#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200019.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200019_Fobs loop_ _publ_author_name 'Kubo, Kanji' 'Yamamoto, Emi' 'Sakurai, Tadamitsu' 'Mori, Akira' _publ_section_title ; N,N',N'',N'''-Tetrakis(1-naphthylmethyl)-1,4,8,11-tetraazacyclotetradecane ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1 _journal_page_last o3 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.462 _cell_angle_gamma 90.000 _cell_length_a 11.6090 _cell_length_b 18.9070 _cell_length_c 9.8780 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high .7579 _[local]_cod_data_source_file cf60021sup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' CF6002' _shelx_refln_list_code 4 _shelx_f_calc_maximum 181.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5944.29 5565.18 65.19 o 4 0 0 2095.29 1925.65 56.70 o 6 0 0 249.40 260.46 11.49 o 8 0 0 137.13 138.92 14.38 o 10 0 0 .88 -6.54 12.32 o 12 0 0 18.90 31.77 14.32 o 14 0 0 18.88 -39.67 51.22 o 2 1 0 1819.68 1655.41 39.43 o 3 1 0 147.23 135.56 8.43 o 4 1 0 56.79 45.56 7.54 o 5 1 0 370.50 452.37 12.73 o 6 1 0 99.29 103.21 9.25 o 7 1 0 17.28 .00 9.84 o 8 1 0 207.70 206.06 15.21 o 9 1 0 139.10 144.64 15.68 o 10 1 0 92.22 113.34 14.85 o 11 1 0 14.10 4.83 13.97 o 12 1 0 42.02 34.95 15.86 o 13 1 0 43.85 12.14 50.16 o 14 1 0 .50 27.23 46.15 o 15 1 0 1.03 -14.68 42.73 o 1 2 0 160.12 163.80 5.72 o 2 2 0 349.52 333.25 10.08 o 3 2 0 1645.89 1660.30 35.19 o 4 2 0 1012.94 989.55 31.53 o 5 2 0 251.37 248.20 11.08 o 6 2 0 60.19 57.00 8.96 o 7 2 0 262.54 212.66 14.09 o 8 2 0 1.25 19.69 31.18 o 9 2 0 56.28 63.01 14.09 o 10 2 0 159.19 159.38 17.62 o 11 2 0 20.17 9.78 40.26 o 12 2 0 19.31 39.14 15.03 o 13 2 0 .10 -51.81 51.81 o 14 2 0 .14 -6.66 39.31 o 15 2 0 .38 22.75 18.63 o 1 3 0 966.65 966.63 22.69 o 2 3 0 7358.56 6773.11 86.58 o 3 3 0 64.43 52.63 8.02 o 4 3 0 182.64 181.89 9.49 o 5 3 0 209.50 238.53 11.08 o 6 3 0 27.44 49.80 9.31 o 7 3 0 1.06 33.30 9.73 o 8 3 0 265.37 296.12 16.68 o 9 3 0 16.21 32.95 13.91 o 10 3 0 177.71 169.51 18.39 o 11 3 0 63.13 70.02 15.74 o 12 3 0 14.84 7.13 14.97 o 13 3 0 11.61 -47.09 47.09 o 14 3 0 .97 -6.72 51.40 o 15 3 0 2.82 -7.43 53.87 o 0 4 0 33074.00 31220.10 170.28 o 1 4 0 2977.11 2879.90 56.58 o 2 4 0 3497.54 3414.79 67.19 o 3 4 0 53.54 46.98 7.54 o 4 4 0 317.15 303.07 11.55 o 5 4 0 41.84 35.95 8.37 o 6 4 0 240.27 256.22 12.55 o 7 4 0 22.13 -14.56 29.53 o 8 4 0 30.00 10.90 13.73 o 9 4 0 85.52 69.90 15.97 o 10 4 0 10.31 -30.35 36.54 o 11 4 0 23.08 15.15 36.01 o 12 4 0 .98 -27.35 42.67 o 13 4 0 3.83 -6.07 41.79 o 14 4 0 12.52 -51.46 51.46 o 15 4 0 .00 .00 51.69 o 1 5 0 1725.49 1563.46 33.71 o 2 5 0 9.20 -19.80 19.80 o 3 5 0 417.41 377.63 11.73 o 4 5 0 399.66 377.28 12.44 o 5 5 0 160.64 159.26 10.55 o 6 5 0 215.85 209.89 12.26 o 7 5 0 15.22 10.79 11.96 o 8 5 0 571.35 566.18 22.40 o 9 5 0 755.66 777.60 26.35 o 10 5 0 6.30 5.25 14.62 o 11 5 0 .06 5.19 33.83 o 12 5 0 8.49 -11.08 42.26 o 13 5 0 10.08 24.81 15.97 o 14 5 0 .14 3.06 16.80 o 0 6 0 3513.21 3277.57 70.08 o 1 6 0 29.86 28.70 6.66 o 2 6 0 372.12 360.48 10.90 o 3 6 0 447.80 471.70 16.39 o 4 6 0 539.05 519.92 16.21 o 5 6 0 685.98 674.52 20.28 o 6 6 0 299.62 318.63 15.27 o 7 6 0 25.95 .00 35.19 o 8 6 0 16.81 22.40 37.66 o 9 6 0 4.42 20.98 40.90 o 10 6 0 103.11 115.17 15.86 o 11 6 0 .87 -43.91 43.91 o 12 6 0 3.02 .00 43.79 o 13 6 0 .61 -6.31 43.03 o 14 6 0 3.54 1.06 20.63 o 1 7 0 68.71 73.15 7.54 o 2 7 0 265.34 275.19 10.43 o 3 7 0 10.47 .00 19.92 o 4 7 0 228.78 240.48 11.55 o 5 7 0 581.89 573.32 17.45 o 6 7 0 65.88 44.32 13.14 o 7 7 0 131.13 100.43 14.85 o 8 7 0 83.23 74.85 16.03 o 9 7 0 89.28 63.48 17.56 o 10 7 0 235.60 214.13 18.39 o 11 7 0 1.37 -6.66 15.27 o 12 7 0 2.75 -14.97 14.97 o 13 7 0 1.31 6.72 40.85 o 14 7 0 8.35 -44.09 44.09 o 0 8 0 556.80 561.70 16.86 o 1 8 0 135.73 152.42 9.08 o 2 8 0 19.78 17.33 7.43 o 3 8 0 34.48 40.85 8.13 o 4 8 0 165.63 173.58 10.79 o 5 8 0 190.81 242.48 12.20 o 6 8 0 165.42 182.42 15.03 o 7 8 0 13.90 -17.15 38.72 o 8 8 0 253.02 273.78 19.39 o 9 8 0 143.98 149.83 17.45 o 10 8 0 .95 -14.38 34.30 o 11 8 0 3.12 -21.34 42.02 o 12 8 0 .06 1.77 15.56 o 13 8 0 .57 13.79 38.96 o 14 8 0 10.08 -7.19 55.29 o 1 9 0 613.29 621.88 17.56 o 2 9 0 5.73 23.10 7.31 o 3 9 0 26.29 -24.05 24.52 o 4 9 0 154.57 158.26 11.96 o 5 9 0 2.49 -8.78 28.11 o 6 9 0 13.37 -5.13 12.38 o 7 9 0 154.84 142.87 16.33 o 8 9 0 203.04 220.85 18.21 o 9 9 0 59.51 55.11 15.50 o 10 9 0 7.56 9.02 15.50 o 11 9 0 1.49 21.57 14.97 o 12 9 0 6.69 -47.45 47.45 o 13 9 0 3.21 50.51 17.21 o 14 9 0 5.81 23.22 44.50 o 0 10 0 .13 -16.39 20.51 o 1 10 0 144.30 149.59 10.49 o 2 10 0 707.88 744.18 22.40 o 3 10 0 777.34 808.02 23.81 o 4 10 0 1.89 -30.41 30.41 o 5 10 0 81.20 89.88 12.97 o 6 10 0 133.43 143.11 15.97 o 7 10 0 .00 -7.60 34.48 o 8 10 0 .14 -42.32 42.32 o 9 10 0 .06 -23.28 36.37 o 10 10 0 7.73 5.42 48.39 o 11 10 0 5.96 17.98 45.33 o 12 10 0 3.38 .00 40.49 o 13 10 0 2.86 .00 53.16 o 1 11 0 1.25 10.85 17.15 o 2 11 0 2.14 8.49 21.34 o 3 11 0 268.80 269.30 14.85 o 4 11 0 .31 -33.36 33.36 o 5 11 0 31.86 52.10 12.32 o 6 11 0 3.45 -31.53 31.53 o 7 11 0 .23 13.26 14.74 o 8 11 0 1.62 16.56 13.97 o 9 11 0 3.62 -29.18 42.97 o 10 11 0 29.84 16.15 16.74 o 11 11 0 3.09 24.87 15.03 o 12 11 0 .71 -44.21 44.21 o 13 11 0 .59 -14.09 50.87 o 0 12 0 356.12 354.94 15.09 o 1 12 0 .55 -11.61 23.93 o 2 12 0 277.38 274.37 14.79 o 3 12 0 20.24 13.03 29.47 o 4 12 0 156.53 163.32 14.03 o 5 12 0 46.76 67.02 13.91 o 6 12 0 177.72 173.34 17.03 o 7 12 0 27.20 35.66 13.91 o 8 12 0 15.10 24.58 37.72 o 9 12 0 65.06 16.15 50.16 o 10 12 0 3.42 11.79 41.67 o 11 12 0 5.46 .00 33.36 o 12 12 0 .00 -13.32 47.98 o 13 12 0 5.59 -36.31 50.87 o 1 13 0 .60 3.30 28.06 o 2 13 0 600.20 585.58 20.63 o 3 13 0 8.85 3.01 11.73 o 4 13 0 151.02 143.40 14.97 o 5 13 0 2.85 -12.14 13.97 o 6 13 0 30.77 16.09 15.44 o 7 13 0 .58 -43.38 43.38 o 8 13 0 12.74 20.69 39.37 o 9 13 0 .03 -5.30 34.07 o 10 13 0 14.31 24.52 15.74 o 11 13 0 4.00 .00 40.96 o 12 13 0 4.90 -2.95 17.98 o 13 13 0 9.65 .00 51.93 o 0 14 0 24.27 11.14 11.55 o 1 14 0 681.31 651.06 22.40 o 2 14 0 512.02 515.38 20.69 o 3 14 0 189.33 188.02 15.32 o 4 14 0 15.71 23.05 13.85 o 5 14 0 51.51 21.45 40.49 o 6 14 0 18.59 13.85 47.21 o 7 14 0 83.53 73.79 15.62 o 8 14 0 .13 -12.50 13.50 o 9 14 0 2.76 7.60 14.68 o 10 14 0 13.79 25.58 46.15 o 11 14 0 .23 9.96 16.50 o 12 14 0 3.30 -18.98 18.98 o 1 15 0 8.80 -26.41 33.12 o 2 15 0 142.55 134.92 15.27 o 3 15 0 1.55 16.50 37.43 o 4 15 0 11.48 -8.37 34.95 o 5 15 0 1.10 -8.84 33.66 o 6 15 0 53.44 45.80 14.44 o 7 15 0 3.18 12.85 14.09 o 8 15 0 1.47 -10.85 39.08 o 9 15 0 .05 24.70 47.09 o 10 15 0 .11 -37.90 48.92 o 11 15 0 .32 -6.84 46.86 o 12 15 0 7.03 7.84 54.99 o 0 16 0 616.21 636.21 23.58 o 1 16 0 101.35 114.34 14.79 o 2 16 0 16.80 8.61 37.01 o 3 16 0 3.14 4.42 33.01 o 4 16 0 .85 4.01 13.08 o 5 16 0 2.79 -8.07 13.32 o 6 16 0 10.69 -10.02 33.95 o 7 16 0 .21 8.78 14.79 o 8 16 0 .02 4.30 15.44 o 9 16 0 6.34 11.08 16.80 o 10 16 0 .45 8.02 16.92 o 11 16 0 3.79 22.69 54.05 o 1 17 0 .22 -1.24 11.55 o 2 17 0 35.92 3.36 13.38 o 3 17 0 41.24 -4.60 35.54 o 4 17 0 12.38 20.75 13.08 o 5 17 0 30.92 25.52 13.85 o 6 17 0 5.68 5.54 13.91 o 7 17 0 .22 -48.86 48.86 o 8 17 0 4.47 9.96 15.80 o 9 17 0 1.15 27.29 43.20 o 10 17 0 2.01 -1.00 16.92 o 11 17 0 .15 15.80 55.76 o 0 18 0 26.91 20.98 12.97 o 1 18 0 72.73 94.54 14.91 o 2 18 0 67.80 93.36 14.26 o 3 18 0 .32 20.69 11.67 o 4 18 0 1.31 5.36 26.82 o 5 18 0 19.32 35.25 14.20 o 6 18 0 .01 -12.55 12.55 o 7 18 0 6.85 -23.87 39.61 o 8 18 0 2.01 2.89 14.91 o 9 18 0 .64 -6.78 17.03 o 10 18 0 .03 -17.56 18.45 o 1 19 0 3.87 -10.20 29.82 o 2 19 0 81.58 93.19 15.21 o 3 19 0 10.09 13.44 14.44 o 4 19 0 2.54 5.72 37.49 o 5 19 0 30.95 51.16 14.44 o 6 19 0 .93 12.55 35.42 o 7 19 0 32.61 30.41 16.21 o 8 19 0 9.49 15.15 17.56 o 9 19 0 3.64 7.49 18.21 o 0 20 0 9.24 -10.90 31.83 o 1 20 0 12.17 -7.07 13.50 o 2 20 0 41.36 42.85 14.38 o 3 20 0 .64 11.85 13.14 o 4 20 0 .02 -23.40 33.12 o 5 20 0 4.41 25.40 43.03 o 6 20 0 2.71 20.04 34.72 o 7 20 0 22.65 -49.92 49.92 o 8 20 0 5.03 23.34 18.15 o 9 20 0 4.61 -17.03 18.68 o 1 21 0 .03 -23.46 38.90 o 2 21 0 .01 -3.42 13.03 o 3 21 0 10.10 -30.30 39.78 o 4 21 0 7.88 -42.79 42.79 o 5 21 0 15.80 20.33 38.90 o 6 21 0 .18 -54.28 54.28 o 7 21 0 7.93 .00 45.68 o 8 21 0 1.42 -22.22 46.27 o 0 22 0 10.86 -12.50 39.43 o 1 22 0 .32 -42.97 42.97 o 2 22 0 .32 -45.27 45.27 o 3 22 0 .48 -19.39 33.60 o 4 22 0 .30 13.91 35.42 o 5 22 0 .00 14.38 47.68 o 6 22 0 .59 .00 42.73 o 7 22 0 1.21 -7.43 35.66 o 1 23 0 1.12 9.96 14.74 o 2 23 0 1.03 .00 33.07 o 3 23 0 8.31 7.19 40.02 o 4 23 0 5.24 22.10 38.31 o 5 23 0 1.62 -29.06 41.08 o 0 24 0 .19 14.74 41.73 o 1 24 0 4.23 -35.54 52.69 o 2 24 0 4.26 -21.51 51.28 o 3 24 0 7.84 7.60 56.52 o 4 24 0 .44 -14.91 39.55 o -14 0 1 11.90 -13.14 44.56 o -12 0 1 26.39 10.79 35.84 o -10 0 1 526.97 563.94 22.93 o -8 0 1 645.61 601.96 20.39 o -6 0 1 228.75 208.00 10.79 o -4 0 1 1766.93 1589.45 37.49 o -2 0 1 13413.05 11542.00 99.02 o 2 0 1 10273.89 10116.87 96.96 o 4 0 1 1439.26 1232.92 34.24 o 6 0 1 15.36 7.19 24.52 o 8 0 1 .82 -19.63 28.88 o 10 0 1 31.22 4.89 14.68 o 12 0 1 28.83 50.34 13.85 o 14 0 1 8.79 -13.44 45.62 o -15 1 1 1.07 -29.12 37.13 o -14 1 1 8.32 13.56 15.80 o -13 1 1 1.39 -35.48 38.31 o -12 1 1 4.10 -3.01 13.79 o -11 1 1 91.61 9.67 46.27 o -10 1 1 182.89 190.02 16.97 o -9 1 1 62.69 77.04 13.85 o -8 1 1 52.39 43.91 12.50 o -7 1 1 .03 -21.51 21.51 o -6 1 1 637.78 665.32 19.86 o -5 1 1 280.08 284.39 10.55 o -4 1 1 57.52 57.82 6.95 o -3 1 1 1606.46 1425.01 32.59 o -2 1 1 376.11 334.61 11.61 o -1 1 1 18883.08 17492.70 103.74 o 1 1 1 .20 5.13 12.73 o 2 1 1 17030.45 16676.61 125.25 o 3 1 1 333.46 316.98 10.14 o 4 1 1 16.40 12.50 7.13 o 5 1 1 1872.79 1941.98 47.33 o 6 1 1 131.74 162.50 10.96 o 7 1 1 74.13 64.60 11.43 o 8 1 1 22.36 16.97 12.02 o 9 1 1 .00 .53 12.97 o 10 1 1 6.82 -8.55 37.31 o 11 1 1 4.19 -19.33 38.08 o 12 1 1 3.28 11.02 41.32 o 13 1 1 15.03 -13.85 17.03 o 14 1 1 7.02 41.44 16.39 o 15 1 1 11.56 -7.43 44.03 o -15 2 1 2.42 .00 43.85 o -14 2 1 1.13 13.62 15.86 o -13 2 1 1.03 18.33 40.90 o -12 2 1 .14 .00 31.95 o -11 2 1 231.25 183.66 18.09 o -10 2 1 1.32 .00 35.60 o -9 2 1 141.20 129.73 15.38 o -8 2 1 2.30 -37.31 37.31 o -7 2 1 1.02 -29.77 29.77 o -6 2 1 205.54 198.22 10.85 o -5 2 1 40.09 14.09 22.69 o -4 2 1 103.09 81.87 7.78 o -3 2 1 929.44 900.26 27.88 o -2 2 1 790.28 807.60 22.40 o -1 2 1 1794.48 1777.89 37.96 o 0 2 1 1596.85 1592.38 43.09 o 1 2 1 3777.63 3453.57 52.63 o 2 2 1 8203.74 7981.51 93.77 o 3 2 1 1805.09 1798.10 53.87 o 4 2 1 .00 -20.22 20.22 o 5 2 1 3780.24 3814.40 92.36 o 6 2 1 224.82 246.20 12.61 o 7 2 1 1.87 -2.89 31.24 o 8 2 1 205.88 228.69 16.03 o 9 2 1 29.88 23.58 14.20 o 10 2 1 17.50 -4.30 33.12 o 11 2 1 68.78 -4.89 40.96 o 12 2 1 .11 -5.48 37.43 o 13 2 1 18.16 -6.95 16.33 o 14 2 1 .99 .00 16.56 o 15 2 1 40.82 14.26 21.98 o -15 3 1 1.36 5.42 16.80 o -14 3 1 7.28 -39.90 51.51 o -13 3 1 5.84 18.51 38.49 o -12 3 1 12.91 .00 41.55 o -11 3 1 .03 -9.55 36.43 o -10 3 1 66.64 77.74 14.74 o -9 3 1 25.63 3.83 38.96 o -8 3 1 112.85 127.84 13.50 o -7 3 1 225.71 215.78 14.50 o -6 3 1 100.56 98.90 9.78 o -5 3 1 227.07 222.74 10.79 o -4 3 1 170.68 162.15 8.90 o -3 3 1 53.92 7.01 22.81 o -2 3 1 4568.21 4117.65 70.43 o -1 3 1 5954.46 5629.66 73.03 o 0 3 1 1392.32 1367.04 25.77 o 1 3 1 11441.69 10924.89 101.32 o 2 3 1 77.39 70.38 8.37 o 3 3 1 3733.71 3647.48 75.50 o 4 3 1 69.46 57.64 8.25 o 5 3 1 6.38 .83 8.61 o 6 3 1 2696.10 2736.97 62.95 o 7 3 1 80.00 86.70 12.67 o 8 3 1 8.74 -33.18 33.18 o 9 3 1 4.38 -34.66 37.13 o 10 3 1 6.18 37.37 13.44 o 11 3 1 9.81 22.99 13.32 o 12 3 1 6.72 -21.98 36.48 o 13 3 1 11.48 19.75 16.68 o 14 3 1 .52 -20.39 45.62 o -15 4 1 15.11 15.38 54.34 o -14 4 1 5.57 6.95 42.38 o -13 4 1 3.69 -13.85 15.03 o -12 4 1 18.33 -32.59 42.08 o -11 4 1 136.11 156.66 17.45 o -10 4 1 332.64 350.52 20.10 o -9 4 1 610.03 600.90 23.40 o -8 4 1 134.80 107.27 13.73 o -7 4 1 59.94 51.69 11.85 o -6 4 1 72.23 77.45 10.20 o -5 4 1 14.36 29.71 7.66 o -4 4 1 341.33 323.94 10.90 o -3 4 1 3.68 -5.89 6.48 o -2 4 1 1509.49 1461.08 33.66 o -1 4 1 12512.72 12190.87 117.35 o 0 4 1 77.25 77.49 4.81 o 1 4 1 206.60 206.88 8.72 o 2 4 1 2899.19 2753.88 62.95 o 3 4 1 45.57 40.79 8.37 o 4 4 1 .01 -24.17 24.17 o 5 4 1 35.86 25.70 9.43 o 6 4 1 463.66 486.50 16.27 o 7 4 1 287.68 313.80 16.80 o 8 4 1 14.83 11.14 13.20 o 9 4 1 5.51 24.11 38.13 o 10 4 1 43.26 44.68 15.50 o 11 4 1 2.78 -44.56 44.56 o 12 4 1 1.39 -41.32 41.32 o 13 4 1 1.45 6.42 50.04 o 14 4 1 2.48 .00 44.50 o -15 5 1 .25 -14.97 57.11 o -14 5 1 2.23 -46.62 46.62 o -13 5 1 8.29 -30.71 34.19 o -12 5 1 3.42 -27.58 40.90 o -11 5 1 113.47 124.84 18.09 o -10 5 1 101.47 4.54 43.44 o -9 5 1 52.44 75.74 16.27 o -8 5 1 10.93 -6.90 29.94 o -7 5 1 46.52 15.68 30.59 o -6 5 1 67.76 75.86 10.49 o -5 5 1 202.53 223.09 11.73 o -4 5 1 93.04 81.93 9.02 o -3 5 1 188.02 170.28 9.14 o -2 5 1 1562.27 1501.69 36.48 o -1 5 1 12446.17 12216.51 128.67 o 0 5 1 14347.54 13829.61 194.77 o 1 5 1 2618.06 2603.47 61.30 o 2 5 1 .82 -1.41 18.98 o 3 5 1 .72 4.18 7.13 o 4 5 1 496.54 491.74 16.09 o 5 5 1 22.68 .00 21.28 o 6 5 1 3.36 11.32 30.71 o 7 5 1 133.12 142.34 14.44 o 8 5 1 84.44 101.79 15.62 o 9 5 1 .01 12.44 38.67 o 10 5 1 35.63 51.63 14.32 o 11 5 1 .63 -2.89 14.68 o 12 5 1 7.56 5.84 43.32 o 13 5 1 26.61 33.54 18.39 o 14 5 1 9.76 -13.91 52.93 o -14 6 1 11.38 -6.90 50.22 o -13 6 1 1.57 19.57 43.79 o 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