#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:00 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180920 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200071.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200071_Fobs loop_ _publ_author_name 'Lynch, Daniel E.' 'McClenaghan, Ian' _publ_section_title ; 2-Amino-5-(4-methoxybenzyl)-4-methyl-1,3-thiazolium chloride ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o24 _journal_page_last o25 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.469 _cell_angle_gamma 90.000 _cell_length_a 7.5746 _cell_length_b 11.8784 _cell_length_c 14.5193 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.7702 _cod_data_source_file ob6000Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '2-Amino-5-(4-methoxybenzyl)-4-methyl-1,3-thiazolium chloride' _shelx_refln_list_code 4 _shelx_f_calc_maximum 125.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 421.81 386.57 64.07 o 6 0 0 792.30 877.32 55.54 o 8 0 0 20.01 31.64 13.83 o 1 1 0 18.40 13.51 1.59 o 2 1 0 321.48 380.71 17.71 o 3 1 0 3149.21 3255.09 127.38 o 4 1 0 457.24 463.59 29.66 o 5 1 0 765.89 838.03 74.60 o 6 1 0 849.21 962.20 66.97 o 7 1 0 1224.42 1397.06 79.38 o 8 1 0 313.43 325.28 53.50 o 9 1 0 3.98 -2.57 12.70 o 0 2 0 1550.74 1411.13 91.30 o 1 2 0 684.24 732.85 40.44 o 2 2 0 2621.68 2727.97 116.97 o 3 2 0 667.02 770.44 29.26 o 4 2 0 723.62 829.98 33.09 o 5 2 0 1246.85 1334.56 62.38 o 6 2 0 36.32 33.20 5.01 o 7 2 0 839.80 876.21 58.11 o 8 2 0 99.00 86.42 11.28 o 9 2 0 40.92 48.64 10.44 o 1 3 0 1298.06 1022.21 85.02 o 2 3 0 265.85 305.21 20.31 o 3 3 0 2414.48 2893.38 117.69 o 4 3 0 193.36 149.18 17.47 o 5 3 0 574.75 630.68 59.71 o 6 3 0 797.01 909.74 49.75 o 7 3 0 133.13 116.55 17.32 o 8 3 0 95.93 92.12 11.54 o 9 3 0 0.09 -3.20 18.16 o 0 4 0 385.71 353.38 36.84 o 1 4 0 1007.95 1020.80 73.47 o 2 4 0 19.12 10.86 1.99 o 3 4 0 2764.96 3208.17 208.86 o 4 4 0 220.52 231.69 19.15 o 5 4 0 10.12 16.17 3.59 o 6 4 0 1151.92 1089.84 99.08 o 7 4 0 126.91 120.30 12.57 o 8 4 0 1.36 -2.46 7.01 o 9 4 0 484.51 468.34 92.61 o 1 5 0 21.64 14.51 1.25 o 2 5 0 1591.79 1518.85 91.99 o 3 5 0 109.28 86.85 6.37 o 4 5 0 29.85 35.41 4.20 o 5 5 0 111.71 132.11 11.35 o 6 5 0 1470.40 1652.31 153.31 o 7 5 0 61.86 58.05 9.56 o 8 5 0 22.15 23.64 16.80 o 9 5 0 9.66 4.36 19.78 o 0 6 0 1052.42 975.83 76.86 o 1 6 0 105.63 103.80 5.37 o 2 6 0 2202.20 2297.44 154.11 o 3 6 0 58.70 49.60 3.47 o 4 6 0 281.86 250.87 9.36 o 5 6 0 79.73 74.54 8.39 o 6 6 0 51.80 44.79 5.82 o 7 6 0 0.86 -4.27 12.42 o 8 6 0 102.82 107.09 21.56 o 1 7 0 3018.40 3005.16 255.31 o 2 7 0 331.45 348.06 26.17 o 3 7 0 472.32 544.08 34.78 o 4 7 0 14.18 20.78 7.65 o 5 7 0 876.27 916.69 63.56 o 6 7 0 0.51 2.13 3.53 o 7 7 0 63.08 46.12 11.62 o 8 7 0 87.36 67.01 11.67 o 0 8 0 262.62 186.01 20.11 o 1 8 0 1.08 2.53 2.57 o 2 8 0 147.27 125.78 17.18 o 3 8 0 32.81 33.59 13.17 o 4 8 0 52.86 60.97 10.26 o 5 8 0 78.35 94.16 13.17 o 6 8 0 0.56 1.17 5.86 o 7 8 0 303.59 318.77 33.80 o 1 9 0 0.91 -1.71 3.04 o 2 9 0 178.97 189.73 12.93 o 3 9 0 970.40 1075.53 66.62 o 4 9 0 89.32 90.97 12.75 o 5 9 0 94.12 107.56 19.64 o 7 9 0 64.51 60.18 17.15 o 0 10 0 540.78 437.13 35.15 o 1 10 0 275.07 259.35 20.79 o 2 10 0 408.38 310.40 27.00 o 3 10 0 31.75 15.91 11.62 o 4 10 0 952.89 893.02 127.38 o 5 10 0 1.83 -4.50 8.48 o 6 10 0 12.72 11.86 16.78 o 7 10 0 13.23 -1.45 23.39 o 1 11 0 20.14 17.74 2.84 o 2 11 0 73.92 98.79 14.18 o 3 11 0 127.72 121.51 13.92 o 4 11 0 542.05 639.68 81.64 o 5 11 0 12.80 19.36 9.94 o 6 11 0 88.12 94.39 25.07 o 0 12 0 0.03 0.45 9.21 o 1 12 0 208.11 195.81 25.12 o 2 12 0 23.79 19.91 7.88 o 5 12 0 224.04 246.33 46.21 o 1 13 0 325.24 272.22 56.65 o 2 13 0 26.46 28.40 11.15 o 4 13 0 5.71 -7.50 15.98 o 5 13 0 34.23 19.82 17.86 o 0 14 0 154.56 185.97 28.82 o 1 14 0 14.49 29.39 9.80 o 3 14 0 3.45 8.06 13.64 o 4 14 0 44.22 50.66 18.56 o -9 0 1 56.44 64.72 15.93 o -7 0 1 1093.29 1186.19 142.45 o -5 0 1 88.57 78.45 7.60 o -3 0 1 831.03 1083.24 64.73 o -1 0 1 5340.78 5908.78 433.47 o 1 0 1 1880.76 1706.78 108.93 o 3 0 1 958.97 1121.62 79.86 o 5 0 1 2863.68 2753.90 176.27 o 7 0 1 102.96 100.12 9.83 o 9 0 1 23.38 17.34 11.58 o -9 1 1 37.67 46.85 14.93 o -8 1 1 3.00 6.36 9.10 o -7 1 1 188.03 201.45 14.07 o -6 1 1 522.97 584.73 33.20 o -5 1 1 152.78 167.95 11.56 o -4 1 1 1914.61 2172.03 126.95 o -3 1 1 1302.44 1432.41 58.64 o -2 1 1 5140.48 5765.76 217.59 o -1 1 1 8540.58 8778.02 472.10 o 0 1 1 88.37 94.14 4.52 o 1 1 1 297.86 301.24 15.63 o 2 1 1 391.23 394.19 20.95 o 3 1 1 205.10 187.22 13.55 o 4 1 1 582.92 548.22 44.47 o 5 1 1 322.16 354.03 18.75 o 6 1 1 547.52 573.24 30.97 o 7 1 1 575.26 577.26 30.23 o 8 1 1 392.44 388.99 34.07 o 9 1 1 84.83 67.50 11.69 o -9 2 1 167.47 176.10 24.25 o -8 2 1 1.26 -6.98 8.48 o -7 2 1 57.73 72.53 8.12 o -6 2 1 1116.68 1223.31 94.54 o -5 2 1 1395.72 1487.90 67.94 o -4 2 1 432.74 505.98 20.41 o -3 2 1 1.24 3.77 3.87 o -2 2 1 649.42 610.97 36.30 o -1 2 1 5446.63 4979.48 307.14 o 0 2 1 6117.57 5155.78 327.89 o 1 2 1 90.04 74.95 4.96 o 2 2 1 804.58 900.62 43.12 o 3 2 1 1547.34 1480.94 116.89 o 4 2 1 2062.82 1979.43 206.42 o 5 2 1 268.53 328.91 21.84 o 6 2 1 77.11 63.30 6.58 o 7 2 1 1.25 -2.11 6.47 o 8 2 1 1.41 2.26 7.78 o 9 2 1 3.16 1.96 11.28 o -9 3 1 57.74 63.88 23.90 o -8 3 1 5.78 11.82 8.03 o -7 3 1 385.59 395.88 37.85 o -6 3 1 464.32 474.79 34.35 o -5 3 1 300.86 317.60 36.90 o -4 3 1 10.50 8.62 3.28 o -3 3 1 5073.65 5204.81 291.73 o -2 3 1 1659.32 1638.57 77.46 o -1 3 1 302.03 246.85 18.40 o 0 3 1 4135.46 3898.59 166.65 o 1 3 1 3748.87 3360.16 195.48 o 2 3 1 1929.51 2127.14 140.23 o 3 3 1 13.17 16.07 2.29 o 4 3 1 79.94 101.47 9.99 o 5 3 1 37.18 39.75 3.94 o 6 3 1 1203.62 1314.17 89.86 o 7 3 1 127.45 137.38 18.88 o 8 3 1 135.47 150.76 59.10 o 9 3 1 149.16 138.91 26.39 o -9 4 1 37.41 28.54 22.17 o -8 4 1 260.00 368.56 38.20 o -7 4 1 17.49 20.97 7.99 o -6 4 1 193.15 235.19 19.06 o -5 4 1 194.60 221.79 29.57 o -4 4 1 2649.93 2646.13 105.45 o -3 4 1 641.12 670.72 31.00 o -2 4 1 8.28 1.19 2.99 o -1 4 1 619.90 587.07 32.08 o 0 4 1 1441.04 1429.98 62.43 o 1 4 1 0.11 2.16 3.80 o 2 4 1 5598.77 5850.52 586.77 o 3 4 1 1020.70 1109.23 67.44 o 4 4 1 748.67 822.09 101.24 o 5 4 1 761.12 763.39 56.77 o 6 4 1 10.52 14.62 9.00 o 7 4 1 111.03 96.30 15.65 o 8 4 1 1.66 3.05 11.67 o 9 4 1 410.62 457.42 67.49 o -9 5 1 6.86 10.83 14.72 o -8 5 1 0.87 10.97 18.98 o -7 5 1 447.76 467.02 46.21 o -6 5 1 46.50 38.06 11.34 o -5 5 1 664.45 653.63 30.12 o -4 5 1 123.36 129.07 10.21 o -3 5 1 209.99 241.36 18.61 o -2 5 1 309.47 274.11 26.61 o -1 5 1 1229.47 1188.62 54.83 o 0 5 1 45.11 42.77 3.06 o 1 5 1 0.14 0.81 1.92 o 2 5 1 6.12 6.76 5.09 o 3 5 1 1958.04 1888.34 176.31 o 4 5 1 4.80 0.00 3.37 o 5 5 1 1880.34 1901.77 192.07 o 6 5 1 39.43 35.52 8.41 o 7 5 1 117.84 117.30 15.80 o 8 5 1 0.86 -9.04 13.66 o 9 5 1 91.39 97.95 21.87 o -8 6 1 68.48 69.18 12.71 o -7 6 1 7.29 5.88 11.25 o -6 6 1 259.72 233.99 14.20 o -5 6 1 177.00 184.95 9.35 o -4 6 1 743.23 689.95 47.87 o -3 6 1 0.69 3.69 4.29 o -2 6 1 57.76 46.70 4.49 o -1 6 1 2.03 9.35 3.44 o 0 6 1 50.46 36.64 2.88 o 1 6 1 128.95 95.46 7.08 o 2 6 1 2404.50 2463.99 167.45 o 3 6 1 2372.50 2409.89 104.68 o 4 6 1 14.88 10.07 3.04 o 5 6 1 54.32 -4.55 4.55 o 6 6 1 130.67 116.59 12.93 o 7 6 1 693.12 777.47 80.28 o 8 6 1 45.06 58.26 17.81 o -8 7 1 334.68 387.30 81.01 o -7 7 1 14.89 3.76 10.57 o -6 7 1 2.22 1.33 8.74 o -5 7 1 1.06 0.63 3.88 o -4 7 1 964.25 985.37 60.25 o -3 7 1 1049.84 1041.49 74.65 o -2 7 1 1268.00 1302.38 133.41 o -1 7 1 1.45 1.84 3.16 o 0 7 1 81.02 64.16 3.99 o 1 7 1 1894.15 1769.45 101.57 o 2 7 1 23.04 16.00 4.44 o 3 7 1 5.90 2.97 8.27 o 4 7 1 0.03 5.31 5.64 o 5 7 1 4.48 10.40 7.15 o 6 7 1 214.33 208.90 21.46 o 7 7 1 71.55 56.08 8.49 o 8 7 1 0.54 5.80 10.94 o -8 8 1 8.46 -1.50 20.72 o -7 8 1 98.60 96.14 14.39 o -6 8 1 2.51 3.04 3.76 o -5 8 1 900.91 925.97 40.46 o -4 8 1 165.53 171.08 11.92 o -3 8 1 2.96 8.13 6.11 o -1 8 1 412.90 445.29 22.04 o 0 8 1 185.66 156.03 8.20 o 1 8 1 82.87 70.68 4.04 o 3 8 1 667.71 569.01 58.44 o 4 8 1 281.83 282.71 32.10 o 5 8 1 47.58 63.23 8.90 o 6 8 1 80.19 74.52 6.38 o 7 8 1 22.39 26.60 8.06 o 8 8 1 0.72 3.33 14.76 o -7 9 1 0.01 -19.40 21.42 o -6 9 1 0.45 18.14 18.14 o -5 9 1 577.04 654.49 65.85 o -4 9 1 247.43 241.51 24.39 o -3 9 1 5.92 10.50 9.94 o -2 9 1 326.10 330.93 32.01 o -1 9 1 786.33 731.54 44.12 o 0 9 1 152.55 131.17 6.98 o 1 9 1 11.46 1.03 6.75 o 2 9 1 287.21 299.91 23.69 o 3 9 1 170.23 142.76 17.81 o 4 9 1 322.84 298.39 16.58 o 5 9 1 8.05 6.47 12.42 o 6 9 1 97.40 85.67 14.25 o 7 9 1 7.75 14.43 19.26 o -7 10 1 143.14 128.32 26.76 o -6 10 1 55.75 54.08 13.03 o -5 10 1 63.82 77.85 14.67 o -4 10 1 230.89 250.23 40.47 o -3 10 1 99.63 83.24 10.49 o -2 10 1 12.58 27.46 7.69 o -1 10 1 311.85 277.48 36.63 o 0 10 1 31.22 28.68 3.14 o 1 10 1 810.48 696.92 49.02 o 2 10 1 104.84 100.95 11.01 o 4 10 1 736.83 855.13 83.19 o 5 10 1 86.85 80.99 17.81 o 7 10 1 90.85 86.23 24.46 o -6 11 1 75.61 59.38 20.95 o -5 11 1 382.57 431.74 52.02 o -4 11 1 35.86 63.88 17.76 o -3 11 1 366.70 392.85 40.49 o -2 11 1 2.68 -4.64 8.25 o -1 11 1 16.08 14.00 4.79 o 0 11 1 3.34 0.75 2.54 o 1 11 1 584.29 444.18 57.15 o 2 11 1 155.52 144.91 13.45 o 3 11 1 103.08 105.21 27.23 o 4 11 1 85.72 74.14 12.47 o 6 11 1 11.19 44.66 17.95 o -6 12 1 282.60 352.67 50.94 o -5 12 1 4.34 2.02 16.54 o -4 12 1 60.98 70.25 19.73 o -3 12 1 9.57 15.28 12.23 o -2 12 1 210.76 216.16 18.57 o -1 12 1 70.22 51.99 5.60 o 0 12 1 205.14 182.07 24.02 o 1 12 1 147.96 130.06 16.26 o 2 12 1 3.92 -2.72 11.48 o 3 12 1 2.06 -3.52 9.51 o 5 12 1 36.95 23.06 15.70 o -5 13 1 8.17 24.61 23.11 o -4 13 1 176.71 231.48 30.98 o -3 13 1 88.33 96.73 19.92 o -2 13 1 169.32 161.97 22.21 o -1 13 1 90.68 83.45 14.02 o 0 13 1 0.04 -0.57 5.20 o 1 13 1 349.71 291.32 42.23 o 2 13 1 20.27 35.29 12.09 o 4 13 1 277.17 341.38 50.90 o -4 14 1 17.06 26.90 17.25 o -3 14 1 14.54 41.43 11.76 o -1 14 1 0.01 4.78 4.16 o 0 14 1 89.01 80.19 10.06 o 1 14 1 135.34 139.05 23.06 o 2 14 1 62.33 68.19 17.20 o 3 14 1 16.25 35.10 16.59 o -2 15 1 0.45 -2.06 12.00 o -1 15 1 61.96 96.17 15.89 o 0 15 1 41.08 43.63 9.89 o 1 15 1 201.95 240.85 26.06 o 2 15 1 31.27 9.19 13.73 o -8 0 2 13.01 22.12 13.08 o -6 0 2 2589.86 3079.43 422.32 o -4 0 2 122.24 171.68 16.47 o -2 0 2 7150.30 7971.10 376.74 o 0 0 2 1122.86 1018.99 56.45 o 2 0 2 292.29 298.07 28.21 o 4 0 2 1130.66 1005.73 139.85 o 6 0 2 7.09 19.82 12.47 o 8 0 2 143.47 90.27 17.58 o -9 1 2 194.53 158.37 25.69 o -8 1 2 8.94 -1.19 13.15 o -7 1 2 190.29 179.70 10.74 o -6 1 2 1704.27 2103.90 255.66 o -5 1 2 2.68 -0.49 3.84 o -4 1 2 583.21 797.73 60.41 o -3 1 2 1136.12 1285.05 48.15 o -2 1 2 103.95 133.70 5.34 o -1 1 2 425.71 475.53 21.02 o 0 1 2 1021.94 937.05 36.20 o 1 1 2 1021.01 985.80 49.29 o 2 1 2 3647.93 3571.62 155.21 o 3 1 2 278.80 273.85 14.42 o 4 1 2 7.53 0.94 3.28 o 5 1 2 595.35 609.44 35.21 o 6 1 2 129.49 137.02 11.11 o 7 1 2 510.05 487.91 31.26 o 8 1 2 83.61 86.65 11.19 o 9 1 2 63.73 37.77 14.82 o -9 2 2 148.15 171.69 20.78 o -8 2 2 27.28 29.64 8.03 o -7 2 2 604.37 639.75 41.43 o -6 2 2 74.79 58.39 6.61 o -5 2 2 13.22 5.25 3.27 o -4 2 2 439.02 456.45 18.87 o -3 2 2 2666.97 2974.05 113.38 o -2 2 2 1676.74 1906.66 73.45 o -1 2 2 7620.97 7506.93 291.20 o 0 2 2 85.47 74.05 3.48 o 1 2 2 2616.01 2389.21 98.90 o 2 2 2 1801.40 1803.69 74.47 o 3 2 2 163.47 180.30 15.48 o 4 2 2 3.51 5.99 2.72 o 5 2 2 2608.22 2760.65 157.74 o 6 2 2 1017.82 1057.75 45.24 o 7 2 2 77.51 70.89 8.81 o 8 2 2 95.27 91.22 13.94 o 9 2 2 256.74 247.29 34.98 o -9 3 2 38.48 22.66 16.40 o -8 3 2 267.17 223.10 22.14 o -7 3 2 848.59 960.22 80.25 o -6 3 2 332.46 331.13 25.68 o -5 3 2 139.06 155.77 12.79 o -4 3 2 619.77 771.35 30.54 o -3 3 2 264.15 269.55 17.34 o -2 3 2 239.00 231.32 8.54 o -1 3 2 1545.73 1432.73 54.95 o 1 3 2 1515.44 607.17 482.60 o 2 3 2 1960.38 1802.98 298.11 o 3 3 2 1083.39 1164.19 49.49 o 4 3 2 2.95 6.83 2.75 o 5 3 2 410.12 492.72 28.02 o 6 3 2 0.33 -1.74 4.20 o 7 3 2 33.37 39.30 10.46 o 8 3 2 42.71 32.36 8.84 o 9 3 2 128.98 95.33 25.17 o -9 4 2 12.25 37.59 20.53 o -8 4 2 22.48 32.48 19.82 o -7 4 2 154.94 139.63 12.84 o -6 4 2 19.01 17.11 9.33 o -5 4 2 956.57 1041.22 43.88 o -4 4 2 163.38 197.10 11.05 o -3 4 2 378.87 353.40 26.96 o -2 4 2 27.40 36.09 3.50 o -1 4 2 566.22 557.17 28.09 o 0 4 2 1834.06 1733.60 74.21 o 1 4 2 766.32 803.78 49.28 o 2 4 2 200.96 171.98 8.55 o 3 4 2 64.78 109.24 8.88 o 4 4 2 487.53 522.41 36.10 o 5 4 2 639.98 655.77 38.78 o 6 4 2 1.82 2.64 3.98 o 7 4 2 1178.62 1218.37 141.98 o 8 4 2 2.08 13.83 11.86 o 9 4 2 25.72 34.96 21.28 o -9 5 2 43.86 1.67 14.13 o -8 5 2 338.55 359.84 97.86 o -7 5 2 124.54 115.24 11.16 o -6 5 2 46.51 38.51 5.56 o -5 5 2 20.16 21.97 5.24 o -4 5 2 557.47 499.24 17.93 o -3 5 2 12.72 13.66 2.97 o -2 5 2 702.94 688.08 28.48 o -1 5 2 379.96 349.83 14.03 o 0 5 2 1679.65 1477.02 75.80 o 1 5 2 141.54 148.33 15.42 o 2 5 2 55.63 63.31 6.89 o 3 5 2 15.69 13.53 2.44 o 4 5 2 268.23 166.62 46.07 o 5 5 2 385.07 376.80 34.94 o 6 5 2 127.88 118.96 8.51 o 7 5 2 4.47 7.36 6.39 o 8 5 2 27.02 18.65 16.73 o -9 6 2 35.49 34.07 18.75 o -8 6 2 2.80 3.19 8.74 o -7 6 2 17.70 16.99 5.58 o -6 6 2 398.75 433.06 22.61 o -5 6 2 161.17 162.25 10.14 o -4 6 2 1251.79 1306.78 54.58 o -3 6 2 7.58 7.09 2.07 o -2 6 2 121.03 118.41 6.32 o -1 6 2 494.88 509.71 24.81 o 0 6 2 583.97 508.22 62.99 o 1 6 2 48.03 50.58 9.02 o 2 6 2 4.52 14.67 6.28 o 3 6 2 347.30 348.58 34.35 o 4 6 2 258.46 240.55 16.58 o 5 6 2 11.20 9.96 3.14 o 6 6 2 523.81 604.71 48.16 o 7 6 2 28.99 34.95 8.76 o 8 6 2 34.05 48.51 16.64 o -8 7 2 6.31 -1.86 8.63 o -7 7 2 171.57 205.48 48.81 o -6 7 2 142.44 139.78 15.85 o -5 7 2 94.78 84.37 7.00 o -4 7 2 32.43 30.15 8.30 o -3 7 2 348.49 371.02 17.20 o -2 7 2 796.38 943.43 122.32 o -1 7 2 2338.11 2458.63 133.27 o 0 7 2 96.04 86.45 5.68 o 1 7 2 80.05 65.41 5.48 o 2 7 2 54.18 44.52 5.40 o 3 7 2 2001.76 1924.91 181.37 o 4 7 2 5.89 10.62 8.29 o 5 7 2 34.21 24.64 4.83 o 6 7 2 59.38 54.96 9.96 o 7 7 2 4.19 18.75 16.83 o 8 7 2 0.86 3.54 11.18 o -8 8 2 56.40 66.36 17.62 o -7 8 2 103.13 104.28 18.84 o -6 8 2 81.47 79.65 18.51 o -5 8 2 21.14 29.37 3.67 o -4 8 2 353.72 374.46 20.11 o -3 8 2 302.28 331.59 15.42 o -2 8 2 25.62 24.62 3.30 o -1 8 2 534.00 540.64 24.13 o 0 8 2 22.05 16.43 2.25 o 1 8 2 470.96 446.77 25.87 o 2 8 2 143.93 135.40 16.59 o 3 8 2 453.05 452.73 42.46 o 4 8 2 170.51 128.41 17.25 o 5 8 2 73.81 79.86 10.28 o 6 8 2 611.58 653.18 68.43 o 7 8 2 98.25 101.65 16.59 o 8 8 2 65.97 66.55 26.25 o -7 9 2 123.63 105.76 14.86 o -6 9 2 0.15 -2.12 4.82 o -5 9 2 3.49 -0.30 5.98 o -3 9 2 143.18 117.87 11.53 o -2 9 2 52.41 41.48 3.46 o -1 9 2 3.07 -1.08 3.39 o 0 9 2 46.55 55.60 5.33 o 1 9 2 667.63 618.27 57.79 o 2 9 2 34.15 29.85 8.25 o 3 9 2 17.21 9.83 13.05 o 4 9 2 93.39 112.36 11.94 o 6 9 2 50.34 56.05 19.36 o -7 10 2 105.52 153.86 28.78 o -6 10 2 271.92 286.03 42.84 o -4 10 2 35.02 28.11 9.40 o -3 10 2 52.53 51.01 5.29 o -2 10 2 1256.30 1347.46 74.47 o -1 10 2 52.70 53.09 5.42 o 0 10 2 70.68 58.73 4.96 o 1 10 2 53.25 43.77 9.42 o 2 10 2 313.31 292.37 42.86 o 3 10 2 41.48 34.68 6.67 o 4 10 2 28.60 20.39 7.45 o 5 10 2 38.36 65.99 16.64 o 6 10 2 13.04 22.59 11.53 o 7 10 2 6.34 -5.20 14.67 o -6 11 2 18.59 66.97 22.82 o -5 11 2 90.83 102.12 18.93 o -4 11 2 79.23 102.78 14.43 o -3 11 2 1.72 2.58 11.39 o -2 11 2 3.22 0.91 2.55 o -1 11 2 5.57 7.12 5.78 o 0 11 2 78.96 66.47 7.49 o 1 11 2 9.21 3.22 4.99 o 2 11 2 6.08 14.87 9.28 o 4 11 2 4.56 6.94 9.89 o 5 11 2 25.99 18.04 14.15 o 6 11 2 27.70 13.40 18.23 o -5 12 2 1.97 -8.15 17.86 o -4 12 2 0.49 1.03 12.33 o -3 12 2 266.65 323.19 38.48 o -2 12 2 182.44 160.42 21.84 o -1 12 2 127.71 142.29 11.81 o 0 12 2 1.15 -3.77 3.77 o 1 12 2 167.80 165.96 20.76 o 2 12 2 83.79 87.55 11.33 o 4 12 2 5.77 17.29 14.81 o 5 12 2 20.43 62.80 21.93 o -5 13 2 65.12 67.86 21.42 o -4 13 2 17.73 2.58 18.47 o -3 13 2 27.85 8.30 17.11 o -2 13 2 6.69 20.89 8.25 o -1 13 2 14.66 7.86 6.29 o 0 13 2 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