#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:00 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180920 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200015.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200015_Fobs loop_ _publ_author_name 'Yokochi, Alex F. T.' 'White, James D.' 'Sturtz, George' _publ_section_title ; Vulgarone B ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o99 _journal_page_last o101 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6280 _cell_length_b 10.2180 _cell_length_c 19.8890 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8339 _cod_data_source_file bt6000Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c:\VULG3 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 108.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 444.76 447.89 13.39 o 6 0 0 140.92 180.29 17.13 o 1 1 0 5962.82 5219.31 469.94 o 2 1 0 127.54 136.90 4.41 o 3 1 0 96.50 91.74 3.11 o 4 1 0 0.07 0.68 0.54 o 5 1 0 2.02 3.21 0.62 o 6 1 0 12.82 13.16 0.69 o 7 1 0 0.35 0.42 0.42 o 0 2 0 79.67 84.04 4.32 o 1 2 0 89.20 111.31 7.28 o 2 2 0 708.35 647.50 66.42 o 3 2 0 0.26 0.23 0.35 o 4 2 0 294.24 312.41 9.50 o 5 2 0 5.61 6.99 0.62 o 6 2 0 43.44 46.86 1.96 o 7 2 0 7.74 6.79 0.59 o 1 3 0 184.17 175.24 7.50 o 2 3 0 748.40 753.19 51.21 o 3 3 0 0.34 0.61 0.39 o 4 3 0 9.70 8.22 0.71 o 5 3 0 6.08 5.66 0.62 o 6 3 0 6.44 6.44 0.56 o 7 3 0 0.00 -0.51 0.57 o 0 4 0 1360.90 1106.56 31.51 o 1 4 0 219.18 244.21 9.10 o 2 4 0 61.67 48.89 3.38 o 3 4 0 1.47 2.42 0.41 o 4 4 0 19.25 21.05 1.09 o 5 4 0 27.95 27.61 1.23 o 6 4 0 1.16 1.10 0.37 o 7 4 0 4.42 3.12 0.67 o 1 5 0 50.56 57.32 3.29 o 2 5 0 152.68 152.75 7.59 o 3 5 0 26.46 22.27 0.78 o 4 5 0 93.25 92.82 8.56 o 5 5 0 11.77 10.71 0.69 o 6 5 0 11.25 8.61 0.48 o 7 5 0 0.81 0.76 0.43 o 0 6 0 23.74 30.81 1.65 o 1 6 0 39.90 35.37 1.42 o 2 6 0 8.47 9.50 0.59 o 3 6 0 45.01 43.99 1.53 o 4 6 0 7.37 7.72 0.64 o 5 6 0 0.11 0.07 0.35 o 6 6 0 0.03 0.49 0.30 o 1 7 0 55.93 50.99 1.40 o 2 7 0 0.32 0.64 0.42 o 3 7 0 0.35 0.66 0.65 o 4 7 0 0.16 0.32 1.26 o 5 7 0 0.06 -0.12 0.71 o 6 7 0 1.60 1.54 0.59 o 0 8 0 45.77 47.49 5.27 o 1 8 0 0.62 0.94 0.48 o 2 8 0 4.56 4.88 0.83 o 3 8 0 40.47 45.54 2.72 o 4 8 0 22.61 24.20 0.78 o 5 8 0 4.14 3.96 0.68 o 6 8 0 1.05 1.76 0.42 o 1 9 0 2.33 2.57 0.49 o 2 9 0 29.04 28.73 0.87 o 3 9 0 0.07 0.21 0.39 o 4 9 0 0.03 0.58 0.34 o 5 9 0 0.51 0.50 0.41 o 0 10 0 58.83 69.02 1.89 o 1 10 0 0.05 0.00 0.35 o 2 10 0 0.27 -0.01 0.85 o 3 10 0 1.37 0.39 0.34 o 4 10 0 0.00 0.03 0.40 o 1 11 0 0.22 1.07 0.43 o 2 11 0 0.78 0.23 0.84 o 3 11 0 0.01 0.08 0.34 o 0 12 0 1.14 0.49 0.93 o 1 12 0 0.18 -0.11 0.34 o 1 0 1 2750.98 3091.19 182.06 o 2 0 1 1238.57 1031.59 21.98 o 3 0 1 47.16 53.05 1.85 o 4 0 1 131.93 125.34 4.51 o 5 0 1 29.51 32.00 1.78 o 6 0 1 1.24 0.98 0.52 o 7 0 1 0.15 -0.45 0.45 o -6 1 1 17.51 18.15 1.08 o -5 1 1 30.99 32.32 1.31 o -4 1 1 9.31 10.14 0.77 o -3 1 1 354.69 330.30 12.65 o -2 1 1 276.72 225.89 9.25 o -1 1 1 3125.34 3217.79 55.67 o 0 1 1 103.98 138.28 3.80 o 1 1 1 3125.32 3850.99 59.31 o 2 1 1 275.50 250.86 9.87 o 3 1 1 354.64 300.34 11.30 o 4 1 1 9.34 8.96 0.76 o 5 1 1 30.99 27.58 1.33 o 6 1 1 17.59 18.49 1.06 o 7 1 1 0.47 0.92 0.43 o -6 2 1 42.25 43.67 1.77 o -5 2 1 28.58 29.19 1.45 o -4 2 1 75.11 69.32 2.60 o -3 2 1 30.81 26.14 1.08 o -2 2 1 143.42 142.20 6.07 o -1 2 1 1091.15 1202.59 34.17 o 0 2 1 1809.93 2266.23 109.97 o 1 2 1 1094.63 1461.05 35.78 o 2 2 1 143.95 143.22 6.69 o 3 2 1 31.10 25.95 1.62 o 4 2 1 75.32 70.68 3.40 o 5 2 1 28.31 25.75 1.40 o 6 2 1 42.21 47.15 1.80 o 7 2 1 5.68 5.63 0.55 o -6 3 1 8.60 6.52 0.76 o -5 3 1 46.22 51.85 2.19 o -4 3 1 33.30 34.47 1.40 o -3 3 1 116.09 125.01 5.80 o -2 3 1 242.11 231.45 10.25 o -1 3 1 225.60 198.43 8.45 o 0 3 1 3.72 2.69 0.87 o 1 3 1 226.17 245.99 9.64 o 2 3 1 241.72 252.16 9.91 o 3 3 1 116.02 128.73 5.43 o 4 3 1 33.90 36.97 1.73 o 5 3 1 46.39 41.37 1.86 o 6 3 1 8.75 8.72 0.80 o 7 3 1 6.67 6.64 0.80 o -6 4 1 12.76 10.86 0.83 o -5 4 1 234.92 248.43 9.49 o -4 4 1 51.77 47.63 1.83 o -3 4 1 138.66 137.70 6.27 o -2 4 1 558.12 467.63 22.33 o -1 4 1 1833.12 1563.81 42.76 o 0 4 1 100.11 95.18 2.92 o 1 4 1 1830.08 1691.66 40.86 o 2 4 1 556.66 507.35 20.87 o 3 4 1 137.48 148.14 5.62 o 4 4 1 51.65 52.01 2.33 o 5 4 1 234.80 253.33 8.16 o 6 4 1 12.70 12.12 0.76 o 7 4 1 6.10 4.76 0.72 o -6 5 1 7.24 7.28 0.70 o -5 5 1 48.73 51.30 2.00 o -4 5 1 24.52 23.05 1.25 o -3 5 1 4.79 7.37 1.02 o -2 5 1 41.78 38.37 1.53 o -1 5 1 290.61 272.15 10.92 o 0 5 1 84.04 84.00 2.70 o 1 5 1 291.21 289.71 10.79 o 2 5 1 42.79 42.70 1.90 o 3 5 1 4.81 4.57 0.60 o 4 5 1 24.68 25.65 1.10 o 5 5 1 48.79 47.14 1.76 o 6 5 1 7.35 8.54 0.61 o 7 5 1 0.76 0.18 0.38 o -5 6 1 21.62 24.60 1.26 o -4 6 1 5.29 6.80 0.91 o -3 6 1 13.12 10.76 1.01 o -2 6 1 88.36 78.00 3.51 o -1 6 1 295.75 258.84 9.65 o 0 6 1 0.67 0.59 0.65 o 1 6 1 296.63 283.14 13.54 o 2 6 1 88.44 86.24 3.40 o 3 6 1 13.45 11.85 0.80 o 4 6 1 5.27 5.23 0.80 o 5 6 1 21.41 21.36 0.94 o 6 6 1 1.20 1.15 0.67 o -5 7 1 2.86 3.16 0.66 o -4 7 1 19.27 18.63 1.48 o -3 7 1 20.77 20.21 1.65 o -2 7 1 24.84 21.19 1.32 o -1 7 1 15.24 16.58 1.06 o 0 7 1 68.10 78.71 4.78 o 1 7 1 15.27 17.51 0.92 o 2 7 1 24.67 21.63 0.96 o 3 7 1 20.74 20.78 1.07 o 4 7 1 19.27 16.54 0.94 o 5 7 1 2.88 1.87 0.56 o 6 7 1 3.43 3.42 0.56 o -4 8 1 19.90 22.06 1.35 o -3 8 1 4.93 3.14 0.96 o -2 8 1 13.01 12.25 1.11 o -1 8 1 47.28 48.66 2.14 o 0 8 1 23.31 23.31 0.94 o 1 8 1 47.07 47.75 2.08 o 2 8 1 12.95 13.06 0.84 o 3 8 1 4.96 3.36 0.61 o 4 8 1 19.87 18.72 0.85 o 5 8 1 1.44 0.68 0.49 o 6 8 1 0.57 0.80 0.40 o -3 9 1 17.32 14.91 1.14 o -2 9 1 5.48 7.38 0.97 o -1 9 1 32.09 34.83 1.69 o 0 9 1 53.66 57.41 1.66 o 1 9 1 32.12 34.19 1.41 o 2 9 1 5.50 5.38 0.64 o 3 9 1 17.35 17.88 0.84 o 4 9 1 12.47 12.75 0.60 o 5 9 1 3.88 1.76 0.51 o -2 10 1 0.10 1.72 0.62 o -1 10 1 3.86 4.32 0.80 o 0 10 1 0.86 0.93 0.80 o 1 10 1 3.85 4.82 0.62 o 2 10 1 0.10 -0.47 0.50 o 3 10 1 5.05 5.16 0.43 o 4 10 1 6.91 7.68 0.61 o -2 11 1 1.81 1.38 0.79 o -1 11 1 0.19 -0.33 0.80 o 0 11 1 2.47 2.33 0.66 o 1 11 1 0.19 -0.16 0.49 o 2 11 1 1.80 1.20 0.65 o 3 11 1 1.26 0.88 0.43 o -1 12 1 0.97 1.97 0.68 o 0 12 1 1.10 0.54 0.53 o 1 12 1 0.97 0.74 0.48 o 0 0 2 1198.35 977.25 16.48 o 1 0 2 11513.98 10428.44 857.98 o 2 0 2 330.50 381.03 10.83 o 3 0 2 30.64 25.92 0.81 o 4 0 2 579.84 563.02 19.97 o 5 0 2 2.92 2.25 0.61 o 6 0 2 20.76 22.75 1.76 o 7 0 2 0.00 0.08 0.40 o -6 1 2 27.26 26.86 1.18 o -5 1 2 10.68 11.67 1.02 o -4 1 2 124.16 121.55 5.15 o -3 1 2 22.52 26.69 1.03 o -2 1 2 16.67 17.77 1.00 o 0 1 2 11819.71 13629.70 210.58 o 2 1 2 15.98 15.89 0.81 o 3 1 2 22.44 26.15 1.64 o 4 1 2 123.63 122.74 5.34 o 5 1 2 10.37 9.28 0.86 o 6 1 2 27.24 30.36 1.26 o 7 1 2 7.79 6.40 0.65 o -6 2 2 34.05 33.22 1.39 o -5 2 2 6.92 6.70 1.14 o -4 2 2 190.69 178.20 7.47 o -3 2 2 150.30 156.23 6.64 o -2 2 2 438.56 418.83 15.16 o -1 2 2 3006.11 2960.06 53.78 o 0 2 2 2064.89 2316.41 47.72 o 1 2 2 3008.09 3365.65 54.70 o 2 2 2 438.88 461.57 21.95 o 3 2 2 151.14 154.35 6.79 o 4 2 2 190.95 170.93 7.15 o 5 2 2 6.80 6.04 0.76 o 6 2 2 34.09 39.86 1.56 o 7 2 2 2.09 2.03 0.41 o -6 3 2 6.80 5.91 0.75 o -5 3 2 61.03 58.48 2.27 o -4 3 2 6.20 6.74 0.85 o -3 3 2 34.87 31.91 1.11 o -2 3 2 105.34 97.12 4.50 o -1 3 2 569.41 526.16 24.04 o 0 3 2 216.59 222.92 12.73 o 1 3 2 570.69 587.14 23.32 o 2 3 2 105.14 98.57 4.16 o 3 3 2 35.01 34.17 1.56 o 4 3 2 6.12 5.40 0.75 o 5 3 2 61.38 53.98 2.35 o 6 3 2 6.81 7.67 0.96 o 7 3 2 1.50 1.89 0.62 o -6 4 2 13.24 13.20 0.88 o -5 4 2 25.38 24.90 1.32 o -4 4 2 24.27 24.92 1.19 o -3 4 2 68.99 61.35 2.35 o -2 4 2 805.46 728.18 27.26 o -1 4 2 319.69 290.78 11.31 o 0 4 2 91.05 77.69 2.41 o 1 4 2 319.48 302.89 11.59 o 2 4 2 803.97 777.88 25.18 o 3 4 2 68.94 63.15 3.18 o 4 4 2 24.31 25.59 1.32 o 5 4 2 25.27 26.25 1.36 o 6 4 2 13.15 13.21 0.80 o 7 4 2 3.93 3.55 0.66 o -5 5 2 11.14 9.30 1.06 o -4 5 2 37.71 33.46 1.58 o -3 5 2 11.97 11.62 0.99 o -2 5 2 54.32 53.16 1.89 o -1 5 2 147.95 134.39 6.04 o 0 5 2 6.69 6.99 0.44 o 1 5 2 148.03 145.15 6.42 o 2 5 2 54.41 51.23 2.24 o 3 5 2 11.97 11.48 0.79 o 4 5 2 37.85 38.42 1.54 o 5 5 2 11.17 10.17 0.85 o 6 5 2 0.67 0.32 0.37 o -5 6 2 1.78 0.96 0.78 o -4 6 2 8.44 5.63 0.99 o -3 6 2 14.84 16.55 1.12 o -2 6 2 9.10 8.61 0.85 o -1 6 2 32.98 31.95 1.26 o 0 6 2 24.65 29.32 3.02 o 1 6 2 32.95 31.26 1.98 o 2 6 2 9.14 10.77 0.86 o 3 6 2 14.86 15.26 0.86 o 4 6 2 8.42 7.39 0.93 o 5 6 2 1.80 1.74 0.69 o 6 6 2 3.11 3.33 0.79 o -5 7 2 2.99 3.59 0.69 o -4 7 2 2.46 3.11 0.88 o -3 7 2 14.71 16.24 1.25 o -2 7 2 46.84 53.05 2.49 o -1 7 2 7.53 10.26 1.05 o 0 7 2 7.20 8.60 0.57 o 1 7 2 7.60 7.72 0.70 o 2 7 2 46.81 50.67 2.27 o 3 7 2 14.60 19.29 1.14 o 4 7 2 2.48 2.28 0.63 o 5 7 2 2.99 2.08 0.49 o 6 7 2 0.26 0.81 0.59 o -4 8 2 5.11 5.64 0.94 o -3 8 2 0.36 0.82 1.12 o -2 8 2 39.84 38.69 1.91 o -1 8 2 43.89 46.20 1.74 o 0 8 2 70.86 72.64 3.03 o 1 8 2 43.78 41.89 1.53 o 2 8 2 40.04 40.14 1.70 o 3 8 2 0.36 0.04 0.49 o 4 8 2 5.16 6.39 0.58 o 5 8 2 0.72 1.05 0.54 o -3 9 2 14.01 17.90 1.14 o -2 9 2 7.95 6.82 0.93 o -1 9 2 1.43 1.43 1.00 o 0 9 2 50.11 50.91 2.63 o 1 9 2 1.39 1.31 0.50 o 2 9 2 7.97 5.39 0.62 o 3 9 2 13.91 14.13 0.84 o 4 9 2 0.41 0.36 0.31 o 5 9 2 1.56 1.45 0.45 o -2 10 2 2.16 1.32 0.66 o -1 10 2 1.16 0.61 0.69 o 0 10 2 0.78 0.52 0.60 o 1 10 2 1.15 1.50 0.43 o 2 10 2 2.19 1.77 0.50 o 3 10 2 3.37 3.51 0.76 o 4 10 2 2.05 1.45 0.43 o -2 11 2 0.71 0.21 0.85 o -1 11 2 3.01 6.29 0.94 o 0 11 2 0.31 0.88 0.50 o 1 11 2 3.00 3.31 0.60 o 2 11 2 0.72 0.97 0.40 o 3 11 2 3.53 3.89 0.49 o -1 12 2 1.11 1.17 0.55 o 0 12 2 0.32 1.16 0.59 o 1 12 2 1.11 0.53 0.37 o 1 0 3 30.00 45.01 7.31 o 2 0 3 127.49 157.83 5.11 o 3 0 3 1234.93 1088.49 27.66 o 4 0 3 0.01 0.33 0.37 o 5 0 3 8.94 10.40 0.66 o 6 0 3 3.00 2.37 0.46 o 7 0 3 6.14 4.76 0.61 o -6 1 3 3.97 3.33 0.62 o -5 1 3 20.57 19.75 1.08 o -4 1 3 22.46 22.87 1.22 o -3 1 3 33.23 31.74 1.02 o -2 1 3 53.27 50.98 2.43 o 2 1 3 53.84 47.19 2.19 o 3 1 3 33.43 31.29 1.05 o 4 1 3 22.68 23.36 1.32 o 5 1 3 20.43 17.36 1.22 o 6 1 3 3.93 3.82 0.72 o 7 1 3 4.96 4.90 0.54 o -6 2 3 25.28 25.99 1.10 o -5 2 3 85.02 93.04 3.87 o -4 2 3 50.65 44.16 1.97 o -3 2 3 492.95 461.74 16.04 o -2 2 3 675.36 614.98 26.25 o -1 2 3 3049.65 2660.84 47.88 o 0 2 3 3588.27 3525.52 37.60 o 1 2 3 3052.92 3067.71 49.31 o 2 2 3 674.09 731.60 27.18 o 3 2 3 493.00 472.97 21.82 o 4 2 3 51.15 41.28 1.47 o 5 2 3 84.75 78.11 3.20 o 6 2 3 25.42 27.66 1.14 o 7 2 3 3.07 4.35 0.74 o -6 3 3 32.90 30.99 1.18 o -5 3 3 83.77 97.42 3.96 o -4 3 3 73.79 76.41 3.38 o -3 3 3 32.47 33.86 1.71 o -2 3 3 446.32 416.15 14.83 o -1 3 3 20.29 19.51 0.96 o 0 3 3 134.43 121.11 3.82 o 1 3 3 20.37 21.28 0.71 o 2 3 3 447.47 435.81 20.35 o 3 3 3 32.06 33.28 1.65 o 4 3 3 73.43 70.67 3.13 o 5 3 3 83.74 77.37 3.08 o 6 3 3 33.17 35.13 1.23 o -6 4 3 0.11 0.68 0.79 o -5 4 3 48.89 51.57 1.92 o -4 4 3 47.35 46.20 1.95 o -3 4 3 136.14 110.10 5.25 o -2 4 3 294.94 240.91 9.75 o -1 4 3 398.80 408.46 14.68 o 0 4 3 45.37 54.17 3.27 o 1 4 3 396.83 412.16 19.60 o 2 4 3 295.57 300.53 10.75 o 3 4 3 136.00 122.56 5.12 o 4 4 3 47.46 46.82 1.91 o 5 4 3 48.66 45.39 1.86 o 6 4 3 0.12 -0.30 0.42 o -5 5 3 41.01 43.27 1.62 o -4 5 3 5.27 4.51 1.10 o -3 5 3 4.20 5.95 0.80 o -2 5 3 5.46 5.43 0.69 o -1 5 3 222.45 228.59 8.96 o 0 5 3 5.27 3.35 0.49 o 1 5 3 222.35 267.62 9.63 o 2 5 3 5.30 5.67 0.56 o 3 5 3 4.27 5.38 0.60 o 4 5 3 5.41 5.90 0.69 o 5 5 3 40.91 41.91 1.46 o 6 5 3 6.81 8.24 0.57 o -5 6 3 13.39 14.15 0.99 o -4 6 3 16.32 18.25 1.37 o -3 6 3 71.96 73.16 2.49 o -2 6 3 22.11 17.21 1.04 o -1 6 3 199.83 175.33 7.45 o 0 6 3 0.73 0.21 0.34 o 1 6 3 199.96 176.91 6.68 o 2 6 3 21.85 19.96 0.90 o 3 6 3 72.20 77.20 3.09 o 4 6 3 16.33 15.08 0.90 o 5 6 3 13.32 11.18 0.76 o 6 6 3 17.99 21.33 1.00 o -5 7 3 2.47 2.21 0.60 o -4 7 3 8.67 10.10 1.28 o -3 7 3 18.48 18.21 1.25 o -2 7 3 18.66 17.79 1.19 o -1 7 3 0.36 0.95 0.64 o 0 7 3 12.22 11.71 0.87 o 1 7 3 0.35 0.29 0.43 o 2 7 3 18.69 15.36 0.82 o 3 7 3 18.53 18.70 0.97 o 4 7 3 8.71 6.43 0.68 o 5 7 3 2.45 1.39 0.43 o 6 7 3 2.77 3.23 0.53 o -4 8 3 7.20 9.01 0.94 o -3 8 3 20.47 16.84 1.25 o -2 8 3 17.20 16.63 1.29 o -1 8 3 62.43 57.52 2.79 o 0 8 3 326.34 342.96 18.04 o 1 8 3 62.21 58.98 2.16 o 2 8 3 17.27 19.46 0.93 o 3 8 3 20.45 17.12 0.87 o 4 8 3 7.19 7.65 0.60 o 5 8 3 2.81 2.25 0.75 o -3 9 3 4.74 5.49 1.12 o -2 9 3 2.72 2.63 0.89 o -1 9 3 63.67 67.92 2.83 o 0 9 3 7.49 8.85 0.66 o 1 9 3 63.71 64.45 2.33 o 2 9 3 2.73 2.41 0.51 o 3 9 3 4.74 4.45 0.54 o 4 9 3 5.60 5.93 0.43 o 5 9 3 3.85 2.23 0.47 o -2 10 3 2.55 3.98 0.81 o -1 10 3 4.55 5.17 0.75 o 0 10 3 0.29 0.70 0.39 o 1 10 3 4.54 3.58 0.58 o 2 10 3 2.54 2.46 0.42 o 3 10 3 1.28 1.68 0.53 o 4 10 3 3.86 3.91 0.49 o -1 11 3 2.71 3.92 0.98 o 0 11 3 0.03 -0.10 0.50 o 1 11 3 2.72 1.72 0.67 o 2 11 3 1.63 2.17 0.42 o 3 11 3 1.25 0.77 0.41 o -1 12 3 1.60 1.08 0.73 o 0 12 3 0.48 -0.36 0.45 o 1 12 3 1.60 0.93 0.39 o 0 0 4 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