#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200062.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200062_Fobs loop_ _publ_author_name 'Virovets, Alexander V.' 'Samsonenko, Denis G.' 'Sokolov, Maxim N.' 'Fedin, Vladimir P.' _publ_section_title ; Supramolecular adduct of tetrachlorogallate with cucurbituril: (H~7~O~3~)~4~[GaCl~4~]~2~Cl~2~·C~36~H~36~N~24~O~12~·2H~2~O ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m33 _journal_page_last m34 _journal_volume 57 _journal_year 2001 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.5665 _cell_length_b 16.7800 _cell_length_c 25.0342 _exptl_crystal_F_000 3568.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file na6021Isup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title NA6021 _shelx_refln_list_code 4 _shelx_f_calc_maximum 633.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2864.54 17525.14 394.88 o 4 0 0 401825.88 452408.16 2784.26 o 6 0 0 145067.23 151320.27 2010.15 o 8 0 0 167064.14 153553.20 2354.37 o 10 0 0 71575.01 62725.28 1792.60 o 12 0 0 39344.54 36060.57 1525.87 o 14 0 0 9351.22 9917.40 403.07 o 16 0 0 33243.25 33057.26 1206.24 o 18 0 0 3899.82 3944.31 136.34 o 20 0 0 13458.39 12256.87 569.22 o 0 2 0 138697.66 200098.16 1227.10 o 2 2 0 3839.96 14170.17 439.58 o 4 2 0 255230.22 272047.94 2261.98 o 6 2 0 2685.82 2303.70 58.11 o 8 2 0 14287.18 14401.88 543.89 o 10 2 0 49860.82 47805.59 1503.52 o 12 2 0 6541.93 6869.39 192.97 o 14 2 0 9730.23 9152.23 379.98 o 16 2 0 1212.75 1116.09 87.92 o 18 2 0 2715.22 3084.52 142.31 o 20 2 0 2400.38 2312.64 129.64 o 0 4 0 74172.63 75877.70 1116.09 o 2 4 0 110253.69 115074.20 1478.93 o 4 4 0 3900.04 4156.65 202.65 o 6 4 0 104883.74 104937.74 1803.03 o 8 4 0 105823.76 100708.08 2070.50 o 10 4 0 7600.90 7691.93 295.04 o 12 4 0 15495.21 16677.27 607.96 o 14 4 0 29213.03 29730.60 1040.09 o 16 4 0 3926.82 3647.03 139.32 o 18 4 0 2986.01 2945.19 126.66 o 20 4 0 343.48 309.20 89.41 o 0 6 0 55.28 141.56 33.53 o 2 6 0 15277.56 14059.90 668.31 o 4 6 0 34803.59 29062.29 989.43 o 6 6 0 50965.80 50136.86 1421.56 o 8 6 0 8116.10 10152.09 396.37 o 10 6 0 831.77 1080.33 70.03 o 12 6 0 4319.18 4658.82 175.09 o 14 6 0 7978.66 7799.96 332.29 o 16 6 0 4193.23 4146.97 134.11 o 18 6 0 54.89 55.88 78.23 o 20 6 0 587.42 628.08 95.37 o 0 8 0 8716.41 10855.42 391.90 o 2 8 0 16111.26 13607.65 488.75 o 4 8 0 4360.32 4239.35 158.70 o 6 8 0 64986.99 63728.11 1794.09 o 8 8 0 49.08 129.64 49.17 o 10 8 0 12013.56 12072.84 435.86 o 12 8 0 50.52 90.15 61.84 o 14 8 0 200.52 253.32 77.49 o 16 8 0 591.57 790.50 90.90 o 18 8 0 9.36 189.99 78.23 o 20 8 0 458.92 386.68 92.39 o 0 10 0 42696.86 35955.52 1343.33 o 2 10 0 1320.20 941.75 60.35 o 4 10 0 673.38 527.50 57.37 o 6 10 0 3277.55 3741.66 99.84 o 8 10 0 24841.01 26342.10 892.57 o 10 10 0 1233.16 1289.69 83.45 o 12 10 0 10810.12 10605.83 459.70 o 14 10 0 1268.83 1177.93 98.35 o 16 10 0 273.94 190.73 85.68 o 18 10 0 7.01 46.19 82.70 o 0 12 0 9830.92 11140.78 505.89 o 2 12 0 645.10 649.69 64.07 o 4 12 0 1088.06 1056.49 71.53 o 6 12 0 3262.86 2934.02 101.33 o 8 12 0 1459.75 1660.72 89.41 o 10 12 0 1407.03 1487.13 91.64 o 12 12 0 29.74 38.74 71.53 o 14 12 0 394.35 369.55 82.70 o 16 12 0 155.86 330.06 90.15 o 0 14 0 125.62 219.79 67.05 o 2 14 0 74.92 61.09 60.35 o 4 14 0 6635.31 7060.12 257.79 o 6 14 0 3048.96 2963.82 123.68 o 8 14 0 114.25 20.86 67.80 o 10 14 0 632.31 579.65 81.96 o 12 14 0 1381.12 1367.92 107.29 o 14 14 0 186.63 83.45 83.45 o 16 14 0 18.11 -23.10 89.41 o 0 16 0 6416.56 6445.45 184.03 o 2 16 0 832.71 631.06 83.45 o 4 16 0 1197.55 1056.49 90.15 o 6 16 0 457.03 447.03 79.72 o 8 16 0 4128.76 3857.14 203.40 o 10 16 0 1026.55 837.44 100.58 o 12 16 0 4.30 -100.58 100.58 o 14 16 0 6.37 110.27 91.64 o 0 18 0 4923.91 4622.31 265.98 o 2 18 0 58.54 25.33 74.51 o 4 18 0 2722.84 2849.83 128.15 o 6 18 0 78.23 -7.45 75.25 o 8 18 0 1790.99 1611.55 114.74 o 10 18 0 375.32 347.94 94.62 o 12 18 0 973.20 1080.33 119.21 o 0 20 0 655.10 692.90 98.35 o 2 20 0 2144.92 2194.18 129.64 o 4 20 0 11.25 -70.03 79.72 o 6 20 0 327.17 213.09 93.88 o 8 20 0 1041.58 1144.40 113.99 o 1 1 1 12992.16 1226.36 37.25 o 3 1 1 106714.77 77355.88 1057.23 o 5 1 1 641.31 247.36 32.04 o 7 1 1 28413.37 28397.70 960.37 o 9 1 1 81738.68 88062.29 1890.20 o 11 1 1 1089.09 885.87 64.07 o 13 1 1 8870.70 9658.87 330.06 o 15 1 1 18.68 -19.37 61.84 o 17 1 1 1597.15 1603.35 100.58 o 19 1 1 2002.12 1752.36 119.95 o 21 1 1 4.33 49.92 81.21 o 0 2 1 20944.38 17668.93 395.62 o 2 2 1 6681.88 7428.18 349.43 o 4 2 1 43554.61 44887.96 949.20 o 6 2 1 13974.69 15157.36 488.01 o 8 2 1 17227.17 18148.00 609.45 o 10 2 1 47035.07 47027.01 1583.24 o 12 2 1 34.72 46.94 54.39 o 14 2 1 187.04 259.28 61.84 o 16 2 1 664.27 730.90 83.45 o 18 2 1 1733.80 1721.82 105.05 o 20 2 1 1.48 103.56 81.96 o 1 3 1 73082.79 58745.95 881.40 o 3 3 1 894.12 2343.19 65.56 o 5 3 1 76618.27 81122.87 1468.50 o 7 3 1 5285.39 5726.48 204.89 o 9 3 1 800.55 1034.13 58.86 o 11 3 1 12095.26 13445.23 498.44 o 13 3 1 5424.28 5818.86 254.81 o 15 3 1 2049.86 2256.77 102.07 o 17 3 1 2790.33 2776.81 120.70 o 19 3 1 525.27 586.36 92.39 o 21 3 1 589.48 546.87 95.37 o 0 4 1 122934.76 127246.88 1438.70 o 2 4 1 26.26 12.67 25.33 o 4 4 1 1489.31 1560.89 48.43 o 6 4 1 1175.48 1192.83 50.66 o 8 4 1 19421.65 18156.94 625.84 o 10 4 1 8437.37 9358.61 409.78 o 12 4 1 4010.29 3398.19 169.87 o 14 4 1 330.07 327.82 69.29 o 16 4 1 1273.80 1302.35 94.62 o 18 4 1 504.82 482.79 92.39 o 20 4 1 1629.02 1431.25 115.48 o 1 5 1 48.09 76.00 30.55 o 3 5 1 86281.51 87782.15 1515.44 o 5 5 1 9346.45 8592.70 320.37 o 7 5 1 12634.67 14592.61 514.83 o 9 5 1 15792.13 15500.83 635.53 o 11 5 1 2673.97 2768.62 119.95 o 13 5 1 1595.45 1292.67 84.94 o 15 5 1 532.71 482.05 77.49 o 17 5 1 2739.16 2404.29 117.72 o 19 5 1 105.20 188.50 80.47 o 0 6 1 1862.94 1822.40 77.49 o 2 6 1 76357.74 74108.20 1404.43 o 4 6 1 40047.30 39528.79 1223.38 o 6 6 1 20259.79 18780.55 929.83 o 8 6 1 24029.64 24071.92 1133.97 o 10 6 1 16874.44 16554.33 574.44 o 12 6 1 46.49 41.72 55.88 o 14 6 1 259.74 282.38 67.80 o 16 6 1 380.88 352.41 78.98 o 18 6 1 1180.43 1254.67 101.33 o 20 6 1 263.58 264.49 84.94 o 1 7 1 34.52 93.88 34.27 o 3 7 1 25404.35 27657.86 1040.09 o 5 7 1 493.44 412.76 47.68 o 7 7 1 17170.43 17351.54 687.68 o 9 7 1 47.77 -31.29 49.92 o 11 7 1 709.33 590.08 67.05 o 13 7 1 14912.71 15085.09 604.98 o 15 7 1 14.52 -55.13 70.03 o 17 7 1 1471.33 1260.63 103.56 o 19 7 1 33.02 90.15 82.70 o 0 8 1 502.91 713.76 46.94 o 2 8 1 6964.23 6256.96 265.24 o 4 8 1 60383.96 62015.98 1575.79 o 6 8 1 8461.71 8358.75 350.92 o 8 8 1 25370.60 24673.18 1209.97 o 10 8 1 62.92 113.99 55.88 o 12 8 1 7938.44 7385.71 255.55 o 14 8 1 1854.75 2147.24 105.05 o 16 8 1 537.74 440.33 91.64 o 18 8 1 116.52 149.01 78.98 o 20 8 1 55.08 119.21 84.19 o 1 9 1 4376.18 4243.82 184.03 o 3 9 1 9271.44 9350.42 312.18 o 5 9 1 34.68 50.66 46.19 o 7 9 1 644.42 792.74 64.82 o 9 9 1 2628.18 2729.13 112.50 o 13 9 1 35.58 -58.86 65.56 o 15 9 1 2181.77 2288.06 135.60 o 17 9 1 12.32 -76.00 76.00 o 19 9 1 114.21 145.29 95.37 o 0 10 1 12524.56 11987.16 474.60 o 2 10 1 3308.27 3238.00 115.48 o 4 10 1 30196.25 28782.15 1224.87 o 6 10 1 532.77 319.63 58.86 o 8 10 1 7051.63 6902.92 362.84 o 10 10 1 370.21 504.40 67.80 o 12 10 1 8335.70 8103.94 330.80 o 14 10 1 895.68 863.52 89.41 o 16 10 1 2706.07 2788.73 133.36 o 18 10 1 100.57 85.68 84.94 o 1 11 1 3732.08 3519.63 137.83 o 3 11 1 0.81 99.84 51.41 o 5 11 1 2513.17 2622.59 87.92 o 7 11 1 96.42 73.02 58.11 o 9 11 1 154.53 229.48 63.33 o 11 11 1 1001.94 1008.06 84.19 o 13 11 1 2026.97 1752.36 107.29 o 15 11 1 462.07 377.74 86.43 o 17 11 1 334.43 324.84 86.43 o 0 12 1 216.27 109.52 55.13 o 2 12 1 5295.42 5261.56 245.12 o 4 12 1 1086.19 1278.51 74.51 o 6 12 1 3173.59 3538.26 164.66 o 8 12 1 309.55 155.72 63.33 o 10 12 1 3361.46 3450.34 151.99 o 12 12 1 363.52 349.43 79.72 o 14 12 1 298.55 454.48 99.09 o 16 12 1 112.23 -31.29 81.21 o 1 13 1 0.96 -19.37 55.13 o 3 13 1 1246.16 1461.79 80.47 o 5 13 1 2852.68 3156.04 105.05 o 7 13 1 309.02 198.93 64.82 o 9 13 1 4547.65 4445.73 194.46 o 11 13 1 17.35 -9.69 68.54 o 13 13 1 3.00 -13.41 73.76 o 15 13 1 40.19 64.82 80.47 o 17 13 1 3.68 -95.37 95.37 o 0 14 1 5705.11 5149.81 216.07 o 2 14 1 9215.76 8766.29 412.76 o 4 14 1 1329.47 1332.15 85.68 o 6 14 1 273.50 373.27 70.78 o 8 14 1 3416.32 3689.50 160.19 o 10 14 1 39.06 208.61 73.02 o 12 14 1 1202.04 1195.81 104.31 o 14 14 1 531.56 421.70 95.37 o 16 14 1 320.56 326.33 99.09 o 1 15 1 5630.80 5824.83 216.07 o 3 15 1 62.77 175.09 68.54 o 5 15 1 5953.58 5830.04 240.65 o 7 15 1 509.77 602.00 81.96 o 9 15 1 422.85 464.17 83.45 o 11 15 1 147.31 119.95 81.96 o 13 15 1 942.41 907.47 111.01 o 15 15 1 14.36 -81.21 81.21 o 0 16 1 106.02 76.00 70.78 o 2 16 1 10222.61 10112.61 400.09 o 4 16 1 1950.24 1890.94 102.07 o 6 16 1 34.23 157.21 70.78 o 8 16 1 892.76 840.42 92.39 o 10 16 1 1355.27 1307.57 108.78 o 12 16 1 688.86 685.45 100.58 o 14 16 1 696.25 581.89 108.78 o 1 17 1 418.70 286.85 78.98 o 3 17 1 1518.24 1583.98 102.82 o 5 17 1 48.86 83.45 73.02 o 7 17 1 68.07 195.95 75.25 o 9 17 1 548.75 472.36 94.62 o 11 17 1 35.01 127.40 82.70 o 13 17 1 70.27 13.41 90.90 o 0 18 1 708.82 593.81 93.88 o 2 18 1 1073.22 1060.96 97.60 o 4 18 1 437.49 357.63 84.19 o 6 18 1 1915.07 1768.76 143.80 o 8 18 1 412.58 329.31 84.94 o 10 18 1 528.00 646.71 99.84 o 12 18 1 222.87 64.07 90.15 o 1 19 1 662.27 651.18 94.62 o 3 19 1 108.91 70.78 79.72 o 5 19 1 1137.65 1315.76 108.78 o 7 19 1 845.97 915.67 102.07 o 9 19 1 152.62 330.80 94.62 o 0 20 1 539.83 396.37 94.62 o 4 20 1 1029.13 973.04 107.29 o 6 20 1 58.90 275.67 87.17 o 8 20 1 7.14 38.00 90.90 o 1 21 1 55.35 158.70 93.13 o 3 21 1 412.79 434.37 98.35 o 5 21 1 58.96 71.53 87.92 o 2 0 2 271513.53 194492.38 1382.07 o 4 0 2 46542.39 70473.08 1139.93 o 6 0 2 16833.24 19487.61 779.33 o 8 0 2 13389.59 13291.75 488.75 o 10 0 2 554.21 470.13 52.15 o 12 0 2 306.96 306.22 58.11 o 14 0 2 803.39 857.56 75.25 o 16 0 2 184.65 242.14 70.78 o 18 0 2 202.52 177.32 73.02 o 20 0 2 36.61 27.57 79.72 o 1 1 2 26448.87 24957.04 444.80 o 3 1 2 2819.69 2285.08 72.27 o 5 1 2 3414.64 2432.60 75.25 o 7 1 2 8502.11 10381.57 369.55 o 9 1 2 1702.15 1948.31 78.23 o 11 1 2 1503.57 1478.19 71.53 o 13 1 2 2773.02 2726.15 120.70 o 15 1 2 821.08 640.75 76.74 o 17 1 2 197.04 258.53 73.02 o 19 1 2 393.40 430.64 91.64 o 21 1 2 836.99 838.93 104.31 o 0 2 2 10391.45 2446.01 76.74 o 2 2 2 78490.80 58707.20 897.79 o 4 2 2 67452.78 79447.99 1275.53 o 6 2 2 54106.36 56574.86 1340.35 o 8 2 2 4537.86 4399.54 158.70 o 10 2 2 8107.05 9374.26 316.65 o 12 2 2 147.59 90.90 55.13 o 16 2 2 77.14 61.09 68.54 o 18 2 2 534.05 418.72 84.19 o 20 2 2 2.08 -58.11 79.72 o 1 3 2 30591.29 25202.17 620.63 o 3 3 2 8017.58 9214.07 326.33 o 5 3 2 78742.02 82291.86 1489.36 o 7 3 2 401.85 703.33 47.68 o 9 3 2 15589.09 13577.10 507.38 o 11 3 2 58.36 -15.65 48.43 o 13 3 2 1233.75 1171.22 78.23 o 15 3 2 389.54 331.55 72.27 o 17 3 2 2376.66 2396.84 170.62 o 19 3 2 6.19 -58.11 76.74 o 21 3 2 538.92 464.91 92.39 o 0 4 2 3806.73 2108.50 74.51 o 2 4 2 45918.30 52713.25 1076.60 o 4 4 2 897.64 680.98 40.98 o 6 4 2 1153.25 1513.95 68.54 o 8 4 2 87.53 24.59 40.98 o 10 4 2 197.13 277.16 51.41 o 12 4 2 30.62 -4.47 52.15 o 14 4 2 832.57 737.60 74.51 o 16 4 2 448.96 329.31 71.53 o 18 4 2 1271.99 1311.29 101.33 o 20 4 2 105.19 40.98 81.21 o 1 5 2 28621.81 28969.90 824.77 o 3 5 2 41198.84 40691.82 1079.58 o 5 5 2 6169.55 6120.61 224.26 o 7 5 2 34302.70 35677.61 1236.04 o 9 5 2 7959.81 8402.71 336.02 o 11 5 2 12037.36 12168.21 483.54 o 13 5 2 10183.72 9771.37 423.19 o 15 5 2 45.27 34.27 64.07 o 17 5 2 4021.83 3573.27 135.60 o 19 5 2 42.05 57.37 81.96 o 0 6 2 894.93 1017.00 43.96 o 2 6 2 31414.89 30085.99 971.55 o 4 6 2 18398.50 21099.90 883.63 o 6 6 2 3700.93 3053.97 109.52 o 8 6 2 2787.00 3046.52 122.93 o 10 6 2 11313.29 12073.59 504.40 o 12 6 2 1257.51 1329.92 78.98 o 14 6 2 482.95 413.50 70.03 o 16 6 2 195.59 143.05 71.53 o 18 6 2 388.24 440.33 88.66 o 20 6 2 61.11 90.15 87.92 o 1 7 2 91275.68 94164.28 1686.80 o 3 7 2 9653.60 10527.60 366.57 o 5 7 2 29619.29 28958.72 1089.27 o 7 7 2 12097.44 11930.54 493.23 o 9 7 2 280.67 405.31 55.88 o 11 7 2 9307.05 8912.33 321.12 o 13 7 2 5336.91 5251.88 201.16 o 15 7 2 6895.22 5978.31 312.18 o 17 7 2 2761.81 2554.04 123.68 o 19 7 2 33.91 -55.13 108.03 o 0 8 2 344.73 323.35 41.72 o 2 8 2 40.83 -3.73 36.51 o 4 8 2 1635.91 1343.33 61.09 o 6 8 2 10115.16 11157.92 409.78 o 8 8 2 1889.11 1773.23 76.74 o 10 8 2 69.92 170.62 56.62 o 12 8 2 897.04 1175.69 81.96 o 14 8 2 185.67 146.03 74.51 o 16 8 2 1342.34 1398.46 101.33 o 18 8 2 103.33 152.74 82.70 o 1 9 2 34115.41 37738.43 1291.18 o 3 9 2 36947.97 36087.39 1280.75 o 5 9 2 60941.45 64268.28 1829.85 o 7 9 2 16441.83 17530.35 669.06 o 9 9 2 5767.98 6211.51 259.28 o 11 9 2 8158.32 7750.04 322.61 o 13 9 2 744.24 745.80 87.17 o 15 9 2 4669.58 4836.14 244.38 o 17 9 2 895.12 946.96 99.09 o 19 9 2 229.02 241.40 93.13 o 0 10 2 1920.76 2104.77 96.86 o 2 10 2 5.34 54.39 46.94 o 4 10 2 7029.98 7604.01 318.88 o 6 10 2 29.35 87.17 51.41 o 8 10 2 3011.69 2899.75 96.86 o 10 10 2 3538.27 3436.18 141.56 o 12 10 2 123.00 162.42 68.54 o 14 10 2 136.28 88.66 73.02 o 16 10 2 6.76 134.85 74.51 o 18 10 2 203.43 286.10 89.41 o 1 11 2 10838.38 11572.17 462.68 o 3 11 2 14444.86 14668.61 554.32 o 5 11 2 16017.35 15675.17 645.96 o 7 11 2 15072.25 16433.64 659.37 o 9 11 2 5211.49 5527.55 188.50 o 11 11 2 1393.61 1480.42 94.62 o 13 11 2 8447.20 9208.86 482.79 o 15 11 2 2341.86 2256.77 124.42 o 17 11 2 17.36 -82.70 83.45 o 0 12 2 92.67 14.16 55.13 o 2 12 2 159.74 239.91 56.62 o 4 12 2 2422.16 2663.56 128.89 o 6 12 2 555.39 614.67 70.03 o 8 12 2 65.92 87.92 62.58 o 10 12 2 405.22 309.20 73.76 o 12 12 2 57.65 7.45 68.54 o 14 12 2 62.84 -58.86 76.00 o 16 12 2 325.47 319.63 90.15 o 1 13 2 10534.19 10544.74 368.80 o 3 13 2 579.84 476.09 65.56 o 5 13 2 9345.20 8699.24 382.21 o 7 13 2 1526.02 1415.60 88.66 o 9 13 2 14656.12 14042.76 618.39 o 11 13 2 2656.60 2579.37 118.46 o 13 13 2 1304.92 1126.52 102.07 o 15 13 2 1502.52 1699.47 119.21 o 17 13 2 300.88 269.71 104.31 o 0 14 2 235.06 211.60 65.56 o 2 14 2 939.37 1123.54 83.45 o 4 14 2 1227.25 1294.16 84.94 o 6 14 2 69.21 76.00 63.33 o 8 14 2 1534.42 1389.52 92.39 o 10 14 2 8.88 37.25 70.78 o 12 14 2 1.91 -8.94 77.49 o 14 14 2 57.69 125.17 86.43 o 16 14 2 7.25 -18.63 88.66 o 1 15 2 5474.76 5636.33 231.71 o 3 15 2 2144.08 1902.12 100.58 o 5 15 2 26091.24 25744.56 1011.78 o 7 15 2 1123.86 1271.06 92.39 o 9 15 2 5147.82 5584.17 278.65 o 11 15 2 2163.74 2253.79 122.93 o 13 15 2 26.13 138.58 84.94 o 15 15 2 321.09 374.02 95.37 o 0 16 2 2331.12 2241.12 131.87 o 2 16 2 5676.01 5980.54 277.16 o 4 16 2 2305.75 2431.11 122.19 o 6 16 2 2676.39 2440.05 113.25 o 8 16 2 0.68 90.15 72.27 o 10 16 2 279.21 211.60 82.70 o 12 16 2 8.79 -14.16 83.45 o 14 16 2 80.20 24.59 98.35 o 1 17 2 4845.93 4860.73 184.03 o 3 17 2 66.12 170.62 71.53 o 5 17 2 2602.40 2437.81 147.52 o 7 17 2 431.78 346.45 81.21 o 9 17 2 583.14 624.35 89.41 o 11 17 2 7.21 40.98 81.96 o 13 17 2 41.89 -23.84 90.90 o 0 18 2 205.63 189.99 77.49 o 2 18 2 2.88 84.19 76.00 o 4 18 2 12.53 -71.53 71.53 o 6 18 2 64.28 101.33 78.98 o 8 18 2 6.82 49.17 87.17 o 10 18 2 61.59 154.23 86.43 o 12 18 2 237.16 121.44 93.13 o 1 19 2 3.69 148.27 84.19 o 3 19 2 1351.91 1401.44 108.03 o 5 19 2 8.20 70.78 76.00 o 7 19 2 153.92 90.90 82.70 o 9 19 2 163.82 231.71 88.66 o 0 20 2 1336.16 1236.79 113.25 o 2 20 2 927.95 988.69 106.54 o 4 20 2 15.01 -8.94 85.68 o 6 20 2 290.94 226.50 91.64 o 8 20 2 27.64 40.23 92.39 o 1 21 2 56.30 -78.98 81.96 o 3 21 2 231.41 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961.12 99.09 o 8 6 26 678.61 660.12 92.39 o 10 6 26 164.83 274.92 90.15 o 1 7 26 245.99 184.77 78.23 o 3 7 26 1474.79 1341.84 108.78 o 5 7 26 3.83 92.39 74.51 o 7 7 26 782.43 1000.61 102.07 o 9 7 26 37.23 183.28 82.70 o 0 8 26 690.98 900.02 93.88 o 2 8 26 341.05 397.86 84.19 o 4 8 26 1037.22 1200.28 111.01 o 6 8 26 33.45 -83.45 83.45 o 8 8 26 40.84 -43.21 83.45 o 10 8 26 55.63 63.33 83.45 o 1 9 26 1572.22 1725.54 113.99 o 3 9 26 774.59 870.22 101.33 o 5 9 26 799.31 922.38 105.05 o 7 9 26 1836.88 1940.86 125.91 o 9 9 26 188.64 141.56 90.15 o 0 10 26 78.81 160.93 84.94 o 2 10 26 99.22 74.51 83.45 o 4 10 26 442.85 454.48 91.64 o 6 10 26 248.15 336.02 92.39 o 8 10 26 107.28 99.84 93.88 o 1 11 26 203.49 194.46 89.41 o 3 11 26 256.80 403.07 96.11 o 5 11 26 1069.25 1139.19 119.21 o 7 11 26 3.61 -84.19 84.19 o 0 12 26 303.97 301.75 94.62 o 2 12 26 13.01 137.09 96.11 o 4 12 26 113.29 240.65 97.60 o 1 13 26 197.17 187.75 96.11 o 1 1 27 2328.04 2003.45 109.52 o 3 1 27 1741.14 1606.33 107.29 o 5 1 27 376.47 394.88 84.19 o 7 1 27 966.47 1025.19 101.33 o 9 1 27 2115.92 2054.11 154.97 o 11 1 27 2136.40 2337.23 131.87 o 0 2 27 680.10 534.95 79.72 o 2 2 27 519.84 606.47 85.68 o 4 2 27 914.35 1019.23 100.58 o 6 2 27 249.32 251.83 77.49 o 8 2 27 160.61 215.32 93.88 o 10 2 27 159.76 87.17 83.45 o 1 3 27 1882.72 1671.90 105.80 o 3 3 27 2200.24 2523.49 121.44 o 5 3 27 2323.85 2562.98 149.76 o 7 3 27 433.50 529.73 88.66 o 9 3 27 1322.97 1318.74 110.27 o 11 3 27 382.00 521.54 97.60 o 0 4 27 4.32 -78.98 78.98 o 2 4 27 193.66 295.79 80.47 o 4 4 27 808.16 636.28 92.39 o 6 4 27 1897.39 1963.96 119.95 o 8 4 27 675.31 612.43 90.90 o 10 4 27 51.43 78.98 80.47 o 1 5 27 232.11 398.60 76.74 o 3 5 27 1107.41 1037.11 98.35 o 5 5 27 850.12 842.66 95.37 o 7 5 27 79.80 99.84 78.98 o 9 5 27 4.53 111.76 78.23 o 0 6 27 52.96 14.16 73.02 o 2 6 27 321.66 341.23 85.68 o 4 6 27 295.10 343.47 81.96 o 6 6 27 723.62 879.91 112.50 o 8 6 27 7.31 -47.68 80.47 o 10 6 27 542.69 452.25 98.35 o 1 7 27 23.09 -81.21 81.21 o 3 7 27 248.38 171.36 84.94 o 5 7 27 1340.88 1416.35 111.76 o 7 7 27 43.61 28.31 80.47 o 9 7 27 140.50 89.41 84.19 o 0 8 27 1733.96 1645.82 125.17 o 2 8 27 78.93 125.91 80.47 o 4 8 27 212.87 91.64 78.98 o 6 8 27 332.26 372.53 88.66 o 8 8 27 93.71 200.42 84.94 o 1 9 27 51.23 -70.78 90.90 o 3 9 27 85.86 85.68 87.17 o 5 9 27 754.29 987.20 105.80 o 7 9 27 9.28 128.89 87.17 o 0 10 27 229.82 205.63 95.37 o 2 10 27 183.76 268.22 93.13 o 6 10 27 1045.23 1174.20 115.48 o 1 11 27 442.40 547.61 99.09 o 3 11 27 68.44 85.68 91.64 o 5 11 27 0.09 28.31 85.68 o 0 12 27 723.03 598.28 108.03 o 0 0 28 12415.06 12079.55 555.06 o 2 0 28 226.22 161.68 71.53 o 4 0 28 1967.94 1906.59 118.46 o 8 0 28 561.26 514.09 91.64 o 10 0 28 320.56 450.76 126.66 o 1 1 28 319.51 145.29 77.49 o 3 1 28 27.08 8.94 67.05 o 5 1 28 347.04 359.12 79.72 o 7 1 28 326.53 242.14 87.92 o 9 1 28 208.54 131.87 90.90 o 0 2 28 1378.45 1036.37 93.13 o 2 2 28 1.27 -43.96 67.05 o 4 2 28 18.75 -35.02 69.29 o 6 2 28 278.70 330.80 86.43 o 8 2 28 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29 493.21 397.11 96.11 o 1 9 29 257.21 198.93 95.37 o 3 9 29 283.63 338.25 96.11 o 0 0 30 3337.04 3478.65 143.80 o 2 0 30 852.76 850.85 97.60 o 4 0 30 11.69 -76.74 76.74 o 6 0 30 62.05 100.58 76.00 o 8 0 30 2345.37 2580.86 138.58 o 1 1 30 94.40 -14.90 78.23 o 3 1 30 99.02 45.45 77.49 o 5 1 30 0.45 -7.45 73.02 o 7 1 30 0.32 68.54 78.23 o 0 2 30 57.46 -27.57 103.56 o 2 2 30 1998.65 2148.73 125.17 o 4 2 30 170.60 207.12 81.21 o 6 2 30 186.80 151.25 88.66 o 8 2 30 53.77 40.23 81.21 o 1 3 30 275.80 78.98 90.90 o 3 3 30 141.84 201.91 82.70 o 5 3 30 775.96 804.66 99.09 o 7 3 30 129.92 166.89 90.90 o 0 4 30 173.56 108.78 79.72 o 2 4 30 227.43 260.77 84.19 o 4 4 30 181.50 90.15 81.96 o 6 4 30 566.33 493.97 99.84 o 1 5 30 77.90 39.49 80.47 o 3 5 30 15.74 38.74 78.23 o 5 5 30 28.52 -85.68 85.68 o 0 6 30 332.79 160.19 86.43 o 2 6 30 178.48 213.09 86.43 o 4 6 30 137.53 236.18 87.92 o 1 7 30 25.22 189.24 89.41 o 3 7 30 12.45 21.61 99.09 o 0 8 30 61.49 0.00 86.43 o 2 8 30 245.55 184.03 102.82 o 1 1 31 819.68 1004.33 128.15 o 3 1 31 217.45 210.85 93.13 o 5 1 31 946.10 1040.84 113.99 o 0 2 31 15.48 -26.08 73.76 o 2 2 31 273.83 267.47 90.15 o 4 2 31 632.72 797.21 105.05 o 6 2 31 137.90 86.43 95.37 o 1 3 31 680.13 549.85 96.11 o 3 3 31 7.72 189.24 79.72 o 5 3 31 523.25 406.80 96.11 o 0 4 31 89.33 -6.71 76.74 o 2 4 31 185.25 149.01 86.43 o 4 4 31 27.63 19.37 84.94 o 1 5 31 299.81 195.95 123.68 o 3 5 31 590.28 569.22 96.86 o 0 6 31 285.14 379.23 91.64 o 2 6 31 1151.66 1369.41 121.44 o 0 0 32 3605.25 3913.76 160.93 o 2 0 32 57.90 30.55 83.45 o 1 1 32 45.20 -10.43 81.21 o 3 1 32 0.16 -9.69 78.23 o 0 2 32 1336.95 1367.17 114.74 o 2 2 32 2273.67 2238.14 140.82 o 1 3 32 344.60 158.70 84.19 o