#------------------------------------------------------------------------------
#$Date: 2016-02-20 02:53:41 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176768 $
#$URL: svn://www.crystallography.net/cod/cif/2/10/56/2105687.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2105687
loop_
_publ_author_name
'Oshchapovsky, Igor'
'Pavlyuk, Volodymyr'
'Chumak, Igor'
_publ_section_title
;
 Tb₃Sn₇: polymorphism and crystal structure of high-temperature
 modification
;
_journal_coeditor_code           DK5011
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              527
_journal_page_last               533
_journal_paper_doi               10.1107/S2052519213024378
_journal_volume                  69
_journal_year                    2013
_chemical_formula_moiety         'Sn6.97 Tb3'
_chemical_formula_sum            'Sn6.97 Tb3'
_chemical_formula_weight         1304.2
_chemical_name_systematic
;
beta-triterbium heptastannide
;
_space_group_IT_number           47
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2 2'
_symmetry_space_group_name_H-M   'P m m m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   4.33520(10)
_cell_length_b                   4.42510(10)
_cell_length_c                   26.7006(9)
_cell_measurement_reflns_used    508
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.44
_cell_measurement_theta_min      2.29
_cell_volume                     512.22(2)
_computing_cell_refinement       'CrysAlis CCD (Oxford Diffraction, 2004)'
_computing_data_collection       'CrysAlis CCD (Oxford Diffraction, 2004)'
_computing_data_reduction        'CrysAlis RED (Oxford Diffraction, 2005)'
_computing_molecular_graphics    'Diamond (Brandenburg, 1999)'
_computing_publication_material  'SHELX-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 0
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Xcalibur Oxford Diffraction'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0514
_diffrn_reflns_av_sigmaI/netI    0.0542
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            4684
_diffrn_reflns_theta_full        27.44
_diffrn_reflns_theta_max         27.44
_diffrn_reflns_theta_min         2.29
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    37.010
_exptl_absorpt_correction_T_max  0.598
_exptl_absorpt_correction_T_min  0.089
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   'CrysAlis RED (Oxford Diffraction, 2005)'
_exptl_crystal_colour            'metallic dark grey'
_exptl_crystal_density_diffrn    8.456
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'irregularly shaped'
_exptl_crystal_F_000             1087.0
_exptl_crystal_size_max          0.079
_exptl_crystal_size_mid          0.068
_exptl_crystal_size_min          0.008
_refine_diff_density_max         1.927
_refine_diff_density_min         -2.185
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_matrix_type           full
_refine_ls_number_parameters     49
_refine_ls_number_reflns         762
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.066
_refine_ls_R_factor_all          0.0425
_refine_ls_R_factor_gt           0.0279
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0215P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0867
_refine_ls_wR_factor_ref         0.0876
_reflns_number_gt                508
_reflns_number_total             762
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            dk5011.cif
_cod_data_source_block           I
_cod_database_code               2105687
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_symmetry_multiplicity
Tb Tb1 0.5000 0.5000 0.0000 0.0228(6) Uani d S 1 8
Tb Tb2 0.0000 0.5000 0.5000 0.0209(5) Uani d S 1 8
Tb Tb3 0.5000 0.5000 0.39449(6) 0.0219(4) Uani d S 1 4
Tb Tb4 0.0000 0.0000 0.19732(6) 0.0248(4) Uani d S 1 4
Sn Sn1 0.0000 0.0000 0.40015(8) 0.0369(9) Uani d S 1 4
Sn Sn2 0.5000 0.5000 0.20214(11) 0.0403(8) Uani d S 1 4
Sn Sn3 0.5000 0.0000 0.29131(10) 0.0391(8) Uani d S 1 4
Sn Sn4 0.0000 0.5000 0.09758(9) 0.0391(9) Uani d S 1 4
Sn Sn5 0.0000 0.5000 0.28940(11) 0.0462(8) Uani d S 1 4
Sn Sn6 0.5000 0.0000 0.10357(9) 0.0337(7) Uani d S 1 4
Sn Sn7 0.0000 0.0000 0.0000 0.023(13) Uiso d SP 0.12(4) 8
Sn Sn7A 0.0000 0.0000 0.0180(5) 0.042(3) Uiso d SP 0.43(3) 4
Sn Sn8A 0.5000 0.0000 0.4841(9) 0.041(4) Uiso d SP 0.36(4) 4
Sn Sn8 0.5000 0.0000 0.5000 0.049(9) Uiso d SP 0.24(8) 8
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Tb Tb -0.1723 4.1537 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
Sn7 Tb1 Sn7 1_665 . 180.0
Sn7 Tb1 Sn7 1_665 1_565 88.824(2)
Sn7 Tb1 Sn7 . 1_565 91.176(2)
Sn7 Tb1 Sn7 1_665 1_655 91.176(2)
Sn7 Tb1 Sn7 . 1_655 88.824(2)
Sn7 Tb1 Sn7 1_565 1_655 180.0
Sn7 Tb1 Sn7A 1_665 1_665 8.8(3)
Sn7 Tb1 Sn7A . 1_665 171.2(3)
Sn7 Tb1 Sn7A 1_565 1_665 88.838(2)
Sn7 Tb1 Sn7A 1_655 1_665 91.162(2)
Sn7 Tb1 Sn7A 1_665 5 171.2(3)
Sn7 Tb1 Sn7A . 5 8.8(3)
Sn7 Tb1 Sn7A 1_565 5 91.162(2)
Sn7 Tb1 Sn7A 1_655 5 88.838(2)
Sn7A Tb1 Sn7A 1_665 5 180.0
Sn7 Tb1 Sn7A 1_665 . 171.2(3)
Sn7 Tb1 Sn7A . . 8.8(3)
Sn7 Tb1 Sn7A 1_565 . 91.162(2)
Sn7 Tb1 Sn7A 1_655 . 88.838(2)
Sn7A Tb1 Sn7A 1_665 . 162.4(5)
Sn7A Tb1 Sn7A 5 . 17.6(5)
Sn7 Tb1 Sn7A 1_665 5_665 8.8(3)
Sn7 Tb1 Sn7A . 5_665 171.2(3)
Sn7 Tb1 Sn7A 1_565 5_665 88.838(2)
Sn7 Tb1 Sn7A 1_655 5_665 91.162(2)
Sn7A Tb1 Sn7A 1_665 5_665 17.6(5)
Sn7A Tb1 Sn7A 5 5_665 162.4(5)
Sn7A Tb1 Sn7A . 5_665 180.0(5)
Sn7 Tb1 Sn7A 1_665 1_565 88.838(2)
Sn7 Tb1 Sn7A . 1_565 91.162(2)
Sn7 Tb1 Sn7A 1_565 1_565 8.8(3)
Sn7 Tb1 Sn7A 1_655 1_565 171.2(3)
Sn7A Tb1 Sn7A 1_665 1_565 87.51(7)
Sn7A Tb1 Sn7A 5 1_565 92.49(7)
Sn7A Tb1 Sn7A . 1_565 89.81(8)
Sn7A Tb1 Sn7A 5_665 1_565 90.19(8)
Sn7 Tb1 Sn7A 1_665 1_655 91.162(2)
Sn7 Tb1 Sn7A . 1_655 88.838(2)
Sn7 Tb1 Sn7A 1_565 1_655 171.2(3)
Sn7 Tb1 Sn7A 1_655 1_655 8.8(3)
Sn7A Tb1 Sn7A 1_665 1_655 89.81(8)
Sn7A Tb1 Sn7A 5 1_655 90.19(8)
Sn7A Tb1 Sn7A . 1_655 87.51(7)
Sn7A Tb1 Sn7A 5_665 1_655 92.49(7)
Sn7A Tb1 Sn7A 1_565 1_655 162.4(5)
Sn7 Tb1 Sn7A 1_665 5_565 88.838(2)
Sn7 Tb1 Sn7A . 5_565 91.162(2)
Sn7 Tb1 Sn7A 1_565 5_565 8.8(3)
Sn7 Tb1 Sn7A 1_655 5_565 171.2(3)
Sn7A Tb1 Sn7A 1_665 5_565 90.19(8)
Sn7A Tb1 Sn7A 5 5_565 89.81(8)
Sn7A Tb1 Sn7A . 5_565 92.49(7)
Sn7A Tb1 Sn7A 5_665 5_565 87.51(7)
Sn7A Tb1 Sn7A 1_565 5_565 17.6(5)
Sn7A Tb1 Sn7A 1_655 5_565 180.0
Sn7 Tb1 Sn7A 1_665 5_655 91.162(2)
Sn7 Tb1 Sn7A . 5_655 88.838(2)
Sn7 Tb1 Sn7A 1_565 5_655 171.2(3)
Sn7 Tb1 Sn7A 1_655 5_655 8.8(3)
Sn7A Tb1 Sn7A 1_665 5_655 92.49(8)
Sn7A Tb1 Sn7A 5 5_655 87.51(7)
Sn7A Tb1 Sn7A . 5_655 90.19(8)
Sn7A Tb1 Sn7A 5_665 5_655 89.81(8)
Sn7A Tb1 Sn7A 1_565 5_655 180.0
Sn7A Tb1 Sn7A 1_655 5_655 17.6(5)
Sn7A Tb1 Sn7A 5_565 5_655 162.4(5)
Sn8 Tb2 Sn8 1_565 1_455 180.0
Sn8 Tb2 Sn8 1_565 1_465 88.824(2)
Sn8 Tb2 Sn8 1_455 1_465 91.176(2)
Sn8 Tb2 Sn8 1_565 . 91.176(2)
Sn8 Tb2 Sn8 1_455 . 88.824(2)
Sn8 Tb2 Sn8 1_465 . 180.0
Sn8 Tb2 Sn8A 1_565 5_666 7.8(4)
Sn8 Tb2 Sn8A 1_455 5_666 172.2(4)
Sn8 Tb2 Sn8A 1_465 5_666 88.835(3)
Sn8 Tb2 Sn8A . 5_666 91.165(3)
Sn8 Tb2 Sn8A 1_565 1_455 172.2(4)
Sn8 Tb2 Sn8A 1_455 1_455 7.8(4)
Sn8 Tb2 Sn8A 1_465 1_455 91.165(3)
Sn8 Tb2 Sn8A . 1_455 88.835(3)
Sn8A Tb2 Sn8A 5_666 1_455 180.0
Sn8 Tb2 Sn8A 1_565 5_556 172.2(4)
Sn8 Tb2 Sn8A 1_455 5_556 7.8(4)
Sn8 Tb2 Sn8A 1_465 5_556 91.165(3)
Sn8 Tb2 Sn8A . 5_556 88.835(3)
Sn8A Tb2 Sn8A 5_666 5_556 164.4(9)
Sn8A Tb2 Sn8A 1_455 5_556 15.6(9)
Sn8 Tb2 Sn8A 1_565 1_565 7.8(4)
Sn8 Tb2 Sn8A 1_455 1_565 172.2(4)
Sn8 Tb2 Sn8A 1_465 1_565 88.835(3)
Sn8 Tb2 Sn8A . 1_565 91.165(3)
Sn8A Tb2 Sn8A 5_666 1_565 15.6(9)
Sn8A Tb2 Sn8A 1_455 1_565 164.4(9)
Sn8A Tb2 Sn8A 5_556 1_565 180.0(9)
Sn8 Tb2 Sn8A 1_565 5_566 88.835(3)
Sn8 Tb2 Sn8A 1_455 5_566 91.165(3)
Sn8 Tb2 Sn8A 1_465 5_566 7.8(4)
Sn8 Tb2 Sn8A . 5_566 172.2(4)
Sn8A Tb2 Sn8A 5_666 5_566 87.79(11)
Sn8A Tb2 Sn8A 1_455 5_566 92.21(11)
Sn8A Tb2 Sn8A 5_556 5_566 90.10(12)
Sn8A Tb2 Sn8A 1_565 5_566 89.90(12)
Sn8 Tb2 Sn8A 1_565 5_656 91.165(3)
Sn8 Tb2 Sn8A 1_455 5_656 88.835(3)
Sn8 Tb2 Sn8A 1_465 5_656 172.2(4)
Sn8 Tb2 Sn8A . 5_656 7.8(4)
Sn8A Tb2 Sn8A 5_666 5_656 90.10(12)
Sn8A Tb2 Sn8A 1_455 5_656 89.90(12)
Sn8A Tb2 Sn8A 5_556 5_656 87.79(11)
Sn8A Tb2 Sn8A 1_565 5_656 92.21(11)
Sn8A Tb2 Sn8A 5_566 5_656 164.4(9)
Sn8 Tb2 Sn8A 1_565 . 91.165(3)
Sn8 Tb2 Sn8A 1_455 . 88.835(3)
Sn8 Tb2 Sn8A 1_465 . 172.2(4)
Sn8 Tb2 Sn8A . . 7.8(4)
Sn8A Tb2 Sn8A 5_666 . 92.21(11)
Sn8A Tb2 Sn8A 1_455 . 87.79(11)
Sn8A Tb2 Sn8A 5_556 . 89.90(12)
Sn8A Tb2 Sn8A 1_565 . 90.10(12)
Sn8A Tb2 Sn8A 5_566 . 180.0
Sn8A Tb2 Sn8A 5_656 . 15.6(9)
Sn8 Tb2 Sn8A 1_565 1_465 88.835(3)
Sn8 Tb2 Sn8A 1_455 1_465 91.165(3)
Sn8 Tb2 Sn8A 1_465 1_465 7.8(4)
Sn8 Tb2 Sn8A . 1_465 172.2(4)
Sn8A Tb2 Sn8A 5_666 1_465 89.90(12)
Sn8A Tb2 Sn8A 1_455 1_465 90.10(12)
Sn8A Tb2 Sn8A 5_556 1_465 92.21(11)
Sn8A Tb2 Sn8A 1_565 1_465 87.79(11)
Sn8A Tb2 Sn8A 5_566 1_465 15.6(9)
Sn8A Tb2 Sn8A 5_656 1_465 180.0
Sn8A Tb2 Sn8A . 1_465 164.4(9)
Sn1 Tb3 Sn1 1_665 . 174.41(11)
Sn1 Tb3 Sn1 1_665 1_565 88.691(6)
Sn1 Tb3 Sn1 . 1_565 91.037(6)
Sn1 Tb3 Sn1 1_665 1_655 91.037(6)
Sn1 Tb3 Sn1 . 1_655 88.691(6)
Sn1 Tb3 Sn1 1_565 1_655 174.41(11)
Sn1 Tb3 Sn8A 1_665 1_565 58.65(17)
Sn1 Tb3 Sn8A . 1_565 116.66(18)
Sn1 Tb3 Sn8A 1_565 1_565 58.65(17)
Sn1 Tb3 Sn8A 1_655 1_565 116.66(18)
Sn1 Tb3 Sn8A 1_665 . 116.66(18)
Sn1 Tb3 Sn8A . . 58.65(17)
Sn1 Tb3 Sn8A 1_565 . 116.66(18)
Sn1 Tb3 Sn8A 1_655 . 58.65(17)
Sn8A Tb3 Sn8A 1_565 . 85.5(6)
Sn1 Tb3 Sn3 1_665 . 119.00(6)
Sn1 Tb3 Sn3 . . 65.87(4)
Sn1 Tb3 Sn3 1_565 . 119.00(6)
Sn1 Tb3 Sn3 1_655 . 65.87(4)
Sn8A Tb3 Sn3 1_565 . 176.0(3)
Sn8A Tb3 Sn3 . . 98.5(3)
Sn1 Tb3 Sn3 1_665 1_565 65.87(4)
Sn1 Tb3 Sn3 . 1_565 119.00(6)
Sn1 Tb3 Sn3 1_565 1_565 65.87(4)
Sn1 Tb3 Sn3 1_655 1_565 119.00(6)
Sn8A Tb3 Sn3 1_565 1_565 98.5(3)
Sn8A Tb3 Sn3 . 1_565 176.0(3)
Sn3 Tb3 Sn3 . 1_565 77.53(6)
Sn1 Tb3 Sn5 1_665 . 117.77(5)
Sn1 Tb3 Sn5 . . 67.12(5)
Sn1 Tb3 Sn5 1_565 . 67.12(5)
Sn1 Tb3 Sn5 1_655 . 117.77(5)
Sn8A Tb3 Sn5 1_565 . 125.52(18)
Sn8A Tb3 Sn5 . . 125.52(19)
Sn3 Tb3 Sn5 . . 51.90(3)
Sn3 Tb3 Sn5 1_565 . 51.90(3)
Sn1 Tb3 Sn5 1_665 1_655 67.12(5)
Sn1 Tb3 Sn5 . 1_655 117.77(5)
Sn1 Tb3 Sn5 1_565 1_655 117.77(5)
Sn1 Tb3 Sn5 1_655 1_655 67.12(5)
Sn8A Tb3 Sn5 1_565 1_655 125.52(19)
Sn8A Tb3 Sn5 . 1_655 125.52(19)
Sn3 Tb3 Sn5 . 1_655 51.90(3)
Sn3 Tb3 Sn5 1_565 1_655 51.90(3)
Sn5 Tb3 Sn5 . 1_655 75.37(6)
Sn1 Tb3 Tb2 1_665 1_655 62.30(4)
Sn1 Tb3 Tb2 . 1_655 112.81(6)
Sn1 Tb3 Tb2 1_565 1_655 112.81(6)
Sn1 Tb3 Tb2 1_655 1_655 62.30(4)
Sn8A Tb3 Tb2 1_565 1_655 54.42(18)
Sn8A Tb3 Tb2 . 1_655 54.42(18)
Sn3 Tb3 Tb2 . 1_655 128.166(17)
Sn3 Tb3 Tb2 1_565 1_655 128.166(17)
Sn5 Tb3 Tb2 . 1_655 179.89(4)
Sn5 Tb3 Tb2 1_655 1_655 104.74(3)
Sn1 Tb3 Tb2 1_665 . 112.81(6)
Sn1 Tb3 Tb2 . . 62.30(4)
Sn1 Tb3 Tb2 1_565 . 62.30(4)
Sn1 Tb3 Tb2 1_655 . 112.81(6)
Sn8A Tb3 Tb2 1_565 . 54.42(18)
Sn8A Tb3 Tb2 . . 54.42(18)
Sn3 Tb3 Tb2 . . 128.166(17)
Sn3 Tb3 Tb2 1_565 . 128.166(17)
Sn5 Tb3 Tb2 . . 104.74(3)
Sn5 Tb3 Tb2 1_655 . 179.89(4)
Tb2 Tb3 Tb2 1_655 . 75.15(3)
Sn2 Tb4 Sn2 . 1_445 175.24(13)
Sn2 Tb4 Sn2 . 1_455 88.727(6)
Sn2 Tb4 Sn2 1_445 1_455 91.075(6)
Sn2 Tb4 Sn2 . 1_545 91.075(6)
Sn2 Tb4 Sn2 1_445 1_545 88.727(6)
Sn2 Tb4 Sn2 1_455 1_545 175.24(13)
Sn2 Tb4 Sn5 . . 59.45(5)
Sn2 Tb4 Sn5 1_445 . 116.52(7)
Sn2 Tb4 Sn5 1_455 . 59.45(5)
Sn2 Tb4 Sn5 1_545 . 116.52(7)
Sn2 Tb4 Sn5 . 1_545 116.52(7)
Sn2 Tb4 Sn5 1_445 1_545 59.45(5)
Sn2 Tb4 Sn5 1_455 1_545 116.52(7)
Sn2 Tb4 Sn5 1_545 1_545 59.45(5)
Sn5 Tb4 Sn5 . 1_545 83.97(8)
Sn2 Tb4 Sn6 . 1_455 119.28(6)
Sn2 Tb4 Sn6 1_445 1_455 64.76(6)
Sn2 Tb4 Sn6 1_455 1_455 64.76(6)
Sn2 Tb4 Sn6 1_545 1_455 119.28(6)
Sn5 Tb4 Sn6 . 1_455 124.19(3)
Sn5 Tb4 Sn6 1_545 1_455 124.19(3)
Sn2 Tb4 Sn6 . . 64.76(6)
Sn2 Tb4 Sn6 1_445 . 119.28(6)
Sn2 Tb4 Sn6 1_455 . 119.28(6)
Sn2 Tb4 Sn6 1_545 . 64.76(6)
Sn5 Tb4 Sn6 . . 124.19(3)
Sn5 Tb4 Sn6 1_545 . 124.19(3)
Sn6 Tb4 Sn6 1_455 . 81.79(6)
Sn2 Tb4 Sn3 . . 60.76(6)
Sn2 Tb4 Sn3 1_445 . 115.19(6)
Sn2 Tb4 Sn3 1_455 . 115.19(6)
Sn2 Tb4 Sn3 1_545 . 60.76(6)
Sn5 Tb4 Sn3 . . 55.77(3)
Sn5 Tb4 Sn3 1_545 . 55.77(3)
Sn6 Tb4 Sn3 1_455 . 179.93(5)
Sn6 Tb4 Sn3 . . 98.29(3)
Sn2 Tb4 Sn3 . 1_455 115.19(6)
Sn2 Tb4 Sn3 1_445 1_455 60.76(6)
Sn2 Tb4 Sn3 1_455 1_455 60.76(6)
Sn2 Tb4 Sn3 1_545 1_455 115.19(6)
Sn5 Tb4 Sn3 . 1_455 55.77(3)
Sn5 Tb4 Sn3 1_545 1_455 55.77(3)
Sn6 Tb4 Sn3 1_455 1_455 98.29(3)
Sn6 Tb4 Sn3 . 1_455 179.93(5)
Sn3 Tb4 Sn3 . 1_455 81.64(6)
Sn2 Tb4 Sn4 . 1_545 119.21(7)
Sn2 Tb4 Sn4 1_445 1_545 64.90(5)
Sn2 Tb4 Sn4 1_455 1_545 119.21(7)
Sn2 Tb4 Sn4 1_545 1_545 64.90(5)
Sn5 Tb4 Sn4 . 1_545 177.74(7)
Sn5 Tb4 Sn4 1_545 1_545 98.30(3)
Sn6 Tb4 Sn4 1_455 1_545 54.45(3)
Sn6 Tb4 Sn4 . 1_545 54.45(3)
Sn3 Tb4 Sn4 . 1_545 125.60(3)
Sn3 Tb4 Sn4 1_455 1_545 125.60(3)
Sn2 Tb4 Sn4 . . 64.90(5)
Sn2 Tb4 Sn4 1_445 . 119.21(7)
Sn2 Tb4 Sn4 1_455 . 64.90(5)
Sn2 Tb4 Sn4 1_545 . 119.21(7)
Sn5 Tb4 Sn4 . . 98.30(3)
Sn5 Tb4 Sn4 1_545 . 177.74(7)
Sn6 Tb4 Sn4 1_455 . 54.45(3)
Sn6 Tb4 Sn4 . . 54.45(3)
Sn3 Tb4 Sn4 . . 125.60(3)
Sn3 Tb4 Sn4 1_455 . 125.60(3)
Sn4 Tb4 Sn4 1_545 . 79.44(7)
Tb3 Sn1 Tb3 1_445 . 174.41(11)
Tb3 Sn1 Tb3 1_445 1_455 91.037(6)
Tb3 Sn1 Tb3 . 1_455 88.691(6)
Tb3 Sn1 Tb3 1_445 1_545 88.691(6)
Tb3 Sn1 Tb3 . 1_545 91.037(6)
Tb3 Sn1 Tb3 1_455 1_545 174.41(11)
Tb3 Sn1 Sn8A 1_445 . 121.40(18)
Tb3 Sn1 Sn8A . . 63.20(18)
Tb3 Sn1 Sn8A 1_455 . 121.40(18)
Tb3 Sn1 Sn8A 1_545 . 63.20(18)
Tb3 Sn1 Sn8A 1_445 1_455 63.20(18)
Tb3 Sn1 Sn8A . 1_455 121.40(18)
Tb3 Sn1 Sn8A 1_455 1_455 63.20(18)
Tb3 Sn1 Sn8A 1_545 1_455 121.40(18)
Sn8A Sn1 Sn8A . 1_455 88.1(6)
Tb3 Sn1 Tb2 1_445 . 119.55(6)
Tb3 Sn1 Tb2 . . 65.28(4)
Tb3 Sn1 Tb2 1_455 . 65.28(4)
Tb3 Sn1 Tb2 1_545 . 119.55(6)
Sn8A Sn1 Tb2 . . 56.4(2)
Sn8A Sn1 Tb2 1_455 . 56.4(2)
Tb3 Sn1 Tb2 1_445 1_545 65.28(4)
Tb3 Sn1 Tb2 . 1_545 119.55(6)
Tb3 Sn1 Tb2 1_455 1_545 119.55(6)
Tb3 Sn1 Tb2 1_545 1_545 65.28(4)
Sn8A Sn1 Tb2 . 1_545 56.4(2)
Sn8A Sn1 Tb2 1_455 1_545 56.4(2)
Tb2 Sn1 Tb2 . 1_545 79.38(5)
Tb4 Sn2 Tb4 . 1_665 175.24(13)
Tb4 Sn2 Tb4 . 1_565 91.075(6)
Tb4 Sn2 Tb4 1_665 1_565 88.727(6)
Tb4 Sn2 Tb4 . 1_655 88.727(6)
Tb4 Sn2 Tb4 1_665 1_655 91.075(6)
Tb4 Sn2 Tb4 1_565 1_655 175.24(13)
Tb4 Sn2 Sn5 . 1_655 120.44(7)
Tb4 Sn2 Sn5 1_665 1_655 63.52(5)
Tb4 Sn2 Sn5 1_565 1_655 120.44(7)
Tb4 Sn2 Sn5 1_655 1_655 63.52(5)
Tb4 Sn2 Sn5 . . 63.52(5)
Tb4 Sn2 Sn5 1_665 . 120.44(7)
Tb4 Sn2 Sn5 1_565 . 63.52(5)
Tb4 Sn2 Sn5 1_655 . 120.44(7)
Sn5 Sn2 Sn5 1_655 . 85.86(9)
Tb4 Sn2 Sn3 . 1_565 121.08(8)
Tb4 Sn2 Sn3 1_665 1_565 62.91(4)
Tb4 Sn2 Sn3 1_565 1_565 62.91(4)
Tb4 Sn2 Sn3 1_655 1_565 121.08(8)
Sn5 Sn2 Sn3 1_655 1_565 57.57(5)
Sn5 Sn2 Sn3 . 1_565 57.57(5)
Tb4 Sn2 Sn3 . . 62.91(4)
Tb4 Sn2 Sn3 1_665 . 121.08(8)
Tb4 Sn2 Sn3 1_565 . 121.08(8)
Tb4 Sn2 Sn3 1_655 . 62.91(4)
Sn5 Sn2 Sn3 1_655 . 57.57(5)
Sn5 Sn2 Sn3 . . 57.57(5)
Sn3 Sn2 Sn3 1_565 . 85.80(11)
Sn5 Sn3 Sn5 1_545 1_655 178.12(18)
Sn5 Sn3 Sn5 1_545 1_645 88.809(4)
Sn5 Sn3 Sn5 1_655 1_645 91.160(4)
Sn5 Sn3 Sn5 1_545 . 91.160(4)
Sn5 Sn3 Sn5 1_655 . 88.809(4)
Sn5 Sn3 Sn5 1_645 . 178.12(18)
Sn5 Sn3 Sn2 1_545 1_545 60.12(6)
Sn5 Sn3 Sn2 1_655 1_545 118.30(10)
Sn5 Sn3 Sn2 1_645 1_545 60.12(6)
Sn5 Sn3 Sn2 . 1_545 118.30(10)
Sn5 Sn3 Sn2 1_545 . 118.30(10)
Sn5 Sn3 Sn2 1_655 . 60.12(6)
Sn5 Sn3 Sn2 1_645 . 118.30(10)
Sn5 Sn3 Sn2 . . 60.12(6)
Sn2 Sn3 Sn2 1_545 . 85.80(11)
Sn5 Sn3 Tb4 1_545 . 61.98(6)
Sn5 Sn3 Tb4 1_655 . 116.42(9)
Sn5 Sn3 Tb4 1_645 . 116.42(9)
Sn5 Sn3 Tb4 . . 61.98(6)
Sn2 Sn3 Tb4 1_545 . 56.33(5)
Sn2 Sn3 Tb4 . . 56.33(5)
Sn5 Sn3 Tb4 1_545 1_655 116.42(9)
Sn5 Sn3 Tb4 1_655 1_655 61.98(6)
Sn5 Sn3 Tb4 1_645 1_655 61.98(6)
Sn5 Sn3 Tb4 . 1_655 116.42(9)
Sn2 Sn3 Tb4 1_545 1_655 56.33(5)
Sn2 Sn3 Tb4 . 1_655 56.33(5)
Tb4 Sn3 Tb4 . 1_655 81.64(6)
Sn5 Sn3 Tb3 1_545 . 117.39(9)
Sn5 Sn3 Tb3 1_655 . 64.25(6)
Sn5 Sn3 Tb3 1_645 . 117.39(9)
Sn5 Sn3 Tb3 . . 64.25(6)
Sn2 Sn3 Tb3 1_545 . 175.87(8)
Sn2 Sn3 Tb3 . . 98.33(3)
Tb4 Sn3 Tb3 . . 126.162(17)
Tb4 Sn3 Tb3 1_655 . 126.162(17)
Sn5 Sn3 Tb3 1_545 1_545 64.25(6)
Sn5 Sn3 Tb3 1_655 1_545 117.39(9)
Sn5 Sn3 Tb3 1_645 1_545 64.25(6)
Sn5 Sn3 Tb3 . 1_545 117.39(9)
Sn2 Sn3 Tb3 1_545 1_545 98.33(3)
Sn2 Sn3 Tb3 . 1_545 175.87(8)
Tb4 Sn3 Tb3 . 1_545 126.162(17)
Tb4 Sn3 Tb3 1_655 1_545 126.162(17)
Tb3 Sn3 Tb3 . 1_545 77.53(6)
Sn7A Sn4 Sn7A . 1_565 92.3(4)
Sn7A Sn4 Sn6 . 1_565 123.38(11)
Sn7A Sn4 Sn6 1_565 1_565 61.40(12)
Sn7A Sn4 Sn6 . 1_455 61.40(12)
Sn7A Sn4 Sn6 1_565 1_455 123.38(11)
Sn6 Sn4 Sn6 1_565 1_455 174.08(12)
Sn7A Sn4 Sn6 . . 61.40(12)
Sn7A Sn4 Sn6 1_565 . 123.38(11)
Sn6 Sn4 Sn6 1_565 . 91.020(7)
Sn6 Sn4 Sn6 1_455 . 88.675(6)
Sn7A Sn4 Sn6 . 1_465 123.38(11)
Sn7A Sn4 Sn6 1_565 1_465 61.40(12)
Sn6 Sn4 Sn6 1_565 1_465 88.675(6)
Sn6 Sn4 Sn6 1_455 1_465 91.020(7)
Sn6 Sn4 Sn6 . 1_465 174.08(12)
Sn7A Sn4 Tb1 . 1_455 57.82(13)
Sn7A Sn4 Tb1 1_565 1_455 57.82(13)
Sn6 Sn4 Tb1 1_565 1_455 119.12(6)
Sn6 Sn4 Tb1 1_455 1_455 65.96(4)
Sn6 Sn4 Tb1 . 1_455 119.12(6)
Sn6 Sn4 Tb1 1_465 1_455 65.96(4)
Sn7A Sn4 Tb1 . . 57.82(13)
Sn7A Sn4 Tb1 1_565 . 57.82(13)
Sn6 Sn4 Tb1 1_565 . 65.96(4)
Sn6 Sn4 Tb1 1_455 . 119.12(6)
Sn6 Sn4 Tb1 . . 65.96(4)
Sn6 Sn4 Tb1 1_465 . 119.12(6)
Tb1 Sn4 Tb1 1_455 . 79.52(5)
Sn7A Sn4 Tb4 . 1_565 173.6(2)
Sn7A Sn4 Tb4 1_565 1_565 94.13(19)
Sn6 Sn4 Tb4 1_565 1_565 60.29(4)
Sn6 Sn4 Tb4 1_455 1_565 114.59(7)
Sn6 Sn4 Tb4 . 1_565 114.59(7)
Sn6 Sn4 Tb4 1_465 1_565 60.29(4)
Tb1 Sn4 Tb4 1_455 1_565 126.248(10)
Tb1 Sn4 Tb4 . 1_565 126.248(10)
Sn7A Sn4 Tb4 . . 94.13(19)
Sn7A Sn4 Tb4 1_565 . 173.6(2)
Sn6 Sn4 Tb4 1_565 . 114.59(7)
Sn6 Sn4 Tb4 1_455 . 60.29(4)
Sn6 Sn4 Tb4 . . 60.29(4)
Sn6 Sn4 Tb4 1_465 . 114.59(7)
Tb1 Sn4 Tb4 1_455 . 126.248(10)
Tb1 Sn4 Tb4 . . 126.248(10)
Tb4 Sn4 Tb4 1_565 . 79.44(7)
Sn3 Sn5 Sn3 1_565 1_455 178.12(18)
Sn3 Sn5 Sn3 1_565 1_465 88.809(4)
Sn3 Sn5 Sn3 1_455 1_465 91.160(4)
Sn3 Sn5 Sn3 1_565 . 91.160(4)
Sn3 Sn5 Sn3 1_455 . 88.809(4)
Sn3 Sn5 Sn3 1_465 . 178.12(18)
Sn3 Sn5 Sn2 1_565 1_455 119.25(9)
Sn3 Sn5 Sn2 1_455 1_455 62.32(7)
Sn3 Sn5 Sn2 1_465 1_455 62.32(7)
Sn3 Sn5 Sn2 . 1_455 119.25(9)
Sn3 Sn5 Sn2 1_565 . 62.32(7)
Sn3 Sn5 Sn2 1_455 . 119.25(9)
Sn3 Sn5 Sn2 1_465 . 119.25(9)
Sn3 Sn5 Sn2 . . 62.32(7)
Sn2 Sn5 Sn2 1_455 . 85.86(9)
Sn3 Sn5 Tb4 1_565 . 119.34(10)
Sn3 Sn5 Tb4 1_455 . 62.25(6)
Sn3 Sn5 Tb4 1_465 . 119.34(10)
Sn3 Sn5 Tb4 . . 62.25(6)
Sn2 Sn5 Tb4 1_455 . 57.03(4)
Sn2 Sn5 Tb4 . . 57.03(4)
Sn3 Sn5 Tb4 1_565 1_565 62.25(6)
Sn3 Sn5 Tb4 1_455 1_565 119.34(10)
Sn3 Sn5 Tb4 1_465 1_565 62.25(6)
Sn3 Sn5 Tb4 . 1_565 119.34(10)
Sn2 Sn5 Tb4 1_455 1_565 57.03(4)
Sn2 Sn5 Tb4 . 1_565 57.03(4)
Tb4 Sn5 Tb4 . 1_565 83.97(8)
Sn3 Sn5 Tb3 1_565 . 63.85(6)
Sn3 Sn5 Tb3 1_455 . 114.50(9)
Sn3 Sn5 Tb3 1_465 . 114.50(9)
Sn3 Sn5 Tb3 . . 63.85(6)
Sn2 Sn5 Tb3 1_455 . 174.75(7)
Sn2 Sn5 Tb3 . . 99.38(3)
Tb4 Sn5 Tb3 . . 126.034(19)
Tb4 Sn5 Tb3 1_565 . 126.034(19)
Sn3 Sn5 Tb3 1_565 1_455 114.50(9)
Sn3 Sn5 Tb3 1_455 1_455 63.85(6)
Sn3 Sn5 Tb3 1_465 1_455 63.85(6)
Sn3 Sn5 Tb3 . 1_455 114.50(9)
Sn2 Sn5 Tb3 1_455 1_455 99.38(3)
Sn2 Sn5 Tb3 . 1_455 174.75(7)
Tb4 Sn5 Tb3 . 1_455 126.034(19)
Tb4 Sn5 Tb3 1_565 1_455 126.034(19)
Tb3 Sn5 Tb3 . 1_455 75.37(6)
Sn4 Sn6 Sn4 1_545 1_655 174.08(12)
Sn4 Sn6 Sn4 1_545 1_645 88.675(6)
Sn4 Sn6 Sn4 1_655 1_645 91.020(7)
Sn4 Sn6 Sn4 1_545 . 91.020(7)
Sn4 Sn6 Sn4 1_655 . 88.675(6)
Sn4 Sn6 Sn4 1_645 . 174.08(12)
Sn4 Sn6 Sn7A 1_545 . 58.78(10)
Sn4 Sn6 Sn7A 1_655 . 116.32(13)
Sn4 Sn6 Sn7A 1_645 . 116.32(13)
Sn4 Sn6 Sn7A . . 58.78(10)
Sn4 Sn6 Sn7A 1_545 1_655 116.32(13)
Sn4 Sn6 Sn7A 1_655 1_655 58.78(10)
Sn4 Sn6 Sn7A 1_645 1_655 58.78(10)
Sn4 Sn6 Sn7A . 1_655 116.32(13)
Sn7A Sn6 Sn7A . 1_655 87.0(4)
Sn4 Sn6 Tb4 1_545 1_655 119.77(6)
Sn4 Sn6 Tb4 1_655 1_655 65.26(5)
Sn4 Sn6 Tb4 1_645 1_655 65.26(5)
Sn4 Sn6 Tb4 . 1_655 119.77(6)
Sn7A Sn6 Tb4 . 1_655 177.41(19)
Sn7A Sn6 Tb4 1_655 1_655 95.63(18)
Sn4 Sn6 Tb4 1_545 . 65.26(5)
Sn4 Sn6 Tb4 1_655 . 119.77(6)
Sn4 Sn6 Tb4 1_645 . 119.77(6)
Sn4 Sn6 Tb4 . . 65.26(5)
Sn7A Sn6 Tb4 . . 95.63(18)
Sn7A Sn6 Tb4 1_655 . 177.41(19)
Tb4 Sn6 Tb4 1_655 . 81.79(6)
Sn4 Sn6 Tb1 1_545 1_545 60.93(4)
Sn4 Sn6 Tb1 1_655 1_545 113.91(6)
Sn4 Sn6 Tb1 1_645 1_545 60.93(4)
Sn4 Sn6 Tb1 . 1_545 113.91(6)
Sn7A Sn6 Tb1 . 1_545 55.49(12)
Sn7A Sn6 Tb1 1_655 1_545 55.49(12)
Tb4 Sn6 Tb1 1_655 1_545 126.176(11)
Tb4 Sn6 Tb1 . 1_545 126.176(11)
Sn4 Sn6 Tb1 1_545 . 113.91(6)
Sn4 Sn6 Tb1 1_655 . 60.93(4)
Sn4 Sn6 Tb1 1_645 . 113.91(6)
Sn4 Sn6 Tb1 . . 60.93(4)
Sn7A Sn6 Tb1 . . 55.49(12)
Sn7A Sn6 Tb1 1_655 . 55.49(12)
Tb4 Sn6 Tb1 1_655 . 126.176(11)
Tb4 Sn6 Tb1 . . 126.176(11)
Tb1 Sn6 Tb1 1_545 . 77.32(5)
Sn7A Sn7 Tb1 5 . 90.0
Sn7A Sn7 Tb1 5 1_445 90.0
Tb1 Sn7 Tb1 . 1_445 180.0
Sn7A Sn7 Tb1 5 1_545 90.0
Tb1 Sn7 Tb1 . 1_545 91.176(2)
Tb1 Sn7 Tb1 1_445 1_545 88.824(2)
Sn7A Sn7 Tb1 5 1_455 90.0
Tb1 Sn7 Tb1 . 1_455 88.824(2)
Tb1 Sn7 Tb1 1_445 1_455 91.176(2)
Tb1 Sn7 Tb1 1_545 1_455 180.0
Sn7A Sn7A Sn4 5 . 133.86(19)
Sn7A Sn7A Sn4 5 1_545 133.86(19)
Sn4 Sn7A Sn4 . 1_545 92.3(4)
Sn7A Sn7A Tb1 5 1_445 81.2(3)
Sn4 Sn7A Tb1 . 1_445 128.0(3)
Sn4 Sn7A Tb1 1_545 1_445 66.23(9)
Sn7A Sn7A Tb1 5 . 81.2(3)
Sn4 Sn7A Tb1 . . 66.23(9)
Sn4 Sn7A Tb1 1_545 . 128.0(3)
Tb1 Sn7A Tb1 1_445 . 162.4(5)
Sn7A Sn7A Tb1 5 1_545 81.2(3)
Sn4 Sn7A Tb1 . 1_545 128.0(3)
Sn4 Sn7A Tb1 1_545 1_545 66.23(9)
Tb1 Sn7A Tb1 1_445 1_545 87.51(8)
Tb1 Sn7A Tb1 . 1_545 89.81(8)
Sn7A Sn7A Tb1 5 1_455 81.2(3)
Sn4 Sn7A Tb1 . 1_455 66.23(9)
Sn4 Sn7A Tb1 1_545 1_455 128.0(3)
Tb1 Sn7A Tb1 1_445 1_455 89.81(8)
Tb1 Sn7A Tb1 . 1_455 87.51(8)
Tb1 Sn7A Tb1 1_545 1_455 162.4(5)
Sn7A Sn7A Sn6 5 . 136.52(18)
Sn4 Sn7A Sn6 . . 59.8(2)
Sn4 Sn7A Sn6 1_545 . 59.8(2)
Tb1 Sn7A Sn6 1_445 . 125.9(3)
Tb1 Sn7A Sn6 . . 68.60(10)
Tb1 Sn7A Sn6 1_545 . 68.60(10)
Tb1 Sn7A Sn6 1_455 . 125.9(3)
Sn7A Sn7A Sn6 5 1_455 136.52(18)
Sn4 Sn7A Sn6 . 1_455 59.8(2)
Sn4 Sn7A Sn6 1_545 1_455 59.8(2)
Tb1 Sn7A Sn6 1_445 1_455 68.60(10)
Tb1 Sn7A Sn6 . 1_455 125.9(3)
Tb1 Sn7A Sn6 1_545 1_455 125.9(3)
Tb1 Sn7A Sn6 1_455 1_455 68.60(10)
Sn6 Sn7A Sn6 . 1_455 87.0(4)
Sn8A Sn8A Sn1 5_656 . 136.0(3)
Sn8A Sn8A Sn1 5_656 1_655 136.0(3)
Sn1 Sn8A Sn1 . 1_655 88.1(6)
Sn8A Sn8A Tb2 5_656 1_655 82.2(4)
Sn1 Sn8A Tb2 . 1_655 125.4(5)
Sn1 Sn8A Tb2 1_655 1_655 67.40(17)
Sn8A Sn8A Tb2 5_656 1_545 82.2(4)
Sn1 Sn8A Tb2 . 1_545 67.40(17)
Sn1 Sn8A Tb2 1_655 1_545 125.4(5)
Tb2 Sn8A Tb2 1_655 1_545 164.4(9)
Sn8A Sn8A Tb2 5_656 . 82.2(4)
Sn1 Sn8A Tb2 . . 67.40(17)
Sn1 Sn8A Tb2 1_655 . 125.4(5)
Tb2 Sn8A Tb2 1_655 . 87.79(11)
Tb2 Sn8A Tb2 1_545 . 90.10(12)
Sn8A Sn8A Tb2 5_656 1_645 82.2(4)
Sn1 Sn8A Tb2 . 1_645 125.4(5)
Sn1 Sn8A Tb2 1_655 1_645 67.40(17)
Tb2 Sn8A Tb2 1_655 1_645 90.10(12)
Tb2 Sn8A Tb2 1_545 1_645 87.79(11)
Tb2 Sn8A Tb2 . 1_645 164.4(9)
Sn8A Sn8A Tb3 5_656 1_545 137.2(3)
Sn1 Sn8A Tb3 . 1_545 58.1(3)
Sn1 Sn8A Tb3 1_655 1_545 58.1(3)
Tb2 Sn8A Tb3 1_655 1_545 125.5(5)
Tb2 Sn8A Tb3 1_545 1_545 67.62(18)
Tb2 Sn8A Tb3 . 1_545 125.5(5)
Tb2 Sn8A Tb3 1_645 1_545 67.62(18)
Sn8A Sn8A Tb3 5_656 . 137.2(3)
Sn1 Sn8A Tb3 . . 58.1(3)
Sn1 Sn8A Tb3 1_655 . 58.1(3)
Tb2 Sn8A Tb3 1_655 . 67.62(18)
Tb2 Sn8A Tb3 1_545 . 125.5(5)
Tb2 Sn8A Tb3 . . 67.62(18)
Tb2 Sn8A Tb3 1_645 . 125.5(5)
Tb3 Sn8A Tb3 1_545 . 85.5(6)
Sn8A Sn8 Tb2 5_656 1_655 90.000(8)
Sn8A Sn8 Tb2 5_656 1_545 90.000(8)
Tb2 Sn8 Tb2 1_655 1_545 180.0
Sn8A Sn8 Tb2 5_656 . 90.0
Tb2 Sn8 Tb2 1_655 . 88.824(2)
Tb2 Sn8 Tb2 1_545 . 91.176(2)
Sn8A Sn8 Tb2 5_656 1_645 90.0
Tb2 Sn8 Tb2 1_655 1_645 91.176(2)
Tb2 Sn8 Tb2 1_545 1_645 88.824(2)
Tb2 Sn8 Tb2 . 1_645 180.0
Sn8A Sn8 Tb3 5_656 1_545 141.854(16)
Tb2 Sn8 Tb3 1_655 1_545 116.181(9)
Tb2 Sn8 Tb3 1_545 1_545 63.819(9)
Tb2 Sn8 Tb3 . 1_545 116.181(9)
Tb2 Sn8 Tb3 1_645 1_545 63.819(9)
Sn8A Sn8 Tb3 5_656 5_666 38.146(16)
Tb2 Sn8 Tb3 1_655 5_666 63.819(10)
Tb2 Sn8 Tb3 1_545 5_666 116.181(10)
Tb2 Sn8 Tb3 . 5_666 63.819(9)
Tb2 Sn8 Tb3 1_645 5_666 116.181(9)
Tb3 Sn8 Tb3 1_545 5_666 180.00(3)
Sn8A Sn8 Tb3 5_656 . 141.854(17)
Tb2 Sn8 Tb3 1_655 . 63.819(10)
Tb2 Sn8 Tb3 1_545 . 116.181(9)
Tb2 Sn8 Tb3 . . 63.819(9)
Tb2 Sn8 Tb3 1_645 . 116.181(9)
Tb3 Sn8 Tb3 1_545 . 76.29(3)
Tb3 Sn8 Tb3 5_666 . 103.71(3)
Sn8A Sn8 Tb3 5_656 5_656 38.146(17)
Tb2 Sn8 Tb3 1_655 5_656 116.181(9)
Tb2 Sn8 Tb3 1_545 5_656 63.819(9)
Tb2 Sn8 Tb3 . 5_656 116.181(9)
Tb2 Sn8 Tb3 1_645 5_656 63.819(9)
Tb3 Sn8 Tb3 1_545 5_656 103.71(3)
Tb3 Sn8 Tb3 5_666 5_656 76.29(3)
Tb3 Sn8 Tb3 . 5_656 180.0
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Tb1 Sn7 1_665 3.0974
Tb1 Sn7 . 3.0974
Tb1 Sn7 1_565 3.0974
Tb1 Sn7 1_655 3.0974
Tb1 Sn7A 1_665 3.134(2)
Tb1 Sn7A 5 3.134(2)
Tb1 Sn7A . 3.134(2)
Tb1 Sn7A 5_665 3.134(2)
Tb1 Sn7A 1_565 3.134(2)
Tb1 Sn7A 1_655 3.134(2)
Tb1 Sn7A 5_565 3.134(2)
Tb1 Sn7A 5_655 3.134(2)
Tb2 Sn8 1_565 3.0974
Tb2 Sn8 1_455 3.0974
Tb2 Sn8 1_465 3.0974
Tb2 Sn8 . 3.0974
Tb2 Sn8A 5_666 3.126(3)
Tb2 Sn8A 1_455 3.126(3)
Tb2 Sn8A 5_556 3.126(3)
Tb2 Sn8A 1_565 3.126(3)
Tb2 Sn8A 5_566 3.126(3)
Tb2 Sn8A 5_656 3.126(3)
Tb2 Sn8A . 3.126(3)
Tb2 Sn8A 1_465 3.126(3)
Tb3 Sn1 1_665 3.10108(16)
Tb3 Sn1 . 3.10108(16)
Tb3 Sn1 1_565 3.10108(16)
Tb3 Sn1 1_655 3.10108(16)
Tb3 Sn8A 1_565 3.259(17)
Tb3 Sn8A . 3.259(17)
Tb3 Sn3 . 3.534(2)
Tb3 Sn3 1_565 3.534(2)
Tb3 Sn5 . 3.546(3)
Tb3 Sn5 1_655 3.546(3)
Tb3 Tb2 1_655 3.5545(12)
Tb4 Sn2 . 3.10007(16)
Tb4 Sn2 1_445 3.10007(16)
Tb4 Sn2 1_455 3.10007(16)
Tb4 Sn2 1_545 3.10007(16)
Tb4 Sn5 . 3.308(3)
Tb4 Sn5 1_545 3.308(3)
Tb4 Sn6 1_455 3.3111(19)
Tb4 Sn6 . 3.3111(19)
Tb4 Sn3 . 3.316(2)
Tb4 Sn3 1_455 3.316(2)
Tb4 Sn4 1_545 3.462(3)
Tb4 Sn4 . 3.462(3)
Sn1 Tb3 1_445 3.10108(16)
Sn1 Tb3 1_455 3.10108(16)
Sn1 Tb3 1_545 3.10108(16)
Sn1 Sn8A . 3.118(17)
Sn1 Sn8A 1_455 3.118(17)
Sn1 Tb2 1_545 3.4645(17)
Sn2 Tb4 1_665 3.10007(16)
Sn2 Tb4 1_565 3.10007(16)
Sn2 Tb4 1_655 3.10007(16)
Sn2 Sn5 1_655 3.182(3)
Sn2 Sn5 . 3.182(3)
Sn2 Sn3 1_565 3.250(3)
Sn2 Sn3 . 3.250(3)
Sn3 Sn5 1_545 3.09780(10)
Sn3 Sn5 1_655 3.09782(10)
Sn3 Sn5 1_645 3.09780(10)
Sn3 Sn5 . 3.09780(10)
Sn3 Sn2 1_545 3.250(3)
Sn3 Tb4 1_655 3.316(2)
Sn3 Tb3 1_545 3.534(2)
Sn4 Sn7A . 3.068(10)
Sn4 Sn7A 1_565 3.068(10)
Sn4 Sn6 1_565 3.10153(18)
Sn4 Sn6 1_455 3.10153(18)
Sn4 Sn6 . 3.10153(18)
Sn4 Sn6 1_465 3.10153(18)
Sn4 Tb1 1_455 3.3892(18)
Sn4 Tb4 1_565 3.462(3)
Sn5 Sn3 1_565 3.09782(10)
Sn5 Sn3 1_455 3.0978(10)
Sn5 Sn3 1_465 3.0978(10)
Sn5 Sn2 1_455 3.182(3)
Sn5 Tb4 1_565 3.308(3)
Sn5 Tb3 1_455 3.546(3)
Sn6 Sn4 1_545 3.10153(18)
Sn6 Sn4 1_655 3.10153(18)
Sn6 Sn4 1_645 3.10153(18)
Sn6 Sn7A . 3.150(10)
Sn6 Sn7A 1_655 3.150(10)
Sn6 Tb4 1_655 3.3111(19)
Sn6 Tb1 1_545 3.5416(18)
Sn7 Sn7A 5 0.480(14)
Sn7 Tb1 1_445 3.0974
Sn7 Tb1 1_545 3.0974
Sn7 Tb1 1_455 3.0974
Sn7A Sn7A 5 0.96(3)
Sn7A Sn4 1_545 3.068(10)
Sn7A Tb1 1_445 3.134(2)
Sn7A Tb1 1_545 3.134(2)
Sn7A Tb1 1_455 3.134(2)
Sn7A Sn6 1_455 3.150(10)
Sn8A Sn8A 5_656 0.85(5)
Sn8A Sn1 1_655 3.118(17)
Sn8A Tb2 1_655 3.126(3)
Sn8A Tb2 1_545 3.126(3)
Sn8A Tb2 1_645 3.126(3)
Sn8A Tb3 1_545 3.259(17)
Sn8 Sn8A 5_656 0.42(2)
Sn8 Tb2 1_655 3.0974
Sn8 Tb2 1_545 3.0974
Sn8 Tb2 1_645 3.0974
Sn8 Tb3 1_545 3.5821(12)
Sn8 Tb3 5_666 3.5821(12)
Sn8 Tb3 5_656 3.5821(12)
