 51.54 3.99 o 1 -5 0 218.81 209.29 2.96 o 2 -5 0 250.21 245.49 3.64 o 3 -5 0 29.09 27.76 2.63 o 4 -5 0 70.41 74.60 4.48 o 0 -4 0 2295.95 2219.59 29.85 o 1 -4 0 139.41 131.28 1.88 o 2 -4 0 176.89 167.96 2.60 o 3 -4 0 365.74 357.44 11.77 o 1 -3 0 83.40 78.52 1.15 o 2 -3 0 36.29 35.91 0.94 o 3 -3 0 108.08 108.78 2.68 o 1 -2 0 1298.85 1323.30 17.96 o 2 -2 0 42.61 42.39 1.00 o 3 -2 0 413.23 384.47 12.52 o 1 -1 0 2484.34 2592.28 35.05 o 2 -1 0 252.91 237.11 4.42 o 3 -1 0 12.86 15.49 1.99 o 1 0 0 2.27 3.29 0.22 o 2 0 0 5.97 4.96 0.62 o 3 0 0 523.60 483.98 15.70 o 1 1 0 2518.75 2646.22 35.03 o 2 1 0 248.95 240.19 4.06 o 3 1 0 12.12 15.46 1.76 o 1 2 0 1299.71 1353.03 17.74 o 2 2 0 42.14 41.82 1.02 o 3 2 0 413.99 394.53 7.31 o 4 2 0 118.03 113.91 4.55 o 1 3 0 78.94 74.63 1.16 o 2 3 0 36.45 37.13 0.97 o 3 3 0 109.23 108.94 2.27 o 4 3 0 35.95 38.93 2.98 o 0 4 0 2329.93 2237.30 28.40 o 1 4 0 133.26 125.43 1.99 o 2 4 0 178.69 171.47 2.60 o 3 4 0 364.14 351.01 7.63 o 4 4 0 129.84 138.51 8.44 o 1 5 0 221.76 214.95 2.82 o 2 5 0 253.31 247.64 3.84 o 3 5 0 28.35 30.33 1.72 o 4 5 0 72.12 75.80 6.74 o 0 6 0 623.39 586.09 8.14 o 1 6 0 1233.39 1225.84 13.88 o 2 6 0 623.01 605.31 8.38 o 3 6 0 78.69 76.42 2.22 o 4 6 0 47.49 51.83 6.06 o 1 7 0 777.57 792.26 8.53 o 2 7 0 148.08 150.11 3.15 o 3 7 0 33.66 33.32 1.90 o 0 8 0 14.06 18.18 0.74 o 1 8 0 191.15 178.04 2.20 o 2 8 0 520.18 510.95 7.54 o 3 8 0 17.54 19.05 2.26 o 1 9 0 104.74 101.10 1.52 o 2 9 0 0.94 1.96 1.07 o 3 9 0 42.10 44.40 4.39 o 0 10 0 17.32 16.59 0.89 o 1 10 0 258.39 248.75 3.08 o 2 10 0 503.34 519.99 10.65 o 3 10 0 29.54 33.35 4.46 o 1 11 0 270.09 269.82 3.31 o 2 11 0 385.80 394.04 12.53 o 3 11 0 20.27 19.21 4.55 o 0 12 0 126.83 128.51 3.01 o 1 12 0 530.27 525.32 6.97 o 2 12 0 103.68 110.60 4.26 o 3 12 0 38.83 39.15 5.34 o 1 13 0 56.11 57.68 2.12 o 2 13 0 20.73 19.65 3.95 o 3 13 0 6.35 3.12 5.04 o 0 14 0 236.39 236.64 10.47 o 1 14 0 21.56 23.26 1.75 o 2 14 0 80.00 76.41 5.89 o 3 14 0 34.13 30.37 5.92 o 1 15 0 40.21 37.22 2.09 o 2 15 0 32.29 27.60 4.85 o 0 16 0 151.93 159.16 8.83 o 1 16 0 42.32 42.00 2.36 o 2 16 0 5.50 1.30 4.88 o 1 17 0 115.30 114.93 4.14 o 0 18 0 276.18 262.11 12.69 o -1 -17 1 50.28 60.81 6.55 o 1 -17 1 126.24 155.99 12.59 o -2 -16 1 29.95 35.37 6.41 o -1 -16 1 88.82 90.90 4.46 o 1 -16 1 47.35 59.72 4.00 o 2 -16 1 18.36 22.58 3.42 o -2 -15 1 152.56 164.25 5.81 o -1 -15 1 70.43 73.42 4.42 o 0 -15 1 70.69 74.24 5.55 o 1 -15 1 113.48 129.44 5.14 o 2 -15 1 26.36 30.28 3.57 o -2 -14 1 6.00 3.38 3.62 o -1 -14 1 33.98 39.97 2.76 o 0 -14 1 68.31 67.59 2.58 o 1 -14 1 42.08 41.97 3.15 o 2 -14 1 31.87 40.89 4.83 o -3 -13 1 91.42 100.73 6.62 o -2 -13 1 23.94 24.19 3.66 o -1 -13 1 26.86 28.10 2.11 o 0 -13 1 192.06 192.16 3.03 o 1 -13 1 75.60 73.85 2.64 o 2 -13 1 197.96 216.46 8.86 o -3 -12 1 0.62 1.11 3.11 o -2 -12 1 58.64 56.41 2.76 o -1 -12 1 223.66 212.71 3.06 o 0 -12 1 102.68 109.46 2.26 o 1 -12 1 148.85 151.47 2.69 o 2 -12 1 97.28 97.20 5.20 o 3 -12 1 42.26 38.22 3.69 o -3 -11 1 113.17 114.83 4.06 o -2 -11 1 15.41 14.29 1.92 o -1 -11 1 144.76 143.79 2.39 o 0 -11 1 1036.39 1020.45 10.96 o 1 -11 1 51.69 50.39 1.14 o 2 -11 1 6.00 5.55 1.90 o 3 -11 1 429.63 446.59 12.25 o -3 -10 1 18.37 17.19 2.28 o -2 -10 1 5.68 5.55 1.66 o -1 -10 1 485.08 486.26 5.30 o 0 -10 1 22.79 25.74 0.87 o 1 -10 1 95.72 94.39 1.65 o 2 -10 1 110.01 104.88 3.94 o 3 -10 1 56.19 54.50 2.81 o -4 -9 1 215.97 213.23 10.89 o -3 -9 1 254.75 260.69 6.09 o -2 -9 1 12.34 12.20 1.28 o -1 -9 1 256.34 242.38 3.29 o 0 -9 1 602.85 567.58 6.20 o 1 -9 1 7.42 6.54 0.66 o 2 -9 1 51.74 49.53 1.63 o 3 -9 1 127.92 132.91 6.30 o 4 -9 1 59.97 55.38 5.84 o -4 -8 1 160.00 164.99 5.83 o -3 -8 1 73.18 76.03 2.67 o -2 -8 1 43.29 39.72 1.96 o -1 -8 1 421.55 407.34 4.42 o 0 -8 1 266.60 276.77 3.41 o 1 -8 1 76.19 77.21 1.21 o 2 -8 1 155.72 152.48 2.53 o 3 -8 1 27.14 24.26 1.76 o 4 -8 1 21.55 18.58 2.98 o -4 -7 1 31.98 32.06 3.99 o -3 -7 1 341.14 336.56 7.44 o -2 -7 1 53.65 46.97 1.61 o -1 -7 1 308.89 306.73 3.26 o 0 -7 1 1585.83 1611.67 15.69 o 1 -7 1 129.81 120.35 1.47 o 2 -7 1 7.52 8.40 0.82 o 3 -7 1 575.52 552.91 10.06 o 4 -7 1 39.21 47.41 4.27 o -4 -6 1 20.79 26.81 3.59 o -3 -6 1 12.20 13.91 1.38 o -2 -6 1 91.09 90.18 1.83 o -1 -6 1 161.43 147.68 2.15 o 0 -6 1 248.53 255.46 2.68 o 1 -6 1 644.16 656.67 6.31 o 2 -6 1 295.24 287.67 4.20 o 3 -6 1 25.06 27.34 1.97 o 4 -6 1 36.25 39.11 3.86 o -4 -5 1 92.20 95.44 5.16 o -3 -5 1 218.41 216.27 5.76 o -2 -5 1 279.37 279.37 4.55 o -1 -5 1 932.96 929.27 9.33 o 0 -5 1 1216.57 1157.84 10.76 o 1 -5 1 158.76 161.40 1.79 o 2 -5 1 451.41 457.09 6.38 o 3 -5 1 139.84 141.71 5.24 o 4 -5 1 101.69 94.95 5.20 o -3 -4 1 32.50 32.34 1.93 o -2 -4 1 265.41 271.10 4.33 o -1 -4 1 582.78 547.88 5.96 o 0 -4 1 158.96 158.30 1.61 o 1 -4 1 260.62 275.94 3.46 o 2 -4 1 107.66 109.39 1.90 o 3 -4 1 1.09 2.18 1.51 o -3 -3 1 165.39 157.12 12.39 o -2 -3 1 1013.87 983.38 14.89 o -1 -3 1 326.73 310.42 3.24 o 0 -3 1 641.12 636.35 5.78 o 1 -3 1 824.13 854.94 10.07 o 2 -3 1 165.17 167.56 2.60 o 3 -3 1 99.49 98.32 2.56 o -3 -2 1 179.98 166.06 7.30 o -2 -2 1 75.32 74.30 1.51 o -1 -2 1 819.91 774.99 8.19 o 0 -2 1 800.24 828.54 7.52 o 1 -2 1 2.44 2.01 0.26 o 2 -2 1 9.62 14.90 0.67 o 3 -2 1 4.09 5.96 1.53 o -3 -1 1 4.94 3.09 1.30 o -2 -1 1 819.52 789.54 12.16 o -1 -1 1 965.52 964.26 10.15 o 0 -1 1 130.86 138.19 1.36 o 1 -1 1 4917.00 5539.84 56.09 o 2 -1 1 1302.24 1323.69 18.48 o 3 -1 1 16.05 15.92 1.21 o -3 0 1 1.37 0.30 0.87 o -2 0 1 407.02 418.34 5.86 o -1 0 1 121.37 127.23 1.37 o 1 0 1 4776.09 5365.70 56.86 o 2 0 1 1774.33 1887.89 22.36 o 3 0 1 28.99 31.13 1.33 o -3 1 1 5.52 3.62 1.17 o -2 1 1 814.75 785.46 11.24 o -1 1 1 959.20 946.63 10.19 o 0 1 1 133.37 141.11 1.37 o 1 1 1 4998.64 5645.25 60.76 o 2 1 1 1306.91 1358.33 19.18 o 3 1 1 17.19 16.33 1.23 o -4 2 1 52.52 48.86 3.86 o -3 2 1 180.36 169.00 3.03 o -2 2 1 80.05 80.30 1.48 o -1 2 1 827.90 790.03 8.89 o 0 2 1 809.92 830.72 7.94 o 1 2 1 1.66 0.77 0.26 o 2 2 1 11.10 16.20 0.68 o 3 2 1 4.23 3.90 0.91 o 4 2 1 74.83 84.88 4.20 o -4 3 1 13.96 16.15 3.91 o -3 3 1 160.36 152.02 2.93 o -2 3 1 1009.48 984.90 13.18 o -1 3 1 334.41 318.21 3.67 o 0 3 1 642.37 638.94 5.94 o 1 3 1 812.05 835.23 9.64 o 2 3 1 174.72 174.06 2.74 o 3 3 1 96.66 95.72 2.21 o 4 3 1 29.59 44.42 4.85 o -4 4 1 36.73 44.97 5.10 o -3 4 1 32.59 33.20 1.45 o -2 4 1 259.44 263.66 3.84 o -1 4 1 583.15 569.03 6.65 o 0 4 1 156.21 156.47 1.52 o 1 4 1 270.85 281.70 3.46 o 2 4 1 110.23 110.67 2.01 o 3 4 1 1.24 2.49 1.22 o 4 4 1 65.65 74.80 6.44 o -4 5 1 91.45 100.95 7.76 o -3 5 1 222.22 217.52 3.96 o -2 5 1 288.05 279.29 4.05 o -1 5 1 915.13 917.23 9.83 o 0 5 1 1202.04 1167.07 10.03 o 1 5 1 166.93 170.38 2.30 o 2 5 1 452.50 451.61 6.31 o 3 5 1 139.97 141.02 3.10 o 4 5 1 99.74 100.98 7.64 o -4 6 1 20.18 22.36 5.67 o -3 6 1 13.50 14.96 1.68 o -2 6 1 93.75 88.62 2.74 o -1 6 1 153.91 142.58 1.78 o 0 6 1 249.71 261.94 2.66 o 1 6 1 636.75 643.45 7.52 o 2 6 1 289.73 277.97 4.14 o 3 6 1 24.18 26.67 2.53 o 4 6 1 34.11 41.90 6.10 o -3 7 1 337.40 345.30 7.51 o -2 7 1 53.37 46.81 1.49 o -1 7 1 312.96 307.44 3.67 o 0 7 1 1590.64 1602.35 14.87 o 1 7 1 126.90 117.13 1.68 o 2 7 1 6.48 7.02 0.92 o 3 7 1 573.12 555.85 12.61 o -3 8 1 71.41 74.09 3.24 o -2 8 1 43.35 41.91 1.41 o -1 8 1 429.35 419.87 4.48 o 0 8 1 266.16 276.44 2.83 o 1 8 1 75.02 74.78 1.22 o 2 8 1 157.31 151.28 2.66 o 3 8 1 26.99 26.71 2.73 o -3 9 1 258.83 267.71 10.52 o -2 9 1 12.59 13.53 1.30 o -1 9 1 255.04 245.54 2.82 o 0 9 1 600.59 566.77 5.54 o 1 9 1 6.55 4.95 0.64 o 2 9 1 50.62 49.51 1.69 o 3 9 1 126.71 134.80 7.04 o -3 10 1 18.93 19.21 4.25 o -2 10 1 5.33 2.44 1.62 o -1 10 1 474.85 475.22 5.76 o 0 10 1 22.83 24.45 0.73 o 1 10 1 97.86 93.87 1.58 o 2 10 1 109.30 100.23 2.88 o 3 10 1 57.04 66.52 5.13 o -3 11 1 112.76 116.77 7.10 o -2 11 1 16.10 15.87 2.09 o -1 11 1 150.03 145.74 2.07 o 0 11 1 1031.01 1023.02 10.08 o 1 11 1 50.44 47.78 1.17 o 2 11 1 5.02 4.05 1.91 o 3 11 1 431.39 447.64 16.15 o -3 12 1 0.74 0.74 4.57 o -2 12 1 58.86 57.36 2.95 o -1 12 1 231.90 218.00 3.40 o 0 12 1 101.95 107.44 1.53 o 1 12 1 150.72 150.49 3.25 o 2 12 1 100.11 102.72 5.82 o 3 12 1 41.85 47.52 5.49 o -3 13 1 90.94 94.40 7.57 o -2 13 1 24.64 23.20 4.16 o -1 13 1 24.95 27.07 1.67 o 0 13 1 201.59 200.59 3.82 o 1 13 1 73.85 78.65 2.37 o 2 13 1 197.38 197.03 8.85 o 3 13 1 45.97 46.64 5.95 o -2 14 1 5.53 4.10 4.20 o -1 14 1 33.23 37.57 1.95 o 0 14 1 69.18 64.95 1.75 o 1 14 1 39.46 43.63 2.03 o 2 14 1 30.22 27.26 4.55 o -2 15 1 149.15 152.65 8.31 o -1 15 1 70.84 64.14 2.57 o 0 15 1 68.87 67.51 2.83 o 1 15 1 114.55 120.52 3.31 o 2 15 1 26.09 27.67 4.98 o -2 16 1 30.75 30.13 5.57 o -1 16 1 87.19 80.90 3.21 o 0 16 1 24.53 25.51 1.78 o 1 16 1 47.73 47.53 2.77 o 2 16 1 17.91 18.86 5.28 o -1 17 1 49.70 57.40 7.52 o 0 17 1 17.88 17.58 2.23 o 1 17 1 124.61 130.05 9.67 o 0 18 1 5.75 0.02 4.06 o -1 -17 2 23.05 21.37 5.06 o -1 -16 2 44.71 41.05 3.55 o 1 -16 2 3.08 1.23 4.71 o -2 -15 2 30.49 32.16 3.24 o -1 -15 2 129.33 127.77 5.07 o 0 -15 2 5.41 8.02 3.86 o 1 -15 2 74.36 75.29 4.32 o 2 -15 2 95.28 103.13 7.63 o -2 -14 2 81.21 78.54 6.11 o -1 -14 2 50.56 55.14 3.29 o 0 -14 2 123.99 126.29 4.63 o 1 -14 2 60.47 65.59 3.73 o 2 -14 2 25.76 28.73 3.72 o -2 -13 2 41.36 47.55 4.42 o -1 -13 2 72.38 75.72 3.36 o 0 -13 2 16.16 13.93 1.45 o 1 -13 2 120.93 120.19 2.81 o -3 -12 2 5.73 6.92 3.31 o -2 -12 2 128.55 145.98 6.72 o -1 -12 2 75.29 74.63 1.97 o 0 -12 2 71.28 70.22 1.63 o 1 -12 2 285.24 283.69 5.16 o 3 -12 2 11.38 9.15 5.87 o -3 -11 2 3.41 4.94 2.94 o -2 -11 2 45.63 45.63 2.50 o -1 -11 2 54.15 50.98 1.30 o 0 -11 2 144.41 142.03 2.32 o 1 -11 2 308.50 304.63 3.72 o 2 -11 2 58.47 60.86 2.86 o 3 -11 2 3.49 0.38 3.09 o -3 -10 2 79.29 75.96 4.70 o -2 -10 2 282.14 278.79 6.28 o -1 -10 2 48.97 48.17 1.08 o 0 -10 2 171.77 171.68 2.23 o 1 -10 2 513.21 514.34 5.34 o 2 -10 2 157.26 158.56 4.19 o 3 -10 2 5.40 6.03 2.90 o -3 -9 2 265.28 263.05 6.23 o -2 -9 2 8.61 11.80 1.64 o -1 -9 2 198.56 183.69 2.22 o 0 -9 2 83.58 76.21 1.27 o 1 -9 2 145.46 139.87 1.70 o 2 -9 2 123.90 122.26 3.14 o 3 -9 2 9.12 10.68 2.68 o -4 -8 2 5.73 0.01 4.74 o -3 -8 2 109.16 109.42 3.54 o -2 -8 2 902.71 884.40 14.69 o -1 -8 2 178.55 169.35 2.53 o 0 -8 2 104.68 103.69 1.40 o 1 -8 2 819.18 816.91 8.05 o 2 -8 2 126.78 127.16 2.37 o 3 -8 2 51.23 45.15 3.89 o -4 -7 2 45.05 42.84 4.57 o -3 -7 2 73.05 69.04 3.77 o -2 -7 2 172.22 168.08 3.44 o -1 -7 2 120.93 116.18 1.43 o 0 -7 2 295.20 302.78 3.39 o 1 -7 2 120.15 129.31 1.59 o 2 -7 2 189.90 197.12 2.92 o 3 -7 2 11.16 9.44 1.58 o 4 -7 2 130.95 120.76 6.67 o -4 -6 2 12.73 11.49 3.54 o -3 -6 2 29.95 28.51 2.43 o -2 -6 2 182.86 174.96 3.30 o -1 -6 2 212.46 196.36 2.26 o 0 -6 2 510.68 515.66 5.01 o 1 -6 2 593.97 617.51 6.07 o 2 -6 2 312.63 317.84 4.69 o 3 -6 2 22.59 23.39 1.76 o 4 -6 2 70.32 74.15 5.27 o -4 -5 2 6.92 8.55 3.16 o -3 -5 2 64.35 63.02 2.66 o -2 -5 2 51.24 47.51 2.32 o -1 -5 2 386.52 390.32 4.00 o 0 -5 2 57.26 68.53 0.85 o 1 -5 2 358.98 357.56 3.56 o 2 -5 2 33.72 34.25 1.00 o 3 -5 2 42.00 39.46 3.27 o 4 -5 2 14.17 16.75 3.35 o -3 -4 2 223.25 216.61 5.89 o -2 -4 2 514.08 502.90 7.02 o -1 -4 2 871.13 888.71 8.84 o 0 -4 2 1070.12 1104.67 9.69 o 1 -4 2 471.45 468.83 4.61 o 2 -4 2 149.06 150.24 2.22 o 3 -4 2 196.06 191.39 5.22 o -3 -3 2 13.26 12.96 2.64 o -2 -3 2 98.74 98.55 1.59 o -1 -3 2 458.03 433.87 3.92 o 0 -3 2 147.57 156.80 1.60 o 1 -3 2 356.09 379.56 3.69 o 2 -3 2 342.96 352.68 4.23 o 3 -3 2 35.30 41.25 5.11 o -3 -2 2 340.67 320.48 12.73 o -2 -2 2 18.83 18.48 0.61 o -1 -2 2 628.30 629.92 5.78 o 0 -2 2 2605.06 2714.49 24.03 o 1 -2 2 3.73 4.41 0.29 o 2 -2 2 187.63 199.44 2.37 o 3 -2 2 296.21 306.51 7.55 o -3 -1 2 31.19 36.94 1.36 o -2 -1 2 64.43 65.09 1.06 o -1 -1 2 1001.63 1000.59 8.74 o 0 -1 2 105.46 102.05 1.04 o 1 -1 2 21.32 21.99 0.45 o 2 -1 2 1157.32 1237.48 13.45 o 3 -1 2 140.94 151.07 4.63 o -3 0 2 227.09 204.60 4.72 o -2 0 2 12.06 12.05 0.54 o -1 0 2 72.48 62.30 0.77 o 0 0 2 1570.97 1682.29 14.49 o 1 0 2 0.72 0.25 0.26 o 2 0 2 269.39 291.23 3.67 o 3 0 2 1434.43 1449.17 25.33 o -4 1 2 25.47 25.23 3.55 o -3 1 2 31.57 34.21 1.07 o -2 1 2 65.69 67.15 1.12 o -1 1 2 1011.24 1016.20 9.59 o 0 1 2 104.69 102.51 1.06 o 1 1 2 21.98 21.59 0.47 o 2 1 2 1187.64 1273.19 14.82 o 3 1 2 138.97 148.53 2.72 o 4 1 2 99.15 95.80 4.61 o -4 2 2 151.15 166.02 9.02 o -3 2 2 342.25 324.66 5.34 o -2 2 2 21.55 22.49 0.70 o -1 2 2 617.11 628.90 6.04 o 0 2 2 2623.50 2755.15 24.75 o 1 2 2 3.18 2.69 0.30 o 2 2 2 192.19 202.96 2.64 o 3 2 2 311.11 321.06 11.37 o 4 2 2 35.20 35.60 4.85 o -4 3 2 234.30 259.14 12.84 o -3 3 2 14.66 19.12 1.27 o -2 3 2 96.83 96.94 1.51 o -1 3 2 450.97 431.26 4.32 o 0 3 2 150.40 162.42 1.68 o 1 3 2 358.90 379.46 4.09 o 2 3 2 339.10 350.46 4.75 o 3 3 2 36.08 41.42 2.34 o 4 3 2 3.70 8.08 4.48 o -4 4 2 78.55 92.58 7.19 o -3 4 2 219.96 213.45 3.94 o -2 4 2 511.06 500.09 5.85 o -1 4 2 874.80 907.13 8.59 o 0 4 2 1045.15 1080.60 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199.26 203.45 11.70 o -3 -10 3 13.44 13.98 3.11 o -2 -10 3 137.64 129.68 3.03 o -1 -10 3 152.88 141.71 2.26 o 0 -10 3 34.34 34.85 1.09 o 1 -10 3 19.07 19.45 0.98 o 2 -10 3 185.20 192.35 10.72 o 3 -10 3 1.18 2.01 5.39 o -3 -9 3 56.91 67.61 4.05 o -2 -9 3 31.57 33.54 1.37 o -1 -9 3 407.31 393.41 4.40 o 0 -9 3 474.05 456.65 4.85 o 1 -9 3 9.84 12.14 0.76 o 2 -9 3 11.09 13.03 2.16 o 3 -9 3 212.62 216.62 11.14 o -3 -8 3 7.08 5.55 2.60 o -2 -8 3 179.18 170.29 3.58 o -1 -8 3 514.37 492.38 5.24 o 0 -8 3 42.43 43.19 0.95 o 1 -8 3 44.24 43.43 0.98 o 2 -8 3 187.83 176.85 4.49 o 3 -8 3 7.97 5.10 4.56 o -3 -7 3 131.13 135.38 4.92 o -2 -7 3 42.79 40.87 1.34 o -1 -7 3 400.82 384.00 4.05 o 0 -7 3 623.69 620.55 6.23 o 1 -7 3 12.65 12.08 0.62 o 2 -7 3 334.51 324.27 5.45 o 3 -7 3 186.19 183.55 9.66 o -4 -6 3 28.19 39.45 4.52 o -3 -6 3 79.30 80.01 3.74 o -2 -6 3 21.47 21.88 0.99 o -1 -6 3 242.30 224.30 2.46 o 0 -6 3 20.88 21.19 0.70 o 1 -6 3 206.98 215.54 2.38 o 2 -6 3 158.54 163.32 2.34 o 3 -6 3 7.71 7.79 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