#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200032.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200032_Fobs loop_ _publ_author_name 'Lynch, Daniel E.' 'McClenaghan, Ian' _publ_section_title ; 7,8,9,10-Tetrahydro-11H-pyrido[2,3-a]carbazol-1-ium chloride ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o43 _journal_page_last o44 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.933 _cell_angle_gamma 90.000 _cell_length_a 15.9111 _cell_length_b 5.0374 _cell_length_c 17.1233 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file cf6018Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '11H-Pyridinium[2,3h]-7,8,9,10-tetrahydrocarbazole chloride' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 731.71 682.43 25.73 o 4 0 0 4682.51 4676.95 124.45 o 5 0 0 6920.88 6696.57 169.81 o 6 0 0 1089.44 1015.34 31.61 o 7 0 0 37.12 40.89 12.77 o 8 0 0 606.05 570.80 25.40 o 9 0 0 1587.50 1661.80 74.58 o 10 0 0 71.30 72.31 14.24 o 11 0 0 261.65 302.03 27.19 o 12 0 0 0.09 1.89 14.26 o 13 0 0 349.89 292.70 32.59 o 14 0 0 478.94 489.21 43.16 o 15 0 0 1.06 -2.75 28.54 o 16 0 0 852.60 809.03 103.31 o 17 0 0 1701.56 1916.33 199.80 o 18 0 0 163.73 203.47 63.76 o 1 1 0 4.51 3.23 1.88 o 2 1 0 402.13 382.63 8.10 o 3 1 0 27859.01 25341.21 436.61 o 4 1 0 2642.50 2628.05 51.89 o 5 1 0 126.31 98.66 5.83 o 6 1 0 1613.62 1643.27 38.59 o 7 1 0 28.02 19.50 6.53 o 8 1 0 257.99 240.11 12.59 o 9 1 0 197.43 202.92 14.77 o 10 1 0 114.29 110.59 12.67 o 11 1 0 281.25 275.54 17.75 o 12 1 0 0.19 -6.10 11.92 o 13 1 0 187.58 194.12 19.39 o 14 1 0 323.94 345.68 27.38 o 15 1 0 320.62 305.95 34.33 o 16 1 0 2.10 3.75 24.74 o 17 1 0 49.04 35.91 29.90 o 18 1 0 1.98 17.27 39.28 o 0 2 0 72.99 57.48 13.75 o 1 2 0 32.39 30.13 1.63 o 2 2 0 1070.75 1121.76 30.19 o 3 2 0 1455.05 1565.13 28.35 o 4 2 0 2336.20 2389.23 49.34 o 5 2 0 3816.64 4106.14 71.73 o 6 2 0 1809.59 1961.07 39.11 o 7 2 0 890.15 903.72 24.09 o 8 2 0 116.60 106.47 9.32 o 9 2 0 455.36 469.67 18.85 o 10 2 0 196.83 183.75 13.70 o 11 2 0 219.27 225.03 15.92 o 12 2 0 817.63 852.92 34.93 o 13 2 0 9.96 4.35 14.02 o 14 2 0 12.94 4.22 16.89 o 15 2 0 29.50 43.32 21.83 o 16 2 0 13.01 -8.93 30.38 o 17 2 0 3.00 -21.05 28.83 o 1 3 0 1070.14 983.38 41.79 o 2 3 0 370.37 375.01 13.94 o 3 3 0 117.65 64.15 21.14 o 4 3 0 462.33 496.59 14.56 o 5 3 0 917.27 994.39 28.40 o 6 3 0 256.58 248.62 11.30 o 7 3 0 303.20 303.59 13.52 o 8 3 0 496.03 473.64 20.30 o 9 3 0 122.13 107.37 10.39 o 10 3 0 301.53 317.21 17.66 o 11 3 0 157.22 172.51 17.24 o 12 3 0 396.09 359.71 24.55 o 13 3 0 10.23 1.87 13.44 o 14 3 0 104.79 90.19 39.79 o 15 3 0 76.44 50.43 28.18 o 16 3 0 93.44 99.74 35.24 o 0 4 0 149.89 113.26 24.88 o 1 4 0 373.78 401.26 28.28 o 2 4 0 55.23 60.45 16.50 o 3 4 0 359.21 356.66 42.55 o 4 4 0 310.64 320.51 13.65 o 5 4 0 4.78 1.51 5.28 o 6 4 0 130.67 146.68 8.68 o 7 4 0 160.82 155.31 11.25 o 8 4 0 333.92 339.54 17.95 o 9 4 0 106.80 122.41 13.53 o 10 4 0 35.38 25.18 10.77 o 11 4 0 178.88 149.27 27.78 o 12 4 0 24.76 11.65 17.80 o 13 4 0 252.48 242.69 34.04 o 14 4 0 72.19 55.25 35.09 o 1 5 0 31.24 9.35 41.37 o 2 5 0 16.18 2.25 35.74 o 3 5 0 249.33 250.05 32.55 o 4 5 0 33.54 7.15 23.11 o 5 5 0 36.35 51.86 22.48 o 6 5 0 40.84 28.38 6.68 o 7 5 0 62.88 58.16 7.71 o 8 5 0 2.75 7.33 9.03 o 9 5 0 7.82 10.21 13.42 o 10 5 0 1.45 0.00 17.55 o 11 5 0 15.49 0.00 20.29 o 12 5 0 24.54 31.16 36.53 o 0 6 0 292.86 301.01 52.24 o 1 6 0 7.56 -22.83 36.56 o 2 6 0 19.87 22.04 38.81 o 3 6 0 0.07 -7.52 33.41 o 4 6 0 62.40 117.80 36.57 o 5 6 0 0.78 35.61 45.17 o 6 6 0 8.26 19.12 35.48 o 7 6 0 5.94 85.50 46.22 o -19 1 1 264.96 124.52 63.63 o -18 1 1 19.57 31.02 35.26 o -17 1 1 23.43 32.69 30.61 o -16 1 1 67.37 84.27 26.64 o -15 1 1 1006.91 1089.90 70.06 o -14 1 1 435.82 448.86 27.90 o -13 1 1 22.97 32.85 15.29 o -12 1 1 48.80 40.04 12.62 o -11 1 1 451.50 461.67 20.24 o -10 1 1 221.69 233.96 13.66 o -9 1 1 203.32 201.88 13.42 o -8 1 1 13.07 25.69 8.04 o -7 1 1 1520.25 1580.31 36.00 o -6 1 1 1088.52 1042.14 27.27 o -5 1 1 743.22 706.29 17.32 o -4 1 1 0.74 -4.06 2.90 o -3 1 1 19689.12 18040.98 321.14 o -2 1 1 1013.10 1004.68 20.24 o -1 1 1 1099.63 982.13 24.57 o 0 1 1 319.85 331.55 9.33 o 1 1 1 1401.25 1292.48 24.72 o 2 1 1 22555.71 20544.88 350.83 o 3 1 1 3.89 -1.68 2.60 o 4 1 1 4487.01 4570.81 89.45 o 5 1 1 866.95 959.15 22.97 o 6 1 1 838.85 852.66 21.40 o 7 1 1 1827.26 1840.66 50.17 o 8 1 1 6.95 17.15 7.60 o 9 1 1 106.46 101.91 9.85 o 10 1 1 0.62 -4.29 7.67 o 11 1 1 854.48 893.74 38.09 o 12 1 1 141.38 124.74 17.86 o 13 1 1 73.23 59.90 15.49 o 14 1 1 31.68 39.70 21.07 o 15 1 1 35.16 66.87 22.40 o 16 1 1 14.92 -2.68 28.79 o 17 1 1 31.32 -6.45 48.24 o 18 1 1 40.41 2.15 38.78 o -18 2 1 0.12 -4.03 38.19 o -17 2 1 337.69 435.28 55.86 o -16 2 1 327.45 285.42 51.36 o -15 2 1 118.26 123.77 26.21 o -14 2 1 27.30 38.50 17.36 o -13 2 1 4.39 32.72 12.77 o -12 2 1 1310.20 1384.78 49.75 o -11 2 1 1321.11 1309.32 44.52 o -10 2 1 121.98 112.23 11.26 o -9 2 1 579.64 601.39 22.04 o -8 2 1 825.45 842.11 21.57 o -7 2 1 14.74 7.01 5.32 o -6 2 1 1589.92 1746.01 34.36 o -5 2 1 688.94 804.17 19.24 o -4 2 1 473.51 433.32 11.09 o -3 2 1 1777.04 1724.67 33.53 o -2 2 1 12.74 5.81 8.91 o -1 2 1 389.81 363.08 14.20 o 0 2 1 4614.63 4333.43 187.55 o 1 2 1 1117.37 458.23 370.06 o 2 2 1 1223.53 1198.72 24.51 o 3 2 1 659.12 709.10 16.82 o 4 2 1 919.62 953.39 19.49 o 5 2 1 7773.70 8067.23 162.55 o 6 2 1 2571.91 2687.98 60.02 o 7 2 1 1092.47 1191.10 28.75 o 8 2 1 876.64 900.20 25.25 o 9 2 1 204.59 212.33 14.25 o 10 2 1 359.85 342.05 18.79 o 11 2 1 74.77 58.86 11.98 o 12 2 1 142.51 122.54 14.58 o 13 2 1 27.00 47.81 15.54 o 14 2 1 502.67 435.84 42.45 o 15 2 1 51.33 57.16 26.64 o 16 2 1 11.11 28.36 31.52 o 17 2 1 1.87 -37.69 35.53 o -17 3 1 3.27 -22.97 30.44 o -16 3 1 27.97 -4.88 24.24 o -15 3 1 0.20 12.63 47.86 o -14 3 1 167.73 181.22 25.97 o -13 3 1 48.61 53.65 17.62 o -12 3 1 50.52 40.47 13.78 o -11 3 1 0.58 -4.38 8.83 o -10 3 1 359.31 312.41 16.60 o -9 3 1 2.96 -10.12 6.75 o -8 3 1 2357.22 2561.57 73.44 o -7 3 1 193.55 221.89 11.49 o -6 3 1 571.30 606.27 18.71 o -5 3 1 82.64 92.32 7.06 o -4 3 1 15.54 16.88 6.02 o -3 3 1 656.32 663.26 19.43 o -2 3 1 54.88 82.88 15.19 o -1 3 1 842.26 758.36 45.70 o 0 3 1 332.95 345.46 19.93 o 1 3 1 75.57 66.25 11.89 o 2 3 1 0.08 0.65 2.40 o 3 3 1 1788.53 1719.47 234.65 o 4 3 1 150.96 144.17 6.91 o 5 3 1 51.25 59.00 5.68 o 6 3 1 5.61 5.71 5.11 o 7 3 1 125.26 135.42 10.51 o 8 3 1 2859.73 3096.10 76.93 o 9 3 1 1959.27 2061.03 69.01 o 10 3 1 266.77 245.20 17.12 o 11 3 1 554.79 498.50 26.97 o 12 3 1 13.37 16.50 15.37 o 13 3 1 199.40 186.51 24.90 o 14 3 1 0.02 18.47 33.58 o 15 3 1 5.29 9.47 28.51 o 16 3 1 0.05 24.59 30.29 o -15 4 1 131.27 145.47 47.14 o -14 4 1 17.26 1.31 31.03 o -13 4 1 7.68 1.59 17.57 o -12 4 1 50.00 10.71 17.45 o -11 4 1 64.19 42.60 12.52 o -10 4 1 93.73 104.46 14.94 o -9 4 1 0.29 5.66 8.25 o -8 4 1 57.13 65.75 8.76 o -7 4 1 500.55 477.78 19.93 o -6 4 1 488.33 517.12 20.88 o -5 4 1 622.74 650.19 24.94 o -4 4 1 559.82 562.40 22.95 o -3 4 1 712.40 575.32 52.11 o -2 4 1 33.98 35.09 27.23 o -1 4 1 115.16 103.33 19.43 o 0 4 1 389.58 383.59 29.90 o 1 4 1 820.92 837.76 60.95 o 2 4 1 6.56 45.64 17.83 o 3 4 1 3.86 3.48 7.23 o 4 4 1 7.78 5.23 10.77 o 5 4 1 25.77 22.44 4.88 o 6 4 1 30.11 23.86 6.42 o 7 4 1 8.52 4.05 6.97 o 8 4 1 40.93 25.29 9.35 o 9 4 1 41.64 41.35 13.63 o 10 4 1 344.28 350.28 21.19 o 11 4 1 42.41 16.41 15.15 o 12 4 1 742.55 661.69 64.31 o 13 4 1 74.21 87.09 27.50 o 14 4 1 0.01 -14.80 33.78 o -12 5 1 17.16 45.96 33.78 o -11 5 1 177.33 164.84 29.72 o -10 5 1 116.46 114.70 31.03 o -9 5 1 138.70 132.24 21.60 o -8 5 1 0.21 -9.28 6.19 o -7 5 1 356.88 334.94 24.57 o -4 5 1 41.35 44.29 24.36 o -3 5 1 631.49 560.44 40.61 o -2 5 1 760.39 788.08 52.38 o -1 5 1 399.05 388.29 37.27 o 0 5 1 318.80 272.95 39.45 o 1 5 1 39.04 33.30 25.53 o 2 5 1 23.36 26.12 18.84 o 3 5 1 4.50 52.46 19.50 o 4 5 1 565.04 520.55 56.63 o 5 5 1 3.43 17.00 23.35 o 6 5 1 93.73 75.28 8.48 o 7 5 1 48.72 61.17 11.73 o 8 5 1 64.18 63.63 14.83 o 9 5 1 1.17 -10.87 20.29 o 10 5 1 216.88 206.09 39.28 o 11 5 1 1.01 -30.44 20.29 o -7 6 1 21.39 -13.62 35.22 o -6 6 1 51.01 83.01 43.60 o -5 6 1 42.90 27.36 43.73 o -4 6 1 102.11 103.24 38.86 o -3 6 1 96.32 114.43 34.93 o -2 6 1 6.90 -25.12 29.26 o -1 6 1 1.74 34.95 32.42 o 0 6 1 68.52 72.25 33.98 o 1 6 1 172.27 186.52 36.75 o 2 6 1 30.81 20.72 68.41 o 3 6 1 51.37 30.68 30.41 o 4 6 1 86.56 91.43 39.88 o 5 6 1 36.78 36.92 39.67 o 6 6 1 1.12 -29.98 42.29 o 7 6 1 19.71 102.00 57.09 o -19 0 2 19.14 2.75 46.09 o -18 0 2 617.58 641.05 78.69 o -17 0 2 404.69 508.41 85.50 o -16 0 2 67.05 71.88 37.97 o -15 0 2 313.33 326.66 41.13 o -14 0 2 197.25 169.37 27.30 o -13 0 2 115.91 100.88 22.90 o -12 0 2 449.93 446.55 34.44 o -11 0 2 1622.86 1764.38 77.61 o -10 0 2 478.54 522.94 28.12 o -9 0 2 386.52 362.92 20.81 o -8 0 2 2475.09 2467.08 75.37 o -7 0 2 1409.11 1390.20 48.41 o -6 0 2 227.97 218.39 13.42 o -5 0 2 1030.07 981.48 37.79 o -4 0 2 2384.36 2271.99 71.75 o -3 0 2 549.35 455.46 38.56 o -2 0 2 315.86 329.03 11.92 o 1 0 2 14756.33 12623.47 378.86 o 2 0 2 3494.56 3613.84 107.36 o 3 0 2 292.62 304.88 14.30 o 4 0 2 950.72 1035.38 34.13 o 5 0 2 1547.79 1459.54 51.42 o 6 0 2 1122.02 1090.11 37.03 o 7 0 2 1655.68 1687.26 48.46 o 8 0 2 1546.73 1619.33 68.15 o 9 0 2 1247.07 1326.58 86.09 o 10 0 2 237.70 223.10 22.48 o 11 0 2 378.67 369.58 33.58 o 12 0 2 272.96 258.46 27.03 o 13 0 2 285.64 297.67 38.10 o 14 0 2 326.58 328.64 53.03 o 15 0 2 8.18 21.73 33.91 o 16 0 2 100.28 65.20 48.84 o 17 0 2 394.81 382.98 78.82 o 18 0 2 3.95 85.50 82.88 o -19 1 2 2.83 33.42 38.03 o -18 1 2 315.12 265.46 47.98 o -17 1 2 0.51 -40.27 35.11 o -16 1 2 18.94 -6.36 30.23 o -15 1 2 555.78 562.19 39.26 o -14 1 2 1365.97 1490.09 61.53 o -13 1 2 12.28 11.21 11.58 o -12 1 2 14.20 15.91 11.56 o -11 1 2 511.80 509.65 24.16 o -10 1 2 295.00 264.67 14.70 o -9 1 2 216.34 197.86 12.07 o -8 1 2 774.95 833.87 24.41 o -7 1 2 71.36 80.02 8.07 o -6 1 2 72.47 60.87 6.08 o -5 1 2 998.84 948.93 21.03 o -4 1 2 966.27 951.00 24.60 o -3 1 2 31.01 36.28 3.48 o -2 1 2 3062.16 2790.74 55.57 o -1 1 2 4999.51 4451.79 85.00 o 0 1 2 82.02 72.67 2.59 o 1 1 2 75.15 66.09 3.52 o 2 1 2 8111.48 7707.76 153.51 o 3 1 2 1443.16 1402.37 30.06 o 4 1 2 771.69 836.80 18.55 o 5 1 2 1228.53 1313.73 28.87 o 6 1 2 30.69 22.78 5.17 o 7 1 2 256.85 242.96 13.00 o 8 1 2 487.42 503.80 18.74 o 9 1 2 205.89 218.84 15.24 o 10 1 2 15.57 10.26 10.84 o 11 1 2 308.29 310.43 21.48 o 12 1 2 221.39 186.52 25.17 o 13 1 2 252.96 267.47 23.02 o 14 1 2 136.92 147.28 28.94 o 15 1 2 1.59 -27.03 23.84 o 16 1 2 223.47 233.75 51.59 o 17 1 2 90.84 82.29 39.69 o -18 2 2 5.29 -2.39 39.66 o -17 2 2 68.53 31.69 28.47 o -16 2 2 18.37 11.59 23.41 o -15 2 2 0.11 -19.18 19.00 o -14 2 2 6.40 27.30 18.70 o -13 2 2 425.96 394.96 31.13 o -12 2 2 65.14 60.72 13.68 o -11 2 2 670.44 676.69 25.09 o -10 2 2 33.78 28.69 7.88 o -9 2 2 6.51 8.47 6.71 o -8 2 2 37.55 42.68 7.09 o -7 2 2 166.10 172.70 9.50 o -6 2 2 34.76 43.40 5.12 o -5 2 2 1094.77 1178.42 33.14 o -4 2 2 14.79 23.03 3.69 o -3 2 2 55.77 59.27 3.97 o -2 2 2 2.10 -2.36 2.09 o -1 2 2 57.97 56.46 3.87 o 0 2 2 18.76 13.71 4.63 o 1 2 2 428.76 435.53 11.18 o 2 2 2 625.80 634.20 15.60 o 3 2 2 16.13 19.27 3.72 o 4 2 2 1168.37 1294.45 26.89 o 5 2 2 1980.99 2107.82 48.03 o 6 2 2 915.95 981.25 25.60 o 7 2 2 816.30 885.82 25.71 o 8 2 2 482.95 466.73 18.17 o 9 2 2 157.34 166.57 12.53 o 10 2 2 200.72 203.06 14.44 o 11 2 2 13.28 8.96 10.05 o 12 2 2 58.57 30.27 13.00 o 13 2 2 0.55 -5.10 13.80 o 14 2 2 3.56 -14.72 22.60 o 15 2 2 18.39 10.37 35.14 o 16 2 2 3.37 -0.95 72.27 o 17 2 2 0.65 -21.60 71.36 o -17 3 2 13.81 -18.73 32.02 o -16 3 2 8.40 20.75 25.16 o -15 3 2 85.65 54.81 23.74 o -14 3 2 180.67 171.67 22.31 o -13 3 2 34.88 46.10 19.48 o -12 3 2 0.52 -8.28 12.38 o -11 3 2 1.85 6.59 9.55 o -10 3 2 1273.87 1304.82 44.79 o -9 3 2 593.81 595.18 25.29 o -8 3 2 363.29 353.61 14.89 o -7 3 2 135.97 142.83 9.43 o -6 3 2 391.54 413.02 17.24 o -5 3 2 462.12 440.95 12.76 o -4 3 2 116.33 96.74 6.76 o -3 3 2 8.68 9.33 2.36 o -2 3 2 1525.25 1603.89 56.53 o -1 3 2 1173.07 1147.27 63.06 o 0 3 2 85.66 73.66 3.66 o 1 3 2 127.60 143.51 6.13 o 2 3 2 0.11 -0.70 2.43 o 3 3 2 362.31 354.47 10.76 o 4 3 2 370.00 366.27 13.59 o 5 3 2 123.69 106.70 10.68 o 6 3 2 95.67 86.96 10.11 o 7 3 2 748.55 742.89 26.36 o 8 3 2 11.46 21.25 9.27 o 9 3 2 207.34 187.58 14.54 o 10 3 2 23.65 28.96 13.55 o 11 3 2 15.40 23.30 11.77 o 12 3 2 232.73 219.46 25.36 o 13 3 2 31.75 26.91 17.73 o 14 3 2 2.05 -36.36 24.24 o 15 3 2 11.54 -10.65 28.34 o -15 4 2 71.85 12.18 33.65 o -14 4 2 0.15 6.55 23.07 o -13 4 2 51.76 30.04 19.42 o -12 4 2 210.23 216.61 32.54 o -11 4 2 367.76 368.67 24.54 o -10 4 2 30.93 35.85 11.41 o -9 4 2 44.13 51.55 9.90 o -8 4 2 121.60 139.15 9.75 o -7 4 2 1118.04 1212.24 37.82 o -6 4 2 644.73 602.42 111.95 o -5 4 2 213.22 216.92 8.65 o -4 4 2 565.80 542.10 33.69 o -3 4 2 244.66 200.98 34.17 o -2 4 2 127.94 137.49 21.29 o -1 4 2 83.50 107.23 17.84 o 0 4 2 70.01 68.39 17.94 o 1 4 2 580.57 535.82 32.72 o 2 4 2 351.78 319.82 29.66 o 3 4 2 0.96 5.76 5.71 o 4 4 2 3.07 0.60 3.85 o 5 4 2 189.94 194.37 11.39 o 6 4 2 689.67 734.77 29.28 o 7 4 2 26.45 36.16 8.92 o 8 4 2 19.45 11.15 7.89 o 9 4 2 60.61 72.08 11.42 o 10 4 2 887.93 915.80 75.91 o 11 4 2 198.32 210.41 26.49 o 12 4 2 345.09 318.78 36.03 o 13 4 2 39.88 -28.41 28.41 o 14 4 2 0.72 4.06 29.72 o -12 5 2 13.53 14.80 21.60 o -11 5 2 78.03 97.02 31.03 o -10 5 2 2.90 1.31 16.10 o -9 5 2 2.75 1.81 9.35 o -8 5 2 185.11 179.95 22.19 o -7 5 2 48.87 34.06 4.85 o -4 5 2 182.97 172.69 30.11 o -3 5 2 327.45 295.36 38.27 o -2 5 2 20.36 6.22 19.38 o -1 5 2 131.29 164.42 35.46 o 0 5 2 48.07 42.04 19.01 o 1 5 2 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399.93 389.09 12.91 o -5 1 3 677.90 651.44 20.39 o -4 1 3 1567.42 1500.42 40.83 o -3 1 3 364.98 364.70 10.96 o -2 1 3 4.31 6.71 2.21 o -1 1 3 230.50 233.45 6.00 o 0 1 3 1000.85 989.50 23.57 o 1 1 3 3724.60 3530.31 67.74 o 2 1 3 106.04 110.91 4.49 o 3 1 3 269.16 269.31 7.82 o 4 1 3 1634.34 1709.98 36.61 o 5 1 3 30.31 22.46 4.93 o 6 1 3 5.78 6.92 4.87 o 7 1 3 6.38 4.03 6.22 o 8 1 3 95.96 83.64 9.45 o 9 1 3 458.54 430.35 19.07 o 10 1 3 0.12 -3.24 8.48 o 11 1 3 209.94 188.56 20.94 o 12 1 3 0.08 0.15 12.35 o 13 1 3 55.52 34.17 14.99 o 14 1 3 197.47 177.71 23.66 o 15 1 3 7.63 -3.82 22.38 o 16 1 3 89.65 61.13 37.43 o 17 1 3 56.95 89.29 41.89 o -18 2 3 0.16 -53.01 36.65 o -17 2 3 166.98 201.28 48.51 o -16 2 3 155.41 180.24 30.05 o -15 2 3 33.03 51.77 23.04 o -14 2 3 136.02 104.51 21.12 o -13 2 3 68.29 70.35 12.86 o -12 2 3 341.60 342.70 30.29 o -11 2 3 37.79 56.08 10.35 o -10 2 3 186.47 171.30 12.51 o -9 2 3 10.05 6.85 7.56 o -8 2 3 866.51 888.32 25.19 o -7 2 3 942.98 936.52 25.55 o -6 2 3 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